Drake Petroleum Company, Inc. Accutest Job Number: JB Total number of pages in report:

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e-hardcopy 2.0 Automated Report New Jersey 05/06/15 05/06/15 Technical Report for Drake Petroleum Company, Inc. 146282.

com ATTN: Jen Maciejewski Total number of pages in report: 14 Test results contained within this data package meet the

NY(10983), CA, CT, DE, FL, IL, IN, KS, KY, LA, MA, MD, MI, MT, NC, OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA, RI,

approval of Accutest Laboratories. Test results relate only to samples analyzed.

1 e-hardcopy 2.0 Automated Report New Jersey 05/06/15 05/06/15 Technical Report for Drake Petroleum Company, Inc PO# Accutest Job Number: Sampling Date: 03/25/15 Report to: Brown & Caldwell ATTN: Jen Maciejewski Total number of pages in report: 14 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Nancy Cole Laboratory Director Client Service contact: Victoria Pushkova Certifications: NJ(12129), NY(10983), CA, CT, DE, FL, IL, IN, KS, KY, LA, MA, MD, MI, MT, NC, OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA, RI, SC, TN, VA, WV, DoD ELAP (L-A-B L2248) This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New Jersey 2235 Route 130 Dayton, NJ tel: fax: Accutest Laboratories is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. 1 of 14

2 Table of Contents Section 1: Sample Summary... 3 Section 2: Summary of Hits... 4 Section 3: Sample Results : -1: SYS-INF : -2: SYS-EFF Section 4: Misc. Forms : Chain of Custody Sections: of 14

3 1 Accutest 10:35 06-May-2015 Sample Summary Drake Petroleum Company, Inc. Job No: Project No: PO# Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID -1 03/25/15 15:00 BG 03/26/15 AQ Influent SYS-INF /25/15 15:10 BG 03/26/15 AQ Effluent SYS-EFF of 14

4 Summary of Hits Page 1 of 1 Job Number: Account: Drake Petroleum Company, Inc. Project: Collected: 03/25/15 2 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method -1 SYS-INF Benzene ug/l SW B Toluene ug/l SW B Ethylbenzene ug/l SW B Xylene (total) ug/l SW B Methyl Tert Butyl Ether ug/l SW B Tert Butyl Alcohol ug/l SW B Naphthalene ug/l SW B Di-Isopropyl ether ug/l SW B tert-amyl Methyl Ether 1.1 J ug/l SW B tert-butyl Ethyl Ether 0.33 J ug/l SW B TPH-GRO (C6-C10) mg/l SW C TPH-DRO (C10-C28) mg/l SW C -2 SYS-EFF Tert Butyl Alcohol ug/l SW B 4 of 14

5 3 Section 3 New Jersey Accutest LabLink@ :35 06-May-2015 Sample Results Report of Analysis 5 of 14

6 Accutest 10:35 06-May-2015 Report of Analysis Page 1 of 1 Client Sample ID: SYS-INF Lab Sample ID: -1 Date Sampled: 03/25/15 Matrix: AQ - Influent Date Received: 03/26/15 Method: SW B Percent Solids: n/a Project: File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1A D 1 03/31/15 MM n/a n/a V1A6449 1A D 10 03/31/15 MM n/a n/a V1A6449 Run #1 Purge Volume 5.0 ml 5.0 ml Purgeable Aromatics, MTBE, TBA, Naphthalene CAS No. Compound Result RL MDL Units Q Benzene ug/l Toluene ug/l Ethylbenzene ug/l Xylene (total) ug/l Methyl Tert Butyl Ether ug/l Tert Butyl Alcohol 1360 a ug/l Naphthalene ug/l Di-Isopropyl ether ug/l tert-amyl Methyl Ether ug/l J tert-butyl Ethyl Ether ug/l J CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits Dibromofluoromethane 86% 87% % ,2-Dichloroethane-D4 92% 93% % Toluene-D8 94% 95% % Bromofluorobenzene 88% 88% % (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 14

7 Accutest 10:35 06-May-2015 Report of Analysis Page 1 of 1 Client Sample ID: SYS-INF Lab Sample ID: -1 Date Sampled: 03/25/15 Matrix: AQ - Influent Date Received: 03/26/15 Method: SW C Percent Solids: n/a Project: File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UV22594.D 1 03/27/15 WO n/a n/a GUV4879 Run #1 Purge Volume 5.0 ml CAS No. Compound Result RL MDL Units Q TPH-GRO (C6-C10) mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits aaa-trifluorotoluene 101% % ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 14

8 Accutest 10:35 06-May-2015 Report of Analysis Page 1 of 1 Client Sample ID: SYS-INF Lab Sample ID: -1 Date Sampled: 03/25/15 Matrix: AQ - Influent Date Received: 03/26/15 Method: SW C SW C Percent Solids: n/a Project: File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2Y68815.D 1 03/31/15 JM 03/30/15 OP82677 G2Y2644 Initial Volume Final Volume Run #1 300 ml 1.0 ml CAS No. Compound Result RL MDL Units Q TPH-DRO (C10-C28) mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits o-terphenyl 101% % Tetracosane-d50 97% % a-Androstane 98% % ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 14

9 Accutest 10:35 06-May-2015 Report of Analysis Page 1 of 1 Client Sample ID: SYS-EFF Lab Sample ID: -2 Date Sampled: 03/25/15 Matrix: AQ - Effluent Date Received: 03/26/15 Method: SW B Percent Solids: n/a Project: File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1A D 1 03/31/15 MM n/a n/a V1A6449 1A D 10 03/31/15 MM n/a n/a V1A6449 Run #1 Purge Volume 5.0 ml 5.0 ml Purgeable Aromatics, MTBE, TBA, Naphthalene CAS No. Compound Result RL MDL Units Q Benzene ND ug/l Toluene ND ug/l Ethylbenzene ND ug/l Xylene (total) ND ug/l Methyl Tert Butyl Ether ND ug/l Tert Butyl Alcohol 2920 a ug/l Naphthalene ND ug/l Di-Isopropyl ether ND ug/l tert-amyl Methyl Ether ND ug/l tert-butyl Ethyl Ether ND ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits Dibromofluoromethane 87% 86% % ,2-Dichloroethane-D4 94% 92% % Toluene-D8 96% 94% % Bromofluorobenzene 88% 87% % (a) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 14

10 Accutest 10:35 06-May-2015 Report of Analysis Page 1 of 1 Client Sample ID: SYS-EFF Lab Sample ID: -2 Date Sampled: 03/25/15 Matrix: AQ - Effluent Date Received: 03/26/15 Method: SW C Percent Solids: n/a Project: File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UV22593.D 1 03/27/15 WO n/a n/a GUV4879 Run #1 Purge Volume 5.0 ml CAS No. Compound Result RL MDL Units Q TPH-GRO (C6-C10) ND mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits aaa-trifluorotoluene 104% % ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 14

11 Accutest 10:35 06-May-2015 Report of Analysis Page 1 of 1 Client Sample ID: SYS-EFF Lab Sample ID: -2 Date Sampled: 03/25/15 Matrix: AQ - Effluent Date Received: 03/26/15 Method: SW C SW C Percent Solids: n/a Project: File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2Y68816.D 1 03/31/15 JM 03/30/15 OP82677 G2Y2644 Initial Volume Final Volume Run #1 300 ml 1.0 ml CAS No. Compound Result RL MDL Units Q TPH-DRO (C10-C28) ND mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits o-terphenyl 92% % Tetracosane-d50 93% % a-Androstane 94% % ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 14

12 Section 4 New Jersey Accutest LabLink@ :35 06-May-2015 Misc. Forms 4 Custody Documents and Other Forms Includes the following where applicable: Chain of Custody 12 of 14

13 4 4.1 : Chain of Custody Page 1 of 2 13 of 14

Accutest Laboratories Sample Receipt Summary Accutest Job Number: Client: Date / Time Received: 3/26/2015 4:40:00 PM Delivery Method: Project: Airbill #'s: Cooler Temps (Initial/Adjusted): #1: (3/1.

14 Accutest Laboratories Sample Receipt Summary Accutest Job Number: Client: Date / Time Received: 3/26/2015 4:40:00 PM Delivery Method: Project: Airbill #'s: Cooler Temps (Initial/Adjusted): #1: (3/1.2); 0 Cooler Security Y or N 1. Custody Seals Present: 2. Custody Seals Intact: 3. COC Present: 4. Smpl Dates/Time OK Cooler Temperature Y or N Y or N Sample Integrity - Documentation Y or N 1. Sample labels present on bottles: 2. Container labeling complete: 3. Sample container label / COC agree: Temp criteria achieved: 2. Cooler temp verification: IR Gun 3. Cooler media: Ice (Bag) 4. No. Coolers: 1 Quality Control Preservation Y or N N/A 1. Trip Blank present / cooler: 2. Trip Blank listed on COC: 3. Samples preserved properly: 4. VOCs headspace free: Sample Integrity - Condition Y or N 1. Sample recvd within HT: 2. All containers accounted for: 3. Condition of sample: Intact Sample Integrity - Instructions 1. Analysis requested is clear: 2. Bottles received for unspecified tests 3. Sufficient volume recvd for analysis: 4. Compositing instructions clear: Y or N N/A 5. Filtering instructions clear: Comments Accutest Laboratories V: US Highway 130 F: Dayton, New Jersey www/accutest.com : Chain of Custody Page 2 of 2 14 of 14

ANALYTICAL REPORT. Job Number: Job Description: Gasoline Uptake Study. For: IRST Commonwealth Dr. Louisville, KY 40299

ANALYTICAL REPORT. Job Number: Job Description: Gasoline Uptake Study. For: IRST Commonwealth Dr. Louisville, KY 40299 ANALYTICAL REPORT Job Number: 580-5165-2 Job Description: Gasoline Uptake Study For: IRST 11760 Commonwealth Dr. Louisville, KY 40299 Attention: Brent Hepner Heather Curbow Project Manager I hcurbow@stl-inc.com