(Kertas soalan ini mengandungi 5 soalan dalam 6 halaman yang dicetak) (This question paper consists of 5 questions on 6 printed pages)

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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE PEPERIKSAAN IJAZAH SARJANA MUDA SAINS DENGAN PENDIDIKAN EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE WITH EDUCATION SESI AKADEMIK 2015/2016 : SEMESTER 1 ACADEMIC SESSION 2015/2016 : SEMESTER 1 SCES2252/SCES2433/SIC2015 : ELEKTROKIMIA ASAS/ ELEKTROKIMIA BASIC ELECTROCHEMISTRY/ ELECTROCHEMISTRY Dis 2016/Jan 2017 Dec 2016/Jan 2017 MASA : 2 jam TIME : 2 hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Kertas ini mengandungi 5 soalan. Jawab 4 soalan sahaja This paper consists of 5 questions. Answer 4 questions only. (Kertas soalan ini mengandungi 5 soalan dalam 6 halaman yang dicetak) (This question paper consists of 5 questions on 6 printed pages)

2 1. (a) Sel kepekatan mengandungi dua sel setengah Ag/Ag +. Pada sel-separuh A, elektrod A dicelup dalam M AgNO 3 ; dalam sel-separuh B, elektrod B dicelup dalam 4.0x10-4 M AgNO 3. Kira keupayaan sel pada 298 K dan nyatakan elektrod yang akan mempunyai cas positif. A concentration cell consists of two Ag/Ag + half-cells. In half-cell A, electrode A is immersed in M AgNO 3 ; in half-cell B, electrode B is immersed in 4.0x10-4 M AgNO 3. Calculate the cell potential at 298 K and indicate which electrode will have a positive charge. Gabung dua tindakbalas setengah berikut ke dalam persamaan tindakbalas spontan yang seimbang dan kira E o cell. Combine the following two half-reactions into a balanced equation for spontaneous reaction and calculate E o cell. (i) - NO 3 (aq) + 4 H + (aq) + 3e - NO (g) + 2H 2 O (l) E o = V (ii) MnO 2 (s) + 4 H + (aq) + 2e - Mn 2+ (aq) + 2H 2 O (l) E o = V (c) Natrium hidroksida dan klorin digunakan secara meluas dalam kehidupan seharian kita. Huraikan proses elektrokimia klor-alkali untuk penghasilannya. Sodium hydroxide and chlorine are widely used in our everyday life. Describe the electrochemical chlor-alkali process for their production. (10 markah/marks) (d) Hitungkan potensi sel bagi tindakbalas berikut apabila tekanan gas oksigen adalah 2.50 atm, kepekatan ion hidrogen adalah 0.10 M, dan kepekatan ion Br - ialah 0.25 M. Calculate the cell potential for the following reaction when the pressure of the oxygen gas is 2.50 atm, the hydrogen ion concentration is 0.10 M, and the Br - ion concentration is 0.25 M. (E o bromine = V and E o water = V). O 2 (g) + 4 H + (aq) + 4 Br - (aq) 2 H 2 O (l) + 2 Br 2 (l) 2/6

3 2. (a) Hitungkan perubahan tenaga Gibbs bebas piawai, G 0, dalam J/mol pada suhu 25 o C bagi tindakbalas berikut dari potensi elektrod piawai. Calculate the standard Gibbs free energy change, G 0, in J/mol at 25 o C for the following reaction from standard electrode potentials. 2Fe 2+ + Sn 4+ = 2Fe 3+ + Sn 2+ Sel solar yang terdiri daripada jalur kuprum dalam 1 M kuprum (II) sulfat dan jalur perak dalam larutan 1M perak. Wayar disambungkan dengan voltmeter dan jambatan garam melengkapkan litar. Tulis pemerhatian anda pada petak anod, petak katod dan bacaan voltmeter. Tulis secara am semua separuh-sel dan tindakbalas sel. Menarik sel dengan gambarajah yang sesuai dengan semua sambungan. A voltaic cell consisting of a strip of Cu immersed in 1 M copper (II) sulfate solution and a strip of silver immersed in 1 M silver nitrate solution. A wire is connected with a voltmeter and a salt bridge completes the circuit. Write your observations on the anodic compartment, cathodic compartment and the voltmeter reading. Write all the half-cell and the overall cell reactions. Draw the cell with a suitable diagram with all the connections. (9 markah/marks) (c) Jelaskan meter ph yang berasaskan prinsip sel kepekatan. Describe a ph meter which is based on the principle of a concentration cell. (6 markah/marks) (d) Seorang ahli kimia mencairkan campuran yang terjadi secara semulajadi NaBr dan MgCl 2 dan menguraikannya di dalam sel elektrolisis. Ramalkan bahan yang terbentuk pada setiap elektrod dan nyatakan tindakbalas kimia separa dan keseluruhan bagi sel tersebut. A chemist melts a naturally occuring mixture of NaBr and MgCl 2 and dissociates it in an electrolytic cell. Predict the substance formed at each electrode and write the balanced half-reactions and the overall cell reaction. 3. (a) Takrifkan persamaan Butler-Volmer yang digunakan secara meluas dalam kinetik elektrokimia Define the Butler-Volmer equation which is widely used in electrochemical kinetics. (2 markah/marks) 3/6

4 Jelaskan elektrod hidrogen piawai (SHE) Describe a standard hydrogen electrode (SHE) (c) Takrifkan yang berikut: Define the followings: (i) (ii) (iii) Elektrod kerja Working electrode Elektrod bertentangan Counter electrode Elektrod rujukan Reference electrode (6 markah/marks) (d) Bincangkan perbezaan di antara pengukuran potensiometrik dan voltametrik. Discuss the differences between potentiometric and voltammetric measurements. (12 markah/marks) 4. (a) Untuk elektrod tindak balas berikut: O x + ne Red Lukiskan profil kepekatan bagi setiap titik yang dilabel bersama-sama dengan linear sweep voltammetry berikut. For the following electrode reaction: O x + ne Red Draw the concentration profiles for each of the labeled points along the following linear sweep voltammetry. (12 markah/marks) 4/6

5 Terangkan dengan jelas bagaimana eksperimen voltammetri siklik (CV) dilakukan, apakah data yang anda akan kumpulkan, dan bagaimana untuk menganalisa data bagi membezakan antara tindak balas elektrokimia berbalik atau tidak berbalik. Lakarkan voltammogram-voltammogram tersebut. Describe exactly how do you conduct cyclic voltammetry (CV) experiment, what data you would collect, and how to analyze the data to distinguish between a reversible and irreversible electrochemical reaction. Sketch the voltammograms. (13 markah/marks) 5. (a) Lukiskan respon polarografik untuk campuran yang mengandungi 3 mm Cu 2+, 2 mm Zn 2+, dan 1 mm Cd 2+. Keupayaan setengah gelombang bagi ionion Cu, Zn dan Cd adalah masing-masing -0.12, -0.95, dan V. Draw the polarographic response for a mixture containing 3 mm Cu 2+, 2 mm Zn 2+, and 1 mm Cd 2+. The half-wave potentials for the Cu, Zn and Cd ions are -0.12, -0.95, and V, respectively. (12 markah/marks) Satu larutan yang dipercayai mengandungi amaun surih Cu 2+ dan Cd 2+ dianalisa menggunakan teknik anodik pelucutan voltammetri. Terangkan secara ringkas langkah-langkah yang terlibat dan bagaimana arus diukur. Lakarkan voltamogram yang mewakili analisis ini. A solution believed to contain trace amounts of Cu 2+ and Cd 2+ is analyzed using anodic stripping voltammetry technique. Briefly describe the steps involved and how current is measured. Sketch a representative voltammogram for this analysis. (13 markah/marks) 5/6

6 Apendiks Appendix TAMAT END 6/6

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