Three Mile Creek Watershed Management Plan

Transcription

1 Three Mile Creek Watershed Management Plan Appendix E Groundwater, sediment and stormwater sampling and s USA Sampling and Testing Plan Assess groundwater contribution up and down gradient. Groundwater flow and samples will be obtained from river craft and will not require site access. Perform Subtitle analysis. Parameters: Groundwater flow rate and volume; Priority Pollutants; TKN, NH, and NOx, SRP and TP; BO; CO; fecal coliform (freshwater reaches), Enterococcus (brackish water reaches); field ph, conductivity, O, temp., ORP. Frequency: Once in September. ry weather - rainfall must be less than 0.-inches for prior hours. Samples: - each from sites; two up gradient and two down gradient of landfill; one pair for One Mile Creek and one pair for TMC. Assumes all samples will be brackish water. Please note brackish water samples on sample containers. Groundwater contribution assessment throughout TMC Assess groundwater contribution at various points throughout the watershed. Groundwater flow and samples can be obtained from river craft and will not require site access. Propose to perform limited list of parameters for analysis. One sample session can be performed this summer. Project also has potential for long term sampling in future years. Parameters: Surface water flow rate; RCRA metals; TKN, NH, and NOx; SRP and TP; BO; CO; fecal coliform (freshwater reaches), Enterococcus (brackish water reaches); field ph, conductivity, O, temp., ORP, turbidity, salinity. Frequency: Once in September. ry weather - rainfall must be less than 0.-inches for prior hours. Sites: 0 each from sites, see map provided in Figure -. Please note brackish water samples on sample containers. Sediment sample assessment throughout TMC Assess sediments at various points throughout the watershed. Three samples will be obtained from each site and composited for analysis. Samples will be obtained from river craft and will not require site access. Mobile Bay National Estuary Program TMC Watershed Management Plan E-

2 Parameters: RCRA metals; moisture content; organic content; TN; TP; BO; CO; fecal coliform (freshwater reaches), Enterococcus (brackish water reaches); visual characterization. Frequency: Once in September. ry weather, rainfall less than 0.-inches for hours. Samples: each from sites, see map. Please note brackish water samples on sample containers. USA Field Report Groundwater and Sediment Sample Collection In The Three Mile Creek Watershed Graduate student researchers from the University of South Alabama Marine Sciences and Environmental Toxicology programs collected groundwater and sediment samples at locations throughout the Three Mile Creek watershed in Mobile, Alabama during September and October 0. The locations of these sample sites are displayed on Figures and below. These samples were collected to: ) Generically assess the chemical makeup of baseflow/groundwater entering Three Mile Creek and selected tributaries throughout the watershed; ) Generally characterize any contaminants entrained in the creek E- revised 0--0 Mobile Bay National Estuary Program TMC Watershed Management Plan

3 Three Mile Creek Watershed Management Plan sediments in the watershed; and ) Specifically assess the chemical composition of groundwater entering the creek system from an abandoned municipal solid waste landfill located near downtown Mobile (the Hickory Street Landfill). The details of each of these sample subsets are described below, along with relevant information regarding sample collection and handing procedures. Watershed Baseflow/Groundwater Samples Baseflow/groundwater (GW) samples were collected at the locations displayed on Figure. The exception was location, where access concerns have prevented the collection of any samples to date. Sampling was accomplished at all other locations using mini piezometers such as the one described schematically in Figure. Each of these was constructed onsite using PVC well screen, riser pipe, and fittings. A clear plastic sampling tube was attached to each mini piezometer. This tube was in turn connected at the surface to a peristaltic pump. Figure. Mini piezometer schematic. PVC cap ~-inch length of -inch diam. PVC pipe PVC tube connector ~ inches of -inch diam. PVC well screen PVC cap At sampling locations GW through GW mini piezometers were emplaced into the creek bottom sediments close to the shoreline so that the screened section was completely buried. Prior to sampling, each piezometer was pumped for a few minutes and then allowed to rest. After a short equilibration period, the pressure of groundwater in the tubes at each sampling location was visually gauged and measured. Positive pressure gradients (groundwater rising in the tube above the level of local surface water) were indicative of groundwater flow into the creek. If no positive gradient was observed, the mini piezometer was relocated to other spots closer to shore at the same sampling location until a positive gradient was observed. Mobile Bay National Estuary Program TMC Watershed Management Plan E-

4 Piezometers displaying positive pressure gradients were sampled. To accomplish this, each was purged using a peristaltic pump and low-flow/low-stress sampling techniques. Purging began with withdrawal of water from each mini piezometer at a rate that balanced discharge and recharge (equilibrium) and ended with the stabilization of field temperature, ph, and specific conductance readings as follows: ph = +/- 0.0 Temperature = +/- 0. ºC Conductivity = +/- % Once the field parameters stabilized, groundwater was collected from the discharge stream of the peristaltic pump. For collection of VOC samples, the peristaltic pump discharge rate was placed on the lowest setting to minimize sample agitation. Once collected, each sample was placed into a laboratory-provided sample container for subsequent laboratory analysis. Sample containers were labeled with waterproof ink, placed on ice in sealed laboratory-supplied coolers, and transported to the laboratory (TestAmerica Laboratories at 00 Lakeside rive, Mobile, Alabama) for analysis within allotted holding times. Complete chain-of-custody documentation accompanied all coolers. Personnel involved in groundwater (and all other) sampling wore clean latex gloves that were disposed of after each sample was collected, along with all tubing and other expendables used during the process. Non-disposable sampling equipment (probes, etc.) was decontaminated prior to reuse using the following five-step procedure: ) Phosphate-free detergent wash ) Potable water rinse ) eionized water rinse ) Isopropanol rinse ) eionized water rinse and air dry E- revised 0--0 Mobile Bay National Estuary Program TMC Watershed Management Plan

5 Three Mile Creek Watershed Management Plan Groundwater Sample s Matrix Reports detailing the Groundwater Sample Resulsts can be found according to the site location in the table below. The reports follow at the end of this Appendix. For example, at site GW, the BO results can be found in the report with on the cover. Sample Site Name GW Groundwater Sample Restults Report Name Gen Chem O-P P Metals BO Enterococci Coliform, Fecal * * GW * * * * * - * * GW GW Mobile Bay National Estuary Program TMC Watershed Management Plan E-

6 Sample Site Name Groundwater Sample Restults Report Name Gen Chem O-P P Metals BO Enterococci Coliform, Fecal GW * * GW GW GW * E- revised 0--0 Mobile Bay National Estuary Program TMC Watershed Management Plan

7 Three Mile Creek Watershed Management Plan Sample Site Name GW Groundwater Sample Restults Report Name Gen Chem O-P P Metals BO Enterococci Coliform, Fecal GW *Sample results not obtained. Sediment Samples Sediment (S) samples were collected at the same locations as the baseflow/groundwater samples (Figure ). These samples were collected from the upper to inches of sediment in the creek bed near the shoreline. At each sampled location (S through S), previously undisturbed sediment was collected using a glass container and then placed in a decontaminated glass mixing bowl. The material was then carefully homogenized with a glass mixing spoon. Subsequently, aliquots from the composited sample were placed in each laboratory-supplied sample container. These were then sealed, labeled, and placed on ice in laboratory-supplied coolers. The sealed coolers, along with completed chain-of-custody forms, were driven to the laboratory within allotted holding times for analysis. Mobile Bay National Estuary Program TMC Watershed Management Plan E-

8 Sediment Sample s Matrix Reports detailing the Sediment Sample Resulsts can be found according to the site location in the table below. The reports follow at the end of this Appendix. For example, at site S, the Coliform, Fecal results can be found in the report with on the cover. Sample Site Sediment Sample Report Restults Name Metals Gen Chem Coliform, Fecal S * S * * * S S S * S E- revised 0--0 Mobile Bay National Estuary Program TMC Watershed Management Plan

9 Three Mile Creek Watershed Management Plan Sample Site Sediment Sample Report Restults Name Metals Gen Chem Coliform, Fecal S S S S *Sample results not obtained. Mobile Bay National Estuary Program TMC Watershed Management Plan E-

10 Hickory Street Landfill Samples Four locations (HS-,,, and ) were targeted for acquisition of groundwater discharge samples in the vicinity of the Hickory Street Landfill at the locations shown on Figure. One of these samples (HS-) was located upgradient of the landfill and three (HS- through ) were located downgradient. The HS- location was accessed by land at Earle Street bridge in the Orange Grove subdivision just north of Beauregard Street. The three downgradient sampling sites were all accessed by boat. At each HS sampling location, a mini piezometer (Figure ) was constructed and emplaced into the creek bottom close to the shoreline as described above. This allowed for low-flow/low-stress sample acquisition using a peristaltic pump. All HS groundwater sample acquisition, handing, and documentation/transport procedures, as well as all decontamination procedures, were carried out as described previously. Four locations (HS-,,, and ) were targeted for acquisition of groundwater discharge samples in the vicinity of the Hickory Street Landfill at the locations shown on Figure. One of these samples (HS-) was located upgradient of the landfill and three (HS- through ) were located downgradient. The HS- location was accessed by land at Earle Street bridge in the Orange Grove subdivision just north of Beauregard Street. The three downgradient sampling sites were all accessed by boat. E- revised 0--0 Mobile Bay National Estuary Program TMC Watershed Management Plan

11 Three Mile Creek Watershed Management Plan Stormwater Sample s Matrix Reports detailing the Stormwater Sample Resulsts can be found according to the site location in the table below. The reports follow at the end of this Appendix. For example, at site HS, the Phenol results can be found in the report with on the cover. Sample Stormwater Sample Report Restults Site Name P O-P Metals VOC Semi-VOC PCB BO Phenol Gen Chem Cyanide HS HS HS Mobile Bay National Estuary Program TMC Watershed Management Plan E-

12 Sample Stormwater Sample Report Restults Site Name P O-P Metals VOC Semi-VOC PCB BO Phenol Gen Chem Cyanide * * HS *Sample results not obtained. E- revised 0--0 Mobile Bay National Estuary Program TMC Watershed Management Plan

13 Three Mile Creek Watershed Management Plan Laboratory Reports from USA Sampling iscussed Above Continued on next page. Mobile Bay National Estuary Program TMC Watershed Management Plan E-

14 ANALYTICAL REPORT TestAmerica Laboratories, Inc. McLemore rive Pensacola, FL Tel: (0)-0 TestAmerica Job I: Client Project/Site: Three Mile CreekUSA-Surface Water/Solids For: ewberry 0 Rexwoods r. Raleigh, North Carolina 0 Attn: Michael Hanson Authorized for release by: /0/0 ::0 PM Mike Nance, Project Manager II ()- mike.nance@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

15 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Table of Contents TestAmerica Job I: Cover Page Table of Contents efinitions Case Narrative Sample Summary Client Sample s QC Sample s Chronicle Method Summary Chain of Custody Page of /0/0

16 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids s Metals J General Chemistry escription efinitions/glossary is less than the but greater than or equal to the ML and the concentration is an approximate value. escription * LCS or LCS exceeds the control limits F J Glossary Abbreviation MS/MS Recovery and/or RP exceeds the control limits is less than the but greater than or equal to the ML and the concentration is an approximate value. These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF ER L, RA, RE, IN LC MA EL MC ML ML NC N PQL QC RER RP TEF TEQ Contains no Free Liquid uplicate error ratio (normalized absolute difference) ilution Factor Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample ecision level concentration Minimum detectable activity Estimated etection Limit Minimum detectable concentration Method etection Limit Minimum Level (ioxin) Not Calculated Not detected at the reporting limit (or ML or EL if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent ifference, a measure of the relative difference between two points Toxicity Equivalent Factor (ioxin) Toxicity Equivalent Quotient (ioxin) TestAmerica Job I: Page of /0/0

17 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Surface Water/Solids Job I: Laboratory: Narrative Comments No additional comments. Job Narrative Receipt The samples were received on //0 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. Metals No analytical or quality issues were noted. General Chemistry Method(s)., SM 0G: The laboratory control sample (LCS) for batch recovered outside control limits for the following analytes: Volatile Total Solids. These analytes were biased high in the LCS. Method(s).: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s).: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s).: The matrix spike duplicate (MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. No other analytical or quality issues were noted. Organic Prep No analytical or quality issues were noted. Page of /0/0

18 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received S- 00 Solid 0// : 0// 0: S-00 Solid 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// :0 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: S-00 Solid 0// :0 0// 0: S-00 Solid 0// :0 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// :0 0// 0: G-00 Water 0// :0 0// 0: Page of /0/0

19 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: S- 00 ate Collected: 0// : ate Received: 0// 0: Method: 0B - Metals (ICP) Client Sample s ML TestAmerica Job I: Lab Sample I: Percent Solids:. Silver < mg/kg 0// 0:0 0// : Arsenic <0. Barium. Cadmium <0. Chromium. Lead. Selenium <0. Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML mg/kg 0// 0:0 0// :. 0. mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// :. 0. mg/kg 0// 0:0 0// : Hg mg/kg 0// 0: 0// : Client Sample I: S-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: Percent Solids:. General Chemistry Nitrogen, Kjeldahl. mg/kg 0// : 0// :0 Phosphorus, Total ML. mg/kg 0// : 0// : Total Volatile Solids 0.0 * % 0// :0 General Chemistry - ASTM Leach ML Chemical Oxygen emand <.0.0 mg/l 0/0/ : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Biochemical Oxygen emand..0.0 mg/l 0// :0 Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// : 0// : Arsenic < mg/l 0// : 0// : Barium mg/l 0// : 0// : Cadmium < mg/l 0// : 0// : Chromium < mg/l 0// : 0// : Lead mg/l 0// : 0// : Selenium < mg/l 0// : 0// : Page of /0/0

20 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: Method: 0A - Mercury (CVAA) Client Sample s ML TestAmerica Job I: Lab Sample I: Mercury < mg/l 0// 0:0 0// : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: General Chemistry ML Lab Sample I: Ammonia mg/l 0// :0 Nitrogen, Kjeldahl. Nitrate Nitrite as N 0.0 J Chemical Oxygen emand mg/l 0// : 0// : mg/l 0// 0:. mg/l 0// : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML ortho-phosphate < mg/l 0// : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Ammonia mg/l 0// :0 Chemical Oxygen emand. mg/l 0// : Client Sample I: S-00 ate Collected: 0// :0 ate Received: 0// 0: Lab Sample I: Percent Solids: 0. Method: 0B - Metals (ICP) Silver < mg/kg 0// 0:0 0// :0 Arsenic. Barium. Cadmium <0. Chromium. Lead. Selenium <0. Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML ML mg/kg 0// 0:0 0// :0. 0. mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// :0. 0. mg/kg 0// 0:0 0// :0 Hg < mg/kg 0// 0: 0// : Page of /0/0

21 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: S-00 ate Collected: 0// :0 ate Received: 0// 0: General Chemistry Client Sample s ML TestAmerica Job I: Lab Sample I: Percent Solids: 0. Nitrogen, Kjeldahl. mg/kg 0/0/ : 0// :0 Phosphorus, Total. mg/kg 0// : 0// : Total Volatile Solids 0.0 * % 0// :0 General Chemistry - ASTM Leach ML Chemical Oxygen emand <.0.0 mg/l 0/0/ : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Ammonia mg/l 0// :0 Nitrogen, Kjeldahl mg/l 0// : 0// : Chemical Oxygen emand. mg/l 0// : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML ortho-phosphate < mg/l 0// : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Phosphorus mg/l 0// : 0// 0:0 Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// : 0// : Arsenic < mg/l 0// : 0// : Barium mg/l 0// : 0// : Cadmium < mg/l 0// : 0// : Chromium < mg/l 0// : 0// : Lead 0.00 J mg/l 0// : 0// : Selenium < mg/l 0// : 0// : Page of /0/0

22 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample s TestAmerica Job I: Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: Method: 0A - Mercury (CVAA) ML Lab Sample I: Mercury < mg/l 0// 0:0 0// : Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: General Chemistry ML Lab Sample I: Biochemical Oxygen emand mg/l 0// :0 Page of /0/0

23 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method: 0B - Metals (ICP) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Silver < mg/kg 0// 0:0 0// : Arsenic Barium Cadmium Chromium Lead Selenium ML < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Silver.. mg/kg - Arsenic mg/kg - Barium 0 mg/kg - Cadmium.0. mg/kg - Chromium mg/kg - Lead mg/kg - Selenium.. mg/kg - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : Prep : MB MB Silver < mg/l 0// : 0// : Arsenic Barium Cadmium Chromium Lead Selenium ML < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : Prep : LCS LCS %Rec Silver mg/l 0 - Arsenic mg/l 0 - Barium.00.0 mg/l 0 - Cadmium mg/l 0 - Chromium.00.0 mg/l 0 - Lead.00.0 mg/l 0 - Selenium.00.0 mg/l 0 - Page of /0/0

24 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method: 0A - Mercury (CVAA) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Mercury < mg/l 0// 0:0 0// :00 ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l 0 - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Mercury J mg/l 0// 0:0 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l 0 - Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Hg < mg/kg 0// 0: 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Hg.. mg/kg 0 - Method:. - Solids, Total Volatile (TVS) Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB Total Volatile Solids < % 0// :0 Page of /0/0

25 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method:. - Solids, Total Volatile (TVS) (Continued) Lab Sample I: LCS 00-/ Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Total Volatile Solids 0.0 <0. * % - Lab Sample I: U Analysis : Sample Sample LCS LCS %Rec Client Sample I: S-00 Prep Type: Total Volatile Solids 0.0 * 0.00 * % Method: 0. - Nitrogen, Ammonia U U RP RP Limit Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Ammonia < mg/l 0// : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Ammonia.00. mg/l 0 - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Ammonia mg/l 0 - Lab Sample I: MS Client Sample I: G-00 Prep Type: Analysis : Sample Sample MS MS %Rec Ammonia mg/l 0 - Lab Sample I: MS Client Sample I: G-00 Prep Type: Analysis : Sample Sample MS MS RP %Rec RP Limit Ammonia mg/l 0 - Page of /0/0

26 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method:. - Nitrogen, Total Kjeldahl QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/l 0// : 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/l 0 - Lab Sample I: M 00-/ M Analysis : Client Sample I: Lab Control Sample Prep Type: Nitrogen, Kjeldahl J mg/l 0 - M M %Rec Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/kg 0/0/ : 0// :0 ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/kg - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Nitrogen, Kjeldahl 0 F mg/kg 0 - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec Nitrogen, Kjeldahl F mg/kg 0-0 Lab Sample I: M 00-/ M Analysis : Nitrogen, Kjeldahl J mg/kg M M %Rec RP Limit Client Sample I: Lab Control Sample Prep Type: Page of /0/0

27 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/kg 0// : 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/kg - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Nitrogen, Kjeldahl F mg/kg 0 - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec Nitrogen, Kjeldahl 0 F mg/kg 0-0 Lab Sample I: M 00-/ M Analysis : Nitrogen, Kjeldahl mg/kg M M %Rec RP Limit Client Sample I: Lab Control Sample Prep Type: Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Nitrate Nitrite as N < mg/l 0// 0: Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Nitrate Nitrite as N mg/l 0 - Page of /0/0

28 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method:. - Nitrogen, Nitrate-Nitrite (Continued) Lab Sample I: M 00-/ M Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N J mg/l 0 - Method:. - Phosphorus, Ortho Lab Sample I: MB 00-/ Analysis : MB MB M M %Rec ML Client Sample I: Method Blank Prep Type: ortho-phosphate < mg/l 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec ortho-phosphate mg/l Method:. - Phosphorus, Total Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phosphorus < mg/l 0// : 0// 0: Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus mg/l 0 - Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec RP Limit Phosphorus mg/l 0-0 Page of /0/0

29 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method:. - Phosphorus, Total QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Phosphorus, Total < mg/kg 0// : 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus, Total.0. mg/kg - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Phosphorus, Total.. mg/kg - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec Phosphorus, Total.. F mg/kg - 0 Lab Sample I: M 00-/ M Analysis : Phosphorus, Total J mg/kg M M %Rec RP Limit Client Sample I: Lab Control Sample Prep Type: Method: SM B - BO, -ay Lab Sample I: USB 00-/ USB Client Sample I: Method Blank Prep Type: Analysis : USB USB ML Biochemical Oxygen emand < mg/l 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Biochemical Oxygen emand 0 mg/l - Page of /0/0

30 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method: SM B - BO, -ay (Continued) Lab Sample I: LCS 00-/ Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample up Prep Type: Biochemical Oxygen emand mg/l - Method: SM 0 - CO Lab Sample I: MB 0-/ Analysis : MB MB LCS LCS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.0.0 mg/l 0/0/ : Lab Sample I: LCS 0-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Chemical Oxygen emand 0.0. mg/l 0 - Lab Sample I: LCS 0-/ Analysis : LCS LCS %Rec Client Sample I: Lab Control Sample up Prep Type: Chemical Oxygen emand mg/l 0-0 Lab Sample I: MB 00-/ Analysis : MB MB LCS LCS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.. mg/l 0// : Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Chemical Oxygen emand 0.0. mg/l 0 - Lab Sample I: LB 0-0/-A LB Analysis : LB LB LCS LCS %Rec ML Client Sample I: Method Blank Prep Type: ASTM Leach Chemical Oxygen emand <.0.0 mg/l 0/0/ : Chemical Oxygen emand <.0.0 mg/l 0/0/ : Page of /0/0

31 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method: SM 0 - CO (Continued) Lab Sample I: U Analysis : Sample Sample QC Sample s TestAmerica Job I: Client Sample I: S-00 Prep Type: ASTM Leach Chemical Oxygen emand <.0 <.0 mg/l NC 0 U U RP RP Limit Page of /0/0

32 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: S- 00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Percent Solids:. Prep Type Type Method Run ilution Factor Number or Analyst Prep B 0// 0: JAP TAL PEN Analysis B 0// : JAP TAL PEN Prep 00B 0// 0:0 NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Analysis Moisture 0// :00 LEC TAL PEN Client Sample I: S-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Lab Prep Type ASTM Leach ASTM Leach Type Method Run ilution Factor Number or Analyst Analysis Moisture 0// :00 LEC TAL PEN Analysis. 0// :0 CAC TAL PEN Prep././ 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Prep. 0// : JAT TAL PEN Analysis. 0// :0 JAT TAL PEN Leach - 0 0// : SJM TAL NSH Analysis SM 0 0/0/ : MSJ TAL NSH Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B GMF TAL PEN (Start) (End) 0// :0 0// :0 Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A 0// 0:0 JAP TAL PEN Analysis 0A 0// : JAP TAL PEN Lab Page of /0/0

33 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis 0. 0// :0 KJR TAL PEN Analysis. 0// 0: KJR TAL PEN Analysis SM 0 0// : JMH TAL PEN Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Lab Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : LSS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0. 0// :0 KJR TAL PEN Analysis SM 0 0// : JMH TAL PEN Lab Client Sample I: S-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Percent Solids: 0. Prep Type Type Method Run ilution Factor Number or Analyst Prep B 0// 0: JAP TAL PEN Analysis B 0// : JAP TAL PEN Prep 00B 0// 0:0 NAB TAL PEN Analysis 0B 0// :0 SLM TAL PEN Analysis Moisture 0// :00 LEC TAL PEN Lab Client Sample I: S-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis Moisture 0// :00 LEC TAL PEN Analysis. 0// :0 CAC TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// :0 JAT TAL PEN Prep././ 0// : JAT TAL PEN Lab Page 0 of /0/0

34 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: S-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Percent Solids: 0. Prep Type ASTM Leach ASTM Leach Type Method Run ilution Factor Number or Analyst Analysis. 0// : JAT TAL PEN Leach - 0 0// : SJM TAL NSH Analysis SM 0 0/0/ : MSJ TAL NSH Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Lab Lab Analysis 0. 0// :0 KJR TAL PEN Analysis SM 0 0// : JMH TAL PEN Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : LSS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Prep././ 0// : QMC TAL TAL Analysis. 0// 0:0 QMC TAL TAL Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A 0// 0:0 JAP TAL PEN Analysis 0A 0// : JAP TAL PEN Lab Page of /0/0

35 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Surface Water/Solids Client Sample I: G-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Laboratory References: Type Method Run ilution Factor Number or Analyst Analysis SM B GMF TAL PEN (Start) (End) TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- 0// :0 0// :0 Lab Page of /0/0

36 Client: ewberry Project/Site: Three Mile CreekUSA-Surface Water/Solids Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory 0B Metals (ICP) SW TAL PEN 0A Mercury (CVAA) SW TAL PEN B Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) SW TAL PEN. Solids, Total Volatile (TVS) MCAWW TAL PEN 0. Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Total Kjeldahl MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN. Phosphorus, Ortho EPA TAL PEN. Phosphorus, Total EPA TAL TAL. Phosphorus, Total EPA TAL PEN Moisture Percent Moisture EPA TAL PEN SM B BO, -ay SM TAL PEN SM 0 CO SM TAL PEN SM 0 CO SM TAL NSH Protocol References: EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of /0/0

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39 ANALYTICAL REPORT TestAmerica Laboratories, Inc. McLemore rive Pensacola, FL Tel: (0)-0 TestAmerica Job I: Client Project/Site: Three Mile CreekUSA Sampling Program For: ewberry 0 Rexwoods r. Raleigh, North Carolina 0 Attn: Michael Hanson Authorized for release by: //0 :0: PM Mike Nance, Project Manager II ()- mike.nance@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

40 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Table of Contents TestAmerica Job I: Cover Page Table of Contents efinitions Case Narrative Sample Summary Client Sample s QC Sample s Chronicle Method Summary Chain of Custody Page of //0

41 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program s Metals J General Chemistry J F escription efinitions/glossary is less than the but greater than or equal to the ML and the concentration is an approximate value. escription is less than the but greater than or equal to the ML and the concentration is an approximate value. MS/MS Recovery and/or RP exceeds the control limits * LCS or LCS exceeds the control limits Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF ER L, RA, RE, IN LC MA EL MC ML ML NC N PQL QC RER RP TEF TEQ Contains no Free Liquid uplicate error ratio (normalized absolute difference) ilution Factor Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample ecision level concentration Minimum detectable activity Estimated etection Limit Minimum detectable concentration Method etection Limit Minimum Level (ioxin) Not Calculated Not detected at the reporting limit (or ML or EL if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent ifference, a measure of the relative difference between two points Toxicity Equivalent Factor (ioxin) Toxicity Equivalent Quotient (ioxin) TestAmerica Job I: Page of //0

42 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Job I: Laboratory: Narrative Comments No additional comments. Job Narrative Receipt The samples were received on //0 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. Metals No analytical or quality issues were noted. General Chemistry Method(s)., SM 0G: The laboratory control sample (LCS) for batch recovered outside control limits for the following analytes: Volatile Total Solids. These analytes were biased high in the LCS. Method(s).: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s).: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s).: The matrix spike / matrix spike duplicate MS recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s).: The matrix spike / matrix spike duplicate MS recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s) SM 0: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. No other analytical or quality issues were noted. Organic Prep No analytical or quality issues were noted. Lab Admin No analytical or quality issues were noted. Page of //0

43 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received G-OO Water 0// : 0// 0: G-00 Water 0// :0 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// :0 0// 0: S-00 Solid 0// :0 0// 0: S-00 Solid 0// :0 0// 0: S-00 Solid 0// : 0// 0: S-00 Solid 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// : 0// 0: G-00 Water 0// :0 0// 0: G-00 Water 0// :00 0// 0: S-00 Solid 0// : 0// 0: S-00 Solid 0// :0 0// 0: Page of //0

44 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-OO ate Collected: 0// : ate Received: 0// 0: Client Sample s TestAmerica Job I: Lab Sample I: General Chemistry ML Ammonia mg/l 0// : Nitrogen, Kjeldahl mg/l 0// : 0// : Nitrate Nitrite as N 0.00 J mg/l 0// : Chemical Oxygen emand 0. mg/l 0/0/ : Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: Lab Sample I: General Chemistry ML ortho-phosphate mg/l 0// :0 Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Phosphorus mg/l 0// : 0// 0: Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// : 0// : Arsenic < mg/l 0// : 0// : Barium mg/l 0// : 0// : Cadmium < mg/l 0// : 0// : Chromium < mg/l 0// : 0// : Lead mg/l 0// : 0// : Selenium < mg/l 0// : 0// : Method: 0A - Mercury (CVAA) ML Mercury mg/l 0// 0:0 0// :0 Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Biochemical Oxygen emand mg/l 0// : Page of //0

45 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Client Sample s TestAmerica Job I: Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: General Chemistry ML Lab Sample I: Ammonia mg/l 0// : Nitrogen, Kjeldahl. Nitrate Nitrite as N <0.0 Chemical Oxygen emand Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: General Chemistry mg/l 0/0/ : 0// : mg/l 0// :. mg/l 0/0/ : ML Lab Sample I: Ammonia mg/l 0// : Nitrogen, Kjeldahl. Nitrate Nitrite as N 0.0 Chemical Oxygen emand mg/l 0/0/ : 0// : mg/l 0// :. mg/l 0/0/ : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML ortho-phosphate < mg/l 0// :0 Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Phosphorus mg/l 0// : 0// 0: Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// : 0// : Arsenic < mg/l 0// : 0// : Barium mg/l 0// : 0// : Cadmium < mg/l 0// : 0// : Chromium < mg/l 0// : 0// : Lead mg/l 0// : 0// : Selenium < mg/l 0// : 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l 0// 0:0 0// :0 Page of //0

46 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: General Chemistry Client Sample s ML TestAmerica Job I: Lab Sample I: Biochemical Oxygen emand..0.0 mg/l 0// : Client Sample I: S-00 ate Collected: 0// :0 ate Received: 0// 0: Method: 0B - Metals (ICP) ML Lab Sample I: Percent Solids:. Silver < mg/kg 0// 0:0 0// : Arsenic. Barium Cadmium 0. J Chromium. Lead Selenium < mg/kg 0// 0:0 0// :. 0. mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// :. 0. mg/kg 0// 0:0 0// : Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML Hg mg/kg 0// 0: 0// : Client Sample I: S-00 ate Collected: 0// :0 ate Received: 0// 0: Lab Sample I: Percent Solids:. General Chemistry Nitrogen, Kjeldahl 0 mg/kg 0/0/ : 0// : Phosphorus, Total 0 Nitrogen, Total 0 ML. mg/kg 0/0/ : 0// :..0 mg/kg 0// : Total Volatile Solids. * % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N < mg/kg 0// : General Chemistry - ASTM Leach Chemical Oxygen emand. J.0 mg/l 0/0/ : ML Client Sample I: S-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: Percent Solids:.0 Method: 0B - Metals (ICP) Silver < mg/kg 0// 0:0 0// : Arsenic. Barium Cadmium 0. J Chromium.0 ML mg/kg 0// 0:0 0// :. 0.0 mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : Page of //0

47 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: S-00 ate Collected: 0// : ate Received: 0// 0: Method: 0B - Metals (ICP) (Continued) Client Sample s ML TestAmerica Job I: Lab Sample I: Percent Solids:.0 Lead mg/kg 0// 0:0 0// : Selenium <0. Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML. 0. mg/kg 0// 0:0 0// : Hg mg/kg 0// 0: 0// : Client Sample I: S-00 ate Collected: 0// : ate Received: 0// 0: General Chemistry ML Lab Sample I: Percent Solids:.0 Nitrogen, Kjeldahl 00 mg/kg 0/0/ : 0// :0 Phosphorus, Total Nitrogen, Total 00. mg/kg 0/0/ : 0// :..0 mg/kg 0// : Total Volatile Solids. * % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N < mg/kg 0// : General Chemistry - ASTM Leach ML Chemical Oxygen emand. J.0 mg/l 0/0/ : Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML Ammonia mg/l 0// :0 Nitrogen, Kjeldahl mg/l 0/0/ : 0// : Nitrate Nitrite as N 0.00 J mg/l 0// : Chemical Oxygen emand 0. mg/l /0/ :0 Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: General Chemistry ML ortho-phosphate mg/l 0// :0 Page of //0

48 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-00 ate Collected: 0// : ate Received: 0// 0: General Chemistry Client Sample s ML TestAmerica Job I: Lab Sample I: Phosphorus mg/l 0// : 0// 0: Client Sample I: G-00 ate Collected: 0// :0 ate Received: 0// 0: Method: 0B - Metals (ICP) - Total Recoverable ML Lab Sample I: Silver < mg/l 0// : 0// : Arsenic <0.000 Barium 0.0 Cadmium <0.00 Chromium <0.000 Lead 0.00 J Selenium < mg/l 0// : 0// : mg/l 0// : 0// : mg/l 0// : 0// : mg/l 0// : 0// : mg/l 0// : 0// : mg/l 0// : 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l 0// 0:0 0// :0 Client Sample I: G-00 ate Collected: 0// :00 ate Received: 0// 0: Lab Sample I: General Chemistry ML Biochemical Oxygen emand..0.0 mg/l 0// : Client Sample I: S-00 ate Collected: 0// : ate Received: 0// 0: Lab Sample I: Percent Solids: 0. Method: 0B - Metals (ICP) Silver < mg/kg 0// 0:0 0// :0 Arsenic <0. Barium. Cadmium <0. Chromium. Lead. Selenium <0. Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML ML mg/kg 0// 0:0 0// :0. 0. mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// : mg/kg 0// 0:0 0// :0. 0. mg/kg 0// 0:0 0// :0 Hg 0.0 J mg/kg 0// 0: 0// : Page of //0

49 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: S-00 ate Collected: 0// :0 ate Received: 0// 0: General Chemistry Client Sample s ML TestAmerica Job I: Lab Sample I: Percent Solids:. Nitrogen, Kjeldahl.0 mg/kg 0/0/ : 0// : Phosphorus, Total Nitrogen, Total. mg/kg 0/0/ : 0// :.. mg/kg 0// : Total Volatile Solids 0.0 * % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N < mg/kg 0// : General Chemistry - ASTM Leach Chemical Oxygen emand <.0.0 mg/l 0/0/ : ML Page of //0

50 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method: 0B - Metals (ICP) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Silver < mg/kg 0// 0:0 0// : Arsenic Barium Cadmium Chromium Lead Selenium ML < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : < mg/kg 0// 0:0 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Silver.. mg/kg - Arsenic mg/kg - Barium 0 mg/kg - Cadmium.0. mg/kg - Chromium mg/kg - Lead mg/kg - Selenium.. mg/kg - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : Prep : MB MB Silver < mg/l 0// : 0// : Arsenic Barium Cadmium Chromium Lead Selenium ML < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : < mg/l 0// : 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : Prep : LCS LCS %Rec Silver mg/l 0 - Arsenic mg/l 0 - Barium.00.0 mg/l 0 - Cadmium mg/l 0 - Chromium.00.0 mg/l 0 - Lead.00.0 mg/l 0 - Selenium.00.0 mg/l 0 - Page of //0

51 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method: 0A - Mercury (CVAA) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Mercury < mg/l 0// 0:0 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Hg < mg/kg 0// 0: 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Hg.. mg/kg 0 - Method:. - Solids, Total Volatile (TVS) Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB Total Volatile Solids < % 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Total Volatile Solids 0.0 <0. * % - Page of //0

52 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method: 0. - Nitrogen, Ammonia Lab Sample I: MB 00-/ Analysis : MB MB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Ammonia < mg/l 0// : Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Ammonia.00. mg/l 0 - Lab Sample I: M 00-/ M Analysis : LCS LCS %Rec Client Sample I: Lab Control Sample Prep Type: Ammonia mg/l 0 - M M %Rec Method:. - Nitrogen, Total Kjeldahl Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Nitrogen, Kjeldahl < mg/l 0// : 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/l 0 - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrogen, Kjeldahl J mg/l 0 - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Nitrogen, Kjeldahl < mg/l 0/0/ : 0// : Page of //0

53 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method:. - Nitrogen, Total Kjeldahl (Continued) QC Sample s TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/l 0 - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/kg 0/0/ : 0// :0 ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/kg - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrogen, Kjeldahl J mg/l 0 - Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Nitrate Nitrite as N < mg/l 0// : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Nitrate Nitrite as N mg/l 0 - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrate Nitrite as N J mg/l 0 - Page of //0

54 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method:. - Nitrogen, Nitrate-Nitrite (Continued) Lab Sample I: M 00-/ M Analysis : QC Sample s Nitrate Nitrite as N J mg/kg Lab Sample I: MB 00-/-A Analysis : MB MB M M %Rec ML TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Client Sample I: Method Blank Prep Type: Soluble Nitrate Nitrite as N < mg/kg 0// : Lab Sample I: LCS 00-/-A Analysis : Client Sample I: Lab Control Sample Prep Type: Soluble Nitrate Nitrite as N mg/kg 0 - LCS LCS %Rec Lab Sample I: MS Analysis : Sample Sample Nitrate Nitrite as N <0... mg/kg 0 - Lab Sample I: MS Analysis : Sample Sample MS MS %Rec Client Sample I: S-00 Prep Type: Soluble Client Sample I: S-00 Prep Type: Soluble Nitrate Nitrite as N <0... mg/kg 0 - MS MS %Rec RP RP Limit Method:. - Phosphorus, Ortho Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML ortho-phosphate < mg/l 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec ortho-phosphate mg/l Page of //0

55 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method:. - Phosphorus, Ortho (Continued) Lab Sample I: MS Analysis : Sample Sample QC Sample s TestAmerica Job I: ortho-phosphate mg/l 0 - Lab Sample I: MS Analysis : Sample Sample MS MS %Rec Client Sample I: G-00 Prep Type: Client Sample I: G-00 Prep Type: ortho-phosphate mg/l 0 - Method:. - Phosphorus, Total MS MS %Rec RP RP Limit Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phosphorus < mg/l 0// : 0// 0: Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus mg/l 0 - Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec RP Limit Phosphorus mg/l 0-0 Method:. - Phosphorus, Total Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phosphorus, Total < mg/kg 0/0/ : 0// :0 Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus, Total.0. mg/kg 0 - Page of //0

56 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method:. - Phosphorus, Total (Continued) QC Sample s TestAmerica Job I: Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Phosphorus, Total 0. F mg/kg - Lab Sample I: MS Client Sample I: S-00 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec Phosphorus, Total 0. F mg/kg Lab Sample I: M 00-/ M Analysis : Phosphorus, Total 0.0 <0. mg/kg M M %Rec RP Limit Client Sample I: Lab Control Sample Prep Type: Method: SM B - BO, -ay Lab Sample I: USB 00-/ USB Client Sample I: Method Blank Prep Type: Analysis : USB USB ML Biochemical Oxygen emand < mg/l 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Biochemical Oxygen emand 0 mg/l - Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample up Prep Type: Analysis : LCS LCS RP %Rec RP Limit Biochemical Oxygen emand mg/l - Method: SM 0 - CO Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Chemical Oxygen emand <.0.0 mg/l 0/0/ : Page of //0

57 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method: SM 0 - CO (Continued) Lab Sample I: LCS 0-/ Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Chemical Oxygen emand 0.0. mg/l 0 - Lab Sample I: LCS 0-/ Analysis : LCS LCS %Rec Client Sample I: Lab Control Sample up Prep Type: Chemical Oxygen emand mg/l 0-0 Lab Sample I: MB 00-/ Analysis : MB MB LCS LCS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.. mg/l 0/0/ : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand 0.0. mg/l 0 - Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand 0.0. mg/l 0 - Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand mg/l 0 - Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand 0.0. mg/l 0 - Lab Sample I: MS Client Sample I: G-OO Prep Type: Analysis : Sample Sample MS MS %Rec Chemical Oxygen emand 0.. F mg/l Page of //0

58 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Lab Sample I: MS Analysis : Sample Sample QC Sample s TestAmerica Job I: Client Sample I: G-OO Prep Type: Chemical Oxygen emand 0.. F mg/l Lab Sample I: MB 00-/ Analysis : MB MB MS MS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.. mg/l /0/ :0 Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Chemical Oxygen emand 00 mg/l 0 - LCS LCS %Rec Lab Sample I: LB 0-0/-A LB Analysis : LB LB ML Client Sample I: Method Blank Prep Type: ASTM Leach Chemical Oxygen emand <.0.0 mg/l 0/0/ : Chemical Oxygen emand Lab Sample I: MS Analysis : Sample <.0.0 mg/l 0/0/ : Sample Chemical Oxygen emand. J 0.0. mg/l 0 - Lab Sample I: MS Analysis : Sample Sample MS MS %Rec Client Sample I: S-00 Prep Type: ASTM Leach Client Sample I: S-00 Prep Type: ASTM Leach Chemical Oxygen emand. J 0.0. mg/l 0-0 MS MS %Rec RP RP Limit Page 0 of //0

59 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-OO Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : KJR TAL PEN Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis 0. 0// : KJR TAL PEN Analysis SM 0 0/0/ : CLS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// :0 LSS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Prep././ 0// : QMC TAL TAL Analysis. 0// 0: QMC TAL TAL Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A 0// 0:0 JAP TAL PEN Analysis 0A 0// :0 JAP TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B GMF TAL PEN (Start) (End) 0// : 0// :0 Lab Page of //0

60 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : KJR TAL PEN Analysis 0. 0// : KJR TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis SM 0 0/0/ : CLS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : KJR TAL PEN Analysis 0. 0// : KJR TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis SM 0 0/0/ : CLS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// :0 LSS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Prep././ 0// : QMC TAL TAL Analysis. 0// 0: QMC TAL TAL Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A 0// 0:0 JAP TAL PEN Analysis 0A 0// :0 JAP TAL PEN Lab Page of //0

61 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B GMF TAL PEN (Start) (End) 0// : 0// :0 Client Sample I: S-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Percent Solids:. Prep Type Type Method Run ilution Factor Number or Analyst Prep B 0// 0: JAP TAL PEN Analysis B 0// : JAP TAL PEN Lab Lab Prep 00B 0// 0:0 NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Analysis Moisture 0// :00 LEC TAL PEN Client Sample I: S-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Soluble Soluble ASTM Leach ASTM Leach Type Method Run ilution Factor Number or Analyst Analysis Moisture 0// :00 LEC TAL PEN Leach I Leach 0// : KJR TAL PEN Analysis. 0// : KJR TAL PEN Analysis. 0// :0 CAC TAL PEN Analysis Total Nitrogen 0// : JAT TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Prep././ 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Leach - 0/0/ : SJM TAL NSH Analysis SM 0 0/0/ : MSJ TAL NSH Lab Client Sample I: S-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Percent Solids:.0 Prep Type Type Method Run ilution Factor Number or Analyst Prep B 0// 0: JAP TAL PEN Analysis B 0// : JAP TAL PEN Prep 00B 0// 0:0 NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Analysis Moisture 0// :00 LEC TAL PEN Lab Page of //0

62 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: S-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Soluble Soluble ASTM Leach ASTM Leach Type Method Run ilution Factor Number or Analyst Analysis Moisture 0// :00 LEC TAL PEN Leach I Leach 0// : KJR TAL PEN Analysis. 0// : KJR TAL PEN Analysis. 0// :0 CAC TAL PEN Analysis Total Nitrogen 0// : JAT TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// :0 JAT TAL PEN Prep././ 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Leach - 0/0/ : SJM TAL NSH Analysis SM 0 0/0/ : MSJ TAL NSH Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : KJR TAL PEN Analysis 0. 0// :0 KJR TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis SM 0 /0/ :0 CLS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// :0 LSS TAL PEN Lab Client Sample I: G-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Prep././ 0// : QMC TAL TAL Analysis. 0// 0: QMC TAL TAL Lab Page of //0

63 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Client Sample I: G-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A 0// 0:0 JAP TAL PEN Analysis 0A 0// :0 JAP TAL PEN Client Sample I: G-00 Lab Sample I: ate Collected: 0// :00 ate Received: 0// 0: Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B GMF TAL PEN (Start) (End) 0// : 0// :0 Lab Lab Client Sample I: S-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0: Percent Solids: 0. Prep Type Type Method Run ilution Factor Number or Analyst Prep B 0// 0: JAP TAL PEN Analysis B 0// : JAP TAL PEN Prep 00B 0// 0:0 NAB TAL PEN Analysis 0B 0// :0 SLM TAL PEN Analysis Moisture 0// :00 LEC TAL PEN Lab Client Sample I: S-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0: Prep Type Soluble Soluble ASTM Leach ASTM Leach Type Method Run ilution Factor Number or Analyst Analysis Moisture 0// :00 LEC TAL PEN Leach I Leach 0// : KJR TAL PEN Analysis. 0// : KJR TAL PEN Analysis. 0// :0 CAC TAL PEN Analysis Total Nitrogen 0// : JAT TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Prep././ 0/0/ : JAT TAL PEN Analysis. 0// : JAT TAL PEN Leach - 0/0/ : SJM TAL NSH Analysis SM 0 0/0/ : MSJ TAL NSH Lab Page of //0

64 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA Sampling Program Laboratory References: TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

65 Client: ewberry Project/Site: Three Mile CreekUSA Sampling Program Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory 0B Metals (ICP) SW TAL PEN 0A Mercury (CVAA) SW TAL PEN B Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) SW TAL PEN. Solids, Total Volatile (TVS) MCAWW TAL PEN 0. Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Total Kjeldahl MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN. Phosphorus, Ortho EPA TAL PEN. Phosphorus, Total EPA TAL TAL. Phosphorus, Total EPA TAL PEN Moisture Percent Moisture EPA TAL PEN SM B BO, -ay SM TAL PEN SM 0 CO SM TAL PEN SM 0 CO SM TAL NSH Total Nitrogen Nitrogen, Total EPA TAL PEN Protocol References: EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

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68 ANALYTICAL REPORT TestAmerica Laboratories, Inc. McLemore rive Pensacola, FL Tel: (0)-0 TestAmerica Job I: Client Project/Site: Three Mile CreekUSA - Groundwater For: ewberry 0 Rexwoods r. Raleigh, North Carolina 0 Attn: Michael Hanson Authorized for release by: //0 ::0 PM Mike Nance, Project Manager II ()- mike.nance@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

69 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Table of Contents TestAmerica Job I: Cover Page Table of Contents efinitions Case Narrative Sample Summary Client Sample s QC Sample s Chronicle Method Summary Chain of Custody Page of //0

70 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater s GC/MS VOA escription * LCS or LCS exceeds the control limits GC/MS Semi VOA J Metals J General Chemistry escription efinitions/glossary is less than the but greater than or equal to the ML and the concentration is an approximate value. escription is less than the but greater than or equal to the ML and the concentration is an approximate value. escription TestAmerica Job I: MS, MS: The analyte present in the original sample is times greater than the matrix spike concentration; therefore, control limits are not J applicable. is less than the but greater than or equal to the ML and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid ER uplicate error ratio (normalized absolute difference) ilution Factor L, RA, RE, IN Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision level concentration MA Minimum detectable activity EL Estimated etection Limit MC Minimum detectable concentration ML Method etection Limit ML Minimum Level (ioxin) NC Not Calculated N Not detected at the reporting limit (or ML or EL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) Page of //0

71 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Job I: Laboratory: Narrative Comments No additional comments. Job Narrative Receipt The samples were received on //0 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. GC/MS VOA Method(s) : A full list spike was utilized for this method. ue to the large number of spiked analytes, there is a high probability that one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for analyte to recover outside criteria for this method when a full list spike is utilized. The LCS associated with batch had analyte outside control limits; therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified.hs-00 (00-0-), HS-00 (00-0-), HS-00 (00-0-) No other analytical or quality issues were noted. GC/MS Semi VOA Method(s) : The continuing calibration verification (CCV) for Benzidine associated with batch recovered above the upper control limit. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. HS-00 (00-0-) No other analytical or quality issues were noted. GC Semi VOA No analytical or quality issues were noted. Metals No analytical or quality issues were noted. General Chemistry No other analytical or quality issues were noted. Organic Prep Method(s) 0: Insufficient sample volume was available to meet method-mandated requirements for matrix spike/matrix spike duplicate (MS/MS) analyses for batch. No other analytical or quality issues were noted. Page of //0

72 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received HS-00 Water 0// : 0// 0: HS-00 Water 0// :0 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-0 Water 0// :0 0// 0: HS-0 Water 0// : 0// 0: HS-0 Water 0// : 0// 0: HS-0 Water 0// : 0// 0: HS-0 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// :0 0// 0: HS-0 Water 0// :0 0// 0: HS-0 Water 0// :0 0// 0: HS-0 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0: HS-00 Water 0// : 0// 0:0 Page of //0

73 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ortho-phosphate mg/l 0// : Client Sample I: HS-00 ate Collected: 0// :0 ate Received: 0// 0:0 Method: 0B - Metals (ICP) - Total Recoverable ML ML Lab Sample I: Antimony < mg/l 0// 0: 0// : Arsenic <0.000 Beryllium <0.00 Cadmium <0.00 Chromium <0.000 Copper 0.0 Lead 0.0 Nickel <0.000 Selenium <0.000 Silver <0.000 Thallium <0.000 Zinc mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: Method: - Volatile Organic Compounds (GC/MS) ML,,-Trichloroethane < ug/l 0// :,,,-Tetrachloroethane < ug/l 0// :,,-Trichloroethane < ug/l 0// :,-ichloroethane < ug/l 0// :,-ichloroethene < ug/l 0// :,-ichlorobenzene < ug/l 0// :,-ichloroethane < ug/l 0// :,-ichloropropane < ug/l 0// :,-ichlorobenzene < ug/l 0// :,-ichlorobenzene < ug/l 0// : Acrolein <0 * 0 0 ug/l 0// : Acrylonitrile <..0. ug/l 0// : Benzene < ug/l 0// : Bromoform < ug/l 0// : Bromomethane < ug/l 0// : Carbon tetrachloride < ug/l 0// : Chlorobenzene < ug/l 0// : ibromochloromethane < ug/l 0// : Chloroethane < ug/l 0// : Page of //0

74 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Method: - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: Chloroform ug/l 0// : Chloromethane <0. cis-,-ichloroethene <0.0 cis-,-ichloropropene <0.0 Bromodichloromethane <0.0 Ethylbenzene <0.0 m-xylene & p-xylene <. Methyl tert-butyl ether <0. Methylene Chloride <.0 o-xylene <0.0 Tetrachloroethene <0. Toluene. trans-,-ichloroethene <0.0 trans-,-ichloropropene <0.0 Trichloroethene <0.0 Trichlorofluoromethane <0. Vinyl chloride <0.0 -Chloroethyl vinyl ether < ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0.0 ug/l 0// : Surrogate %Recovery -Bromofluorobenzene - 0// : ibromofluoromethane - 0// : Toluene-d (Surr) 0-0// : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: Method: - Semivolatile Organic Compounds (GC/MS) ML Acenaphthene < ug/l 0// : 0// : Acenaphthylene < ug/l 0// : 0// : Anthracene < ug/l 0// : 0// : Benzidine < ug/l 0// : 0// : Benzo[a]anthracene < ug/l 0// : 0// : Benzo[b]fluoranthene < ug/l 0// : 0// : Benzo[k]fluoranthene < ug/l 0// : 0// : Benzo[g,h,i]perylene < ug/l 0// : 0// : Benzo[a]pyrene < ug/l 0// : 0// : -Bromophenyl phenyl ether < ug/l 0// : 0// : Butyl benzyl phthalate < ug/l 0// : 0// : Bis(-chloroethoxy)methane < ug/l 0// : 0// : Bis(-chloroethyl)ether < ug/l 0// : 0// : -Chloro--methylphenol <... ug/l 0// : 0// : -Chloronaphthalene < ug/l 0// : 0// : -Chlorophenol <... ug/l 0// : 0// : -Chlorophenyl phenyl ether <... ug/l 0// : 0// : Chrysene < ug/l 0// : 0// : ibenz(a,h)anthracene < ug/l 0// : 0// : i-n-butyl phthalate <... ug/l 0// : 0// : Page of //0

75 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Method: - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 00-0-,-ichlorobenzene < ug/l 0// : 0// :,-ichlorobenzene <0.,-ichlorobenzene <0.,'-ichlorobenzidine <.,-ichlorophenol <. iethyl phthalate 0. J,-imethylphenol <. imethyl phthalate <0.,-initro--methylphenol <.,-initrophenol <.,-initrotoluene <.,-initrotoluene <. i-n-octyl phthalate <0. Bis(-ethylhexyl) phthalate <. Fluoranthene <0. Fluorene <0. Hexachlorobenzene <0. Hexachlorobutadiene <. Hexachlorocyclopentadiene <. Hexachloroethane <.0 Indeno[,,-cd]pyrene <0. Isophorone <0. Naphthalene <0. Nitrobenzene <0. -Nitrophenol <.0 -Nitrophenol <.0 N-Nitrosodimethylamine <. N-Nitrosodiphenylamine <0. N-Nitrosodi-n-propylamine <. Pentachlorophenol <. Phenanthrene <0. Phenol <. Pyrene <0.0,,-Trichlorobenzene <0.,,-Trichlorophenol <.. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. ug/l 0// : 0// :.. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. ug/l 0// : 0// :..0 ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :..0 ug/l 0// : 0// :..0 ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0.0 ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// : Surrogate %Recovery,,-Tribromophenol - 0// : 0// : -Fluorobiphenyl - 0// : 0// : -Fluorophenol - 0// : 0// : Nitrobenzene-d - 0// : 0// : Phenol-d - 0// : 0// : Terphenyl-d - 0// : 0// : Page of //0

76 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Method: 0 - Organochlorine Pesticides/PCBs in Water ML Lab Sample I: Aldrin < ug/l 0// :0 0// : alpha-bhc <0.00 beta-bhc <0.00 delta-bhc <0.00 gamma-bhc (Lindane) <0.0 Chlordane (technical) <0.0,'- <0.00,'-E <0.00,'-T <0.00 ieldrin <0.00 Endosulfan I <0.00 Endosulfan II <0.00 Endosulfan sulfate <0.00 Endrin <0.00 Endrin aldehyde <0.00 Heptachlor <0.00 Heptachlor epoxide <0.00 PCB- <0.0 PCB- <0. PCB- <0.0 PCB- <0.0 PCB- <0.00 PCB- <0.0 PCB- <0.0 Toxaphene < ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// :. 0. ug/l 0// :0 0// : Surrogate %Recovery CB ecachlorobiphenyl - 0// :0 0// : Tetrachloro-m-xylene - 0// :0 0// : Client Sample I: HS-0 ate Collected: 0// :0 ate Received: 0// 0:0 Lab Sample I: General Chemistry ML Biochemical Oxygen emand < mg/l 0/0/ : Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ML Phenols, Total < mg/l 0// :0 /0/ : Page of //0

77 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// 0:0 General Chemistry ML Lab Sample I: Ammonia < mg/l 0/0/ : Nitrogen, Kjeldahl. Nitrate Nitrite as N. Chemical Oxygen emand Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// 0:0 General Chemistry mg/l 0// : 0// : mg/l 0// :. mg/l /0/ :0 ML Lab Sample I: Cyanide, Total mg/l 0// :0 0// 0: Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ML Ammonia mg/l 0/0/ : Nitrogen, Kjeldahl mg/l 0// : 0// : Nitrate Nitrite as N mg/l 0// :0 Chemical Oxygen emand. mg/l /0/ :0 Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ML ortho-phosphate mg/l 0// : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Antimony < mg/l 0// 0: 0// : Arsenic < mg/l 0// 0: 0// : Beryllium < mg/l 0// 0: 0// : Cadmium < mg/l 0// 0: 0// : Chromium < mg/l 0// 0: 0// : Copper 0.00 J mg/l 0// 0: 0// : Lead mg/l 0// 0: 0// : Nickel < mg/l 0// 0: 0// : Selenium < mg/l 0// 0: 0// : Silver < mg/l 0// 0: 0// : Thallium < mg/l 0// 0: 0// : Zinc mg/l 0// 0: 0// : Page of //0

78 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Method: 0A - Mercury (CVAA) ML Lab Sample I: Mercury < mg/l /0/ 0: /0/ : Client Sample I: HS-00 ate Collected: 0// :0 ate Received: 0// 0:0 Method: - Volatile Organic Compounds (GC/MS) ML Lab Sample I: 00-0-,,-Trichloroethane < ug/l 0// :,,,-Tetrachloroethane <0.0,,-Trichloroethane <0.0,-ichloroethane <0.0,-ichloroethene <0.0,-ichlorobenzene <0.0,-ichloroethane <0.0,-ichloropropane <0.0,-ichlorobenzene <0.,-ichlorobenzene <0. Acrolein <0 * Acrylonitrile <. Benzene <0. Bromoform <0. Bromomethane <0. Carbon tetrachloride <0.0 Chlorobenzene <0.0 ibromochloromethane <0.0 Chloroethane <0. Chloroform. Chloromethane <0. cis-,-ichloroethene <0.0 cis-,-ichloropropene <0.0 Bromodichloromethane <0.0 Ethylbenzene <0.0 m-xylene & p-xylene <. Methyl tert-butyl ether <0. Methylene Chloride <.0 o-xylene <0.0 Tetrachloroethene <0. Toluene <0.0 trans-,-ichloroethene <0.0 trans-,-ichloropropene <0.0 Trichloroethene <0.0 Trichlorofluoromethane <0. Vinyl chloride <0.0 -Chloroethyl vinyl ether < ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : 0 0 ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0.0 ug/l 0// : Surrogate %Recovery -Bromofluorobenzene - 0// : ibromofluoromethane - 0// : Toluene-d (Surr) 0-0// : Page of //0

79 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-0 ate Collected: 0// :0 ate Received: 0// 0:0 General Chemistry ML Lab Sample I: Biochemical Oxygen emand..0.0 mg/l 0/0/ : Client Sample I: HS-0 ate Collected: 0// :0 ate Received: 0// 0:0 General Chemistry ML Lab Sample I: Phenols, Total < mg/l 0// :0 /0/ : Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ML Cyanide, Total < mg/l 0// :0 0// 0: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ML ortho-phosphate mg/l 0// : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Antimony < mg/l 0// 0: 0// : Arsenic < mg/l 0// 0: 0// : Beryllium < mg/l 0// 0: 0// : Cadmium < mg/l 0// 0: 0// : Chromium < mg/l 0// 0: 0// : Copper 0.00 J mg/l 0// 0: 0// : Lead mg/l 0// 0: 0// : Nickel 0.00 J mg/l 0// 0: 0// : Selenium < mg/l 0// 0: 0// : Silver < mg/l 0// 0: 0// : Thallium < mg/l 0// 0: 0// : Zinc mg/l 0// 0: 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ : Page of //0

80 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Method: - Volatile Organic Compounds (GC/MS) ML Lab Sample I: 00-0-,,-Trichloroethane < ug/l 0// :,,,-Tetrachloroethane <0.0,,-Trichloroethane <0.0,-ichloroethane <0.0,-ichloroethene <0.0,-ichlorobenzene <0.0,-ichloroethane <0.0,-ichloropropane <0.0,-ichlorobenzene <0.,-ichlorobenzene <0. Acrolein <0 * Acrylonitrile <. Benzene <0. Bromoform <0. Bromomethane <0. Carbon tetrachloride <0.0 Chlorobenzene <0.0 ibromochloromethane <0.0 Chloroethane <0. Chloroform <0.0 Chloromethane <0. cis-,-ichloroethene <0.0 cis-,-ichloropropene <0.0 Bromodichloromethane <0.0 Ethylbenzene <0.0 m-xylene & p-xylene <. Methyl tert-butyl ether <0. Methylene Chloride <.0 o-xylene <0.0 Tetrachloroethene <0. Toluene <0.0 trans-,-ichloroethene <0.0 trans-,-ichloropropene <0.0 Trichloroethene <0.0 Trichlorofluoromethane <0. Vinyl chloride <0.0 -Chloroethyl vinyl ether < ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : 0 0 ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0.0 ug/l 0// : Surrogate %Recovery -Bromofluorobenzene - 0// : ibromofluoromethane - 0// : Toluene-d (Surr) 0-0// : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: General Chemistry ML Phosphorus mg/l /0/ : /0/ : Page of //0

81 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 General Chemistry ML Lab Sample I: Phosphorus mg/l /0/ : /0/ : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// 0:0 General Chemistry ML Lab Sample I: Phosphorus mg/l /0/ : /0/ : Page of //0

82 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method: - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 00-/ Analysis : MB MB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type:,,-Trichloroethane < ug/l 0// 0:,,,-Tetrachloroethane,,-Trichloroethane,-ichloroethane,-ichloroethene,-ichlorobenzene,-ichloroethane,-ichloropropane,-ichlorobenzene,-ichlorobenzene Acrolein Acrylonitrile Benzene Bromoform Bromomethane Carbon tetrachloride Chlorobenzene ibromochloromethane Chloroethane Chloroform Chloromethane cis-,-ichloroethene cis-,-ichloropropene Bromodichloromethane Ethylbenzene m-xylene & p-xylene Methyl tert-butyl ether Methylene Chloride o-xylene Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride -Chloroethyl vinyl ether < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: <0 0 0 ug/l 0// 0: <..0. ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: <.. ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: < ug/l 0// 0: Surrogate MB %Recovery MB -Bromofluorobenzene - 0// 0: ibromofluoromethane - 0// 0: Toluene-d (Surr) 0-0// 0: Page of //0

83 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 00-/00 Analysis : TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type:,,-Trichloroethane 0.0. ug/l - LCS LCS %Rec,,,-Tetrachloroethane 0.0. ug/l -,,-Trichloroethane 0.0. ug/l -,-ichloroethane ug/l -,-ichloroethene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l -,-ichloroethane 0.0. ug/l -,-ichloropropane 0.0. ug/l -,-ichlorobenzene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l - Acrolein 00 * ug/l - Acrylonitrile 00 ug/l - Benzene 0.0. ug/l - Bromoform 0.0. ug/l - Bromomethane 0.0. ug/l - Carbon tetrachloride 0.0. ug/l 0 - Chlorobenzene 0.0. ug/l - ibromochloromethane 0.0. ug/l - Chloroethane 0.0. ug/l - 0 Chloroform 0.0. ug/l - Chloromethane ug/l - cis-,-ichloroethene 0.0. ug/l - cis-,-ichloropropene 0.0. ug/l - Bromodichloromethane 0.0. ug/l 0 - Ethylbenzene 0.0. ug/l - m-xylene & p-xylene 0.0. ug/l - Methyl tert-butyl ether ug/l - Methylene Chloride 0.0. ug/l - o-xylene 0.0. ug/l - Tetrachloroethene 0.0. ug/l - Toluene 0.0. ug/l - trans-,-ichloroethene 0.0. ug/l - trans-,-ichloropropene ug/l - Trichloroethene ug/l 0 - Trichlorofluoromethane 0.0. ug/l - Vinyl chloride 0.0. ug/l - -Chloroethyl vinyl ether 0.0. ug/l 0-0 Surrogate LCS %Recovery LCS -Bromofluorobenzene - ibromofluoromethane - Toluene-d (Surr) 0 - Page of //0

84 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Acenaphthene <0. 0. ug/l 0// 0: 0// : Acenaphthylene Anthracene Benzidine Benzo[a]anthracene Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[g,h,i]perylene Benzo[a]pyrene -Bromophenyl phenyl ether Butyl benzyl phthalate Bis(-chloroethoxy)methane Bis(-chloroethyl)ether -Chloro--methylphenol -Chloronaphthalene -Chlorophenol -Chlorophenyl phenyl ether Chrysene ibenz(a,h)anthracene i-n-butyl phthalate,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene,'-ichlorobenzidine,-ichlorophenol iethyl phthalate,-imethylphenol imethyl phthalate,-initro--methylphenol,-initrophenol,-initrotoluene,-initrotoluene i-n-octyl phthalate Bis(-ethylhexyl) phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[,,-cd]pyrene Isophorone Naphthalene Nitrobenzene -Nitrophenol -Nitrophenol N-Nitrosodimethylamine N-Nitrosodiphenylamine ML <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0 0 0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : < ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : < ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.0.0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.0.0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.0.0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : Page of //0

85 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB N-Nitrosodi-n-propylamine <.. ug/l 0// 0: 0// : Pentachlorophenol Phenanthrene Phenol Pyrene,,-Trichlorobenzene,,-Trichlorophenol Surrogate ML <. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : MB %Recovery MB,,-Tribromophenol - 0// 0: 0// : -Fluorobiphenyl - 0// 0: 0// : -Fluorophenol - 0// 0: 0// : Nitrobenzene-d - 0// 0: 0// : Phenol-d - 0// 0: 0// : Terphenyl-d - 0// 0: 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Acenaphthene 0.0. ug/l - Acenaphthylene 0.0. ug/l - Anthracene 0.0. ug/l - Benzo[a]anthracene 0.0. ug/l - Benzo[b]fluoranthene 0.0. ug/l - Benzo[k]fluoranthene ug/l - Benzo[g,h,i]perylene 0.0. ug/l - Benzo[a]pyrene 0.0. ug/l - -Bromophenyl phenyl ether 0.0. ug/l 0 - Butyl benzyl phthalate 0.0. ug/l - Bis(-chloroethoxy)methane 0.0. ug/l - Bis(-chloroethyl)ether 0.0. ug/l - -Chloro--methylphenol 0.0. ug/l - -Chloronaphthalene 0.0. ug/l 0 - -Chlorophenol 0.0. ug/l - -Chlorophenyl phenyl ether 0.0. ug/l - Chrysene ug/l 0 - ibenz(a,h)anthracene 0.0. ug/l - i-n-butyl phthalate 0.0. ug/l -,-ichlorobenzene 0.0. ug/l 0 -,-ichlorobenzene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l 0 -,'-ichlorobenzidine 0.0. ug/l 0 -,-ichlorophenol 0.0. ug/l 0 - iethyl phthalate ug/l -,-imethylphenol 0.0. ug/l - imethyl phthalate 0.0. ug/l - Page of //0

86 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec,-initro--methylphenol 0. ug/l -,-initrophenol 0. ug/l 0 -,-initrotoluene ug/l -,-initrotoluene 0.0. ug/l 0 - i-n-octyl phthalate 0.0. ug/l - Bis(-ethylhexyl) phthalate 0.0. ug/l - Fluoranthene 0.0. ug/l - Fluorene 0.0. ug/l - Hexachlorobenzene 0.0. ug/l - Hexachlorobutadiene 0.0. ug/l - Hexachlorocyclopentadiene 0.0. ug/l - Hexachloroethane 0.0. ug/l 0 - Indeno[,,-cd]pyrene ug/l - Isophorone ug/l - Naphthalene 0.0. ug/l 0 - Nitrobenzene 0.0. ug/l - 0 -Nitrophenol 0.0. ug/l - -Nitrophenol 0. ug/l - N-Nitrosodimethylamine 0.0. ug/l - N-Nitrosodiphenylamine.. ug/l - N-Nitrosodi-n-propylamine 0.0. ug/l - 0 Pentachlorophenol 0. ug/l - Phenanthrene ug/l - Phenol ug/l - Pyrene ug/l 0 -,,-Trichlorobenzene 0.0. ug/l -,,-Trichlorophenol ug/l - Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - Nitrobenzene-d - Phenol-d - Terphenyl-d - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Acenaphthene ug/l - 0 Acenaphthylene 0.0. ug/l - 0 Anthracene 0.0. ug/l - 0 Benzo[a]anthracene ug/l - 0 Benzo[b]fluoranthene 0.0. ug/l - 0 Benzo[k]fluoranthene 0.0. ug/l - 0 Benzo[g,h,i]perylene 0.0. ug/l 0-0 RP Limit Page of //0

87 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Benzo[a]pyrene 0.0. ug/l - 0 -Bromophenyl phenyl ether 0.0. ug/l - 0 Butyl benzyl phthalate 0.0. ug/l - 0 Bis(-chloroethoxy)methane 0.0. ug/l - 0 Bis(-chloroethyl)ether 0.0. ug/l 0-0 -Chloro--methylphenol 0.0. ug/l - 0 -Chloronaphthalene 0.0. ug/l 0-0 -Chlorophenol 0.0. ug/l - 0 -Chlorophenyl phenyl ether 0.0. ug/l - 0 Chrysene ug/l ibenz(a,h)anthracene ug/l - 0 i-n-butyl phthalate 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l 0-0,'-ichlorobenzidine 0.0. ug/l - 0,-ichlorophenol 0.0. ug/l - 0 iethyl phthalate ug/l 0-0,-imethylphenol 0.0. ug/l - 0 imethyl phthalate 0.0. ug/l - 0,-initro--methylphenol 0. ug/l - 0,-initrophenol 0. ug/l 0-0,-initrotoluene 0.0. ug/l - 0,-initrotoluene 0.0. ug/l 0-0 i-n-octyl phthalate ug/l - 0 Bis(-ethylhexyl) phthalate 0.0. ug/l - 0 Fluoranthene 0.0. ug/l - 0 Fluorene 0.0. ug/l - 0 Hexachlorobenzene 0.0. ug/l - 0 Hexachlorobutadiene ug/l - 0 Hexachlorocyclopentadiene 0.0. ug/l - 0 Hexachloroethane 0.0. ug/l 0-0 Indeno[,,-cd]pyrene ug/l - 0 Isophorone ug/l Naphthalene 0.0. ug/l - 0 Nitrobenzene 0.0. ug/l Nitrophenol 0.0. ug/l - 0 -Nitrophenol 0. ug/l - 0 N-Nitrosodimethylamine 0.0. ug/l - 0 N-Nitrosodiphenylamine. 0. ug/l - 0 N-Nitrosodi-n-propylamine 0.0. ug/l Pentachlorophenol 0. ug/l - 0 Phenanthrene 0.0. ug/l - 0 Phenol 0.0. ug/l - 0 Pyrene 0.0. ug/l - 0,,-Trichlorobenzene 0.0. ug/l - 0,,-Trichlorophenol 0.0. ug/l - 0 RP Limit Page 0 of //0

88 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - Nitrobenzene-d - Phenol-d - Terphenyl-d - Method: 0 - Organochlorine Pesticides/PCBs in Water Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : 0 Prep : MB MB PCB- < ug/l 0// :0 0// 0: PCB- PCB- PCB- PCB- PCB- PCB- ML < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: Surrogate MB %Recovery MB CB ecachlorobiphenyl - 0// :0 0// 0: Tetrachloro-m-xylene - 0// :0 0// 0: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Aldrin < ug/l 0// :0 0// : alpha-bhc beta-bhc delta-bhc gamma-bhc (Lindane) Chlordane (technical),'-,'-e,'-t ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor ML < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : Page of //0

89 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: 0 - Organochlorine Pesticides/PCBs in Water (Continued) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Heptachlor epoxide < ug/l 0// :0 0// : Toxaphene Surrogate ML < ug/l 0// :0 0// : MB %Recovery MB CB ecachlorobiphenyl - 0// :0 0// : Tetrachloro-m-xylene - 0// :0 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Aldrin ug/l - alpha-bhc ug/l - beta-bhc ug/l - delta-bhc ug/l - gamma-bhc (Lindane) ug/l -,' ug/l -,'-E ug/l 0 0 -,'-T ug/l - ieldrin ug/l - Endosulfan I ug/l - Endosulfan II ug/l - 0 Endosulfan sulfate ug/l - Endrin ug/l 0 - Endrin aldehyde ug/l 0 - Heptachlor ug/l - Heptachlor epoxide ug/l - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : 0 Prep : LCS LCS %Rec PCB-.00. ug/l 0 - PCB-.00. ug/l - Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Aldrin ug/l - 0 alpha-bhc ug/l - 0 RP Limit Page of //0

90 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: 0 - Organochlorine Pesticides/PCBs in Water (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec beta-bhc ug/l 0-0 delta-bhc ug/l - 0 gamma-bhc (Lindane) ug/l - 0,' ug/l - 0,'-E ug/l 0-0,'-T ug/l - 0 ieldrin ug/l - 0 Endosulfan I ug/l - 0 Endosulfan II ug/l Endosulfan sulfate ug/l - 0 Endrin ug/l Endrin aldehyde ug/l 0-0 Heptachlor ug/l - 0 Heptachlor epoxide ug/l 0-0 RP Limit Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : 0 Prep : LCS LCS RP %Rec PCB-.00. ug/l 0-0 PCB-.00. ug/l - 0 Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - RP Limit Method: 0B - Metals (ICP) Lab Sample I: MB 00-0/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : Prep : 0 MB MB Antimony < mg/l 0// 0: 0// : Arsenic Beryllium Cadmium Chromium Copper Lead Nickel Selenium Silver Thallium Zinc ML < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : Page of //0

91 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method: 0B - Metals (ICP) (Continued) QC Sample s TestAmerica Job I: Lab Sample I: LCS 00-0/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : Prep : 0 LCS LCS %Rec Antimony.00.0 mg/l 0 - Arsenic.00.0 mg/l 0 - Beryllium mg/l 0 - Cadmium mg/l 0 - Chromium.00.0 mg/l 0 - Copper.00.0 mg/l 0 - Lead.00.0 mg/l 0 - Nickel.00.0 mg/l 0 - Selenium.00.0 mg/l 0 - Silver mg/l 0 - Thallium.00.0 mg/l 0 - Zinc.00.0 mg/l 0 - Method: 0A - Mercury (CVAA) Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Mercury < mg/l /0/ 0: /0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l 0 - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Mercury < mg/l /0/ 0: /0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l 0 - Page of //0

92 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method:. - Cyanide, Total QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Cyanide, Total < mg/l 0// :0 0// 0: ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Cyanide, Total mg/l - Lab Sample I: MS Client Sample I: HS-0 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Cyanide, Total < mg/l - Lab Sample I: MS Client Sample I: HS-0 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec RP Limit Cyanide, Total < mg/l - Method: 0. - Nitrogen, Ammonia Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Ammonia < mg/l 0/0/ :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Ammonia.00.0 mg/l 0 - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Ammonia mg/l 0 - Page of //0

93 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method:. - Nitrogen, Total Kjeldahl QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/l 0// : 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0.0 mg/l 0 - Lab Sample I: MS Client Sample I: HS-0 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Nitrogen, Kjeldahl mg/l 0 - Lab Sample I: MS Client Sample I: HS-0 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec RP Limit Nitrogen, Kjeldahl mg/l 0-0 Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrogen, Kjeldahl mg/l 0 - Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Nitrate Nitrite as N < mg/l 0// 0: Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Nitrate Nitrite as N mg/l 0 - Page of //0

94 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method:. - Nitrogen, Nitrate-Nitrite (Continued) Lab Sample I: M 00-/ M Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N J mg/l 0 - Lab Sample I: MB 00-/ Analysis : MB MB M M %Rec ML Client Sample I: Method Blank Prep Type: Nitrate Nitrite as N < mg/l 0// : Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N mg/l 0 - LCS LCS %Rec Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrate Nitrite as N J mg/l 0 - Method:. - Phosphorus, Ortho Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML ortho-phosphate < mg/l 0// : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec ortho-phosphate mg/l 0 - Method:. - Phosphorus, Total Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phosphorus < mg/l /0/ : /0/ : Page of //0

95 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method:. - Phosphorus, Total (Continued) QC Sample s TestAmerica Job I: Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus mg/l 0 - Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Phosphorus mg/l 0-0 Lab Sample I: MS Client Sample I: HS-00 Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Phosphorus mg/l 0 - RP Limit Lab Sample I: MS Client Sample I: HS-00 Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec RP Limit Phosphorus mg/l 0-0 Lab Sample I: U Client Sample I: HS-00 Prep Type: Analysis : Prep : Sample Sample U U RP RP Limit Phosphorus mg/l 0 Method: 0. - Phenolics, Total Recoverable Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phenols, Total < mg/l 0// :0 /0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phenols, Total mg/l - Page of //0

96 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method: SM B - BO, -ay Lab Sample I: USB 00-00/ USB Analysis : 00 USB USB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Biochemical Oxygen emand < mg/l 0/0/ : Lab Sample I: LCS 00-00/ Analysis : 00 Client Sample I: Lab Control Sample Prep Type: Biochemical Oxygen emand mg/l 0 - Lab Sample I: LCS 00-00/ Analysis : 00 LCS LCS %Rec Client Sample I: Lab Control Sample up Prep Type: Biochemical Oxygen emand 0 mg/l - LCS LCS %Rec RP RP Limit Method: SM 0 - CO Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Chemical Oxygen emand <.. mg/l /0/ :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand 0.0. mg/l 0 - Page of //0

97 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : LSS TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0:0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0 0// 0: NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0// : WP TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep 0// : KH TAL PEN Analysis 0// : AJR TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0 0 0// : VC TAL PEN Prep 0 0// :0 KH TAL PEN Prep 0 0// :0 KH TAL PEN Analysis 0 0// : VC TAL PEN Lab Page 0 of //0

98 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Client Sample I: HS-0 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B 00 GMF TAL PEN (Start) (End) 0/0/ : 0// :0 Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep istill/phenol 0// :0 CLS TAL PEN Analysis 0. /0/ : JMH TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0. 0/0/ : KJR TAL PEN Analysis. 0// : KJR TAL PEN Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis SM 0 /0/ :0 CLS TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep istill/cn 0// :0 BAB TAL PEN Analysis. 0// 0: BAB TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0. 0/0/ : KJR TAL PEN Analysis. 0// :0 KJR TAL PEN Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis SM 0 /0/ :0 CLS TAL PEN Lab Page of //0

99 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : LSS TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0 0// 0: NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0// : WP TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B 00 GMF TAL PEN (Start) (End) 0/0/ : 0// :0 Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// :0 ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep istill/phenol 0// :0 CLS TAL PEN Analysis 0. /0/ : JMH TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep istill/cn 0// :0 BAB TAL PEN Analysis. 0// 0: BAB TAL PEN Lab Page of //0

100 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis. 0// : LSS TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0 0// 0: NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0// : WP TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Lab Page of //0

101 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Laboratory References: TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

102 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory Volatile Organic Compounds (GC/MS) 0CFRA TAL PEN Semivolatile Organic Compounds (GC/MS) 0CFRA TAL PEN 0 Organochlorine Pesticides/PCBs in Water 0CFRA TAL PEN 0B Metals (ICP) SW TAL PEN 0A Mercury (CVAA) SW TAL PEN. Cyanide, Total MCAWW TAL PEN 0. Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Total Kjeldahl MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN. Phosphorus, Total EPA TAL TAL. Phosphorus, Ortho EPA TAL PEN 0. Phenolics, Total Recoverable MCAWW TAL PEN SM B BO, -ay SM TAL PEN SM 0 CO SM TAL PEN Protocol References: 0CFRA = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 0CFR, Part, Appendix A, October, and subsequent revisions. EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

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107 ANALYTICAL REPORT TestAmerica Laboratories, Inc. McLemore rive Pensacola, FL Tel: (0)-0 TestAmerica Job I: Client Project/Site: Three Mile CreekUSA - Groundwater For: ewberry 0 Rexwoods r. Raleigh, North Carolina 0 Attn: Michael Hanson Authorized for release by: //0 :: PM Mike Nance, Project Manager II ()- mike.nance@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

108 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Table of Contents TestAmerica Job I: Cover Page Table of Contents efinitions Case Narrative Sample Summary Client Sample s QC Sample s Chronicle Method Summary Chain of Custody Page of //0

109 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater s GC/MS Semi VOA J GC Semi VOA X General Chemistry B b J Glossary Abbreviation escription efinitions/glossary is less than the but greater than or equal to the ML and the concentration is an approximate value. escription Surrogate is outside control limits escription Compound was found in the blank and sample. etected in the Unseeded Control blank (USB). is less than the but greater than or equal to the ML and the concentration is an approximate value. These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF ER L, RA, RE, IN LC MA EL MC ML ML NC N PQL QC RER RP TEF TEQ Contains no Free Liquid uplicate error ratio (normalized absolute difference) ilution Factor Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample ecision level concentration Minimum detectable activity Estimated etection Limit Minimum detectable concentration Method etection Limit Minimum Level (ioxin) Not Calculated Not detected at the reporting limit (or ML or EL if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent ifference, a measure of the relative difference between two points Toxicity Equivalent Factor (ioxin) Toxicity Equivalent Quotient (ioxin) TestAmerica Job I: Page of //0

110 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Job I: Laboratory: Narrative Comments No additional comments. Job Narrative Receipt The samples were received on //0 :0 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. GC/MS Semi VOA Method(s) : The continuing calibration verification (CCV) for Benzidine associated with batch recovered above the upper control limit. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. HS-00 (00-0-), HS-00 (00-0-) No other analytical or quality issues were noted. GC Semi VOA No analytical or quality issues were noted. General Chemistry Method(s) 0., 00 NH H: The following sample(s) showed a negative result greater than the reporting limit -0-MOS-AP-SO-EB (00-0-). These samples were re-analyzed with a dilution and were non-detect, therefore the original result is reported. Method(s) 0., 00 NH H: The method blank for batch contained NH above the method detection limit. This target analyte concentration was less than the reporting limit (); therefore, re-extraction and/or re-analysis of samples was not performed. Method(s)., SM 00 NO F: The matrix spike / matrix spike duplicate MS recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s) SM B: The USB dilution water.o. depletion was greater than 0. mg/l but less than the reporting limit of.0 mg/l. The associated sample results are reported. No other analytical or quality issues were noted. Organic Prep No other analytical or quality issues were noted. Page of //0

111 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received HS-00 Water 0// : 0// : HS-00 Water 0// : 0// : HS-00 Water 0// : 0// : HS-00 Water 0// : 0// : HS-0 Water 0// : 0// : HS-0 Water 0// : 0// : HS-0 Water 0// : 0// : HS-0 Water 0// :00 0// :0 Page of //0

112 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// :0 Lab Sample I: Method: - Semivolatile Organic Compounds (GC/MS) ML Acenaphthene < ug/l 0// : 0// : Acenaphthylene < ug/l 0// : 0// : Anthracene < ug/l 0// : 0// : Benzidine < ug/l 0// : 0// : Benzo[a]anthracene < ug/l 0// : 0// : Benzo[b]fluoranthene < ug/l 0// : 0// : Benzo[k]fluoranthene < ug/l 0// : 0// : Benzo[g,h,i]perylene < ug/l 0// : 0// : Benzo[a]pyrene < ug/l 0// : 0// : -Bromophenyl phenyl ether < ug/l 0// : 0// : Butyl benzyl phthalate < ug/l 0// : 0// : Bis(-chloroethoxy)methane < ug/l 0// : 0// : Bis(-chloroethyl)ether < ug/l 0// : 0// : -Chloro--methylphenol <... ug/l 0// : 0// : -Chloronaphthalene < ug/l 0// : 0// : -Chlorophenol <... ug/l 0// : 0// : -Chlorophenyl phenyl ether <... ug/l 0// : 0// : Chrysene < ug/l 0// : 0// : ibenz(a,h)anthracene < ug/l 0// : 0// : i-n-butyl phthalate <... ug/l 0// : 0// :,-ichlorobenzene < ug/l 0// : 0// :,-ichlorobenzene < ug/l 0// : 0// :,-ichlorobenzene < ug/l 0// : 0// :,'-ichlorobenzidine <... ug/l 0// : 0// :,-ichlorophenol <... ug/l 0// : 0// : iethyl phthalate 0. J. 0. ug/l 0// : 0// :,-imethylphenol <... ug/l 0// : 0// : imethyl phthalate < ug/l 0// : 0// :,-initro--methylphenol <... ug/l 0// : 0// :,-initrophenol <.. ug/l 0// : 0// :,-initrotoluene <... ug/l 0// : 0// :,-initrotoluene <... ug/l 0// : 0// : i-n-octyl phthalate < ug/l 0// : 0// : Bis(-ethylhexyl) phthalate <... ug/l 0// : 0// : Fluoranthene < ug/l 0// : 0// : Fluorene < ug/l 0// : 0// : Hexachlorobenzene < ug/l 0// : 0// : Hexachlorobutadiene <... ug/l 0// : 0// : Hexachlorocyclopentadiene <.. ug/l 0// : 0// : Hexachloroethane <.0..0 ug/l 0// : 0// : Indeno[,,-cd]pyrene < ug/l 0// : 0// : Isophorone < ug/l 0// : 0// : Naphthalene < ug/l 0// : 0// : Nitrobenzene < ug/l 0// : 0// : -Nitrophenol <.0..0 ug/l 0// : 0// : -Nitrophenol <.0..0 ug/l 0// : 0// : N-Nitrosodimethylamine <... ug/l 0// : 0// : N-Nitrosodiphenylamine < ug/l 0// : 0// : N-Nitrosodi-n-propylamine <... ug/l 0// : 0// : Page of //0

113 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// :0 Method: - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: Pentachlorophenol <.. ug/l 0// : 0// : Phenanthrene <0. Phenol <. Pyrene <0.0,,-Trichlorobenzene <0.,,-Trichlorophenol <. Surrogate %Recovery. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0.0 ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :,,-Tribromophenol - 0// : 0// : -Fluorobiphenyl - 0// : 0// : -Fluorophenol - 0// : 0// : Nitrobenzene-d - 0// : 0// : Phenol-d - 0// : 0// : Terphenyl-d - 0// : 0// : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// :0 Lab Sample I: Method: 0 - Organochlorine Pesticides/PCBs in Water ML Aldrin < ug/l 0// :0 0// : alpha-bhc < ug/l 0// :0 0// : beta-bhc < ug/l 0// :0 0// : delta-bhc < ug/l 0// :0 0// : gamma-bhc (Lindane) < ug/l 0// :0 0// : Chlordane (technical) < ug/l 0// :0 0// :,'- < ug/l 0// :0 0// :,'-E < ug/l 0// :0 0// :,'-T < ug/l 0// :0 0// : ieldrin < ug/l 0// :0 0// : Endosulfan I < ug/l 0// :0 0// : Endosulfan II < ug/l 0// :0 0// : Endosulfan sulfate < ug/l 0// :0 0// : Endrin < ug/l 0// :0 0// : Endrin aldehyde < ug/l 0// :0 0// : Heptachlor < ug/l 0// :0 0// : Heptachlor epoxide < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : Toxaphene < ug/l 0// :0 0// : Surrogate %Recovery CB ecachlorobiphenyl - 0// :0 0// : Tetrachloro-m-xylene 0-0// :0 0// : Page of //0

114 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// :0 Method: - Semivolatile Organic Compounds (GC/MS) ML Lab Sample I: Acenaphthene < ug/l 0// : 0// : Acenaphthylene <0. Anthracene <0. Benzidine < Benzo[a]anthracene <0. Benzo[b]fluoranthene <0. Benzo[k]fluoranthene <0. Benzo[g,h,i]perylene <0. Benzo[a]pyrene <0. -Bromophenyl phenyl ether <0. Butyl benzyl phthalate 0.0 J Bis(-chloroethoxy)methane <0. Bis(-chloroethyl)ether <0. -Chloro--methylphenol <. -Chloronaphthalene <0. -Chlorophenol <. -Chlorophenyl phenyl ether <. Chrysene <0. ibenz(a,h)anthracene <0. i-n-butyl phthalate <.,-ichlorobenzene <0.,-ichlorobenzene <0.,-ichlorobenzene <0.,'-ichlorobenzidine <.,-ichlorophenol <. iethyl phthalate 0. J,-imethylphenol <. imethyl phthalate <0.,-initro--methylphenol <.,-initrophenol <.,-initrotoluene <.,-initrotoluene <. i-n-octyl phthalate <0. Bis(-ethylhexyl) phthalate <. Fluoranthene <0. Fluorene <0. Hexachlorobenzene <0. Hexachlorobutadiene <. Hexachlorocyclopentadiene <. Hexachloroethane <.0 Indeno[,,-cd]pyrene <0. Isophorone <0. Naphthalene <0. Nitrobenzene <0. -Nitrophenol <.0 -Nitrophenol <.0 N-Nitrosodimethylamine <. N-Nitrosodiphenylamine <0. N-Nitrosodi-n-propylamine <.. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// : ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. ug/l 0// : 0// :.. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. ug/l 0// : 0// :..0 ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :. 0. ug/l 0// : 0// :..0 ug/l 0// : 0// :..0 ug/l 0// : 0// :.. ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// : Page of //0

115 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// :0 Method: - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: Pentachlorophenol <.. ug/l 0// : 0// : Phenanthrene <0. Phenol <. Pyrene <0.0,,-Trichlorobenzene <0.,,-Trichlorophenol <. Surrogate %Recovery. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :. 0.0 ug/l 0// : 0// :. 0. ug/l 0// : 0// :.. ug/l 0// : 0// :,,-Tribromophenol - 0// : 0// : -Fluorobiphenyl - 0// : 0// : -Fluorophenol 0-0// : 0// : Nitrobenzene-d - 0// : 0// : Phenol-d - 0// : 0// : Terphenyl-d - 0// : 0// : Client Sample I: HS-00 ate Collected: 0// : ate Received: 0// :0 Lab Sample I: Method: 0 - Organochlorine Pesticides/PCBs in Water ML Aldrin < ug/l 0// :0 0// : alpha-bhc < ug/l 0// :0 0// : beta-bhc < ug/l 0// :0 0// : delta-bhc < ug/l 0// :0 0// : gamma-bhc (Lindane) < ug/l 0// :0 0// : Chlordane (technical) < ug/l 0// :0 0// :,'- < ug/l 0// :0 0// :,'-E < ug/l 0// :0 0// :,'-T < ug/l 0// :0 0// : ieldrin < ug/l 0// :0 0// : Endosulfan I < ug/l 0// :0 0// : Endosulfan II < ug/l 0// :0 0// : Endosulfan sulfate < ug/l 0// :0 0// : Endrin < ug/l 0// :0 0// : Endrin aldehyde < ug/l 0// :0 0// : Heptachlor < ug/l 0// :0 0// : Heptachlor epoxide < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : PCB- < ug/l 0// :0 0// : Toxaphene < ug/l 0// :0 0// : Surrogate %Recovery CB ecachlorobiphenyl X - 0// :0 0// : Tetrachloro-m-xylene - 0// :0 0// : Page of //0

116 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Client Sample s TestAmerica Job I: Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// :0 General Chemistry ML Lab Sample I: Biochemical Oxygen emand. b.0.0 mg/l 0/0/ :0 Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// :0 General Chemistry ML Lab Sample I: Phenols, Total mg/l 0// :0 /0/ : Client Sample I: HS-0 ate Collected: 0// : ate Received: 0// :0 Lab Sample I: General Chemistry ML Cyanide, Total < mg/l 0// :0 0// 0: Client Sample I: HS-0 ate Collected: 0// :00 ate Received: 0// :0 Lab Sample I: General Chemistry ML Ammonia 0.0 B mg/l 0/0/ : Nitrogen, Kjeldahl mg/l 0// : 0// : Nitrate Nitrite as N mg/l 0// :0 Chemical Oxygen emand 0. mg/l /0/ :0 Page of //0

117 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Acenaphthene <0. 0. ug/l 0// 0: 0// : Acenaphthylene Anthracene Benzidine Benzo[a]anthracene Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[g,h,i]perylene Benzo[a]pyrene -Bromophenyl phenyl ether Butyl benzyl phthalate Bis(-chloroethoxy)methane Bis(-chloroethyl)ether -Chloro--methylphenol -Chloronaphthalene -Chlorophenol -Chlorophenyl phenyl ether Chrysene ibenz(a,h)anthracene i-n-butyl phthalate,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene,'-ichlorobenzidine,-ichlorophenol iethyl phthalate,-imethylphenol imethyl phthalate,-initro--methylphenol,-initrophenol,-initrotoluene,-initrotoluene i-n-octyl phthalate Bis(-ethylhexyl) phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[,,-cd]pyrene Isophorone Naphthalene Nitrobenzene -Nitrophenol -Nitrophenol N-Nitrosodimethylamine N-Nitrosodiphenylamine ML <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0 0 0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : < ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : < ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.0.0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.0.0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.0.0 ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : Page of //0

118 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB N-Nitrosodi-n-propylamine <.. ug/l 0// 0: 0// : Pentachlorophenol Phenanthrene Phenol Pyrene,,-Trichlorobenzene,,-Trichlorophenol Surrogate ML <. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <0. 0. ug/l 0// 0: 0// : <.. ug/l 0// 0: 0// : MB %Recovery MB,,-Tribromophenol - 0// 0: 0// : -Fluorobiphenyl - 0// 0: 0// : -Fluorophenol - 0// 0: 0// : Nitrobenzene-d - 0// 0: 0// : Phenol-d - 0// 0: 0// : Terphenyl-d - 0// 0: 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Acenaphthene 0.0. ug/l - Acenaphthylene 0.0. ug/l - Anthracene 0.0. ug/l - Benzo[a]anthracene 0.0. ug/l - Benzo[b]fluoranthene 0.0. ug/l - Benzo[k]fluoranthene ug/l - Benzo[g,h,i]perylene 0.0. ug/l - Benzo[a]pyrene 0.0. ug/l - -Bromophenyl phenyl ether 0.0. ug/l 0 - Butyl benzyl phthalate 0.0. ug/l - Bis(-chloroethoxy)methane 0.0. ug/l - Bis(-chloroethyl)ether 0.0. ug/l - -Chloro--methylphenol 0.0. ug/l - -Chloronaphthalene 0.0. ug/l 0 - -Chlorophenol 0.0. ug/l - -Chlorophenyl phenyl ether 0.0. ug/l - Chrysene ug/l 0 - ibenz(a,h)anthracene 0.0. ug/l - i-n-butyl phthalate 0.0. ug/l -,-ichlorobenzene 0.0. ug/l 0 -,-ichlorobenzene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l 0 -,'-ichlorobenzidine 0.0. ug/l 0 -,-ichlorophenol 0.0. ug/l 0 - iethyl phthalate ug/l -,-imethylphenol 0.0. ug/l - imethyl phthalate 0.0. ug/l - Page of //0

119 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec,-initro--methylphenol 0. ug/l -,-initrophenol 0. ug/l 0 -,-initrotoluene ug/l -,-initrotoluene 0.0. ug/l 0 - i-n-octyl phthalate 0.0. ug/l - Bis(-ethylhexyl) phthalate 0.0. ug/l - Fluoranthene 0.0. ug/l - Fluorene 0.0. ug/l - Hexachlorobenzene 0.0. ug/l - Hexachlorobutadiene 0.0. ug/l - Hexachlorocyclopentadiene 0.0. ug/l - Hexachloroethane 0.0. ug/l 0 - Indeno[,,-cd]pyrene ug/l - Isophorone ug/l - Naphthalene 0.0. ug/l 0 - Nitrobenzene 0.0. ug/l - 0 -Nitrophenol 0.0. ug/l - -Nitrophenol 0. ug/l - N-Nitrosodimethylamine 0.0. ug/l - N-Nitrosodiphenylamine.. ug/l - N-Nitrosodi-n-propylamine 0.0. ug/l - 0 Pentachlorophenol 0. ug/l - Phenanthrene ug/l - Phenol ug/l - Pyrene ug/l 0 -,,-Trichlorobenzene 0.0. ug/l -,,-Trichlorophenol ug/l - Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - Nitrobenzene-d - Phenol-d - Terphenyl-d - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Acenaphthene ug/l - 0 Acenaphthylene 0.0. ug/l - 0 Anthracene 0.0. ug/l - 0 Benzo[a]anthracene ug/l - 0 Benzo[b]fluoranthene 0.0. ug/l - 0 Benzo[k]fluoranthene 0.0. ug/l - 0 Benzo[g,h,i]perylene 0.0. ug/l 0-0 RP Limit Page of //0

120 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Benzo[a]pyrene 0.0. ug/l - 0 -Bromophenyl phenyl ether 0.0. ug/l - 0 Butyl benzyl phthalate 0.0. ug/l - 0 Bis(-chloroethoxy)methane 0.0. ug/l - 0 Bis(-chloroethyl)ether 0.0. ug/l 0-0 -Chloro--methylphenol 0.0. ug/l - 0 -Chloronaphthalene 0.0. ug/l 0-0 -Chlorophenol 0.0. ug/l - 0 -Chlorophenyl phenyl ether 0.0. ug/l - 0 Chrysene ug/l ibenz(a,h)anthracene ug/l - 0 i-n-butyl phthalate 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l 0-0,'-ichlorobenzidine 0.0. ug/l - 0,-ichlorophenol 0.0. ug/l - 0 iethyl phthalate ug/l 0-0,-imethylphenol 0.0. ug/l - 0 imethyl phthalate 0.0. ug/l - 0,-initro--methylphenol 0. ug/l - 0,-initrophenol 0. ug/l 0-0,-initrotoluene 0.0. ug/l - 0,-initrotoluene 0.0. ug/l 0-0 i-n-octyl phthalate ug/l - 0 Bis(-ethylhexyl) phthalate 0.0. ug/l - 0 Fluoranthene 0.0. ug/l - 0 Fluorene 0.0. ug/l - 0 Hexachlorobenzene 0.0. ug/l - 0 Hexachlorobutadiene ug/l - 0 Hexachlorocyclopentadiene 0.0. ug/l - 0 Hexachloroethane 0.0. ug/l 0-0 Indeno[,,-cd]pyrene ug/l - 0 Isophorone ug/l Naphthalene 0.0. ug/l - 0 Nitrobenzene 0.0. ug/l Nitrophenol 0.0. ug/l - 0 -Nitrophenol 0. ug/l - 0 N-Nitrosodimethylamine 0.0. ug/l - 0 N-Nitrosodiphenylamine. 0. ug/l - 0 N-Nitrosodi-n-propylamine 0.0. ug/l Pentachlorophenol 0. ug/l - 0 Phenanthrene 0.0. ug/l - 0 Phenol 0.0. ug/l - 0 Pyrene 0.0. ug/l - 0,,-Trichlorobenzene 0.0. ug/l - 0,,-Trichlorophenol 0.0. ug/l - 0 RP Limit Page of //0

121 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - Nitrobenzene-d - Phenol-d - Terphenyl-d - Method: 0 - Organochlorine Pesticides/PCBs in Water Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : 0 Prep : MB MB PCB- < ug/l 0// :0 0// 0: PCB- PCB- PCB- PCB- PCB- PCB- ML < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: < ug/l 0// :0 0// 0: Surrogate MB %Recovery MB CB ecachlorobiphenyl - 0// :0 0// 0: Tetrachloro-m-xylene - 0// :0 0// 0: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Aldrin < ug/l 0// :0 0// : alpha-bhc beta-bhc delta-bhc gamma-bhc (Lindane) Chlordane (technical),'-,'-e,'-t ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor ML < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : < ug/l 0// :0 0// : Page of //0

122 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: 0 - Organochlorine Pesticides/PCBs in Water (Continued) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Heptachlor epoxide < ug/l 0// :0 0// : Toxaphene Surrogate ML < ug/l 0// :0 0// : MB %Recovery MB CB ecachlorobiphenyl - 0// :0 0// : Tetrachloro-m-xylene - 0// :0 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Aldrin ug/l - alpha-bhc ug/l - beta-bhc ug/l - delta-bhc ug/l - gamma-bhc (Lindane) ug/l -,' ug/l -,'-E ug/l 0 0 -,'-T ug/l - ieldrin ug/l - Endosulfan I ug/l - Endosulfan II ug/l - 0 Endosulfan sulfate ug/l - Endrin ug/l 0 - Endrin aldehyde ug/l 0 - Heptachlor ug/l - Heptachlor epoxide ug/l - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : 0 Prep : LCS LCS %Rec PCB-.00. ug/l 0 - PCB-.00. ug/l - Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Aldrin ug/l - 0 alpha-bhc ug/l - 0 RP Limit Page of //0

123 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater QC Sample s Method: 0 - Organochlorine Pesticides/PCBs in Water (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec beta-bhc ug/l 0-0 delta-bhc ug/l - 0 gamma-bhc (Lindane) ug/l - 0,' ug/l - 0,'-E ug/l 0-0,'-T ug/l - 0 ieldrin ug/l - 0 Endosulfan I ug/l - 0 Endosulfan II ug/l Endosulfan sulfate ug/l - 0 Endrin ug/l Endrin aldehyde ug/l 0-0 Heptachlor ug/l - 0 Heptachlor epoxide ug/l 0-0 RP Limit Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : 0 Prep : LCS LCS RP %Rec PCB-.00. ug/l 0-0 PCB-.00. ug/l - 0 Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - RP Limit Method:. - Cyanide, Total Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Cyanide, Total < mg/l 0// :0 0// 0: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Cyanide, Total mg/l - Page of //0

124 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method: 0. - Nitrogen, Ammonia Lab Sample I: MB 00-/ Analysis : MB MB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Ammonia 0.0 J mg/l 0/0/ :0 Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Ammonia.00.0 mg/l 0 - Lab Sample I: M 00-/ M Analysis : LCS LCS %Rec Client Sample I: Lab Control Sample Prep Type: Ammonia J mg/l 0 - M M %Rec Method:. - Nitrogen, Total Kjeldahl Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Nitrogen, Kjeldahl < mg/l 0// : 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0.0 mg/l 0 - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrogen, Kjeldahl mg/l 0 - Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Nitrate Nitrite as N < mg/l 0// 0: Page of //0

125 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method:. - Nitrogen, Nitrate-Nitrite (Continued) Lab Sample I: LCS 00-/ Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N mg/l 0 - Lab Sample I: M 00-/ M Analysis : LCS LCS %Rec Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N J mg/l 0 - Method: 0. - Phenolics, Total Recoverable M M %Rec Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phenols, Total < mg/l 0// :0 /0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phenols, Total mg/l - Method: SM B - BO, -ay Lab Sample I: USB 00-00/ USB Client Sample I: Method Blank Prep Type: Analysis : 00 USB USB ML Biochemical Oxygen emand < mg/l 0/0/ : Lab Sample I: LCS 00-00/ Client Sample I: Lab Control Sample Prep Type: Analysis : 00 LCS LCS %Rec Biochemical Oxygen emand mg/l 0 - Lab Sample I: LCS 00-00/ Client Sample I: Lab Control Sample up Prep Type: Analysis : 00 LCS LCS RP %Rec RP Limit Biochemical Oxygen emand 0 mg/l - Page of //0

126 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method: SM 0 - CO Lab Sample I: MB 00-/ Analysis : MB MB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.. mg/l /0/ :0 Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Chemical Oxygen emand 0.0. mg/l 0 - LCS LCS %Rec Page 0 of //0

127 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Prep 0// : KH TAL PEN Analysis 0// : AJR TAL PEN Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Prep 0 0// :0 KH TAL PEN Analysis 0 0 0// : VC TAL PEN Lab Lab Prep 0 0// :0 KH TAL PEN Analysis 0 0// : VC TAL PEN Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Prep 0// : KH TAL PEN Analysis 0// : AJR TAL PEN Lab Client Sample I: HS-00 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Prep 0 0// :0 KH TAL PEN Analysis 0 0 0// : VC TAL PEN Prep 0 0// :0 KH TAL PEN Analysis 0 0// : VC TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis SM B 00 GMF TAL PEN (Start) (End) 0/0/ :0 0// :0 Lab Page of //0

128 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA - Groundwater Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Prep istill/phenol 0// :0 CLS TAL PEN Analysis 0. /0/ : JMH TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// : ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Prep istill/cn 0// :0 BAB TAL PEN Analysis. 0// 0: BAB TAL PEN Lab Client Sample I: HS-0 Lab Sample I: ate Collected: 0// :00 ate Received: 0// :0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis 0. 0/0/ : KJR TAL PEN Analysis. 0// :0 KJR TAL PEN Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis SM 0 /0/ :0 CLS TAL PEN Lab Laboratory References: TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 Page of //0

129 Client: ewberry Project/Site: Three Mile CreekUSA - Groundwater Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory Semivolatile Organic Compounds (GC/MS) 0CFRA TAL PEN 0 Organochlorine Pesticides/PCBs in Water 0CFRA TAL PEN. Cyanide, Total MCAWW TAL PEN 0. Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Total Kjeldahl MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN 0. Phenolics, Total Recoverable MCAWW TAL PEN SM B BO, -ay SM TAL PEN SM 0 CO SM TAL PEN Protocol References: 0CFRA = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 0CFR, Part, Appendix A, October, and subsequent revisions. MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", Laboratory References: TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 Page of //0

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132 ANALYTICAL REPORT TestAmerica Laboratories, Inc. McLemore rive Pensacola, FL Tel: (0)-0 TestAmerica Job I: Client Project/Site: Three Mile CreekUSA- Groundwater/Sediment For: ewberry 0 Rexwoods r. Raleigh, North Carolina 0 Attn: Michael Hanson Authorized for release by: //0 :: PM Mike Nance, Project Manager II ()- mike.nance@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

133 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Table of Contents TestAmerica Job I: Cover Page Table of Contents efinitions Case Narrative Sample Summary Client Sample s QC Sample s Chronicle Method Summary Chain of Custody Page of //0

134 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment s Metals J General Chemistry J B Glossary Abbreviation escription efinitions/glossary is less than the but greater than or equal to the ML and the concentration is an approximate value. escription is less than the but greater than or equal to the ML and the concentration is an approximate value. Compound was found in the blank and sample. These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF ER L, RA, RE, IN LC MA EL MC ML ML NC N PQL QC RER RP TEF TEQ Contains no Free Liquid uplicate error ratio (normalized absolute difference) ilution Factor Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample ecision level concentration Minimum detectable activity Estimated etection Limit Minimum detectable concentration Method etection Limit Minimum Level (ioxin) Not Calculated Not detected at the reporting limit (or ML or EL if shown) Practical Quantitation Limit Quality Control Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) Relative Percent ifference, a measure of the relative difference between two points Toxicity Equivalent Factor (ioxin) Toxicity Equivalent Quotient (ioxin) TestAmerica Job I: Page of //0

135 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Job I: Laboratory: Narrative Comments No additional comments. Job Narrative Receipt The samples were received on /0/0 :0 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. Except: Sample S for fecal was not listed on COC. but was received in sample cooler Metals No analytical or quality issues were noted. General Chemistry No other analytical or quality issues were noted. Organic Prep No analytical or quality issues were noted. Lab Admin No analytical or quality issues were noted. Page of //0

136 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received G Water 0/0/ 0: 0/0/ : G Water 0/0/ 0: 0/0/ : G Water 0/0/ : 0/0/ : G Water 0/0/ :0 0/0/ : G Water 0/0/ :0 0/0/ : G Water 0/0/ : 0/0/ : G Water 0/0/ : 0/0/ : S Solid 0/0/ 0: 0/0/ : S Solid 0/0/ : 0/0/ : S Solid 0/0/ 0: 0/0/ : S(F)-00 Solid 0/0/ : 0/0/ : S(F)-00 Solid 0/0/ : 0/0/ : S(F)-00 Solid 0/0/ : 0/0/ : S(F)-00 Solid 0/0/ : 0/0/ :0 Page of //0

137 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: G ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Client Sample s TestAmerica Job I: Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// 0: 0// : Arsenic < mg/l 0// 0: 0// : Barium mg/l 0// 0: 0// : Cadmium < mg/l 0// 0: 0// : Chromium < mg/l 0// 0: 0// : Lead 0.00 J mg/l 0// 0: 0// : Selenium < mg/l 0// 0: 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ : General Chemistry ML Nitrogen, Kjeldahl 0. J mg/l 0// : 0// :0 ortho-phosphate < mg/l 0// : Phosphorus mg/l /0/ : /0/ : Biochemical Oxygen emand < mg/l 0// : Method: Enterolert - Enterococcus by Enterolert (Quantitray) Enterococci.0.0 MPN/0mL 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal CFU/0mL 0/0/ :0 Client Sample I: G ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// 0: 0// : Arsenic < mg/l 0// 0: 0// : Barium mg/l 0// 0: 0// : Cadmium < mg/l 0// 0: 0// : Chromium < mg/l 0// 0: 0// : Lead < mg/l 0// 0: 0// : Selenium < mg/l 0// 0: 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ : General Chemistry ML Nitrogen, Kjeldahl mg/l 0// : 0// : ortho-phosphate mg/l 0// : Phosphorus mg/l /0/ : /0/ : Biochemical Oxygen emand < mg/l 0// : Page of //0

138 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample s TestAmerica Job I: Client Sample I: G ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Method: Enterolert - Enterococcus by Enterolert (Quantitray) Lab Sample I: Enterococci.0.0 MPN/0mL 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal.0.0 CFU/0mL 0/0/ :0 Client Sample I: G ate Collected: 0/0/ : ate Received: 0/0/ :0 Method: Enterolert - Enterococcus by Enterolert (Quantitray) Lab Sample I: Enterococci.0.0 MPN/0mL 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal 0 CFU/0mL 0/0/ :0 Client Sample I: G ate Collected: 0/0/ :0 ate Received: 0/0/ :0 Lab Sample I: Method: Enterolert - Enterococcus by Enterolert (Quantitray) Enterococci..0.0 MPN/0mL 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal 0 CFU/0mL 0/0/ :0 Client Sample I: G ate Collected: 0/0/ :0 ate Received: 0/0/ :0 Lab Sample I: Method: Enterolert - Enterococcus by Enterolert (Quantitray) Enterococci.0.0 MPN/0mL 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal CFU/0mL 0/0/ :0 Client Sample I: G ate Collected: 0/0/ : ate Received: 0/0/ :0 Lab Sample I: Method: Enterolert - Enterococcus by Enterolert (Quantitray) Enterococci.0.0 MPN/0mL 0/0/ :0 Page of //0

139 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: G ate Collected: 0/0/ : ate Received: 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Client Sample s TestAmerica Job I: Lab Sample I: Coliform, Fecal 0 CFU/0mL 0/0/ :0 Client Sample I: G ate Collected: 0/0/ : ate Received: 0/0/ :0 Method: 0B - Metals (ICP) - Total Recoverable ML Lab Sample I: Silver < mg/l 0// 0: 0// : Arsenic 0.0 Barium 0. Cadmium <0.00 Chromium <0.000 Lead 0.0 Selenium < mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ :0 General Chemistry ML ortho-phosphate mg/l 0// : Phosphorus mg/l /0/ : /0/ : Biochemical Oxygen emand.0.0 mg/l 0// : Method: Enterolert - Enterococcus by Enterolert (Quantitray) Enterococci.0.0 MPN/0mL 0/0/ :0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal 0 CFU/0mL 0/0/ :0 Client Sample I: S ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Lab Sample I: Percent Solids:. Method: 0B - Metals (ICP) Silver < mg/kg 0// : 0// : Arsenic <0. Barium. Cadmium <0. Chromium 0. Lead 0. Selenium <0. Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML ML mg/kg 0// : 0// :. 0. mg/kg 0// : 0// : mg/kg 0// : 0// : mg/kg 0// : 0// : mg/kg 0// : 0// :. 0. mg/kg 0// : 0// : Hg < mg/kg 0// : 0/0/ :0 Page of //0

140 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S ate Collected: 0/0/ 0: ate Received: 0/0/ :0 General Chemistry Client Sample s ML TestAmerica Job I: Lab Sample I: Percent Solids:. Nitrogen, Kjeldahl. mg/kg 0// : 0// : Phosphorus, Total Nitrogen, Total J. mg/kg 0// : 0// :.. mg/kg /0/ : Total Volatile Solids 0.0 B % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N < mg/kg 0// : General Chemistry - ASTM Leach Chemical Oxygen emand. J.0 mg/l /0/ : ML Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) Coliform, Fecal MPN/g.W. 0/0/ :0 0/0/ :0 Client Sample I: S ate Collected: 0/0/ : ate Received: 0/0/ :0 Lab Sample I: Percent Solids:. Method: 0B - Metals (ICP) Silver < mg/kg 0// : 0// : Arsenic.0 Barium 0 Cadmium 0. J Chromium Lead Selenium. J Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML ML.. mg/kg 0// : 0// :.0 0. mg/kg 0// : 0// :. 0.0 mg/kg 0// : 0// :. 0. mg/kg 0// : 0// :. 0. mg/kg 0// : 0// :.0. mg/kg 0// : 0// : Hg mg/kg 0// : 0/0/ :0 General Chemistry Nitrogen, Kjeldahl 0 mg/kg 0// : 0// :0 Phosphorus, Total 0 Nitrogen, Total 0 ML mg/kg 0// : 0// :.. mg/kg /0/ : Total Volatile Solids B % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N.0. mg/kg 0// : General Chemistry - ASTM Leach Chemical Oxygen emand 0.0 mg/l /0/ : ML Page of //0

141 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S ate Collected: 0/0/ : ate Received: 0/0/ :0 Client Sample s Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) TestAmerica Job I: Lab Sample I: Percent Solids:. Coliform, Fecal MPN/g.W. 0/0/ :0 0/0/ :0 Client Sample I: S ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Method: 0B - Metals (ICP) ML Lab Sample I: Percent Solids:. Silver < mg/kg 0// : 0// :00 Arsenic <0. Barium. Cadmium <0. Chromium. Lead. Selenium < mg/kg 0// : 0// : mg/kg 0// : 0// : mg/kg 0// : 0// : mg/kg 0// : 0// : mg/kg 0// : 0// : mg/kg 0// : 0// :00 Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML Hg < mg/kg 0// : 0/0/ :0 General Chemistry Nitrogen, Kjeldahl.. mg/kg 0// : 0// : Phosphorus, Total Nitrogen, Total ML..0 mg/kg 0// : 0// :.. mg/kg /0/ : Total Volatile Solids 0.0 B % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N < mg/kg 0// : General Chemistry - ASTM Leach Chemical Oxygen emand.0 mg/l /0/ : Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) ML Coliform, Fecal MPN/g.W. 0/0/ :0 0/0/ :0 Client Sample I: S(F)-00 ate Collected: 0/0/ : ate Received: 0/0/ :0 Lab Sample I: Percent Solids:. Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) Coliform, Fecal MPN/g.W. 0/0/ :0 0/0/ :0 Page of //0

142 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S(F)-00 ate Collected: 0/0/ : ate Received: 0/0/ :0 Client Sample s Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) TestAmerica Job I: Lab Sample I: Percent Solids:. Coliform, Fecal 00.. MPN/g.W. 0/0/ :0 0/0/ :0 Client Sample I: S(F)-00 ate Collected: 0/0/ : ate Received: 0/0/ :0 Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) Lab Sample I: Percent Solids:. Coliform, Fecal MPN/g.W. 0/0/ :0 0/0/ :0 Client Sample I: S(F)-00 ate Collected: 0/0/ : ate Received: 0/0/ :0 Lab Sample I: Percent Solids:. Method: SM E - Coliforms, Fecal (Multiple-Tube Fermentation) Coliform, Fecal MPN/g.W. 0/0/ :0 0/0/ :0 Page of //0

143 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: 0B - Metals (ICP) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-0/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : 0 MB MB Silver < mg/kg 0// : 0// : Arsenic Barium Cadmium Chromium Lead Selenium ML < mg/kg 0// : 0// : < mg/kg 0// : 0// : < mg/kg 0// : 0// : < mg/kg 0// : 0// : < mg/kg 0// : 0// : < mg/kg 0// : 0// : Lab Sample I: LCS 00-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : 0 LCS LCS %Rec Silver. 0. mg/kg - Arsenic mg/kg 0 - Barium 0 mg/kg - Cadmium.0. mg/kg - Chromium mg/kg - Lead mg/kg - Selenium.. mg/kg - Lab Sample I: MB 00-0/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : Prep : 0 MB MB Silver < mg/l 0// 0: 0// : Arsenic Barium Cadmium Chromium Lead Selenium ML < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : < mg/l 0// 0: 0// : Lab Sample I: LCS 00-0/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : Prep : 0 LCS LCS %Rec Silver mg/l 0 - Arsenic.00.0 mg/l 0 - Barium.00.0 mg/l 0 - Cadmium mg/l 0 - Chromium.00.0 mg/l 0 - Lead.00.0 mg/l 0 - Selenium.00.0 mg/l 0 - Page of //0

144 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: 0A - Mercury (CVAA) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Mercury < mg/l /0/ 0: /0/ : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l 0 - Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Hg < mg/kg 0// : 0/0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Hg.. mg/kg 0 - Method:. - Solids, Total Volatile (TVS) Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB Total Volatile Solids % 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Total Volatile Solids 0.0 <0. % - Page of //0

145 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Nitrogen, Total Kjeldahl QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/l 0// : 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0.0 mg/l 0 - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/kg 0// : 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/kg - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrogen, Kjeldahl mg/l 0 - Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Nitrate Nitrite as N J mg/kg Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Soluble Analysis : MB MB ML Nitrate Nitrite as N < mg/kg 0// : Page of //0

146 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Nitrogen, Nitrate-Nitrite (Continued) Lab Sample I: LCS 00-/-A Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Soluble Nitrate Nitrite as N mg/kg 0 - Lab Sample I: MS Analysis : Sample Sample LCS LCS %Rec Nitrate Nitrite as N.. mg/kg 0 - Lab Sample I: MS Analysis : Sample Sample MS MS %Rec Client Sample I: S Prep Type: Soluble Client Sample I: S Prep Type: Soluble Nitrate Nitrite as N.. mg/kg 0 - MS MS %Rec RP RP Limit Method:. - Phosphorus, Ortho Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML ortho-phosphate < mg/l 0// : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec ortho-phosphate mg/l Lab Sample I: MS Client Sample I: G Prep Type: Analysis : Sample Sample MS MS %Rec ortho-phosphate < mg/l Lab Sample I: MS Client Sample I: G Prep Type: Analysis : Sample Sample MS MS RP %Rec RP Limit ortho-phosphate < mg/l 0 - Page of //0

147 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Phosphorus, Total QC Sample s TestAmerica Job I: Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Phosphorus < mg/l /0/ : /0/ : ML Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus mg/l 0 - Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Phosphorus mg/l 0-0 RP Limit Method:. - Phosphorus, Total Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phosphorus, Total < mg/kg 0// : 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus, Total.0. mg/kg - Lab Sample I: M 00-/ M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Phosphorus, Total J mg/kg Lab Sample I: M 00-/0 M Client Sample I: Lab Control Sample Prep Type: Analysis : M M %Rec Phosphorus, Total 0.0 <0. mg/kg Page of //0

148 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: SM B - BO, -ay Lab Sample I: USB 00-/ USB Analysis : USB USB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Biochemical Oxygen emand < mg/l 0// : Lab Sample I: LCS 00-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Biochemical Oxygen emand mg/l - Lab Sample I: LCS 00-/ Analysis : LCS LCS %Rec Client Sample I: Lab Control Sample up Prep Type: Biochemical Oxygen emand mg/l - LCS LCS %Rec RP RP Limit Method: SM 0 - CO Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Chemical Oxygen emand <.0.0 mg/l /0/ : Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Chemical Oxygen emand <.0.0 mg/l /0/ : Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand 00 0 mg/l 0 - Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand mg/l Page of //0

149 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: SM 0 - CO (Continued) Lab Sample I: LCS 0-/ Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample up Prep Type: Chemical Oxygen emand 00 0 mg/l 0-0 Lab Sample I: LCS 0-/ Analysis : LCS LCS %Rec RP RP Limit Client Sample I: Lab Control Sample up Prep Type: Chemical Oxygen emand mg/l 0-0 Lab Sample I: LB 0-/-A LB Analysis : LB LB LCS LCS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: ASTM Leach Chemical Oxygen emand <.0.0 mg/l /0/ : Method: Enterolert - Enterococcus by Enterolert (Quantitray) Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB Enterococci < MPN/0mL 0/0/ : Page of //0

150 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: G Lab Sample I: ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0 0// 0: NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Analysis. 0// : LSS TAL PEN Analysis SM B LSS TAL PEN (Start) (End) 0// : 0// :0 Prep. 0// : JAT TAL PEN Analysis. 0// :0 JAT TAL PEN Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Analysis SM 0/0/ :0 JP TAL MOB Analysis Enterolert 0/0/ :0 JP TAL MOB Lab Client Sample I: G Lab Sample I: ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0 0// 0: NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Analysis. 0// : LSS TAL PEN Analysis SM B LSS TAL PEN (Start) (End) 0// : 0// :0 Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Analysis SM 0/0/ :0 JP TAL MOB Analysis Enterolert 0/0/ :0 JP TAL MOB Lab Client Sample I: G Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor or Analyst Analysis SM 0/0/ :0 JP TAL MOB Number Analysis Enterolert 0/0/ :0 JP TAL MOB Lab Page of //0

151 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: G Lab Sample I: ate Collected: 0/0/ :0 ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor or Analyst Analysis SM 0/0/ :0 JP TAL MOB Number Analysis Enterolert 0/0/ :0 JP TAL MOB Client Sample I: G Lab Sample I: ate Collected: 0/0/ :0 ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor or Analyst Analysis SM 0/0/ :0 JP TAL MOB Number Lab Lab Analysis Enterolert 0/0/ :0 JP TAL MOB Client Sample I: G Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor or Analyst Analysis SM 0/0/ :0 JP TAL MOB Number Analysis Enterolert 0/0/ :0 JP TAL MOB Lab Client Sample I: G Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0 0// 0: NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ :0 JAP TAL PEN Analysis. 0// : LSS TAL PEN Analysis SM B LSS TAL PEN (Start) (End) 0// : 0// :0 Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Analysis SM 0/0/ :0 JP TAL MOB Analysis Enterolert 0/0/ :0 JP TAL MOB Lab Page 0 of //0

152 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S Lab Sample I: ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Percent Solids:. Prep Type Soluble Soluble Type Method Run ilution Factor Number or Analyst Prep 00B 0 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep B 0// : JAP TAL PEN Analysis B 0/0/ :0 JAP TAL PEN Analysis Moisture 0// 0: LEC TAL PEN Analysis. 0// :0 SLT TAL PEN Leach I Leach 0// 0:0 KJR TAL PEN Analysis. 0// : KJR TAL PEN Prep././ 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Lab ASTM Leach ASTM Leach Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis Total Nitrogen /0/ : JMH TAL PEN Leach - 0// :0 SJM TAL NSH Analysis SM 0 /0/ : MSJ TAL NSH Analysis SM E 0/0/ :0 JP TAL MOB Prep SterileWatSusp 0/0/ :0 JP TAL MOB Client Sample I: S Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Percent Solids:. Prep Type Soluble Soluble ASTM Leach ASTM Leach Type Method Run ilution Factor Number or Analyst Prep 00B 0 0// : NAB TAL PEN Analysis 0B 0// : SLM TAL PEN Prep B 0// : JAP TAL PEN Analysis B 0/0/ :0 JAP TAL PEN Analysis Moisture 0// 0: LEC TAL PEN Analysis. 0// :0 SLT TAL PEN Leach I Leach 0// : KJR TAL PEN Analysis. 0// : KJR TAL PEN Prep././ 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Prep. 0// : JAT TAL PEN Analysis. 0// :0 JAT TAL PEN Analysis Total Nitrogen /0/ : JMH TAL PEN Leach - 0// :0 SJM TAL NSH Analysis SM 0 /0/ : MSJ TAL NSH Analysis SM E 0/0/ :0 JP TAL MOB Prep SterileWatSusp 0/0/ :0 JP TAL MOB Lab Page of //0

153 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S Lab Sample I: ate Collected: 0/0/ 0: ate Received: 0/0/ :0 Percent Solids:. Prep Type Soluble Soluble Type Method Run ilution Factor Number or Analyst Prep 00B 0 0// : NAB TAL PEN Analysis 0B 0// :00 SLM TAL PEN Prep B 0// : JAP TAL PEN Analysis B 0/0/ :0 JAP TAL PEN Analysis Moisture 0// 0: LEC TAL PEN Analysis. 0// :0 SLT TAL PEN Leach I Leach 0// : KJR TAL PEN Analysis. 0// : KJR TAL PEN Prep././ 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Lab ASTM Leach ASTM Leach Prep. 0// : JAT TAL PEN Analysis. 0// : JAT TAL PEN Analysis Total Nitrogen /0/ : JMH TAL PEN Leach - 0// :0 SJM TAL NSH Analysis SM 0 /0/ : MSJ TAL NSH Analysis SM E 0/0/ :0 JP TAL MOB Prep SterileWatSusp 0/0/ :0 JP TAL MOB Client Sample I: S(F)-00 Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis Moisture 0/0/ :00 CJM TAL PEN Analysis SM E 0/0/ :0 JP TAL MOB Prep SterileWatSusp 0/0/ :0 JP TAL MOB Lab Client Sample I: S(F)-00 Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis Moisture 0/0/ :00 CJM TAL PEN Analysis SM E 0/0/ :0 JP TAL MOB Prep SterileWatSusp 0/0/ :0 JP TAL MOB Lab Client Sample I: S(F)-00 Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis Moisture 0/0/ :00 CJM TAL PEN Lab Page of //0

154 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S(F)-00 Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Percent Solids:. Prep Type Type Method Run ilution Factor or Analyst Analysis SM E 0/0/ :0 JP TAL MOB Number Prep SterileWatSusp 0/0/ :0 JP TAL MOB Client Sample I: S(F)-00 Lab Sample I: ate Collected: 0/0/ : ate Received: 0/0/ :0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis Moisture 0/0/ :00 CJM TAL PEN Analysis SM E 0/0/ :0 JP TAL MOB Prep SterileWatSusp 0/0/ :0 JP TAL MOB Lab Lab Laboratory References: TAL MOB = TestAmerica Mobile, 00 Lakeside rive, Mobile, AL, TEL ()- TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

155 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory 0B Metals (ICP) SW TAL PEN 0A Mercury (CVAA) SW TAL PEN B Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) SW TAL PEN. Solids, Total Volatile (TVS) MCAWW TAL PEN. Nitrogen, Total Kjeldahl MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN. Phosphorus, Total EPA TAL TAL. Phosphorus, Ortho EPA TAL PEN. Phosphorus, Total EPA TAL PEN Moisture Percent Moisture EPA TAL PEN SM B BO, -ay SM TAL PEN SM 0 CO SM TAL NSH Total Nitrogen Nitrogen, Total EPA TAL PEN Enterolert Enterococcus by Enterolert (Quantitray) IEXX TAL MOB SM E Coliforms, Fecal (Multiple-Tube Fermentation) SM TAL MOB SM Coliforms, Fecal (Membrane Filter) SM TAL MOB Protocol References: EPA = US Environmental Protection Agency IEXX = IEXX Laboratories MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL MOB = TestAmerica Mobile, 00 Lakeside rive, Mobile, AL, TEL ()- TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

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160 ANALYTICAL REPORT TestAmerica Laboratories, Inc. McLemore rive Pensacola, FL Tel: (0)-0 TestAmerica Job I: Client Project/Site: Three Mile CreekUSA- Groundwater/Sediment For: ewberry 0 Rexwoods r. Raleigh, North Carolina 0 Attn: Michael Hanson Authorized for release by: //0 :0:0 PM Mike Nance, Project Manager II ()- mike.nance@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

161 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Table of Contents TestAmerica Job I: Cover Page Table of Contents efinitions Case Narrative Sample Summary Client Sample s QC Sample s Chronicle Method Summary Chain of Custody Page of //0

162 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment s GC/MS VOA escription * LCS or LCS exceeds the control limits GC/MS Semi VOA J GC Semi VOA X Metals J General Chemistry B F H J escription efinitions/glossary is less than the but greater than or equal to the ML and the concentration is an approximate value. escription Surrogate is outside control limits escription is less than the but greater than or equal to the ML and the concentration is an approximate value. escription Compound was found in the blank and sample. MS/MS Recovery and/or RP exceeds the control limits Sample was prepped or analyzed beyond the specified holding time is less than the but greater than or equal to the ML and the concentration is an approximate value. TestAmerica Job I: Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid ER uplicate error ratio (normalized absolute difference) ilution Factor L, RA, RE, IN Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision level concentration MA Minimum detectable activity EL Estimated etection Limit MC Minimum detectable concentration ML Method etection Limit ML Minimum Level (ioxin) NC Not Calculated N Not detected at the reporting limit (or ML or EL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) Page of //0

163 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Job I: Laboratory: Narrative Comments No additional comments. Job Narrative Receipt The samples were received on //0 :0 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. GC/MS VOA Method(s) : A full list spike was utilized for this method. ue to the large number of spiked analytes, there is a high probability that one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for analytes to recover outside criteria for this method when a full list spike is utilized. The LCS associated with batch had analyte outside control limits; therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified. No other analytical or quality issues were noted. GC/MS Semi VOA Method(s) : The continuing calibration verification (CCV) for Benzidine associated with batch recovered above the upper control limit. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. HSI-00-0 (00-0-) No other analytical or quality issues were noted. GC Semi VOA Method(s) 0, 0A: The TCMX surrogate recovery for samplehsi-00-0 (00-0-) is within control limits, however, the CB surrogate recovery is low outside control limits. The sample is non-detect and reported. No other analytical or quality issues were noted. Metals Method(s) A, B: The matrix spike / matrix spike duplicate (MS/MS) recoveries for prep batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s) A, B: The closing CRA recovered below limits due to the spike being ommited before digestion. The beginning CRA and all other instrument QC passed criteria therefore the data is reported with this narrative. No other analytical or quality issues were noted. General Chemistry Method(s).: The matrix spike / matrix spike duplicate (MS/MS) recoveries for. batch 0- were outside control limits. The associated laboratory control samples met acceptance criteria. Method(s).: The following sample(s) was received outside of holding time: G (00-0-), HSI-00-0 (00-0-). Method(s).: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s) SM B: The following sample(s) were received in the Mobile Lab on but did not arrive to the Pensacola Lab until PM was notified that samples were out of hold upon receipt. Analyst was instructed to proceed with analyzing sample out of hold.: G (00-0-), HSI-00-0 (00-0-). Method(s) SM 0: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The Page of //0

164 Case Narrative Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Job I: (Continued) Laboratory: (Continued) associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s)., SM 0: The matrix spike (MS) recovery for batch was outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. No other analytical or quality issues were noted. Organic Prep No other analytical or quality issues were noted. Lab Admin No analytical or quality issues were noted. Page of //0

165 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received S Solid 0/0/ :0 0// 0: G Water 0/0/ : 0// 0: HSI-00-0 Water 0/0/ : 0// 0:0 Page of //0

166 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S ate Collected: 0/0/ :0 ate Received: 0// 0:0 Method: 0B - Metals (ICP) Client Sample s ML TestAmerica Job I: Lab Sample I: Percent Solids:.0 Silver < mg/kg 0// :0 0// 0: Arsenic <0. Barium. Cadmium 0. J Chromium. Lead. Selenium <0. Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) ML mg/kg 0// :0 0// 0:. 0. mg/kg 0// :0 0// 0: mg/kg 0// :0 0// 0: mg/kg 0// :0 0// 0: mg/kg 0// :0 0// 0:. 0. mg/kg 0// :0 0// 0: Hg < mg/kg /0/ : /0/ : General Chemistry Nitrogen, Kjeldahl 0. mg/kg 0/0/ : /0/ : Phosphorus, Total Nitrogen, Total 0 ML. mg/kg 0/0/ : /0/ :.. mg/kg /0/ : Total Volatile Solids. B % 0// :0 General Chemistry - Soluble ML Nitrate Nitrite as N < mg/kg 0// : General Chemistry - ASTM Leach Chemical Oxygen emand <.. mg/l /0/ : ML Client Sample I: G ate Collected: 0/0/ : ate Received: 0// 0:0 Lab Sample I: Method: 0B - Metals (ICP) - Total Recoverable ML Silver < mg/l 0// 0: 0// : Arsenic < mg/l 0// 0: 0// : Barium mg/l 0// 0: 0// : Cadmium < mg/l 0// 0: 0// : Chromium < mg/l 0// 0: 0// : Lead 0.00 J mg/l 0// 0: 0// : Selenium < mg/l 0// 0: 0// : Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ : General Chemistry ML Nitrogen, Kjeldahl mg/l 0/0/ : /0/ : ortho-phosphate 0.0 H mg/l 0// : Phosphorus mg/l /0/ : /0/ :00 Page of //0

167 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample s TestAmerica Job I: Client Sample I: G ate Collected: 0/0/ : ate Received: 0// 0:0 General Chemistry (Continued) ML Lab Sample I: Biochemical Oxygen emand. H.0.0 mg/l 0// :0 Client Sample I: HSI-00-0 ate Collected: 0/0/ : ate Received: 0// 0:0 Method: - Volatile Organic Compounds (GC/MS) ML Lab Sample I: 00-0-,,-Trichloroethane < ug/l /0/ 00:,,,-Tetrachloroethane <0.0,,-Trichloroethane <0.0,-ichloroethane <0.0,-ichloroethene <0.0,-ichlorobenzene <0.0,-ichloroethane <0.0,-ichloropropane <0.0,-ichlorobenzene <0.,-ichlorobenzene <0. Acrolein <0 * Acrylonitrile <. Benzene <0. Bromoform <0. Bromomethane <0. Carbon tetrachloride <0.0 Chlorobenzene <0.0 ibromochloromethane <0.0 Chloroethane <0. Chloroform <0.0 Chloromethane <0. cis-,-ichloroethene <0.0 cis-,-ichloropropene <0.0 Bromodichloromethane <0.0 Ethylbenzene <0.0 m-xylene & p-xylene <. Methyl tert-butyl ether <0. Methylene Chloride <.0 o-xylene <0.0 Tetrachloroethene <0. Toluene <0.0 trans-,-ichloroethene <0.0 trans-,-ichloropropene <0.0 Trichloroethene <0.0 Trichlorofluoromethane <0. Vinyl chloride <0.0 -Chloroethyl vinyl ether < ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00:.0 0. ug/l /0/ 00:.0 0. ug/l /0/ 00: 0 0 ug/l /0/ 00:.0. ug/l /0/ 00:.0 0. ug/l /0/ 00:.0 0. ug/l /0/ 00:.0 0. ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00:.0 0. ug/l /0/ 00: ug/l /0/ 00:.0 0. ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00:. ug/l /0/ 00:.0 0. ug/l /0/ 00:.0.0 ug/l /0/ 00: ug/l /0/ 00:.0 0. ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00: ug/l /0/ 00:.0 0. ug/l /0/ 00: ug/l /0/ 00:.0.0 ug/l /0/ 00: Surrogate %Recovery -Bromofluorobenzene - /0/ 00: ibromofluoromethane 0 - /0/ 00: Toluene-d (Surr) 0 - /0/ 00: Page of //0

168 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample s TestAmerica Job I: Client Sample I: HSI-00-0 ate Collected: 0/0/ : ate Received: 0// 0:0 Method: - Semivolatile Organic Compounds (GC/MS) ML Lab Sample I: Acenaphthene < ug/l 0// : 0// 0:0 Acenaphthylene <0. Anthracene <0. Benzidine < Benzo[a]anthracene <0. Benzo[b]fluoranthene <0. Benzo[k]fluoranthene <0. Benzo[g,h,i]perylene <0. Benzo[a]pyrene <0. -Bromophenyl phenyl ether <0. Butyl benzyl phthalate 0. J Bis(-chloroethoxy)methane <0. Bis(-chloroethyl)ether <0. -Chloro--methylphenol <. -Chloronaphthalene <0. -Chlorophenol <. -Chlorophenyl phenyl ether <. Chrysene <0. ibenz(a,h)anthracene <0. i-n-butyl phthalate <.,-ichlorobenzene <0.,-ichlorobenzene <0.,-ichlorobenzene <0.,'-ichlorobenzidine <.,-ichlorophenol <. iethyl phthalate 0. J,-imethylphenol <. imethyl phthalate <0.,-initro--methylphenol <.,-initrophenol <.,-initrotoluene <.,-initrotoluene <. i-n-octyl phthalate <0. Bis(-ethylhexyl) phthalate <. Fluoranthene <0. Fluorene <0. Hexachlorobenzene <0. Hexachlorobutadiene <. Hexachlorocyclopentadiene <. Hexachloroethane <.0 Indeno[,,-cd]pyrene <0. Isophorone <0. Naphthalene <0. Nitrobenzene <0. -Nitrophenol <.0 -Nitrophenol <.0 N-Nitrosodimethylamine <. N-Nitrosodiphenylamine <0. N-Nitrosodi-n-propylamine <.. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0 ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. ug/l 0// : 0// 0:0..0 ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0..0 ug/l 0// : 0// 0:0..0 ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0 Page of //0

169 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample s TestAmerica Job I: Client Sample I: HSI-00-0 ate Collected: 0/0/ : ate Received: 0// 0:0 Method: - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: Pentachlorophenol <.. ug/l 0// : 0// 0:0 Phenanthrene <0. Phenol <. Pyrene <0.0,,-Trichlorobenzene <0.,,-Trichlorophenol <. Surrogate %Recovery. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0: ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0.. ug/l 0// : 0// 0:0,,-Tribromophenol - 0// : 0// 0:0 -Fluorobiphenyl 0-0// : 0// 0:0 -Fluorophenol - 0// : 0// 0:0 Nitrobenzene-d - 0// : 0// 0:0 Phenol-d - 0// : 0// 0:0 Terphenyl-d - 0// : 0// 0:0 Method: 0 - Organochlorine Pesticides/PCBs in Water ML Aldrin < ug/l 0// : 0// : alpha-bhc < ug/l 0// : 0// : beta-bhc < ug/l 0// : 0// : delta-bhc < ug/l 0// : 0// : gamma-bhc (Lindane) < ug/l 0// : 0// : Chlordane (technical) < ug/l 0// : 0// :,'- < ug/l 0// : 0// :,'-E < ug/l 0// : 0// :,'-T < ug/l 0// : 0// : ieldrin < ug/l 0// : 0// : Endosulfan I < ug/l 0// : 0// : Endosulfan II < ug/l 0// : 0// : Endosulfan sulfate < ug/l 0// : 0// : Endrin < ug/l 0// : 0// : Endrin aldehyde < ug/l 0// : 0// : Heptachlor < ug/l 0// : 0// : Heptachlor epoxide < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : PCB- < ug/l 0// : 0// : Toxaphene < ug/l 0// : 0// : Surrogate %Recovery CB ecachlorobiphenyl X - 0// : 0// : Tetrachloro-m-xylene - 0// : 0// : Method: 0B - Metals (ICP) - Total Recoverable ML Antimony < mg/l 0// 0: 0// :0 Page of //0

170 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample s TestAmerica Job I: Client Sample I: HSI-00-0 ate Collected: 0/0/ : ate Received: 0// 0:0 Method: 0B - Metals (ICP) - Total Recoverable (Continued) ML Lab Sample I: Arsenic < mg/l 0// 0: 0// :0 Beryllium <0.00 Cadmium <0.00 Chromium <0.000 Copper 0.0 Lead 0.0 Nickel <0.000 Selenium <0.000 Silver <0.000 Thallium <0.000 Zinc mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// :0 Method: 0A - Mercury (CVAA) ML Mercury < mg/l /0/ 0: /0/ : General Chemistry ML Cyanide, Total < mg/l 0// 0: 0// : Ammonia mg/l 0// :0 Nitrogen, Kjeldahl mg/l 0/0/ : /0/ : Nitrate Nitrite as N mg/l 0// 0: ortho-phosphate 0. H mg/l 0// : Phosphorus mg/l /0/ : /0/ : Phenols, Total < mg/l 0// :0 /0/ : Biochemical Oxygen emand. H.0.0 mg/l 0// : Chemical Oxygen emand. mg/l /0/ :0 Page of //0

171 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 00-/ Analysis : MB MB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type:,,-Trichloroethane < ug/l /0/ :0,,,-Tetrachloroethane,,-Trichloroethane,-ichloroethane,-ichloroethene,-ichlorobenzene,-ichloroethane,-ichloropropane,-ichlorobenzene,-ichlorobenzene Acrolein Acrylonitrile Benzene Bromoform Bromomethane Carbon tetrachloride Chlorobenzene ibromochloromethane Chloroethane Chloroform Chloromethane cis-,-ichloroethene cis-,-ichloropropene Bromodichloromethane Ethylbenzene m-xylene & p-xylene Methyl tert-butyl ether Methylene Chloride o-xylene Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride -Chloroethyl vinyl ether < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 <0 0 0 ug/l /0/ :0 <..0. ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 <.. ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 < ug/l /0/ :0 Surrogate MB %Recovery MB -Bromofluorobenzene - /0/ :0 ibromofluoromethane 0 - /0/ :0 Toluene-d (Surr) 0 - /0/ :0 Page of //0

172 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 00-/00 Analysis : TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type:,,-Trichloroethane ug/l - LCS LCS %Rec,,,-Tetrachloroethane 0.0. ug/l -,,-Trichloroethane ug/l 0 -,-ichloroethane 0.0. ug/l -,-ichloroethene ug/l -,-ichlorobenzene 0.0. ug/l -,-ichloroethane ug/l -,-ichloropropane 0.0. ug/l -,-ichlorobenzene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l - Acrolein 00 * ug/l - Acrylonitrile 00 ug/l - Benzene 0.0. ug/l - Bromoform ug/l - Bromomethane 0.0. ug/l - Carbon tetrachloride 0.0. ug/l 0 - Chlorobenzene ug/l - ibromochloromethane ug/l - Chloroethane ug/l - 0 Chloroform ug/l - Chloromethane 0.0. ug/l - cis-,-ichloroethene 0.0. ug/l - cis-,-ichloropropene 0.0. ug/l - Bromodichloromethane 0.0. ug/l - Ethylbenzene 0.0. ug/l - m-xylene & p-xylene 0.0. ug/l - Methyl tert-butyl ether ug/l - Methylene Chloride 0.0. ug/l - o-xylene 0.0. ug/l - Tetrachloroethene 0.0. ug/l - Toluene 0.0. ug/l - trans-,-ichloroethene 0.0. ug/l - trans-,-ichloropropene 0.0. ug/l - Trichloroethene 0.0. ug/l - Trichlorofluoromethane 0.0. ug/l - Vinyl chloride 0.0. ug/l - -Chloroethyl vinyl ether 0.0. ug/l - 0 Surrogate LCS %Recovery LCS -Bromofluorobenzene - ibromofluoromethane 0 - Toluene-d (Surr) 0 - Page of //0

173 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Acenaphthene <0. 0. ug/l 0// 0: 0// :0 Acenaphthylene Anthracene Benzidine Benzo[a]anthracene Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[g,h,i]perylene Benzo[a]pyrene -Bromophenyl phenyl ether Butyl benzyl phthalate Bis(-chloroethoxy)methane Bis(-chloroethyl)ether -Chloro--methylphenol -Chloronaphthalene -Chlorophenol -Chlorophenyl phenyl ether Chrysene ibenz(a,h)anthracene i-n-butyl phthalate,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene,'-ichlorobenzidine,-ichlorophenol iethyl phthalate,-imethylphenol imethyl phthalate,-initro--methylphenol,-initrophenol,-initrotoluene,-initrotoluene i-n-octyl phthalate Bis(-ethylhexyl) phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[,,-cd]pyrene Isophorone Naphthalene Nitrobenzene -Nitrophenol -Nitrophenol N-Nitrosodimethylamine N-Nitrosodiphenylamine ML <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0 0 0 ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 < ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 < ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <.0.0 ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <.0.0 ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.0.0 ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 Page of //0

174 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB N-Nitrosodi-n-propylamine <.. ug/l 0// 0: 0// :0 Pentachlorophenol Phenanthrene Phenol Pyrene,,-Trichlorobenzene,,-Trichlorophenol Surrogate ML <. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <0. 0. ug/l 0// 0: 0// :0 <.. ug/l 0// 0: 0// :0 MB %Recovery MB,,-Tribromophenol - 0// 0: 0// :0 -Fluorobiphenyl - 0// 0: 0// :0 -Fluorophenol - 0// 0: 0// :0 Nitrobenzene-d 0-0// 0: 0// :0 Phenol-d - 0// 0: 0// :0 Terphenyl-d - 0// 0: 0// :0 Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Acenaphthene 0.0. ug/l - Acenaphthylene ug/l 0 - Anthracene 0.0. ug/l - Benzo[a]anthracene 0.0. ug/l - Benzo[b]fluoranthene 0.0. ug/l - Benzo[k]fluoranthene ug/l - Benzo[g,h,i]perylene 0.0. ug/l 0 - Benzo[a]pyrene 0.0. ug/l - -Bromophenyl phenyl ether 0.0. ug/l - Butyl benzyl phthalate 0.0. ug/l 0 - Bis(-chloroethoxy)methane 0.0. ug/l - Bis(-chloroethyl)ether 0.0. ug/l - -Chloro--methylphenol 0.0. ug/l - -Chloronaphthalene ug/l Chlorophenol 0.0. ug/l - -Chlorophenyl phenyl ether 0.0. ug/l - Chrysene 0.0. ug/l - ibenz(a,h)anthracene 0.0. ug/l - i-n-butyl phthalate 0.0. ug/l -,-ichlorobenzene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l -,-ichlorobenzene 0.0. ug/l 0 -,'-ichlorobenzidine ug/l -,-ichlorophenol ug/l - iethyl phthalate 0.0. ug/l -,-imethylphenol ug/l - imethyl phthalate 0.0. ug/l - Page of //0

175 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec,-initro--methylphenol 0. ug/l -,-initrophenol 0. ug/l 0 -,-initrotoluene 0.0. ug/l -,-initrotoluene ug/l 0 - i-n-octyl phthalate 0.0. ug/l - Bis(-ethylhexyl) phthalate 0.0. ug/l - Fluoranthene 0.0. ug/l - Fluorene 0.0. ug/l - Hexachlorobenzene 0.0. ug/l - Hexachlorobutadiene 0.0. ug/l - Hexachlorocyclopentadiene 0.0. ug/l - Hexachloroethane 0.0. ug/l 0 - Indeno[,,-cd]pyrene 0.0. ug/l - Isophorone ug/l - Naphthalene 0.0. ug/l - Nitrobenzene 0.0. ug/l - 0 -Nitrophenol 0.0. ug/l - -Nitrophenol 0. ug/l - N-Nitrosodimethylamine 0.0. ug/l - N-Nitrosodiphenylamine.. ug/l 0 - N-Nitrosodi-n-propylamine 0.0. ug/l - 0 Pentachlorophenol 0. ug/l - Phenanthrene 0.0. ug/l - Phenol 0.0. ug/l - Pyrene 0.0. ug/l -,,-Trichlorobenzene 0.0. ug/l -,,-Trichlorophenol 0.0. ug/l - Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol 0 - Nitrobenzene-d - Phenol-d - Terphenyl-d 0 - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Acenaphthene 0.0. ug/l - 0 Acenaphthylene ug/l - 0 Anthracene 0.0. ug/l - 0 Benzo[a]anthracene 0.0. ug/l - 0 Benzo[b]fluoranthene 0.0. ug/l - 0 Benzo[k]fluoranthene 0.0. ug/l - 0 Benzo[g,h,i]perylene 0.0. ug/l - 0 RP Limit Page of //0

176 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Benzo[a]pyrene 0.0. ug/l - 0 -Bromophenyl phenyl ether 0.0. ug/l Butyl benzyl phthalate 0.0. ug/l - 0 Bis(-chloroethoxy)methane 0.0. ug/l - 0 Bis(-chloroethyl)ether 0.0. ug/l - 0 -Chloro--methylphenol ug/l - 0 -Chloronaphthalene 0.0. ug/l 0-0 -Chlorophenol 0.0. ug/l - 0 -Chlorophenyl phenyl ether 0.0. ug/l Chrysene 0.0. ug/l - 0 ibenz(a,h)anthracene 0.0. ug/l - 0 i-n-butyl phthalate ug/l - 0,-ichlorobenzene 0.0. ug/l - 0,-ichlorobenzene 0.0. ug/l - 0,-ichlorobenzene ug/l 0-0,'-ichlorobenzidine ug/l - 0,-ichlorophenol 0.0. ug/l - 0 iethyl phthalate 0.0. ug/l - 0,-imethylphenol 0.0. ug/l - 0 imethyl phthalate ug/l 0-0,-initro--methylphenol 0. ug/l - 0,-initrophenol 0. ug/l 0-0,-initrotoluene 0.0. ug/l - 0,-initrotoluene ug/l i-n-octyl phthalate 0.0. ug/l - 0 Bis(-ethylhexyl) phthalate 0.0. ug/l - 0 Fluoranthene ug/l - 0 Fluorene ug/l - 0 Hexachlorobenzene 0.0. ug/l - 0 Hexachlorobutadiene 0.0. ug/l - 0 Hexachlorocyclopentadiene 0.0. ug/l - 0 Hexachloroethane 0.0. ug/l 0-0 Indeno[,,-cd]pyrene 0.0. ug/l - 0 Isophorone 0.0. ug/l - 0 Naphthalene 0.0. ug/l Nitrobenzene 0.0. ug/l Nitrophenol 0.0. ug/l - 0 -Nitrophenol 0. ug/l - 0 N-Nitrosodimethylamine 0.0. ug/l - 0 N-Nitrosodiphenylamine..0 ug/l N-Nitrosodi-n-propylamine ug/l Pentachlorophenol 0. ug/l - 0 Phenanthrene 0.0. ug/l - 0 Phenol 0.0. ug/l - 0 Pyrene 0.0. ug/l - 0,,-Trichlorobenzene 0.0. ug/l - 0,,-Trichlorophenol ug/l - 0 RP Limit Page of //0

177 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - Nitrobenzene-d - Phenol-d - Terphenyl-d - Method: 0 - Organochlorine Pesticides/PCBs in Water Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB PCB- < ug/l 0// 0: 0// : PCB- PCB- PCB- PCB- PCB- PCB- ML < ug/l 0// 0: 0// : < ug/l 0// 0: 0// : < ug/l 0// 0: 0// : < ug/l 0// 0: 0// : < ug/l 0// 0: 0// : < ug/l 0// 0: 0// : Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Aldrin < ug/l 0// 0: 0/0/ : alpha-bhc beta-bhc delta-bhc gamma-bhc (Lindane) Chlordane (technical),'-,'-e,'-t ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Toxaphene ML < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : < ug/l 0// 0: 0/0/ : Page of //0

178 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: 0 - Organochlorine Pesticides/PCBs in Water (Continued) TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : Surrogate MB %Recovery MB CB ecachlorobiphenyl - 0// 0: 0/0/ : Tetrachloro-m-xylene - 0// 0: 0/0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Aldrin ug/l - alpha-bhc ug/l - beta-bhc ug/l - delta-bhc ug/l - gamma-bhc (Lindane) ug/l -,' ug/l -,'-E ug/l 0 -,'-T ug/l - ieldrin ug/l - Endosulfan I ug/l 0 - Endosulfan II ug/l - 0 Endosulfan sulfate ug/l 0 - Endrin ug/l 0 - Endrin aldehyde ug/l 0 - Heptachlor ug/l - Heptachlor epoxide ug/l - Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec PCB ug/l PCB-.00. ug/l - Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec Aldrin ug/l - 0 RP Limit Page of //0

179 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment QC Sample s Method: 0 - Organochlorine Pesticides/PCBs in Water (Continued) TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec alpha-bhc ug/l - 0 beta-bhc ug/l - 0 delta-bhc ug/l - 0 gamma-bhc (Lindane) ug/l - 0,' ug/l - 0,'-E ug/l 0-0,'-T ug/l - 0 ieldrin ug/l - 0 Endosulfan I ug/l - 0 Endosulfan II ug/l Endosulfan sulfate ug/l - 0 Endrin ug/l 0-0 Endrin aldehyde ug/l 0-0 Heptachlor ug/l 0-0 Heptachlor epoxide ug/l - 0 RP Limit Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec PCB-.00. ug/l 0-0 PCB-.00. ug/l Surrogate LCS %Recovery LCS CB ecachlorobiphenyl - Tetrachloro-m-xylene - RP Limit Method: 0B - Metals (ICP) Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Arsenic < mg/kg 0// : 0// 0: Barium Cadmium Chromium Lead Selenium Silver ML < mg/kg 0// : 0// 0: < mg/kg 0// : 0// 0: < mg/kg 0// : 0// 0: < mg/kg 0// : 0// 0: < mg/kg 0// : 0// 0: < mg/kg 0// : 0// 0: Page 0 of //0

180 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: 0B - Metals (ICP) (Continued) QC Sample s TestAmerica Job I: Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Arsenic mg/kg - Barium 0 mg/kg 0 - Cadmium.0. mg/kg - Chromium mg/kg - Lead mg/kg - Selenium.. mg/kg - Silver. 0. mg/kg - Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : Prep : MB MB Antimony < mg/l 0// 0: 0// :0 Arsenic Barium Beryllium Cadmium Chromium Copper Lead Nickel Selenium Silver Thallium Zinc ML < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 < mg/l 0// 0: 0// :0 Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : Prep : LCS LCS %Rec Antimony.00.0 mg/l 0 - Arsenic.00.0 mg/l 0 - Barium.00.0 mg/l 0 - Beryllium mg/l 0 - Cadmium mg/l 0 - Chromium.00.0 mg/l 0 - Copper.00.0 mg/l 0 - Lead.00.0 mg/l 0 - Nickel.00.0 mg/l 0 - Selenium.00.0 mg/l 0 - Silver mg/l 0 - Thallium.00.0 mg/l 0 - Zinc.00.0 mg/l 0 - Page of //0

181 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: 0A - Mercury (CVAA) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Mercury < mg/l /0/ 0: /0/ : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Mercury mg/l 0 - Method: B - Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Hg < mg/kg 0/0/ 0: /0/ :0 Lab Sample I: LCS 00-/-A ^ Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Hg.. mg/kg 0 - Method:. - Solids, Total Volatile (TVS) Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB Total Volatile Solids % 0// :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Total Volatile Solids 0.0 <0. % - Page of //0

182 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Cyanide, Total QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Cyanide, Total < mg/l 0// 0: 0// : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Cyanide, Total mg/l - Method: 0. - Nitrogen, Ammonia Lab Sample I: MB 00-0/ Client Sample I: Method Blank Prep Type: Analysis : 0 MB MB ML Ammonia < mg/l 0// : Lab Sample I: LCS 00-0/ Client Sample I: Lab Control Sample Prep Type: Analysis : 0 LCS LCS %Rec Ammonia.00.0 mg/l 0 - Lab Sample I: M 00-0/ M Client Sample I: Lab Control Sample Prep Type: Analysis : 0 M M %Rec Ammonia mg/l 0 - Method:. - Nitrogen, Total Kjeldahl Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Nitrogen, Kjeldahl < mg/l 0/0/ : /0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/l 0 - Page of //0

183 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Nitrogen, Total Kjeldahl (Continued) QC Sample s TestAmerica Job I: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Nitrogen, Kjeldahl < mg/kg 0/0/ : /0/ : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Nitrogen, Kjeldahl.0. mg/kg - Lab Sample I: MS Client Sample I: S Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Nitrogen, Kjeldahl 0 F mg/kg 0 - Lab Sample I: MS Client Sample I: S Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec Nitrogen, Kjeldahl 0 0 F mg/kg 0-0 Lab Sample I: M 00-/ M Analysis : RP Limit Client Sample I: Lab Control Sample Prep Type: Nitrogen, Kjeldahl mg/l 0 - M M %Rec Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Nitrate Nitrite as N < mg/l 0// 0: Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Nitrate Nitrite as N mg/l 0 - Page of //0

184 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Nitrogen, Nitrate-Nitrite (Continued) Lab Sample I: M 00-/ M Analysis : QC Sample s TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N J mg/l 0 - Lab Sample I: M 00-/ M Analysis : M M %Rec Nitrate Nitrite as N J mg/kg Lab Sample I: MB 00-/-A Analysis : MB MB M M %Rec ML Client Sample I: Lab Control Sample Prep Type: Client Sample I: Method Blank Prep Type: Soluble Nitrate Nitrite as N < mg/kg 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Soluble Analysis : LCS LCS %Rec Nitrate Nitrite as N mg/kg 0 - Method:. - Phosphorus, Ortho Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML ortho-phosphate < mg/l 0// : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec ortho-phosphate mg/l 0 - Lab Sample I: 00-0-B- MS Client Sample I: 00-0-B- MS Prep Type: Analysis : Sample Sample MS MS %Rec ortho-phosphate mg/l 0 - Page of //0

185 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Phosphorus, Ortho (Continued) Lab Sample I: 00-0-B- MS Analysis : Sample Sample QC Sample s TestAmerica Job I: Client Sample I: 00-0-B- MS Prep Type: ortho-phosphate mg/l 0 - Method:. - Phosphorus, Total MS MS %Rec Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Phosphorus < mg/l /0/ : /0/ : ML RP RP Limit Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus mg/l 0 - Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis : Prep : LCS LCS RP %Rec RP Limit Phosphorus mg/l 0-0 Method:. - Phosphorus, Total Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB Phosphorus, Total < mg/kg 0/0/ : /0/ : ML Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phosphorus, Total.0. mg/kg - Lab Sample I: MS Client Sample I: S Prep Type: Analysis : Prep : Sample Sample MS MS %Rec Phosphorus, Total.. F mg/kg - Page of //0

186 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method:. - Phosphorus, Total (Continued) QC Sample s TestAmerica Job I: Lab Sample I: 00-0-A--H MS Client Sample I: 00-0-A--H MS Prep Type: Analysis : Prep : Sample Sample MS MS RP %Rec Phosphorus, Total.. F mg/kg - 0 Lab Sample I: M 00-/ M Analysis : Phosphorus, Total 0.0 <0. mg/kg Method: 0. - Phenolics, Total Recoverable M M %Rec RP Limit Client Sample I: Lab Control Sample Prep Type: Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis : Prep : MB MB ML Phenols, Total < mg/l 0// :0 /0/ : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis : Prep : LCS LCS %Rec Phenols, Total mg/l - Method: SM B - BO, -ay Lab Sample I: USB 00-/ USB Client Sample I: Method Blank Prep Type: Analysis : USB USB ML Biochemical Oxygen emand < mg/l 0// : Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Biochemical Oxygen emand mg/l - Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample up Prep Type: Analysis : LCS LCS RP %Rec RP Limit Biochemical Oxygen emand mg/l - Page of //0

187 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method: SM 0 - CO Lab Sample I: MB 0-/ Analysis : MB MB QC Sample s ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.0.0 mg/l /0/ : Lab Sample I: MB 0-/ Analysis : MB MB ML Client Sample I: Method Blank Prep Type: Chemical Oxygen emand <.0.0 mg/l /0/ : Lab Sample I: LCS 0-/ Analysis : Client Sample I: Lab Control Sample Prep Type: Chemical Oxygen emand 00 0 mg/l 0 - LCS LCS %Rec Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand mg/l Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample up Prep Type: Analysis : LCS LCS RP %Rec RP Limit Chemical Oxygen emand 00 0 mg/l 0-0 Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample up Prep Type: Analysis : LCS LCS RP %Rec RP Limit Chemical Oxygen emand mg/l 0-0 Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Analysis : MB MB ML Chemical Oxygen emand <.. mg/l /0/ :0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Analysis : LCS LCS %Rec Chemical Oxygen emand 0.0. mg/l 0 - Page of //0

188 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Lab Sample I: MS Analysis : Sample Sample QC Sample s TestAmerica Job I: Chemical Oxygen emand.. F mg/l 0 - Lab Sample I: MS Analysis : Sample Sample MS MS %Rec Client Sample I: HSI-00-0 Prep Type: Client Sample I: HSI-00-0 Prep Type: Chemical Oxygen emand.. F mg/l 0 - Lab Sample I: LB 0-/-A LB Analysis : LB LB MS MS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: ASTM Leach Chemical Oxygen emand <.0.0 mg/l /0/ : Lab Sample I: U Analysis : Sample Sample Client Sample I: S Prep Type: ASTM Leach Chemical Oxygen emand <. <. mg/l NC 0 U U RP RP Limit Page of //0

189 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: S Lab Sample I: ate Collected: 0/0/ :0 ate Received: 0// 0:0 Percent Solids:.0 Prep Type Soluble Soluble Type Method Run ilution Factor Number or Analyst Prep 00B 0// :0 KWN TAL PEN Analysis 0B 0// 0: SLM TAL PEN Prep B /0/ : JAP TAL PEN Analysis B /0/ : JAP TAL PEN Analysis. 0// :0 SLT TAL PEN Leach I Leach 0// : KJR TAL PEN Analysis. 0// : KJR TAL PEN Analysis Moisture 0// :00 LEC TAL PEN Prep. 0/0/ : JAT TAL PEN Analysis. /0/ : JAT TAL PEN Lab ASTM Leach ASTM Leach Prep././ 0/0/ : JAT TAL PEN Analysis. /0/ : JAT TAL PEN Analysis Total Nitrogen /0/ : JMH TAL PEN Leach - 0// :0 SJM TAL NSH Analysis SM 0 /0/ : MSJ TAL NSH Client Sample I: G Lab Sample I: ate Collected: 0/0/ : ate Received: 0// 0:0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Prep 00A 0// 0: KWN TAL PEN Analysis 0B 0// : SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Analysis. 0// : LSS TAL PEN Analysis SM B GMF TAL PEN (Start) (End) 0// :0 0// : Prep. 0/0/ : JAT TAL PEN Analysis. /0/ : JAT TAL PEN Prep././ /0/ : AJN TAL TAL Analysis. /0/ :00 AJN TAL TAL Lab Client Sample I: HSI-00-0 Lab Sample I: ate Collected: 0/0/ : ate Received: 0// 0:0 Prep Type Type Method Run ilution Factor Number or Analyst Analysis /0/ 00: WP TAL PEN Prep 0// : KH TAL PEN Analysis 0// 0:0 AJR TAL PEN Prep 0 0// : KH TAL PEN Lab Page 0 of //0

190 Lab Chronicle Client: ewberry TestAmerica Job I: Project/Site: Three Mile CreekUSA-Groundwater/Sediment Client Sample I: HSI-00-0 Lab Sample I: ate Collected: 0/0/ : ate Received: 0// 0:0 Prep Type Total Recoverable Total Recoverable Type Method Run ilution Factor Number or Analyst Analysis 0 0// : VC TAL PEN Prep 0 0// : KH TAL PEN Analysis 0 0// : VC TAL PEN Prep 00A 0// 0: KWN TAL PEN Analysis 0B 0// :0 SLM TAL PEN Prep 0A /0/ 0: JAP TAL PEN Analysis 0A /0/ : JAP TAL PEN Analysis. 0// : LSS TAL PEN Analysis // :0 KJR TAL PEN Prep istill/cn 0// 0: BAB TAL PEN Analysis. 0// : BAB TAL PEN Analysis. 0// 0: KJR TAL PEN Analysis SM B GMF TAL PEN (Start) (End) 0// : 0// : Prep. 0/0/ : JAT TAL PEN Analysis. /0/ : JAT TAL PEN Analysis SM 0 /0/ :0 CLS TAL PEN Prep istill/phenol 0// :0 CLS TAL PEN Analysis 0. /0/ : JMH TAL PEN Prep././ /0/ : AJN TAL TAL Analysis. /0/ : AJN TAL TAL Lab Laboratory References: TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

191 Client: ewberry Project/Site: Three Mile CreekUSA-Groundwater/Sediment Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory Volatile Organic Compounds (GC/MS) 0CFRA TAL PEN Semivolatile Organic Compounds (GC/MS) 0CFRA TAL PEN 0 Organochlorine Pesticides/PCBs in Water 0CFRA TAL PEN 0B Metals (ICP) SW TAL PEN 0A Mercury (CVAA) SW TAL PEN B Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) SW TAL PEN. Solids, Total Volatile (TVS) MCAWW TAL PEN. Cyanide, Total MCAWW TAL PEN 0. Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Total Kjeldahl MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN. Phosphorus, Ortho EPA TAL PEN. Phosphorus, Total EPA TAL TAL. Phosphorus, Total EPA TAL PEN 0. Phenolics, Total Recoverable MCAWW TAL PEN Moisture Percent Moisture EPA TAL PEN SM B BO, -ay SM TAL PEN SM 0 CO SM TAL NSH SM 0 CO SM TAL PEN Total Nitrogen Nitrogen, Total EPA TAL PEN Protocol References: 0CFRA = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 0CFR, Part, Appendix A, October, and subsequent revisions. EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 0 Foster Creighton rive, Nashville, TN 0, TEL ()-0 TAL PEN =, McLemore rive, Pensacola, FL, TEL (0)-0 TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- Page of //0

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