(Kertas soalan ini mengandungi 9 soalan dalam 6 halaman yang dicetak) (This question paper consists of 9 questions on 6 printed pages)

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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2010/2011 : SEMESTER 1 ACADEMIC SESSION 2010/2011 : SEMESTER 1 SCES2241/ SCES2441/ :KIMIA ANALISIS ASAS/ KIMIA ANALISIS I BASIC ANALYTICAL CHEMISTRY/ ANALYTICAL CHEMISTRY I November/ Disember 2010 November/ December 2010 MASA : 2 jam TIME : 2 hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Kertas soalan ini mengandungi Bahagian A dan B. This paper consists of Section A and B. Jawab soalan mengikut arahan yang diberikan dalam setiap bahagian. Answer the questions according to the instructions given in each section. (Kertas soalan ini mengandungi 9 soalan dalam 6 halaman yang dicetak) (This question paper consists of 9 questions on 6 printed pages)

2 SCES2241/ SCES2441/ 02 Jawab SEMUA soalan dalam bahagian ini. Answer ALL questions in this section. BAHAGIAN A (50 MARKAH) SECTION A (50 MARKS) 1. Diberikan suatu sebatian X yang mempunyai berat molekul sebanyak 150 dan kepekatannya dalam air adalah 0.15 x 10ˉ³ M. Hitungkan kepekatan ini dalam unit ppm. A compound X has a molecular weight of 150 and its concentration in water is 0.15 x 10ˉ ³ M. Calculate its concentration in ppm units. [1 ppm = 1 g cmˉ³ atau 1 mg dmˉ³] [1 ppm = 1 g cmˉ³ or 1 mg dmˉ³] (5 markah/ marks) 2. Jadual berikut menunjukkan nilai keupayaan yang diperolehi apabila suatu elektrod pilihan ion fluorida direndam dalam larutan yang mengandungi ion fluorida. The following table shows the potential values which are obtained when a fluoride ion selective electrode is immersed in solutions containing fluoride ions: a ( Fˉ) / mg dmˉ³ E / mv Apakah kepekatan ion fluorida dalam suatu larutan yang memberikan nilai keupayaan sebanyak mv dengan menggunakan elektrod pilihan ion itu? What is the concentration of fluoride ions in a solution which shows a potential value of mv when this ion selective electrode is used? (5 markah/ marks) 3. Dalam teknik tambahan piawai dalam analisis polarografi, persamaan berikut digunakan:- In the standard addition technique in polarographic analysis, the following equation is employed: id = kc di mana id ialah arus difusi, c ialah kepekatan spesis dalam larutan dan k adalah pemalar perkadaran. Bincang bagaimana anda boleh pastikan bahawa pemalar perkadaran, k, tidak berubah semasa suatu analisis dijalankan? where id is the diffusion current, c is the concentration of the species in solution and k is the proportionality constant. Discuss how this proportionality constant can be fixed when an analysis is being carried out.

3 SCES2241/ SCES2441/ Lukiskan suatu gambarajah berlabel bagi menunjukkan suatu elektrod kaca ph. Mengapakah pentingnya untuk elektrod kaca ph direndam dalam air sebelum dan selepas digunakan? Terangkan. Draw a labelled diagram to show a ph glass electrode. Why is it important to keep a ph glass electrode immersed in water before and after use? Explain. 5. Dalam proses pengekstrakan pelarut, tunjukkan bagaimana pengekstrakan berbilang-tahap adalah lebih cekap dibandingkan dengan pengekstrakan tunggal. Dalam penjelasan anda, anggapkan nisbah pembahagian D = 1.0 dan tujuan adalah untuk mengekstrak 90% bahan zat terlarut ke dalam fasa organik. In the solvent extraction process, show how multiple extraction is more efficient when compared to single extraction. In your explanation, assume that the distribution ratio D = 1.0 and the objective is to extract 90% of the solute material into the organic phase. 6. (a) Berikan dua penggunaan resin penukar ion diguna. Give two applications where ion exchange resins are used. Apakah implikasinya apabila sesuatu jenis ion menunjukkan nilai pekali kepilihan yang besar terhadap suatu resin penukar ion? What is the implication when a particular ion shows a high selectivity coefficient towards an ion exchange resin?

4 SCES2241/ SCES2441/ 04 BAHAGIAN B (50 MARKAH) SECTION B (50 MARKS) Jawab SEMUA soalan daripada bahagian ini. Answer ALL questions from this section. 7. [15 markah/ marks] (a) Bezakan antara Differentiate between (i) pensampelan berperingkat dan pensampelan berterusan. batch sampling and continuous sampling. (ii) pencernaan basah dan abu kering. wet digestion and dry ashing. (iii) ralat rambang dan ralat sistematik. random error and systematic error. (9 markah/ marks) Hitungkan jisim pepejal La(IO 3 ) 3 (663.6 g mol -1 ) yang terbentuk apabila 50.0 ml suatu larutan 0.20 M La 3+ dicampurkan dengan 75.0 ml larutan M IO 3. Beri jawapan akhir anda dalam tiga angka bererti. Calculate tha mass of solid La(IO 3 ) 3 (663.6 g mol -1 ) that is formed when 50.0 ml of 0.20 M La 3+ is mixed with 75.0 ml of M IO 3. Your final answer should be written in three significant figures. (6 markah/ marks) 8. [20 markah/ marks] (a) (i) Nyatakan Hukum Beer. Kenalpasti TIGA (3) faktor yang menyebabkan hubungan hukum Beer lari daripada garis lurus. State Beer s Law. Identify THREE (3) factors that cause Beer s Law relationship to depart from linearity.

5 SCES2241/ SCES2441/ 05 (ii) Kepekatan suatu sampel cecair yang terkandung dalam sel inframerah ketebalan 0.15 m adalah 0.5 M. Hitungkan molar keterserapan bagi sampel itu jika daya serap pada jarak gelombang tertentu adalah The concentration of a liquid sample contained in an infrared cell of thickness 0.15 m is 0.5 M. Calculate the molar absorptivity of the sample if the absorbance at a specified wavelength is Lakar dan label gambar rajah blok bagi spektrofotometer alur tunggal. Nyatakan perbezaan di antara spektrofotometer alur tunggal dan spektrofotometer dua alur. Sketch and label a block diagram of a single-beam spectrophotometer. State the difference between a single-beam and a double-beam spectrophotometer. 9. [15 markah/ marks] (a) Takrifkan istilah kejituan dan kepersisan sebagaimana digunakan dalam kimia analisis. Terangkan secara ringkas bagaimana ianya ditentukan secara kuantitatif. Define the terms accuracy and precision as they are used in the analytical chemistry. Briefly explain how they may be estimated quantitatively. (8 markah/ marks) Lima keputusan penentuan Zn dalam satu sampel adalah seperti berikut (dalam unit ppm): The results for five determinations of Zn in a sample are as follow (in ppm unit): Hitung Calculate the (i) purata, mean, (ii) sisihan piawai relatif, dan relative standard deviation, and (iii) 95% had keyakinan bagi purata. 95% confidence limit of the mean. (7 markah/ marks)

6 SCES2241/ SCES2441/ 06 TAMAT END TAMAT END

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