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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2014/2015 : SEMESTER 2 ACADEMIC SESSION 2014/2015 : SEMESTER 2 SCES3319 : ELEKTROSINTESIS ELECTROSYNTHESIS Jun 2015 June 2015 Masa : 2 jam Time : 2 hours ARAHAN KEPADA CALON : INSTRUCTIONS TO CANDIDATES : Kertas soalan ini mengandungi Bahagian A dan B. This paper consists of Section A and B. Jawab soalan mengikut arahan yang diberikan dalam setiap bahagian. Questions should be answered according to the instructions given in each section. (Kertas ini mengandungi 6 soalan dalam 5 halaman yang dicetak) (This question paper consists of 6 questions on 5 printed pages)

2 BAHAGIAN A ( 50 MARKAH) SECTION A ( 50 MARKS) Jawab SEMUA soalan dalam Bahagian ini Answer ALL questions in this Section 1. Kinetik elektrod adalah kajian kadar tindak balas elektrokimia yang berlaku merentasi diantara fasa elektrod-elektrolit. Electrode kinetics is the study on the rate of electrochemical reaction that occurs across the electrode-electrolyte interface. (a) Namakan parameter-parameter yang diukur dalam eksperimen elektrod kinetik. Name the parameters that are measured in electrode kinetic experiment. Kenalpasti dan jelaskan faktor-faktor yang menjejaskan kinetik suatu tindak balas. Identify and explain the factors which influence the kinetics of a reaction. (5 markah/marks) Berdasarkan persamaan Butler-Volmer dan terbitan seterusnya, terangkan batasan potensi dalam kinetik elektrod. By using the Butler-Volmer equation and its derivation, explain the potential limitation in electrode kinetics. (8 markah/marks) 2. Suatu sel elektrokimia terdiri dari FeCl 3 (ak), CuCl 2 (ak) dan KCl(ak) sebagai elektrolit. Tindakbalas penurunan elektrod yang berlaku pada permukaan elektrod karbon gelas adalah: Fe 3+ (ak) + e - Fe 2+ (ak) Cu 2+ (ak) + 2Cl - (ak) + e - CuCl 2- (ak) (I) (II) An electrochemical cell consists of FeCl 3 (aq), CuCl 2 (aq) and KCl(aq) as supporting electrolyte. The electro-reduction reactions which occur at the glassy carbon working electrode surface are: Fe 3+ (aq) + e - Fe 2+ (aq) Cu 2+ (aq) + 2Cl - (aq) + e - CuCl 2- (aq) (I) (II) 2/5

3 (a) Berikan ion-ion yang bergerak ke arah permukaan elektrod dengan proses pembauran. Give the ions which move towards the electrode surface by diffusion. Berikan ion-ion yang bergerak ke arah permukaan elektrod dengan proses penghijrahan ion. Give the ions which move towards the electrode surface by ionic migration. Apakah peranan elektrolit KCl? What is the role of the electrolyte, KCl? (d) Jelaskan perubahan yang berlaku terhadap arus penurunan dan pergerakan ion-ion bagi tindakbalas (I) dan (II) apabila elektrod karbon gelas diputarkan dengan kelajuan tinggi. When the glassy carbon electrode is rotated at high speeds, explain the changes on reduction current and movement of each ion species for both reaction (I) and (II). (7 markah/marks) 3. (a) Nama dan jelaskan satu bahan yang biasa digunakan dalam pengubahsuaian permukaan elektrod. Name and explain one of the common materials used in electrode surface modification. (3 markah/marks) Berdasarkan pada bahan yang anda pilih di 3 (a), terangkan persediaan eksperimen bagi proses elektropempolimeran. Based on your chosen material in 3 (a), describe the experimental setup for an electropolymerisation process. Namakan TIGA kebaikan dan keburukan dalam kaedah elektroenapan. Name THREE advantages and disadvantages of electrodeposition method. 3/5

4 (d) Bincangkan kepentingan pra-rawatan bagi permukaan elektrod sebelum proses elektroenapan. Discuss the importance of having electrode surface pre-treatment before carrying out electrodeposition. (7 markah/marks) BAHAGIAN B ( 50 MARKAH) SECTION B ( 50 MARKS) Jawab SEMUA soalan Answer ALL questions 4. (a) Kirakan had arus yang dijangkakan daripada penurunan 2 x 10-4 M Pb 2+ menggunakan elektro mikro disk, d=10 m dan pekali pembauran bagi Pb 2+ ialah 1.01 x10-5 cm 2 /s. Bagaimanakah mengurangkan kesan pemindahan ion. Berikan satu contoh. Calculate the limiting current that would be expected from the reduction of 2 x10-4 M Pb 2+, using micro disc electrode, d= 10 m and the diffusion coefficient of Pb2+ is 1.01 x10-5 cm 2 /s. How to reduce the ion migration effect. Give one example. Lakarkan tindak balas siklik voltamogram untuk satu campuran yang mengandungi 3 mm Cu 2+, 2 mm Z n2+ and 1 mm Cd 2+. Keupayaan permulaan adalah 0 V, mengimbas ke arah keupayaan positif kepada 1.5 V, kemudian berbalik dan mengimbas kepada -1.5 V dan berakhir pada 0 V. Keupayaan voltammogram bagi unsur Cu, Zn, dan Cd masing-masing adalah -0.12, dan V. Tulis tindak balas elektrokimia daripada semua spesies. Kaitkan siklik voltammogram di atas dengan plot keupayaan vs masa. Sketch the cyclic voltammogram response for a mixture containing 3 mm Cu 2+, 2 mm Zn 2+ and 1 mm Cd 2+. The start potential is 0 V, scan towards positive potential to 1.5 V, than reverse and scan to -1.5 V and end at 0 V. The voltammogram potentials for the elemental Cu, Zn, and Cd are -0.12, and respectively. Write the electrochemical reaction of all species. Relate the above cyclic voltammogram with potential vs time plot. 4/5

5 Tuliskan mekanisme umum bagi dua langkah keupayaan kronokulometri. Lakarkan bentuk gelombang keupayaan bagi (a) teknik dua langkah tidakbalas arus dan tindakbalas cas. Write the general mechanism for double potential steps chronocoulometry. Sketch potential wave form of (a) double step technique the current response and the charge response. (10 markah/marks) 5. (a) Proses industri yang manakan boleh menghasilkan larutan kaustik soda yang sangat tulen? Terangkan proses tersebut dan sertakan kebaikan dan keburukannya. Lukiskan digram yang ringkas untuk menerangkan proses itu. Which industrial process can produce extremely pure caustic soda solution? Describe the process and include an advantage and disadvantage. Draw a simple diagram to explain the process. (8 markah/marks) Terangkan proses diaphragm. Describe the diaphragm process. 6. (a) Apakah proses electrokimia berpasangan? Senaraikan jenis-jenis proses elektrokimia berpasangan dan berikan contoh bagi setiap jenis. What is the paired electrochemical process? List the types of paired electrochemical process and give example for each type. (10 markah/marks) Apa yang anda faham tentang tindak/balas Kolbe atau electrolysis Kolbe? Tuliskan tindak/balas keseluruhan umum. Apakah yang akan berlaku jika dua karboksilat yang berbeza digunakan di dalam tindak balas? What do you understand by Kolbe reaction or Kolbe electrolysis? Write the general overall reaction. What will happen if two different carboxylates are used in the reaction? (4 markah/marks) TAMAT END 5/5

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