Jawab soalan mengikut arahan yang diberikan dalam setiap bahagian. Questions should be answered according to the instruction given in each section.

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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2014/2015 : SEMESTER 1 ACADEMIC SESSION 2014/2015 : SEMESTER 1 SCES3334 : KIMIA POLIMER II POLYMER CHEMISTRY II Disember 2014/Januari 2015 December 2014/Januari 2015 Masa : 2 jam Time : 2 Hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Kertas ini mengandungi Bahagian A dan Bahagian B. This examination paper consists of sections A and B. Jawab soalan mengikut arahan yang diberikan dalam setiap bahagian. Questions should be answered according to the instruction given in each section. Tandakan nombor soalan pada muka hadapan buku jawapan dalam urutan yang sama seperti dalam buku jawapan. Indicate question number on the front page of answer book in the same order as answer in the book(s). Jawapan boleh diberi sama ada dalam Bahasa Melayu atau Bahasa Inggeris. Answer can be written in either Malay or English. (Kertas ini mengandungi 7 soalan dalam 10 halaman yang dicetak) (This question paper consists of 7 questions on 10 printed pages)

2 BAHAGIAN A (50 MARKAH) SECTION A (50 MARKS) Jawab SEMUA 4 soalan dalam bahagian ini. Answer ALL 4 questions 1. Jelaskan cara untuk membezakan High Density Polyethylene (HDPE) dan Low Density Polyethylene (LDPE) berdasarkan ujian berikut. Penjelasan anda haruslah meliputi prosedur dan jangkaan keputusan ujian tersebut yang membolehkan anda membezakan kedua-dua sampel polimer. Describe how to differentiate High Density Polyethylene (HDPE) from Low Density Polyethylene (LDPE) based on the following tests. Your description should include brief procedure and the expected results of each test that could help to differentiate the two. (a) Ujian ketumpatan Density test Analisis Fourier Transform Infrared (FTIR) Fourier Transform Infrared (FTIR) analysis (10markah/marks) 2. Spektrum FTIR bagi sampel Poly(vinyl alcohol) adalah seperti Rajah 1.Ramal dan terangkan perubahan kepada spektrum selepas polimer itu telah dibenarkan untuk bertindak balas dengan asid etanoik. Baki asid yang berlebihan dan air (produk sampingan daripada tindak balas) telah diasingkan sebelum sampel dianalisis. Figure 1 shows the FTIR spectrum of Poly(vinyl alcohol). Predict and explain the changes to the spectrum after the polymer was allowed to react with excess ethanoic acid. Note that any unreacted acid and water (by-product from the reaction) has been removed prior to FTIR analysis. Rajah 1:Spektrum FTIR Poly(vinyl alcohol) Figure 1: FTIR absorbance spectrum of Poly(vinyl alcohol) (6markah/marks) 2/10

3 3. (a) Rajah 2 menunjukkan spectrum proton Nuclear Magnetic Resonance( 1 H- NMR) bagipoli ( etena co- propena). Dapatkan yang nisbah etena : propena dalam kopolimer ini. Nilai integrasi di dalam spectrum dinyatakan sebagai x dan y. Figure 2 shows the proton Nuclear Magnetic Resonance ( 1 H-NMR) spectrum of poly (ethene-co-propene). Find what is the ratio of ethene : propene in the copolymer. Peak integration value is expressed as x and y in the spectrum. Rajah 2: Spektrum 1 H-NMR poli(etena co- propena) Figure 2: H-NMR spectrum of poly(ethene-co-propene) (8 markah/mark) Berikut adalah spectra 1 H-NMR bagi 3 sampel polimer yang berbeza. Pilih spektrum yang menunjukkan polimer: Followings are the 1 H-NMR spectra of 3 different polymer samples. Select from the given spectra, which reflects: (i) (ii) Poly(vinyl chloride), PVC Poly(ethylene terephthalate), PET Jelaskan jawapan anda. Explain your selection. (10markah/marks) 3/10

4 Spektrum A /Spectrum A Spektrum B /Spectrum B Spektrum C /Spectrum C 4/10

5 4. Analisis terma adalah satu cabang sains bahan yang membolehkan seseorang untuk mengkaji sifat bahan sebagai fungsi suhu. Antara teknik yang biasa digunakan adalah Differential Scanning Calorimetry (DSC) dan Thermal Gravimetric Analysis (TGA). Thermal analysis is a branch of material science that allows one to study properties of material as a function of temperature. Among the commonly employed techniques are Differential Scanning Calorimetry (DSC) dan Thermal Gravimetric Analysis (TGA) analyses. (a) DSC termogram Polimer Z menunjukkan bahan tersebut mengalami kedua-dua peralihan kaca dan peralihan lebur. DSC thermogram of Polymer Z shows that the material exhibit both glass transition and melting transition. (i) (ii) (iii) Terangkan mengapa bahan tersebut mampu mempamerkan kedua-dua peralihan. Explain why the material is able to exhibit both transitions. Terangkan morfologi polimer tersebut. Describe the morphology of the polymer. Lakarkan termogram DSC Polimer Z yang menunjukkan kedua-dua peralihan. Sketch DSC thermogram of Polymer Z that shows the two transitions. (9 markah/marks) Rajah 3 menunjukkan termogram TGA bagi cat X yang telah dikeringkan. Graf tersebut diperolehi daripada analisis TGA dalam N 2. Cat kering tersebut mengandungi Resin X dan CaCO 3. Jika CaCO 3 terurai kepada CaO (s ) dan CO 2 (g ) pada suhu kira-kira 800 o C, kira % berat CaCO 3 dalam cat kering X. Plot tersebut tidak dilukis berdasarkan skala. Segala jalan kerja dan pengiraan haruslah ditunjukkan dengan jelas. Figure 3 shows the TGA curve of dried paint X obtained from TGA scan in N 2 atmosphere. The dried paint comprised of Resin X and CaCO 3. Given that CaCO 3 decomposes to CaO(s) and CO 2 (g) at temperature around 800 o C. Calculate the weight % of CaCO 3 in Dried Paint X.Note that the plot is not drawn to scale. Explicitly show the working involved. [Atomic mass of Ca = 40 g/mol ; C = 12 g/mol ; O = 16 g/mol] 5/10

6 Rajah 3: Termogram TGA bagi cat X yang telah dikeringkan Figure 3: TGA thermogram of Dried Paint X (7 markah/marks) 6/10

7 Jawab soalan 5, 6 dan 7. Answer questions 5, 6 and 7. BAHAGIAN B (50 MARKAH) SECTION B (50 MARKS) 5. Jawab BETUL atau SALAH dan berikan alasan anda. Answer TRUE or FALSE and give your reason(s). (a) (c) Pseudoplastik dicirikan oleh penurunan kelikatan apabila kadar ricih meningkat. Pseudoplastic is characterized by a decrease in viscosity with increasing shear rate. Tanda tenggelam muncul di permukaan produk, sangat berkemungkinan terjadi pada bahagian produk yang nipis, terbentuk akibat tekanan tidak sekata yang disebabkan oleh keadaan suhu melampau. Sink mark appears on the surface of the product, it is very likely to occur on the thin product, which is formed due to uneven pressure caused by extreme temperature condition. Pada keadaan spinodal, pemisahan fasa berlaku melalui penukleusan dan pertumbuhan yang memerlukan lebih daripada satu halangan tenaga. At the spinodal conditions, phase separation occurs by nucleation and growth which requires exceeding an energy barrier. (d) Suhu peralihan di mana perubahan polimer daripada lembut/ liat kepada cair dipanggil suhu peralihan kaca. The transition temperature at which a polymer changes from soft/ tough to a molten is called the glass transition temperature. (e) Modulus Young adalah tetap dan tidak berubah untuk bahan yang diberi, tanpa mengira saiz sampel yang diuji. Young s Modulus is constant and does not change for a given material, regardless of the size of sample tested. 7/10

8 6. Berikan penerangan ringkas mengenai pernyataan berikut. Give brief explanation on the following statements. (a) Namakan DUA jenis umum pengacuan mampatan. Senaraikan kelemahan kedua-duanya dan namakan SATU lagi jenis pengacuan mampatan yang dapat mengatasi kelemahan kedua-dua pengacuan mampatan tersebut. Name TWO general types of compression moulding. List the disadvantageous of both and name ANOTHER type of compression moulding that can overcome the disadvantageous of these two general compression moulding. (4 markah/marks) Melalui pencampuran dan kopolimerisasi sekurang-kurangnya dua jenis polimer, kita dapat memperbaiki sifat akhir sesuatu bahan. Apakah perbezaan di antara pencampuran dan pengkopolimeran? Memberikan satu contoh bagi setiap jenis. Through blending and copolymerization of at least two types of polymers, we can improve the properties of the end product. What are the differences between blending and copolymerization? Provide one example of each type. (4 markah/marks) (c) (d) Jelaskan hubungan antara Newtonion dan Bukan Newtonion dalam pemprosesan polimer. Describe the relationship between Newtonion and Non-Newtonion in the polymer processing. (4 markah/marks) Sifat tahan api adalah sangat penting untuk bahan polimer yang terdedah kepada haba semasa hayat penggunaannya. Cadangkan sejenis polimer dan bahan tambahan yang sesuai untuk sifat tahan api. Nyatakan kelebihan bahan yang dipilih. Flame retardant character is very important for polymer material which is exposed to heat during its service life. Suggest a polymer and a suitable additive for the flame retardant property. State the advantageous of the chosen of material. (4 markah/marks) (e) Jelaskan kinetik pemisahan fasa bagi campuran polimer. Explain the kinetics of phase separation for a polymer blend. (4 markah/marks) 8/10

9 7. (a) Pakej pengkapsulan untuk semikonduktor biasanya dihasilkan melalui pengacuan pemindahan. Cadangkan polimer yang sesuai dan gambarkan kitaran umum pengeluaran pakej pengkapsulan. Package encapsulation for semiconductor is usually made by transfer moulding. Suggest a suitable polymer and describe general cycle of the production of package encapsulation. (5 markah/marks) Gegancu plastik (lihat Gambar A) boleh membantu untuk memanjangkan hayat rantai dengan mengurangkan penggunaan rantai gegancu logam dan sesuai dalam aplikasi pemacu rantai yang memerlukan pencucian kerap dan persekitaran berdebu. Ia diperbuat daripada bahan polimer yang tahan kakisan yang boleh dilincirkan dengan minyak. Plastic sprockets (refer Figure A) can help to prolong the life of the chain by reducing the use of chain metal sprockets and suitable in applications of chain drive that require frequent washdown and dusty environments. They are manufactured from polymer materials that are resistant to corrosion which could be lubricated with oil. Gambar A: Gegancu plastik Figure A: Plastic sprockets (i) Cadangkan jenis polimer yang boleh digunakan untuk produk tersebut dan nyatakan bahan tambahan yang sesuai. Berikan alasan anda. Suggest a polymer which can be used to manufacture the product and indicate a suitable additive. Give your reasons. (ii) Cadangkan satu mesin yang boleh digunakan untuk pengeluaran. Beri alasan anda. Suggest a machine that can be used for the production. Give your reasons. 9/10

10 (iii) Lakarkan gambarajah kasar mesin dalam (ii). Label sekurangkurangnya enam komponen utama serta nyatakan fungsinya. Sketch a rough diagram of the machine in (ii). Label at least six major components and state their functions. (6 markah/marks) (iv) Jelaskan secara ringkas prosedur pengeluaran produk. Describe briefly the production procedure of the product. (5 markah/marks) TAMAT END 10/10

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