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1 UNIVERSITI MALAYA UNIVERSITY OF MALAYA PEPERIKSAAN IJAZAH SARJANA MUDA SAINS EXAMINATION FOR THE DEGREE OF BACHELOR OF SCIENCE SESI AKADEMIK 2016/2017 ACADEMIC SESSION 2016/2017 : SEMESTER I : SEMESTER I SCES3352 : BAHAN KOMPOSIT POLIMER POLYMER COMPOSITE MATERIALS Dis 2016/Jan 2017 Dec 2016/Jan 2017 Masa: 2 jam Time: 2 hours ARAHAN KEPADA CALON: INSTRUCTIONS TO CANDIDATES: (1) Jawab SEMUA soalan. Answer ALL questions. (2) Mulakan jawapan untuk soalan baru di atas muka surat yang baru. Answer for new question should start on the new page. (3) Tandakan nombor soalan pada muka hadapan buku jawapan mengikut urutan/susunan jawapan di dalam buku jawapan. Indicate question number on the front page of answer book in the same order as answer in the book(s). (4) Jawapan boleh diberikan samada di dalam Bahasa Malaysia atau Bahasa Inggeris. Answer can be written in either Malay or English. (Kertas soalan ini mengandungi 4 soalan dalam 7 halaman yang bercetak) (This question paper consists of 4 questions on 7 printed pages)

2 1. Terangkan secara ringkas kenyataan berikut:- Briefly explain the following statements:- Perbezaan diantara pemprosesan komposit dengan menggunakan kaedah berterusan dan satu demi satu/kumpulan demi kumpulan (batch). The differences between processing of composites using continuous and batch processes Persamaan hukum campuran mudah berikut untuk menjangka modulus Young bahan komposit adalah susuai untuk komposit diperkuat dengan gentian selanjar dan juga tidak selanjar. Terangkan. The following simple rule of mixture equation for the Young s modulus of composite materials is also a good approximation for both continuous and discontinuous fibre reinforced composites. Explain. E c = E f V f + E m V m (c) (d) (e) Tidak semua sifat-sifat komposit gentian pendek adalah kurang baik daripada komposit gentian panjang. Not all properties of short fibre composites are worst than those of long fibre composites Jika partikel getah digunakan sebagai pengisi tambahan dalam bakan untuk membuat bumper kereta, apakah alasan disebalik penggunaan ini?. If rubber particles were added as additional filler for the materials in making bumper for cars, what is the reason behind this application? Bahan yang sama mungkin mengalami mekanisma kegagalan yang berbeza apabila pemutusan/pemecahan berlaku dengan halaju beban yang berbeza. The same materials may fail in different failure mechanisms when breakage occurred due to different speed loading. (4 markah setiap satu, jumlah 20 markah/4 marks each, total 20 marks) 2. Dengan merujuk kepada komposit diperkuat dengan gentian kaca:- With reference to the composite reinforced with glass fibres:- 2/7

3 Terangkan kaedah untuk menyediakan sampel pengujian komposit termoplastik diperkuat dengan gentian pendek dan gentian panjang secara acuan suntikan daripada bahan mentah. Describe the procedure to prepare injection moulded test specimens of short and long fibre reinforced thermoplastic composites from starting materials. Terangkan kebaikan dan kekurangan komposit gentian panjang dibandingkan dengan komposit gentian pendek dari segi sifat-sifatnya. Discuss the advantages and disadvantages of long fibre composites over short fibre composites, in terms of their properties. (6 markah/marks) (c) Dalam satu penggunaan, komposit gentian hibrid disediakan dengan menggunakan gentian kaca dan aramida sebagai pengkuat untuk acrylonitrile butadiene styrene (ABS). Apakah sebab yang mungkin untuk pemilihan ini? In one application, a hybrid fibre composite was prepared using glass and aramid fibres as reinforcement for acrylonitrile butadiene styrene (ABS). What is the possible reason behind this selection? (4 markah/marks) 3. Seberat 1.93 g sampel komposit poliamida 6,6 diperkuat dengan gentian tidak selanjar daripada bahagian tengah kepingan ujian regangan yang disediakan dengan acuan suntikan telah dipotong. Matriks polimer diasingkan dengan membakar di dalam ketuhar dan 0.43 g gentian telah dikumpul. Hasil daripada analisis taburan panjang gentian dan analisis komposit secara teori menggunakan model Kelly-Tyson diberikan dalam Jadual 1. A 1.93 g sample of discontinuous fibre reinforced polyamide 6,6 composite was cut from the central portion of an injection moulded tensile test piece. The polymer matrix was burnt-off by heating the composite specimen in a muffle furnace and 0.43 g of fibre was collected. Results from the fibre length distribution (FLD) and the theoretical analyses using Kelly-Tyson model of the composites are given in Table 1. 3/7

4 Jadual 1 / Table 1 L i V f,i σ uc,i (mm) N i (%) (MPa) A B C Dalam Jadual 1, L i, N i, V f,i dan σ uc,i ialah panjang gentian untuk pecahan ke-i, nombor (bilangan) gentian dengan pajang L i, pecahan isipadu gentian dengan panjang L i dan kekuatan regangan komposit yang disumbangkan oleh gentian dengan panjang L i masing-masingnya. Jumlah isipadu gentian yang dikira (ΣL i N i r f 2 ) ialah x m 3. In Table 1, L i, N i, V f,i and σ uc,i are the fibre length of fraction i, the number (count) of fibre with length L i, the volume fraction of fibre with length L i and the tensile strength of the composite contributed by the fibre with length L i respectively. The total volume of counted fibres (ΣL i N i r f 2 ) is x m 3. 4/7

5 Sifat-sifat matrik, gentian dan komposit yang ditentukan secara percubaan diberikan dalam Jadual 2. Regangan matrik pada pemanjangan 2.46% ialah 45 MPa dan kekuatan ricih antaramuka gentian-matrik ialah 48 MPa. Diameter and modulus Young gentian ialah 10 μm dan 73 Gpa, masingmasingnya. Some of the properties of matrix, fibre and composite determined experimentally are given in Table 2. Stress in the matrix at 2.46% strain is 45 MPa and the fibre-matrix interfacial shear strength is 48 MPa. Diameter and Young s modulus of the fibre are 10 μm and 73 Gpa, respectively. Jadual 2 / Table 2 Sifat Unit Matrik Gentian Komposit Properties Unit Matrix Fibre Composite Kekuatan regangan Tensile strength Ketumpatan Density Pemanjangan pemutusan Tensile strain MPa kg/m (%) Apakah jenis gentian yang digunakan dalam komposit ini? Terangkan. Takrifkan panjang gentian kritikal, L c dan kirakan nilainya. What was the type of fibre used in this composite? Explain. Define critical fibre length, L c and calculate its value. (4 markah/marks) Kirakan pecahan isipadu gentian dan matrik dalam komposit. Calculate the volume fractions of fibre and matrix in the composite. (4 markah/marks) (c) Kirakan nilai-nilai A, B dan C dalam Jadual 1. Calculate the values of A, B and C in Table 1. (12 markah/marks) 5/7

6 (d) Kirakan sumbangan daripada matrik, gentian sub-kritikal dan gentian super-kritikal kepada komposit. Calculate the contribution from the matrix, sub-critical fibre and super-critical fibre to the composite. (5 markah/marks) (e) Kirakan kekuatan regangan dijangka bagi komposit. Jika nilai ini banyak berbeza dibadingkan dengan nilai yang didapati secara percubaan (Jadual 2), apakah kemungkinan alasan untuk ini? Calculate the expected tensile strength of the composite. If this value is significantly different compared to the experimentally determined strength (Table 2), what are the possible reasons for this? 4. Jawab tiga (3) daripada yang berikut:- Answer three (3) of the following:- (5 markah/marks) Apakah yang dimaksudkan dengan satu kitar operasi dalam pemprosesan bahan komposit? Dengan merujuk kepada samada mesin acuan suntikan atau mesin acuan tekan atau mesin vacuum bag autoclave, jelaskan jawapan anda. What is the meaning of one cycle of operation in composite materials processing? With reference to either an injection moulding machine or a compression moulding machine or vacuum bag autoclave, explain your answer. Bincangkan potensi kegunaan gentian asli sebagai pengisi/pengkuat kepada komposit polimer. Discuss the potential application of natiral fibre as filler/reinforcement for polymer composites. 6/7

7 (c) Berikan lakaran asas pembinaan mesin/rekabentuk untuk samada mesin acuan suntikan, mesin acuan tekan atau ekstruder. Terangkan fungsi asasnya. Give the diagram of the basic machine construction / design for either an injection moulding machine, a compression moulding machine or an extruder. Label the important parts or components and explain their functions. (d) Penyediaan, sifat-sifat dan kegunaan gentian aramida sebagai tetulang untuk bahan komposit Preparation, properties and applications of aramid fibre as reinforcement for composite materials. TAMAT END 7/7

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