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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2016/2017 ACADEMIC SESSION 2016/2017 : SEMESTER I : SEMESTER I SCES3333 : ELEKTROKIMIA GUNAAN APPLIED ELECTROCHEMISTRY Dis 2016/Jan 2017 Dec 2016/Jan 2017 Masa: 2 jam Time: 2 hours ARAHAN KEPADA CALON: INSTRUCTIONS TO CANDIDATES: Jawab empat (4) soalan sahaja. Answer four (4) questions only. (Kertas soalan ini mengandungi 5 soalan dalam 5 halaman yang bercetak) (This question paper consists of 5 questions on 5 printed pages)

2 1. (a) Suatu larutan elektrosaduran Cr 3+ di dalam larutan penimbal ph 5.5 memberikan kecekapan arus sebanyak 70%. Apabila ph dinaikkan ke 8.5, kecekapan arus bertambah kepada 85%. An electroplating solution of Cr 3+ in ph buffer 5.5 gives a current efficiency of 70%. When the ph was increased to 8.5, the current efficiency increased to 85%. Terangkan perbezaan di antara kecekapan arus di dalam larutan asid dan alkali. Explain the differences in current efficiencies for acidic and alkaline solutions. Apakah kepentingan larutan penimbal ph di dalam larutan elektrosaduran? What is the importance of a buffer in an electroplating solution? Terangkan yang berikut: Perapuhan hidrogen di dalam elektrosaduran. Hydrogen embrittlement in electroplating. Tindakbalas penurunan oksigen pada katod. Oxygen reduction at cathode. Tindakbalas pembebasan oksigen di anod. Oxygen evolution at anode. 2. (a) Terangkan yang berikut: Pemisah membrane di dalam bateri. Membrane separator in a battery. Ciri-ciri bahan elektrod positif di dalam bateri litium. Properties of a positive electrode material in lithium batteries. Keupayaan litar terbuka suatu bateri. Open Circuit Potential (OCP) of a battery. 2/5

3 Terangkan yang berikut: Pengoksidaan gas hidrogen di dalam Sel Bahan api Membran Pertukaran Proton berlainan daripada pembakaran gas hidrogen dengan oksigen. Hydrogen oxidation in Proton Exchange Membrane (PEM) fuel cells is not the same as hydrogen combustion with the presence of oxygen. Bateri Logam Nikel Hidrida mempunyai ketumpatan simpanan cas (mah g -1 ) yang lebih besar daripada bateri Lithium ion. Nickel Metal Hydride (NiMH) battery has greater charge storage density (mah g -1 ) than the Lithium Ion Battery (LIB). 3. (a) Gambarajah di atas menunjukkan plot Ragone (dalam skala log) bagi semua jenis alat penyimpan tenaga seperti bateri, sel bahanapi and kapasitor. Plot Ragone memberikan hubungan diantara ketumpatan kuasa (W/L) lawan ketumpatan tenaga (Wh/L). The diagram shows a Ragone plot (in log scale) for all types of energy storage devices such as batteries, fuel-cells and capacitors. The Ragone plot shows the power density (W/L) vs. energy density (Wh/L). Mengapakah bateri Ion Litium mempunyai ketumpatan tenaga yang tinggi tetapi ketumpatan kuasa yang rendah? Why lithium ion batteries (LIB) have very high energy density but very low power density? 3/5

4 Mengapakah kapasitor dielektrik mempunyai ketumpatan kuasa yang tinggi tetapi ketumpatan tenaga yang rendah? Why dielectric capacitors have very high power density but very low energy density? Semasa discas di dalam bateri interkalasi aluminum dan natrium, kedua-dua logam aluminum and natrium akan teroksida untuk menghasilkan ion yang akan diturunkan pada katod. During discharge in aluminum and sodium intercalation batteries, both aluminum and sodium metal oxidize to produce ions which reduce at the cathode. Terangkan kenapa elektrod positif bagi kedua-dua bateri interkalasi Al dan Na tidak boleh daripada bahan yang sama. Explain why the positive electrodes of both Al and Na intercalation batteries cannot be the same type of material. Kira ketumpatan cas teori bagi kedua-dua bateri Al dan Na. Calculate the theoretical charge density of both Al and Na intercalation batteries. Jejari ionik bagi Na + and Al 3+ adalah 116 and 68 picometer (10-12 m) masingmasing. Pemalar Faraday adalah C mol -1. Jisim atom bagi Na and Al adalah 23 g/mol and 27 g/mol, masing-masing. The ionic radii for the Na + and Al 3+ are 116 and 68 picometers (10-12 m) respectively. The Faraday constant is C mol -1. The atomic mass of Na and Al is 23 g/mol and 27 g/mol, respectively. 4. Terangkan yang berikut: Membran ion terpilih. Ion selective membrane. Kekurangan aplikasikan enzim alat penderia elektrokimia. Limitations of an enzyme incorporated electrochemical sensor. Kelebihan dan kekurangan penderia potentiometrik. Advantages and disadvantages of potentiometric sensors. 4/5

5 (iv) Pemiawaian elektrod ph. Calibration of a ph electrode. (25 markah/marks) 5. (a) Terangkan secara ringkas yang berikut: Explain briefly the following: Penganodan sebagai perlindungan pengarataan bagi logam aluminum. Anodization as corrosion protection in aluminum. Perapuhan hidrogen di dalam perlindungan katod. Hydrogen embrittlement in cathodic protection. Pengaratan disebabkan oleh dua logam yang bersentuhan antara satu sama lain. Corrosion due to the two metals in contact. (15 arkah/marks) Tindakbalas pembebasan hidrogen pada katod di dalam sel pengaratan Galvanic diberikan seperti berikut: The hydrogen evolution reaction (HER) at cathode in a Galvanic corrosion ell is given as follows: 2H 2 O + 2e - 2OH - + H 2 E θ / V vs. SHE = H + + 2e - H 2 E θ / V vs. SHE = 0 Terangkan sama ada pengaratan akan menjadi mudah di dalam medium berasid atau neutral. Explain whether the corrosion of metals will be easier in acidic or neutral medium. Selain daripada air dan asid, apakah jenis molekul yang lain di katod yang akan meningkatkan proses pengaratan logam. What other existing molecule apart from water and acids, at the cathode which will definitely enhance the corrosion of metals. TAMAT END 5/5

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