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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2014/2015 : SEMESTER 1 ACADEMIC SESSION 2014/2015 : SEMESTER 1 SCES2324 : PETROKIMIA PETROCHEMISTRY Disember 2014/Januari 2015 December 2014/January 2015 MASA : 2 jam TIME : 2 hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Kertas soalan ini mengandungi Bahagian A dan B. This paper consists of Section A and B. Jawab soalan mengikut arahan yang diberikan dalam setiap bahagian. Answer the questions according to the instructions given in each section. (Kertas soalan ini mengandungi 6 soalan dalam 7 halaman yang dicetak) (This question paper consists of 6 questions on 7 printed pages)

2 BAHAGIAN A (50 MARKAH) SECTION A (50 MARKS) Jawab SEMUA soalan. Answer ALL questions. 1. Isikan petak kosong dan lukiskan struktur untuk sebatian yang terlibat. Fill in the boxes and draw the structures of the missing compounds. (a) Nyahhidroisomerisasi Dehydroisomerisation Gabungan proses (i) dan (ii) Combination of (i) and (ii) processes Kebanyakkan daripada (iii) tertukarganti Mostly from substituted (iii) Keadaan: ~500 o C, ~15 atm, atmosfera (iv) Condition: ~500 o C, ~15 atm, (iv) atmosphere Mangkin: (v) oksida Pt, Cu Catalyst: (v) oxide, Pt, Cu 2/7

3 Fotonitrosasi Photonitrosation (vi) tindak balas (vi) reaction Keadaan: lampu Hg 20 kw, pendedahan cahaya pada 600 nm atau kurang Condition: Hg lamp 20 kw, light exposure at 600 nm or less Produk: (vii) Product: (vii) Penyediaan nitrosil klorida Preparation of nitrosyl chloride Pengoksidaan (viii) kepada (xi) Oxidation of (viii) to (xi) Dirawat dengan H 2 SO 4 pada tekanan atmosfera untuk menghasilkan asid (x) Treated with H 2 SO 4 at atmospheric pressure to produce (x) acid (16 markah/ marks) 2. (a) Namakan dua monomer untuk pembuatan nilon-6,6. Perihalkan dengan ringkas proses pembuatan kedua-dua monomer daripada n-heksana. Tuliskan semua persamaan yang terlibat. Name two monomers for the production of nylon-6,6. Describe briefly the processes for producing both monomers from n-hexane. Write all the equations involved. 3/7

4 Jelaskan satu konsep penting yang anda pelajari daripada kursus petrokimia. Explain one important concept that you have learnt from petrochemistry. (17 markah/ marks) 3. (a) Namakan dua kaedah fizikal yang digunakan untuk pemisahan sebatian aromatik dalam kursus ini. Perihalkan satu kaedah yang telah anda namakan. Name two physical methods for the separation of aromatics that you have learnt from this course. Describe briefly one of the methods. (c) Namakan dua kegunaan sebatian anhidrida. Name two uses of anhydride. Namakan tiga jenis sebatian anhidrida. Tuliskan persamaan untuk penghasilan tiga jenis sebatian anhidrida dan jelaskan mengapa tiga sebatian ini mempunyai warna yang berbeza. Name three types of anhydrides. Write the equations for the production of these anhydrides and explain why these compounds are different in colour. (17 markah/ marks) 4/7

5 BAHAGIAN B (50 MARKAH) SECTION B (50 MARKS) Jawab SEMUA soalan. Answer ALL questions. 4. (a) Tuliskan persamaan tindak balas bagi penghasilan petrokimia berikut daripada metanol. Write the equation for the production of the following petrochemicals from methanol. (i) (ii) formaldehid formaldehyde metal tetiar butyl eter, MTBE methyl tertiary butyl eter, MTBE (4 markah/ marks) Tuliskan susunan tindak balas bagi penghasilan MTBE dengan menggunakan isobutana, propena dan metanol. Write the reaction sequence for the production of MTBE by using isobutane, propene and methanol. (5 markah/ marks) (c) Terangkan secara teknikal penghasilan urea berdasarkan tindak balas ammonia dengan karbon dioksida. Describe the technical production of urea based on the reaction of ammonia with carbon dioxide. (6 markah/ marks) (d) Kegunaan utama asid nitrik ialah bagi penghasilan ammonium nitrat untuk pengeluaran baja. Apakah kegunaan lain asid nitrik dalam industri kimia? The primary use of nitric acid is for the production of ammonium nitrate for fertilizer product. What is another nitric acid application in chemical industry? 5. (a) Kenapa proses pembentukan stim dari gas asli adalah lebih menjimatkan berbanding proses elektrolisis air dalam penghasilan gas hidrogen? Why steam reforming process of natural gas is more economical than that of water electrolysis process in producing hydrogen gas? 5/7

6 Bagi penghasilan gas hidrogen di dalam proses pembentukan stim: For the production of hydrogen gas in steam reforming process: (i) Senaraikan dua mangkin utama yang digunakan List two primary catalysts used (ii) Apakah fungsi potassium dalam mangkin ini? What is the function of potassium in the catalyst? (iii) Terangkan keadaan proses yang biasa dilakukan Describe the typical process condition (4 markah/ marks) (iv) Bagaimana pembentukan karbon pada permukaan mangkin boleh terbentuk? Bagaimanakah langkah pembentukan karbon ini boleh diminimumkan? How the carbon formation is formed on catalyst surface? How to minimize the carbon formation? (6 markah/ marks) 6. Butadiena merupakan salah satu komoditi penting dalam industri petrokimia. Butadiene is one of the most important commodities in the petrochemical industry. (a) Apakah aplikasi utama butadiena What is the main application of butadiene? Apakah ciri butadiena? Apakah masalah yang sering berlaku dalam penyimpanan butadiena di dalam skala kecil (dalam penyimpanan makmal)? What are the properties of butadiene? What is the typical problem in storing butadiene in a small scale (in laboratory storage)? (4 markah/ marks) (c) Berikut adalah aliran gambarajah proses Lummus komersial dalam penghasilan butadiena. Below is the flow diagram of commercial Lummus process in butadiene production: 6/7

7 Labelkan (1) hingga (6) bagi setiap peringkat pemprosesan. Label stage (1) to (6) of the process. (6 markah/ marks) (d) Butadiena boleh disintesis dengan melibatkan beberapa bahan kimia dalam fasa wap menggunakan mangkin heterogenus Butadiene can be synthesized by the reaction of few chemicals in vapour phase over a heterogeneous catalyst. (i) Mengikut gambarajah berikut, lukiskan struktur sebatian A, B, C dan tuliskan nama mangkin D As shown below, draw the structure of compound A,B,C and write the name of catalyst D (ii) Namakan langkah dalam penghasilan butadiene daripada sebatian C? Name the step for producing butadiene from compound C? TAMAT END (5 markah/ marks) 7/7

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