ANALYTICAL REPORT. Job Number: Job Description: TO4-2012, RACER, GM Wilmington
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1 ANALYTICAL REPORT Job Number: Job Description: TO4-2012, RACER, GM Wilmington For: Conestoga-Rovers & Associates, Inc Niagara Falls Blvd., Suite 3 Niagara Falls, NY Attention: Ms. Sue Scrocchi Designee for Jamie Capaci Project Manager I jamie.capaci@testamericainc.com Approved for release. Janet Mosley Project Mgmt. Assistant 4:17 PM cc: Chris Barton The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. All questions regarding this report should be directed to the TestAmerica Edison Project Manager. TestAmerica Edison Certifications and Approvals: Connecticut: CTDOH #PH-0200, New Jersey: NJDEP (NELAP) #12028, New York: NYDOH (NELAP) #11452, NYDOH (ELAP) #11452, Pennsylvania: PADEP (NELAP) and Rhode Island: RIDOH LAO00132 TestAmerica Laboratories, Inc. TestAmerica Edison 777 New Durham Road, Edison, NJ Tel (732) Fax (732) Page 1 of 267
2 Table of Contents Cover Title Page Data Summaries Report Narrative Sample Summary Executive Summary Method Summary Method / Analyst Summary Sample Datasheets QC Data Summary Data Qualifiers QC Association Summary Lab Chronicle Inorganic Sample Data Metals Data Met Cover Page Met Sample Data Met QC Data Met ICV/CCV Met Blanks Met ICSA/ICSAB Met MS/MSD/PDS Met Dup/Trip Met LCS/LCSD Met Serial Dilution Met MDL Met Preparation Log Page 2 of 267
3 Table of Contents Met Analysis Run Log Met Raw Data Met Prep Data General Chemistry Data Gen Chem Cover Page Gen Chem MDL Gen Chem Analysis Run Log Gen Chem Prep Data Shipping and Receiving Documents Client Chain of Custody Sample Receipt Checklist Page 3 of 267
4 CASE NARRATIVE Client: Conestoga-Rovers & Associates, Inc. Project: TO4-2012, GM Wilmington Report Number: This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a statement that documents that there are no relevant data issues. It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting limits in some cases. Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables quantification of target analytes or interferences which exceed the calibration range of the instrument. Calculations are performed before rounding to avoid round-off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. RECEIPT The samples were received on 08/23/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 2.7 C. Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required temperature or method specified range. For samples with a specified temperature of 4C, samples with a temperature ranging from just above freezing temperature of water to 6C shall be acceptable. Samples that are hand delivered immediately following collection may not meet these criteria, however they will be deemed acceptable according to NELAC standards, if there is evidence that the chilling process has begun, such as arrival on ice, etc. TOTAL METALS Samples , and were analyzed for total metals in accordance with EPA SW-846 Method 6010B. The samples were prepared on 11/08/2012 and analyzed on 11/10/2012. Samples (4X), and (4X) required dilution prior to analysis. The reporting limits have been adjusted accordingly. As a standard practice all soil samples and related QC samples (i.e., MB, LCS, Dup, MS, SD) are diluted 2X-4X prior to analysis. Further dilutions may be required dependent upon analyte levels in the samples. Refer to the analytical results forms for dilutions. No difficulties were encountered during the metals analyses. All quality control parameters were within the acceptance limits. PERCENT SOLIDS/PERCENT MOISTURE Samples through were analyzed for percent solids/percent moisture in accordance with EPA Method CLPISM01.2 (Exhibit D). The samples were analyzed on 08/26/2012. No difficulties were encountered during the %solids/moisture analyses. All quality control parameters were within the acceptance limits. Page 4 of 267
5 SAMPLE SUMMARY Client: Conestoga-Rovers & Associates, Inc. Job Number: Date/Time Date/Time Lab Sample ID Client Sample ID Client Matrix Sampled Received SO mm-209 Solid 08/23/ /23/ SO mm-210 Solid 08/23/ /23/ SO mm-211 Solid 08/23/ /23/ SO mm-212 Solid 08/23/ /23/ SO mm-213 Solid 08/23/ /23/ SO mm-214 Solid 08/23/ /23/ SO mm-215 Solid 08/23/ /23/ SO mm-216 Solid 08/23/ /23/ SO mm-217 Solid 08/23/ /23/ SO mm-218 Solid 08/23/ /23/ SO mm-219 Solid 08/23/ /23/ TestAmerica Edison Page 5 of 267
6 EXECUTIVE SUMMARY - Detections Client: Conestoga-Rovers & Associates, Inc. Job Number: Lab Sample ID Client Sample ID Analyte Result Qualifier Reporting Limit Method SO MM-209 Percent Moisture 20.2 Percent Solids % Moisture 1.0 % Moisture SO MM-210 Percent Moisture 14.6 Percent Solids % Moisture 1.0 % Moisture SO MM-211 Percent Moisture 18.3 Percent Solids % Moisture 1.0 % Moisture SO MM-212 Percent Moisture 7.1 Percent Solids % Moisture 1.0 % Moisture SO MM-213 Percent Moisture 11.7 Percent Solids % Moisture 1.0 % Moisture SO MM-214 Percent Moisture 8.4 Percent Solids % Moisture 1.0 % Moisture SO MM-215 Percent Moisture 10.3 Percent Solids % Moisture 1.0 % Moisture SO MM-216 Percent Moisture 11.0 Percent Solids % Moisture 1.0 % Moisture SO MM-217 Arsenic 3.9 Percent Moisture 8.4 Percent Solids mg/kg 6010B 1.0 % Moisture 1.0 % Moisture TestAmerica Edison Page 6 of 267
7 EXECUTIVE SUMMARY - Detections Client: Conestoga-Rovers & Associates, Inc. Job Number: Lab Sample ID Client Sample ID Analyte Result Qualifier Reporting Limit Method SO MM-218 Arsenic 3.5 Percent Moisture 7.9 Percent Solids mg/kg 6010B 1.0 % Moisture 1.0 % Moisture SO MM-219 Percent Moisture 9.3 Percent Solids % Moisture 1.0 % Moisture TestAmerica Edison Page 7 of 267
8 METHOD SUMMARY Client: Conestoga-Rovers & Associates, Inc. Job Number: Description Lab Location Method Preparation Method Matrix: Solid Metals (ICP) TAL EDI SW B Preparation, Metals TAL EDI SW B Percent Moisture TAL EDI EPA Moisture Lab References: TAL EDI = TestAmerica Edison Method References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Edison Page 8 of 267
9 METHOD / ANALYST SUMMARY Client: Conestoga-Rovers & Associates, Inc. Job Number: Method Analyst Analyst ID SW B EPA Moisture Chang, Churn Der Dave, Virendra CDC VD TestAmerica Edison Page 9 of 267
10 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: Client Sample ID: SO mm-210 Lab Sample ID: Client Matrix: Solid % Moisture: 14.6 Date Sampled: 08/23/ Date Received: 08/23/ B Metals (ICP) Analysis Method: 6010B Analysis Batch: Instrument ID: ICP5 Prep Method: 3050B Prep Batch: Lab File ID: asc Dilution: 4.0 Initial Weight/Volume: 1.01 g Analysis Date: 11/10/ Final Weight/Volume: 50 ml Prep Date: 11/08/ Analyte DryWt Corrected: Y Result (mg/kg) Qualifier MDL RL Arsenic 1.1 U TestAmerica Edison Page 10 of 267
11 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: Client Sample ID: SO mm-217 Lab Sample ID: Client Matrix: Solid % Moisture: 8.4 Date Sampled: 08/23/ Date Received: 08/23/ B Metals (ICP) Analysis Method: 6010B Analysis Batch: Instrument ID: ICP5 Prep Method: 3050B Prep Batch: Lab File ID: asc Dilution: 4.0 Initial Weight/Volume: 1.04 g Analysis Date: 11/10/ Final Weight/Volume: 50 ml Prep Date: 11/08/ Analyte DryWt Corrected: Y Result (mg/kg) Qualifier MDL RL Arsenic TestAmerica Edison Page 11 of 267
12 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: Client Sample ID: SO mm-218 Lab Sample ID: Client Matrix: Solid % Moisture: 7.9 Date Sampled: 08/23/ Date Received: 08/23/ B Metals (ICP) Analysis Method: 6010B Analysis Batch: Instrument ID: ICP5 Prep Method: 3050B Prep Batch: Lab File ID: asc Dilution: 4.0 Initial Weight/Volume: 1.05 g Analysis Date: 11/10/ Final Weight/Volume: 50 ml Prep Date: 11/08/ Analyte DryWt Corrected: Y Result (mg/kg) Qualifier MDL RL Arsenic TestAmerica Edison Page 12 of 267
13 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 20.2 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 79.8 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 13 of 267
14 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 14.6 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 85.4 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 14 of 267
15 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 18.3 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 81.7 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 15 of 267
16 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 7.1 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 92.9 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 16 of 267
17 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 11.7 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 88.3 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 17 of 267
18 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 8.4 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 91.6 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 18 of 267
19 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 10.3 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 89.7 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 19 of 267
20 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 11.0 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 89.0 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 20 of 267
21 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 8.4 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 91.6 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 21 of 267
22 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 7.9 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 92.1 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 22 of 267
23 Analytical Data Client: Conestoga-Rovers & Associates, Inc. Job Number: General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: SO mm Solid Date Sampled: 08/23/ Date Received: 08/23/ Analyte Result Qual RL RL Dil Method Percent Moisture 9.3 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N Percent Solids 90.7 % Moisture Analysis Batch: Analysis Date: 08/26/ DryWt Corrected: N TestAmerica Edison Page 23 of 267
24 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Method Blank - Batch: Method: 6010B Preparation: 3050B Lab Sample ID: MB /1-A ^2 Client Matrix: Solid Dilution: 2.0 Analysis Date: 11/10/ Prep Date: 11/08/ Leach Date: N/A Analysis Batch: Prep Batch: Leach Batch: : N/A mg/kg Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ICP asc 1.00 g 50 ml Analyte Result Qual MDL RL Arsenic LCS-Certified Reference Material - Batch: U Method: 6010B Preparation: 3050B Lab Sample ID: LCSSRM Client Matrix: Dilution: Solid 4.0 Analysis Date: 11/10/ Prep Date: 11/08/ Leach Date: N/A Analysis Batch: Prep Batch: Leach Batch: : N/A mg/kg Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ICP asc 1.04 g 50 ml Analyte Arsenic Spike Amount Result % Rec. Limit Qual TestAmerica Edison Page 24 of 267
25 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Matrix Spike - Batch: Method: 6010B Preparation: 3050B Lab Sample ID: A-13-F MS ^4 Client Matrix: Dilution: Solid 4.0 Analysis Date: 11/10/ Prep Date: 11/08/ Leach Date: N/A Analysis Batch: Prep Batch: Leach Batch: N/A : mg/kg Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ICP asc 1.05 g 50 ml Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual Arsenic 1.1 U Post Digestion Spike - Batch: Method: 6010B Preparation: 3050B Lab Sample ID: A-13-D PDS Client Matrix: Dilution: Solid 4.0 Analysis Date: 11/10/ Prep Date: 11/08/ Leach Date: N/A Analysis Batch: Prep Batch: Leach Batch: N/A : mg/kg Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ICP asc 1.01 g 50 ml Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual Arsenic 1.1 U TestAmerica Edison Page 25 of 267
26 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Duplicate - Batch: Method: 6010B Preparation: 3050B Lab Sample ID: A-13-E DU ^4 Client Matrix: Solid Dilution: 4.0 Analysis Date: 11/10/ Prep Date: 11/08/ Leach Date: N/A Analysis Batch: Prep Batch: Leach Batch: : N/A mg/kg Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ICP asc 1.05 g 50 ml Analyte Sample Result/Qual Result RPD Limit Qual Arsenic Serial Dilution - Batch: U 1.1 NC 20 U Method: 6010B Preparation: 3050B Lab Sample ID: A-13-D SD Client Matrix: Solid Dilution: 20 Analysis Date: 11/10/ Prep Date: 11/08/ Leach Date: N/A Analysis Batch: Prep Batch: Leach Batch: : N/A mg/kg Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ICP asc 1.01 g 50 ml Analyte Sample Result/Qual Result %Diff Limit Qual Arsenic 1.1 U 5.6 NC 10 U TestAmerica Edison Page 26 of 267
27 DATA REPORTING QUALIFIERS Client: Conestoga-Rovers & Associates, Inc. Job Number: Lab Section Qualifier Description Metals U J Indicates the analyte was analyzed for but not detected. Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. TestAmerica Edison Page 27 of 267
28 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: QC Association Summary Lab Sample ID Client Sample ID Report Basis Client Matrix Method Prep Batch Metals Prep Batch: LCSSRM /2-A ^4 LCS-Certified Reference Material T Solid 3050B MB /1-A ^2 Method Blank T Solid 3050B SO mm-210 T Solid 3050B SO mm-217 T Solid 3050B SO mm-218 T Solid 3050B A-13-E DU ^4 Duplicate T Solid 3050B A-13-F MS ^4 Matrix Spike T Solid 3050B Analysis Batch: LCSSRM /2-A ^4 LCS-Certified Reference Material T Solid 6010B MB /1-A ^2 Method Blank T Solid 6010B SO mm-210 T Solid 6010B SO mm-217 T Solid 6010B SO mm-218 T Solid 6010B A-13-E DU ^4 Duplicate T Solid 6010B A-13-F MS ^4 Matrix Spike T Solid 6010B Report Basis T = Total General Chemistry Analysis Batch: A-1 MS Matrix Spike T Solid Moisture A-1 MSD Matrix Spike Duplicate T Solid Moisture SO mm-209 T Solid Moisture SO mm-210 T Solid Moisture SO mm-211 T Solid Moisture SO mm-212 T Solid Moisture SO mm-213 T Solid Moisture SO mm-214 T Solid Moisture SO mm-215 T Solid Moisture SO mm-216 T Solid Moisture SO mm-217 T Solid Moisture SO mm-218 T Solid Moisture SO mm-219 T Solid Moisture Report Basis T = Total TestAmerica Edison Page 28 of 267
29 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Laboratory Chronicle Lab ID: Client ID: SO mm-209 Sample Date/Time: 08/23/ :30 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-210 Sample Date/Time: 08/23/ :50 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst P:3050B A-2-A ^ /08/ :41 4 TAL EDI MC A:6010B A-2-A ^ /10/ :32 4 TAL EDI CDC A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-211 Sample Date/Time: 08/23/ :05 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-212 Sample Date/Time: 08/23/ :30 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-213 Sample Date/Time: 08/23/ :20 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-214 Sample Date/Time: 08/23/ :05 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD TestAmerica Edison A = Analytical Method P = Prep Method Page 29 of 267
30 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Laboratory Chronicle Lab ID: Client ID: SO mm-215 Sample Date/Time: 08/23/ :15 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-216 Sample Date/Time: 08/23/ :30 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-217 Sample Date/Time: 08/23/ :00 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst P:3050B A-9-A ^ /08/ :41 4 TAL EDI MC A:6010B A-9-A ^ /10/ :36 4 TAL EDI CDC A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-218 Sample Date/Time: 08/23/ :00 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst P:3050B A-10-A ^ /08/ :41 4 TAL EDI MC A:6010B A-10-A ^ /10/ :40 4 TAL EDI CDC A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: Client ID: SO mm-219 Sample Date/Time: 08/23/ :40 Received Date/Time: 08/23/ :30 Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A /26/ :17 1 TAL EDI VD Lab ID: MB Client ID: N/A Sample Date/Time: N/A Received Date/Time: N/A Method Bottle ID Run P:3050B A:6010B MB /1-A ^2 MB /1-A ^2 Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst /08/ :15 2 TAL EDI MC /10/ :58 2 TAL EDI CDC TestAmerica Edison A = Analytical Method P = Prep Method Page 30 of 267
31 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Laboratory Chronicle Lab ID: LCSSRM Client ID: N/A Sample Date/Time: N/A Received Date/Time: N/A Method Bottle ID Run P:3050B A:6010B LCSSRM /2-A ^4 LCSSRM /2-A ^4 Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst /08/ :15 4 TAL EDI MC /10/ :47 4 TAL EDI CDC Lab ID: MS Client ID: N/A Method Bottle ID Run Sample Date/Time: N/A Received Date/Time: N/A Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst P:3050B A-13-F MS /08/ :15 4 TAL EDI MC ^4 A:6010B A-13-F MS /10/ :12 4 TAL EDI CDC ^4 A:Moisture A-1 MS /26/ :17 1 TAL EDI VD Lab ID: MSD Client ID: N/A Method Bottle ID Run Sample Date/Time: N/A Received Date/Time: N/A Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst A:Moisture A-1 MSD /26/ :17 1 TAL EDI VD Lab ID: DU Client ID: N/A Sample Date/Time: N/A Received Date/Time: N/A Method Bottle ID Run P:3050B A:6010B A-13-E DU ^ A-13-E DU ^4 Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst /08/ :15 4 TAL EDI MC /10/ :01 4 TAL EDI CDC Lab ID: SD Client ID: N/A Sample Date/Time: N/A Received Date/Time: N/A Method Bottle ID Run P:3050B A:6010B P:3050B A:6010B A-13-D SD ^ A-13-D SD ^ A-13-D PDS ^ A-13-D PDS ^4 Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst /08/ :15 20 TAL EDI MC /10/ :09 20 TAL EDI CDC /08/ :15 4 TAL EDI MC /10/ :16 4 TAL EDI CDC TestAmerica Edison A = Analytical Method P = Prep Method Page 31 of 267
32 Quality Control Results Client: Conestoga-Rovers & Associates, Inc. Job Number: Laboratory Chronicle Lab References: TAL EDI = TestAmerica Edison TestAmerica Edison Page 32 of 267 A = Analytical Method P = Prep Method
33 METALS Page 33 of 267
34 COVER PAGE METALS Lab Name: TestAmerica Edison SDG No.: Project: TO4-2012, GM Wilmington Job Number: Client Sample ID SO mm-210 SO mm-217 SO mm-218 Lab Sample ID Comments: Page 34 of 267
35 1A-IN INORGANIC ANALYSIS DATA SHEET METALS Client Sample ID: SO mm-210 Lab Sample ID: Lab Name: TestAmerica Edison Job No.: SDG ID.: Matrix: Solid Date Sampled: 08/23/ :50 Reporting Basis: DRY Date Received: 08/23/ :30 % Solids: 85.4 CAS No. Analyte Result RL MDL C Q DIL Method Arsenic mg/kg U B FORM IA-IN Page 35 of 267
36 1A-IN INORGANIC ANALYSIS DATA SHEET METALS Client Sample ID: SO mm-217 Lab Sample ID: Lab Name: TestAmerica Edison Job No.: SDG ID.: Matrix: Solid Date Sampled: 08/23/ :00 Reporting Basis: DRY Date Received: 08/23/ :30 % Solids: 91.6 CAS No. Analyte Result RL MDL C Q DIL Method Arsenic mg/kg B FORM IA-IN Page 36 of 267
37 1A-IN INORGANIC ANALYSIS DATA SHEET METALS Client Sample ID: SO mm-218 Lab Sample ID: Lab Name: TestAmerica Edison Job No.: SDG ID.: Matrix: Solid Date Sampled: 08/23/ :00 Reporting Basis: DRY Date Received: 08/23/ :30 % Solids: 92.1 CAS No. Analyte Result RL MDL C Q DIL Method Arsenic mg/kg B FORM IA-IN Page 37 of 267
38 2A-IN CALIBRATION VERIFICATIONS METALS Lab Name: TestAmerica Edison Job No.: SDG No.: ICV Source: ME_CCV_DUO_00062 Concentration : CCV Source: ME_CCV_DUO_00062 ug/l ICV /7 11/10/ :38 CCV /31 11/10/ :07 CCV /43 11/10/ :50 Analyte Found C True %R Found C True %R Found C True %R Arsenic Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. FORM II-IN Page 38 of 267
39 2A-IN CALIBRATION VERIFICATIONS METALS Lab Name: TestAmerica Edison Job No.: SDG No.: ICV Source: ME_CCV_DUO_00062 Concentration : CCV Source: ME_CCV_DUO_00062 ug/l CCV /55 11/10/ :34 Analyte Found C True %R Found C True %R Found C True %R Arsenic Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. FORM II-IN Page 39 of 267
40 3-IN INSTRUMENT BLANKS METALS Lab Name: TestAmerica Edison Job No.: SDG No.: Concentration : ug/l ICB /8 CCB /32 CCB /44 CCB /56 11/10/ :41 11/10/ :10 11/10/ :54 11/10/ :38 Analyte RL Found C Found C Found C Found C Arsenic U 3.7 U 3.7 U 3.7 U Italicized analytes were not requested for this sequence. FORM III-IN Page 40 of 267
41 3-IN METHOD BLANK METALS Lab Name: TestAmerica Edison SDG No.: Concentration : mg/kg Instrument Code: ICP5 Job No.: Lab Sample ID: MB /1-A ^2 Batch No.: CAS No. Analyte Concentration C Q Method Arsenic 0.47 U 6010B FORM III-IN Page 41 of 267
42 4A-IN INTERFERENCE CHECK STANDARD METALS Lab Name: TestAmerica Edison Job No.: SDG No.: Lab Sample ID: ICSA /9 Instrument ID: ICP5 Lab File ID: asc ICS Source: ME_ICSA_Duo_00040 Concentration : ug/l Analyte True Solution A Solution A Found Percent Recovery Arsenic Aluminum Antimony 3.48 Barium Beryllium Boron Cadmium 3.45 Calcium Chromium 1.80 Cobalt Copper Iron Lead 1.18 Magnesium Manganese Molybdenum Nickel Potassium 206 Selenium 3.29 Silver Sodium 15.5 Strontium Thallium 7.46 Tin Titanium Vanadium Zinc Calculations are performed before rounding to avoid round-off errors in calculated results. FORM IVA-IN Page 42 of 267
43 4A-IN INTERFERENCE CHECK STANDARD METALS Lab Name: TestAmerica Edison Job No.: SDG No.: Lab Sample ID: ICSAB /10 Instrument ID: ICP5 Lab File ID: asc ICS Source: ME_ICSAB_DUO_00041 Concentration : ug/l Analyte True Solution AB Solution AB Found Percent Recovery Arsenic Aluminum Antimony Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Calculations are performed before rounding to avoid round-off errors in calculated results. FORM IVA-IN Page 43 of 267
44 5A-IN MATRIX SPIKE SAMPLE RECOVERY METALS Client ID: Lab Name: TestAmerica Edison SDG No.: Matrix: Solid % Solids: 82.9 Lab ID: A-13-F MS ^4 Job No.: Concentration : mg/kg Analyte SSR C Sample Result (SR) C Control Spike Limit Added (SA) %R %R Q Method Arsenic U B SSR = Spiked Sample Result Calculations are performed before rounding to avoid round-off errors in calculated results. Note - Results and Reporting Limits have been adjusted for dry weight. FORM VA - IN Page 44 of 267
45 5B-IN POST DIGESTION SPIKE SAMPLE RECOVERY METALS Client ID: Lab Name: TestAmerica Edison SDG No.: Matrix: Solid Lab ID: A-13-D PDS ^4 Job No.: Concentration : mg/kg Analyte SSR C Sample Result (SR) C Control Spike Limit Added (SA) %R %R Q Method Arsenic U B SSR = Spiked Sample Result Calculations are performed before rounding to avoid round-off errors in calculated results. Note - Results and Reporting Limits have been adjusted for dry weight. FORM VB - IN Page 45 of 267
46 6-IN DUPLICATES METALS Client ID: Lab ID: A-13-E DU ^4 Lab Name: TestAmerica Edison Job No.: SDG No.: % Solids for Sample: 82.9 % Solids for Duplicate: 82.9 Matrix: Solid Concentration : mg/kg Arsenic Analyte Control Limit Sample (S) C Duplicate (D) C RPD Q Method U 1.1 U NC 6010B Calculations are performed before rounding to avoid round-off errors in calculated results. FORM VI-IN Page 46 of 267
47 7A-IN LCS-CERTIFIED REFERENCE MATERIAL METALS Lab ID: LCSSRM /2-A ^4 Lab Name: TestAmerica Edison Job No.: Sample Matrix: Solid LCS Source: ME_LCSS_77_00002 Analyte Solid(mg/Kg) True Found C %R Limits Q Method Arsenic B Calculations are performed before rounding to avoid round-off errors in calculated results. FORM VIIA - IN Page 47 of 267
48 8-IN ICP-AES AND ICP-MS SERIAL DILUTIONS METALS Lab ID: A-13-D SD ^20 SDG No: Lab Name: TestAmerica Edison Matrix: Solid Job No: Concentration : mg/kg Analyte Initial Sample Result (I) C Serial Dilution Result (S) C % Difference Q Method Arsenic 1.1 U 5.6 U NC 6010B Calculations are performed before rounding to avoid round-off errors in calculated results. FORM VIII-IN Page 48 of 267
49 9-IN DETECTION LIMITS METALS Lab Name: TestAmerica Edison Job Number: SDG Number: Matrix: Solid Instrument ID: ICP5 Method: 6010B MDL Date: 02/08/ :17 Prep Method: 3050B Analyte Wavelength/ Mass RL (mg/kg) MDL (mg/kg) Arsenic FORM IX - IN Page 49 of 267
50 9-IN CALIBRATION BLANK DETECTION LIMITS METALS Lab Name: TestAmerica Edison Job Number: SDG Number: Matrix: Solid Instrument ID: ICP5 Method: 6010B XMDL Date: 11/14/ :14 Analyte Wavelength/ Mass XRL (ug/l) XMDL (ug/l) Arsenic FORM IX - IN Page 50 of 267
51 12-IN PREPARATION LOG METALS Lab Name: TestAmerica Edison SDG No.: Prep Method: 3050B Job No.: Lab Sample ID Preparation Date Prep Batch Initial Weight (g) Initial Volume Final Volume (ml) MB /1-A ^2 11/08/ : LCSSRM /2-A 11/08/ : ^ A-13-E DU ^4 11/08/ : A-13-F MS ^4 11/08/ : /08/ : /08/ : /08/ : FORM XII-IN Page 51 of 267
52 13-IN ANALYSIS RUN LOG METALS Lab Name: TestAmerica Edison Job No.: SDG No.: Instrument ID: ICP5 Method: 6010B Start Date: 11/10/ :16 End Date: 11/10/ :48 Lab Sample ID D / F T y p e Time A s Analytes ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ICV /7 ICB /8 ICSA /9 ICSAB /10 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV /19 CCB /20 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV /31 CCB /32 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ 12:16 12:19 12:23 12:27 12:30 12: :38 X 1 12:41 X 1 12:45 X 1 12:49 X 12:52 12:56 13:00 13:03 13:07 13:11 13:14 13:18 13:22 13:25 13:29 13:33 13:36 13:40 13:44 13:48 13:51 13:55 13:59 14: :07 X 1 14:10 X 14:14 14:18 14:21 14:25 14: T 14:32 X T 14:36 X T 14:40 X ZZZZZZ 14:43 FORM XIII-IN Page 52 of 267
53 13-IN ANALYSIS RUN LOG METALS Lab Name: TestAmerica Edison Job No.: SDG No.: Instrument ID: ICP5 Method: 6010B Start Date: 11/10/ :16 End Date: 11/10/ :48 Lab Sample ID D / F T y p e Time A s Analytes LCSSRM /2-A ^4 CCV /43 CCB /44 MB /1-A ^ A-13-E DU ^4 ZZZZZZ A-13-D SD ^ A-13-F MS ^ A-13-D PDS ^4 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV /55 CCB /56 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV /67 CCB /68 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV /79 CCB /80 ZZZZZZ 4 T 14:47 X 1 14:50 X 1 14:54 X 2 T 14:58 X 4 T 15:01 X 15:05 20 T 15:09 X 4 T 15:12 X 4 T 15:16 X 15:19 15:23 15:27 15: :34 X 1 15:38 X 15:41 15:45 15:49 15:52 15:56 16:00 16:03 16:07 16:10 16:14 16:17 16:21 16:25 16:28 16:32 16:36 16:39 16:43 16:47 16:50 16:54 16:57 17:01 17:05 17:08 FORM XIII-IN Page 53 of 267
54 13-IN ANALYSIS RUN LOG METALS Lab Name: TestAmerica Edison Job No.: SDG No.: Instrument ID: ICP5 Method: 6010B Start Date: 11/10/ :16 End Date: 11/10/ :48 Lab Sample ID D / F T y p e Time A s Analytes ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV /91 CCB /92 17:12 17:16 17:19 17:23 17:27 17:30 17:34 17:37 17:41 17:45 17:48 Prep Types T = Total/NA FORM XIII-IN Page 54 of 267
55 Al { 85} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis As {478} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc Page 55 of 267
56 A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Ag {103} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Page 56 of 267
57 Ba {445} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Be {108} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: Page 57 of 267
58 A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Ca { 80} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Page 58 of 267
59 Cd {449} Date of Fit: 11/10/ :37:52 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Co {447} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: Page 59 of 267
60 A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Cr {126} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Page 60 of 267
61 Cu {104} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL DCAL Emphasis Fe {124} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc Page 61 of 267
62 A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL DCAL Emphasis K { 44} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Page 62 of 267
63 Mg {121} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: A1 (Gain): Y-int: A2 (Curvature): n (Exponent): Correlation: Status: OK. Std Error of Est: Predicted MDL: Predicted MQL: Std. Name Stated Conc. Found Conc. Difference % Diff. (S)IR Std Dev CAL_BLK DCAL DCAL DCAL DCAL Emphasis Mn {131} Date of Fit: 11/10/ :37:53 Type of Fit: ar Weighting: 1/Conc A0 (Offset): Re-Slope: Page 63 of 267
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