SCES2250/SIC2006 : SPEKTROSKOPI MOLEKUL & INTERPRETASI/ SPEKTROSKOPI MOLEKUL MOLECULAR SPECTROSCOPY & INTERPRETATION/ MOLECULAR SPECTROSCOPY

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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2016/2017 : SEMESTER 1 ACADEMIC SESSION 2016/2017 : SEMESTER 1 SCES2250/SIC2006 : SPEKTROSKOPI MOLEKUL & INTERPRETASI/ SPEKTROSKOPI MOLEKUL MOLECULAR SPECTROSCOPY & INTERPRETATION/ MOLECULAR SPECTROSCOPY Dis 2016/Jan 2017 Dec 2016/Jan 2017 MASA : 3 jam TIME : 3 hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Kertas soalan ini mengandungi Bahagian A dan B. This paper consists of Section A and B. Jawab soalan mengikut arahan yang diberikan dalam setiap bahagian. Questions should be answered according to the instructions given in each section. (Kertas soalan ini mengandungi 8 soalan dalam 6 halaman yang dicetak) (This question paper consists of 8 questions on 6 printed pages)

2 Jawab semua soalan dalam bahagian ini. Answer all questions in this Section. BAHAGIAN A (67 MARKAH) SECTION A (67 MARKS) 1. (a) Nyata jenis sinaran yang diperhatikan pada sinaran elektromagnet dalam urutan frekuensi meningkat. Apakah jenis fenomena yang akan diperhatikan dalam molekul semasa interaksi mereka dengan setiap jenis radiasi? Write the types of radiation observed in the electromagnetic spectrum in a sequence of increasing frequency. What types of phenomena will be observed in molecules during their interaction with each type of radiation? (7 markah/marks) Satu molekul dalam cecair mengalami kira-kira perlanggaran setiap saat. Berdasarkan andaian berikut, A molecule in a liquid undergoes about collisions each second. Based on the following assumptions, (i) (ii) setiap perlanggaran berkesan dalam menyahaktifkan molekul getaran. every collision is effective in deactivating the molecule vibrationally. yang satu perlanggaran di antara 100 adalah berkesan. that one collision in 100 is effective. Kira lebar (dalam cm 1 ) peralihan getaran dalam molekul untuk setiap keadaan. Calculate the width (in cm 1 ) of vibrational transitions in the molecule for each of the conditions. (8 markah/marks) 2. Interferometer ialah komponen yang terpenting pada sebuah spektroskop Fourier Transform. Hurai bagaimana komponen ini berfungsi dalam menghasilkan corak gangguan daripada sumber cahaya monokromatik dengan menggunakan gambarajah yang sesuai. The interferometer is the most important component of a Fourier Transform spectroscope. Describe how this component functions in producing an interference pattern from a monochromatic light source by using appropriate diagram(s). (8 markah/marks) 2/6

3 3. (a) Jelas mengapa garisan dengan keamatan yang paling tinggi dalam spektrum putaran bukan garisan yang pertama. Explain why the most intense line in a rotational spectrum is not the first line. (7 markah/marks) Hitung jarak antara garisan dalam satu spektrum putaran untuk ClO diberi panjang ikatan ialah Å. Andaikan molekul adalah tegar. Calculate the line spacing for the rotational spectrum of ClO given that its bond length is Å. Assume the molecule is rigid. (8 markah/marks) 4. Suatu foton cahaya yang panjang gelombang 2.42 μm telah dipancarkan semasa peralihan antara dua paras tenaga getaran yang bersebelahan bagi molekul HF molekul. A photon of wavelength 2.42 μm was emitted during a transition between two adjacent vibrational energy levels of the HF molecule. (a) Dengan frekuensi apa molekul HF bergetar? With what frequency does the HF molecule vibrate? (4 markah/marks) Apakah pemalar daya untuk molekul ini? What is the force constant for this molecule? 5. (a) Takrif bahagian-p dan bahagian-r bagi spektroskopi putaran-getaran. Dengan melukis gambar rajah paras tenaga yang sesuai, tunjukkan peralihan untuk P(2) dan R(2) bagi satu molekul dwiatom yang tegar. Define P-branch and R-branch in rotational-vibrational spectroscopy. By drawing the appropriate energy level diagram, show the P(2) and R(2) transitions for a rigid diatomic molecule. (6 markah/marks) Apakah yang anda boleh kata tentang pemalar putaran, B 0 di v = 0 dan B 1 di v = 1. Adakah mereka sama? Beri justifikasi. What can you say about the rotational constants, B 0 at v = 0 and B 1 at v = 1. Are they equal? Provide justifications. (4 markah/marks) 3/6

4 6. (a) Terang mengapa pendarfluoran berlaku pada jarak gelombang yang lebih panjang daripada penyerapan. Explain why fluorescence occurs at a longer wavelength than absorption. (4 markah/marks) Tentukan simbol sebutan atom yang boleh diperolehi daripada konfigurasi elektron 2p 1 3d 1. Determine all the atomic term symbols that can be obtained from a 2p 1 3d 1 electron configuration. (6 markah/marks) [JAR 35 Cl, 35.5 g mol -1 ; JAR 16 O, 16.0 g mol -1 ; JAR 1 H, 1.0 g mol -1 ; JAR 19 F, 19.0 g mol -1 ; pemalar Planck, 6.63 x J s; kelajuan cahaya, 3.0 x 10 8 m s -1 ; pemalar Avogadro, 6.02 x mol -1 ] [RAM 35 Cl, 35.5 g mol -1 ; RAM 16 O, 16.0 g mol -1 ; RAM 1 H, 1.0 g mol -1 ; RAM 19 F, 19.0 g mol -1 ; Planck s constant, 6.63 x J s; speed of light, 3.0 x 10 8 m s -1 ; Avogadro constant, 6.02 x mol -1 ] 4/6

5 BAHAGIAN B (33 MARKAH) SECTION B (33 MARKS) Jawab semua soalan. Answer all questions. 7. (a) 1 H dan 15 N memiliki spin, I, 1 2. Namun begitu, belahan Zeeman untuk 1 H adalah lebih besar dari yang dipunyai 15 N. Apakah faktor yang menyumbang kepada perbezaan yang ketara pada belahan Zeeman di antara kedua-dua nukleus tersebut? 1 H and 15 N have a spin, I, of 1 2. However, the Zeeman splitting for 1 H is larger than that of 15 N. What factor contributes to the significant difference in the Zeeman splitting between both nuclei? Beri takrifan frekuensi Larmor berserta persamaan yang menakrifnya. Give the definition of Larmor frequency and the equation which defines it. (c) Dengan bantuan Segitiga Pascal yang diberi, lakar spektra RMN proton bagi: With the help of the given Pascal Triangle, sketch the proton NMR spectra of: (i) sistem AX 3 an AX 3 system (ii) sistem A 2 X 3 an A 2 X 3 system (Nota: Kebiasaannya, A lebih dinyahperisai daripada X) (Note: By convention, A is more deshielded than X) (6 markah/marks) 5/6

6 8. (a) Senarai tiga kelebihan penyahgandingan spin. List three advantages of spin decoupling. (3 markah/marks) Gambarajah berikut menunjukkan spektrum RMN bagi etanol, CH 3 CH 2 OH, di mana kumpulan alkil adalah yang paling terperisai, dan kumpulan hidroksil adalah yang paling ternyahperisai. Terangkan fenomena yang menyebabkan terhasilnya spektrum tersebut. The following figure shows the proton NMR spectrum of ethanol, CH 3 CH 2 OH, in which the alkyl group is the most shielded, and the hydroxyl group is the most deshielded. Explain the phenomenon which gives rise to the spectrum. (c) Satu proton melompat di antara dua lokasi yang mempunyai δ = 3.0 dan δ = 5.0. Pada kadar berapakah pertukaran ini akan menyebabkan keduadua isyarat itu bertembung menjadi satu garisan pada spektrometer yang beroperasi pada 400 MHz? A proton jumps between two sites with δ = 3.0 and δ = 5.0. At what rate of interconversion will the two signals collapse to a single line in a spectrometer operating at 400 MHz? (7 markah/marks) (d) Imbasan Resonan Magnetik (IRM) menggunakan prinsip-prinsip RMN untuk mendiagnosis tumor otak. Mengapakah perkataan nuklear" tidak digunakan pada terma IRM? The Magnetic Resonance Imaging (MRI) uses the principles of NMR to diagnose brain tumor. Why is the word nuclear not used in the term MRI? TAMAT END (2 markah/marks) 6/6

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