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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2013/2014 : SEMESTER 2 ACADEMIC SESSION 2013/2014 : SEMESTER 2 SCES3340 : PEMANGKINAN CATALYSIS Jun 2014 June 2014 MASA : 2 jam TIME : 2 hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Jawab SEMUA soalan. Answer ALL questions. (Kertas ini mengandungi 5 soalan dalam 5 halaman yang dicetak) (This question paper consists of 5 questions on 5 printed pages)

2 1. Untuk tindak balas bermangkin dimana mangkin berliang adalah dalam fasa pepejal manakala bahan suapan adalah dalam fasa gas, For a two phase catalytic reactions whereby the porous catalyst is in solid phase whilst the feed is in gas phase, Bincang langkah-langkah fizikal dan kimia dalam transformasi bahan tindak balas menerusi tapak mangkin. Discuss the physical and chemical steps in the transformation of reactants across a catalyst bed. Berikan ulasan dalam situasi bagaimanakah luas permukaan dalaman memberi kesan yang kecil keatas aktiviti mangkin. Comments on circumstances where internal surface area has a small effect on catalyst activity. 2. Bagaimanakah saiz dan bentuk partikel mangkin dapat mempengaruhi diffuse luaran dan dalaman untuk memastikan sistem tidak terkongkong daripada aliran jisim dan haba menerusi tapak mangkin. In designing a good catalyst, careful identification and selection chemical composition are important. For a reaction that will be involved dehydrogenation and isomerization reactions, Cadangkan kemungkinan fungsi-fungsi aktif untuk mengeluarkan hasil yang tinggi. Suggest probable active functions to give high product yield Bahan-bahan yang dapat digunakan untuk menambahbaik sifat-sifat mangkin seperti diatas. Materials that can be used to improve their catalytic properties of. 3. Titanium dwioksida adalah merupakan sistem mangkin persekitaran yang berpotensi untuk meleraikan bahan pencemaran di dalam air. Titanium dioxide is a promising environmental catalyst system to degrade pollutants in water. Bincangkan kaedah penyediaan prekursor titanium dwioksida secara kaedah mendakan. Discuss the method of preparing titanium dioxide precursor by solgel technique. 2/5

3 Nyatakan proses pengaktifan seterusnya untuk menghasilkan titanium dwiokasida yang aktif dan stabil. State the subsequent activation process to produce an active and stable titanium dioxide. 4. Reformasi nafta bermangkin untuk menghasilkan reformat yang beroktan tinggi menggunakan mangkin Pt-Re-Sn/Al 2 O 3 -Cl. ini aktif tetapi prestasinya menurun selepas beberapa jangka masa. Catalytic reforming of naphtha to produce high octane number reformate use Pt- Re-Sn/Al 2 O 3 -Cl catalyst. The catalyst is active but its performance decline over a period of time. Nyata dan bincangkan tiga (3) penyebab utama Pt-Re-Sn/Al 2 O 3 -Cl mengalami kedeaktifan berulang samada ke atas platinum atau alumina berklorida, State and discuss three (3) major causes for Pt-Re-Sn/Al 2 O 3 -Cl reversible deactivation either on platinum or chlorinated alumina, Cadangkan bagaimana ianya dapat dibaiki. Recommend on how the deactivated catalyst can be corrected 5. Bahan api hidrokarbon terpecah boleh dihasilkan secara pemecahan terma hidrokarbon berat. Kecekapan proses adalah optima dibantu oleh mangkin. Tindak balas ini selalunya di lakukan pada C, 50 barg dan LHSV 5. Proses ini apabila disokong oleh beberapa jenis sistem mangkin akan memberi prestasi pemangkinan yang berbeza. Pecahan distillate berat yang mengandungi campuran C15-C25 hidrokarbon alifatik dicampur dengan nitrogen sebelum tindak balas untuk meningkatkan tahap kecekepan proses. Cracked hydrocarbon fuels can be obtained by thermally cracking heavy hydrocarbons. The efficiency of the process is optimal assisted by catalyst. The reaction is typically run at C and 50 barg and LHSV of 5. The process supported by different types of catalyst systems give different catalytic performances. A heavy distillate fractions comprising of C15-C25 aliphatic hydrocarbons mixture were co-mixed with nitrogen prior to their catalytic reaction to increase process efficiency. 3/5

4 Jadual 1: Taburan komposisi (mol %) campuran tindak balas selepas 24 jam tindak balas ditambahbaikan oleh sistem A, B, C dan D. Table 1: Compositional distribution (mol%) of reaction mixture after 24 hours of reaction promoted by System A and B No Komposisi Components MASUK INLET A B C D Mol% Mol% Mol% Mol% KELUAR OUTLET 1 Hidrogen Hydrogen Nitrogen C15-C C C14- C C10 C C6 C C Untuk setiap sistem A dan B, hitungkan prestasi mangkin mengikut Jadual 2 dibawah: For each system A and B, calculate their catalytic performance as per Table 2 below: 4/5

5 Jadual 2: Prestasi Sistem A dan B. Table 2: Catalytic Performance of System A and B. Prestasi Catalytic Performance % Penukaran Bahan Suapan Hidrorkarbon % Conversion of Hydrocarbon Feed % Semua Hasil % All products % Selektiviti Metana % Selectivity of Diesel Fraction % Selektiviti Hidrogen % Yield of Hydrogen % Hasil Hidrokarbon ringan % Yield of Kerosene Fraction Isikan Jadual 2 untuk Sistem A dan B. Fill up Table 2, for the System A and B. Sistem System A Mol% Sistem System B Mol% (c) Bolehkah nitrogen didalam campuran bahan tindak balas ditukar dengan gas oksigen? Can nitrogen in the reaction feed be changed to oxygen? Sistem mangkin manakah yang boleh dicadangkan untuk proses ini dan berikan justifikasinya. Which catalyst system would you recommend for this process and provide justification. TAMAT END 5/5

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