Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, February 25, 2010.
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1 Environmental Conservation Laboratories, Inc Central Port Drive Orlando FL, Phone: FAX: Friday, March 5, 2010 Jones Edmunds & Associates (JO005) Attn: Javier DuQuesne 3910 S Washington Ave Titusville, fl RE: Laboratory Results for Project Number: , Project Name/Desc: ENCO Workorder: A Dear Javier DuQuesne, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, February 25, Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Orlando. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, David Camacho Project Manager Enclosure(s) The total number of pages in this report, including this page is 21.
2 SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Exterior Residence White Lab ID: A Sampled: 01/26/10 16:00 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :21 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :24 Client ID: Exterior Blue VS&V Lab ID: A Sampled: 01/26/10 16:00 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :22 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :51 Client ID: Interior Res. White Lab ID: A Sampled: 01/26/10 16:00 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :24 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :54 Client ID: Exterior VS&V yello/white Lab ID: A Sampled: 01/26/10 16:30 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :26 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :34 Client ID: GMWTP White Lab ID: A Sampled: 01/26/10 08:00 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :28 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :37 Client ID: Int. V. yellow Lab ID: A Sampled: 01/26/10 10:00 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :30 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :41 Client ID: Int. White V.S. Lab ID: A Sampled: 01/26/10 10:20 Received: 02/25/10 12:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010C 07/25/10 03/03/10 08:59 3/4/ :36 EPA 7471B 02/23/10 03/01/10 16:13 3/2/ :44 Page 2 of 21
3 SAMPLE DETECTION SUMMARY Client ID: Exterior Residence White Lab ID: A Results Flag MDL PQL Units Method Barium - Total 19.5 I mg/kg wet EPA 6010C Mercury - Total mg/kg wet EPA 7471B O-04 Client ID: Exterior Blue VS&V Lab ID: A Results Flag MDL PQL Units Method Barium - Total mg/kg wet EPA 6010C Chromium - Total 4.02 I mg/kg wet EPA 6010C Lead - Total mg/kg wet EPA 6010C Mercury - Total mg/kg wet EPA 7471B O-04 Client ID: Interior Res. White Lab ID: A Results Flag MDL PQL Units Method Barium - Total mg/kg wet EPA 6010C Chromium - Total 14.8 I mg/kg wet EPA 6010C Lead - Total 10.4 I mg/kg wet EPA 6010C Mercury - Total mg/kg wet EPA 7471B O-04 Client ID: Exterior VS&V yello/white Lab ID: A Results Flag MDL PQL Units Method Barium - Total mg/kg wet EPA 6010C Chromium - Total 7.84 I mg/kg wet EPA 6010C Lead - Total 17.0 I mg/kg wet EPA 6010C Mercury - Total mg/kg wet EPA 7471B O-04 Client ID: GMWTP White Lab ID: A Results Flag MDL PQL Units Method Arsenic - Total mg/kg wet EPA 6010C Barium - Total mg/kg wet EPA 6010C Chromium - Total mg/kg wet EPA 6010C Lead - Total mg/kg wet EPA 6010C Mercury - Total mg/kg wet EPA 7471B O-04 Client ID: Int. V. yellow Lab ID: A Results Flag MDL PQL Units Method Barium - Total mg/kg wet EPA 6010C Cadmium - Total 1.06 I mg/kg wet EPA 6010C Chromium - Total 7.12 I mg/kg wet EPA 6010C Lead - Total 7.97 I mg/kg wet EPA 6010C Mercury - Total I mg/kg wet EPA 7471B O-04 Silver - Total 3.83 I mg/kg wet EPA 6010C Client ID: Int. White V.S. Lab ID: A Results Flag MDL PQL Units Method Barium - Total 14.9 I mg/kg wet EPA 6010C Chromium - Total 3.44 I mg/kg wet EPA 6010C Mercury - Total I mg/kg wet EPA 7471B O-04 Selenium - Total 16.1 I mg/kg wet EPA 6010C Page 3 of 21
4 ANALYTICAL RESULTS Description: Exterior Residence White Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:00 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ mg/kg wet B25008 EPA 7471B 03/02/10 09:24 JMA O-04 Page 4 of 21
5 Description: Exterior Residence White Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:00 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 13.0 U mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV Barium [ ] ^ 19.5 I mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV Cadmium [ ] ^ U mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV Chromium [ ] ^ 2.55 U mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV Lead [ ] ^ 6.68 U mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV Selenium [ ] ^ 15.7 U mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV Silver [ ] ^ 3.42 U mg/kg wet C03001 EPA 6010C 03/04/10 14:21 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 21
6 Description: Exterior Blue VS&V Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:00 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ 1.21 mg/kg wet B25008 EPA 7471B 03/02/10 09:51 JMA O-04 Page 6 of 21
7 Description: Exterior Blue VS&V Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:00 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 16.5 U mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV Barium [ ] ^ 157 mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV Cadmium [ ] ^ 1.20 U mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV Chromium [ ] ^ 4.02 I mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV Lead [ ] ^ 1210 mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV Selenium [ ] ^ 20.0 U mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV Silver [ ] ^ 4.35 U mg/kg wet C03001 EPA 6010C 03/04/10 14:22 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 21
8 Description: Interior Res. White Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:00 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ 26.3 mg/kg wet B25008 EPA 7471B 03/02/10 09:54 JMA O-04 Page 8 of 21
9 Description: Interior Res. White Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:00 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 12.0 U mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV Barium [ ] ^ 20.9 mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV Cadmium [ ] ^ U mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV Chromium [ ] ^ 14.8 I mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV Lead [ ] ^ 10.4 I mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV Selenium [ ] ^ 14.5 U mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV Silver [ ] ^ 3.16 U mg/kg wet C03001 EPA 6010C 03/04/10 14:24 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 21
10 Description: Exterior VS&V yello/white Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:30 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ mg/kg wet B25008 EPA 7471B 03/02/10 09:34 JMA O-04 Page 10 of 21
11 Description: Exterior VS&V yello/white Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 16:30 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 12.5 U mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV Barium [ ] ^ 241 mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV Cadmium [ ] ^ U mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV Chromium [ ] ^ 7.84 I mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV Lead [ ] ^ 17.0 I mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV Selenium [ ] ^ 15.2 U mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV Silver [ ] ^ 3.30 U mg/kg wet C03001 EPA 6010C 03/04/10 14:26 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 21
12 Description: GMWTP White Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 08:00 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ mg/kg wet B25008 EPA 7471B 03/02/10 09:37 JMA O-04 Page 12 of 21
13 Description: GMWTP White Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 08:00 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 102 mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV Barium [ ] ^ 50.2 mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV Cadmium [ ] ^ U mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV Chromium [ ] ^ 586 mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV Lead [ ] ^ 214 mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV Selenium [ ] ^ 15.5 U mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV Silver [ ] ^ 3.37 U mg/kg wet C03001 EPA 6010C 03/04/10 14:28 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 21
14 Description: Int. V. yellow Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 10:00 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ I mg/kg wet B25008 EPA 7471B 03/02/10 09:41 JMA O-04 Page 14 of 21
15 Description: Int. V. yellow Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 10:00 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 11.8 U mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV Barium [ ] ^ 115 mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV Cadmium [ ] ^ 1.06 I mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV Chromium [ ] ^ 7.12 I mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV Lead [ ] ^ 7.97 I mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV Selenium [ ] ^ 14.3 U mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV Silver [ ] ^ 3.83 I mg/kg wet C03001 EPA 6010C 03/04/10 14:30 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 21
16 Description: Int. White V.S. Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 10:20 Work Order: A ^ - ENCO Orlando certified analyte [NELAC E83182] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Mercury [ ] ^ I mg/kg wet B25008 EPA 7471B 03/02/10 09:44 JMA O-04 Page 16 of 21
17 Description: Int. White V.S. Lab Sample ID: A Received: 02/25/10 12:05 Matrix: Soil Sampled: 01/26/10 10:20 Work Order: A ^ - ENCO Jacksonville certified analyte [NELAC E82277] [CAS Number] Results Flag Units DF MDL PQL Batch Method Analyzed By Arsenic [ ] ^ 12.9 U mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV Barium [ ] ^ 14.9 I mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV Cadmium [ ] ^ U mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV Chromium [ ] ^ 3.44 I mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV Lead [ ] ^ 6.65 U mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV Selenium [ ] ^ 16.1 I mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV Silver [ ] ^ 3.41 U mg/kg wet C03001 EPA 6010C 03/04/10 14:36 ACV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 21
18 - Quality Control QUALITY CONTROL Batch 0C EPA 3050B Blank (0C03001-BLK1) Prepared: 03/03/ :59 Analyzed: 03/04/ :13 Arsenic Result Flag U PQL Units mg/kg wet Spike Level Source Result %REC %REC Limits RPD RPD Limit Barium U mg/kg wet Cadmium U mg/kg wet Chromium U mg/kg wet Lead U mg/kg wet Selenium U mg/kg wet Silver U mg/kg wet LCS (0C03001-BS1) Prepared: 03/03/ :59 Analyzed: 03/04/ :15 Arsenic Result 25.8 Flag PQL Units Spike Level Source Result %REC %REC Limits mg/kg wet RPD RPD Limit Barium mg/kg wet Cadmium mg/kg wet Chromium mg/kg wet Lead mg/kg wet Selenium mg/kg wet Silver mg/kg wet Matrix Spike (0C03001-MS1) Source: B Arsenic Barium Cadmium Chromium Lead Selenium Silver Prepared: 03/03/ :59 Analyzed: 03/04/ :16 Spike Source %REC RPD Result Flag PQL Units Level Result %REC Limits RPD Limit mg/kg wet mg/kg wet mg/kg wet mg/kg wet QM mg/kg wet NR QM U 2.00 mg/kg wet U QM mg/kg wet Matrix Spike Dup (0C03001-MSD1) Source: B Arsenic Barium Cadmium Chromium Lead Selenium Silver Prepared: 03/03/ :59 Analyzed: 03/04/ :19 Spike Source %REC RPD Result Flag PQL Units Level Result %REC Limits RPD Limit mg/kg wet mg/kg wet mg/kg wet mg/kg wet QM mg/kg wet NR QM U 2.00 mg/kg wet U QM mg/kg wet Quality Control QUALITY CONTROL Batch 0B EPA 7471B Page 18 of 21
19 - Quality Control QUALITY CONTROL Batch 0B EPA 7471B Blank (0B25008-BLK1) Prepared: 03/01/ :13 Analyzed: 03/02/ :30 Mercury Result Flag U PQL Units mg/kg wet Spike Level Source Result %REC %REC Limits RPD RPD Limit LCS (0B25008-BS1) Prepared: 03/01/ :13 Analyzed: 03/02/ :33 Mercury Result Flag PQL Units Spike Level Source Result %REC %REC Limits mg/kg wet RPD RPD Limit Matrix Spike (0B25008-MS1) Source: A Prepared: 03/01/ :13 Analyzed: 03/02/ :46 Mercury Result Flag Spike Source %REC PQL Units Level Result %REC Limits mg/kg dry RPD RPD Limit Matrix Spike Dup (0B25008-MSD1) Prepared: 03/01/ :13 Analyzed: 03/02/ :50 Source: A Mercury Result Flag Spike Source %REC RPD PQL Units Level Result %REC Limits RPD Limit mg/kg dry Page 19 of 21
20 FLAGS/NOTES AND DEFINITIONS PQL B I J K L M N O Q T U V Y Z PQL: Practical Quantitation Limit. Results are based upon membrane filter colony counts that are outside the method indicated ideal range. The reported value is between the laboratory method detection limit (MDL) and the practical quantitation limit (PQL). Estimated value. The associated sample note or project narrative indicate the causative reason. Off-scale low; Actual value is known to be less than the value given. Off-scale high; Actual value is known to be greater than value given. Presence of analyte is verified but not quantified; the actual value is less than the MRL but greater than the MDL. Presumptive evidence of presence of material. Sampled, but analysis lost or not performed. Sample exceeded the accepted holding time. Value reported is less than the laboratory method detection limit. The value is reported for informational purposes only and shall not be used in statistical analysis. Indicates that the compound was analyzed for but not detected. Indicates that the analyte was detected in both the sample and the associated method blank. The laboratory analysis was from an improperly preserved sample. The data may not be accurate. Too many colonies were present (TNTC); the numeric value represents the filtration volume.? Data are rejected and should not be used. Some or all of the quality control data for the analyte were outside criteria, and the presence or absence of the analyte cannot be determined from the data. * Not reported due to interference. O-04 This sample was analyzed outside the EPA recommended holding time. QM-02 QM-07 The RPD and/or percent recovery for this QC spike sample cannot be accurately calculated due to the high concentration of analyte inherent in the sample. The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. Page 20 of 21
21 Page 21 of 21
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