ANALYTICAL REPORT. Job Number: Job Description: Gasoline Uptake Study. For: IRST Commonwealth Dr. Louisville, KY 40299

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1 ANALYTICAL REPORT Job Number: Job Description: Gasoline Uptake Study For: IRST Commonwealth Dr. Louisville, KY Attention: Brent Hepner Heather Curbow Project Manager I hcurbow@stl-inc.com 03/21/2007 cc: Dan Parker Project Manager: Heather Curbow is a part of Severn Trent Laboratories, Inc. This report is issued solely for the use of the person or company to whom it is addressed. Any use, copying or disclosure other than by the intended recipient is unauthorized. If you have received this report in error, please notify the sender immediately at and destroy this report immediately. Severn Trent Laboratories, Inc th Street East, Tacoma, WA Tel (253) Fax (253) Page 1 of 15

2 METHOD SUMMARY Client: IRST Job Number: Description Lab Location Method Preparation Method Matrix: Solid Volatile Organic Compounds by GC/MS Toxicity Characteristic Leaching Procedure (ZHE) Purge and Trap on Leachates STL SEA STL SEA STL SEA SW B SW SW B Pensky-Martens Closed-Cup Method for Determining Ignitability STL SEA SW Matrix: Water Volatile Petroleum Products Purge-and-Trap STL SEA STL SEA NWTPH NWTPH-Gx SW B LAB REFERENCES: STL SEA = METHOD REFERENCES: SW846 - "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Page 2 of 15

3 SAMPLE SUMMARY Client: IRST Job Number: Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received CI Agent/Gasoline Leachability 1.79 Solid CI Agent/Gasoline Water Leachability /07/ /07/ /07/ /07/ Page 3 of 15

4 Analytical Data Client: IRST Job Number: Client Sample ID: CI Agent/Gasoline Leachability 1.79 Lab Sample ID: Client Matrix: Solid Date Sampled: Date Received: 03/07/ /07/ B Volatile Organic Compounds by GC/MS -TCLP Method: Preparation: Dilution: Date Analyzed: Date Prepared: Date Leached: 8260B Analysis Batch: B 50 Leachate Batch: /13/ /13/ /08/ Instrument ID: SEA001 Lab File ID: AG31242.D Initial Weight/Volume: Final Weight/Volume: Analyte DryWt Corrected: N Result (ug/l) Qualifier MDL RL Vinyl chloride ND ,1-Dichloroethene ND Butanone ND Chloroform ND Carbon tetrachloride ND Benzene ND ,2-Dichloroethane ND Trichloroethene ND Tetrachloroethene ND Chlorobenzene ND Toluene ND m-xylene & p-xylene 44 J o-xylene 38 J Surrogate %Rec Acceptance Limits Fluorobenzene (Surr) Toluene-d8 (Surr) Ethylbenzene-d Bromofluorobenzene (Surr) Trifluorotoluene (Surr) Page 4 of 15

5 Analytical Data Client: IRST Job Number: Client Sample ID: CI Agent/Gasoline Leachability 1.79 Lab Sample ID: Client Matrix: Water Date Sampled: Date Received: 03/07/ /07/ NWTPH-Gx Volatile Petroleum Products Method: Preparation: Dilution: Date Analyzed: Date Prepared: NWTPH-Gx Analysis Batch: B 50 03/09/ /09/ Instrument ID: SEA041 Lab File ID: GX D Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: PRIMARY Analyte Result (mg/l) Qualifier MDL RL Gasoline 3.6 B Surrogate %Rec Acceptance Limits 4-Bromofluorobenzene (Surr) Trifluorotoluene (Surr) Ethylbenzene-d10 Fluorobenzene (Surr) Toluene-d8 (Surr) Page 5 of 15

6 Analytical Data Client: IRST Job Number: Client Sample ID: CI Agent/Gasoline Leachability 1.79 General Chemistry Lab Sample ID: Client Matrix: Solid Date Sampled: Date Received: 03/07/ /07/ Analyte Flashpoint Result Qual Units Dil Method >212 Degrees F Anly Batch: Date Analyzed 03/19/ DryWt Corrected: N Page 6 of 15

7 Quality Control Results Client: IRST Job Number: Method Blank - Batch: Lab Sample ID: MB /1 Client Matrix: Solid Dilution: 50 Date Analyzed: 03/13/ Date Prepared: 03/13/ Analysis Batch: Prep Batch: N/A Units: ug/l Method: 8260B Preparation: 5030B TCLP Instrument ID: Lab File ID: SEA001 AG31241.D Initial Weight/Volume: Final Weight/Volume: Analyte Result Qual MDL RL Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform Carbon tetrachloride Benzene 1,2-Dichloroethane Trichloroethene Tetrachloroethene Chlorobenzene Toluene m-xylene & p-xylene o-xylene ND ND ND ND ND ND ND ND ND ND ND ND ND Surrogate % Rec Acceptance Limits Fluorobenzene (Surr) Toluene-d8 (Surr) Ethylbenzene-d Bromofluorobenzene (Surr) Trifluorotoluene (Surr) Calculations are performed before rounding to avoid round-off errors in calculated results. Page 7 of 15

8 Quality Control Results Client: IRST Job Number: Lab Control Spike - Batch: Lab Sample ID: LCS /2 Client Matrix: Solid Dilution: 50 Date Analyzed: 03/13/ Date Prepared: 03/13/ Analysis Batch: Prep Batch: N/A Units: ug/l Method: 8260B Preparation: 5030B TCLP Instrument ID: Lab File ID: SEA001 AG31239.D Initial Weight/Volume: Final Weight/Volume: Analyte Spike Amount Result % Rec. Limit Qual Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform Carbon tetrachloride Benzene 1,2-Dichloroethane Trichloroethene Tetrachloroethene Chlorobenzene Toluene m-xylene & p-xylene o-xylene Surrogate % Rec Acceptance Limits Fluorobenzene (Surr) Toluene-d8 (Surr) Ethylbenzene-d Bromofluorobenzene (Surr) Trifluorotoluene (Surr) Calculations are performed before rounding to avoid round-off errors in calculated results. Page 8 of 15

9 Quality Control Results Client: IRST Job Number: Matrix Spike - Batch: Lab Sample ID: Client Matrix: Solid Dilution: 50 Date Analyzed: 03/13/ Date Prepared: Date Leached: 03/13/ /08/ Analysis Batch: Prep Batch: N/A Units: ug/l Leachate Batch: Method: 8260B Preparation: 5030B TCLP Instrument ID: Lab File ID: SEA001 AG31244.D Initial Weight/Volume: Final Weight/Volume: Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform Carbon tetrachloride Benzene 1,2-Dichloroethane Trichloroethene Tetrachloroethene Chlorobenzene Toluene m-xylene & p-xylene o-xylene ND ND ND ND ND ND ND ND ND ND ND J J Calculations are performed before rounding to avoid round-off errors in calculated results. Page 9 of 15

10 Quality Control Results Client: IRST Job Number: Method Blank - Batch: Method: NWTPH-Gx Preparation: 5030B Lab Sample ID: MB /1 Client Matrix: Water Dilution: 50 Date Analyzed: 03/09/ Date Prepared: 03/09/ Analysis Batch: Prep Batch: N/A Units: mg/l Instrument ID: SEA041 Lab File ID: GX D Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: PRIMARY Analyte Result Qual MDL RL Gasoline 0.51 J Surrogate % Rec Acceptance Limits 4-Bromofluorobenzene (Surr) Trifluorotoluene (Surr) Ethylbenzene-d Fluorobenzene (Surr) Toluene-d8 (Surr) Lab Control Spike - Batch: Method: NWTPH-Gx Preparation: 5030B Lab Sample ID: LCS /2 Client Matrix: Water Dilution: 50 Date Analyzed: 03/09/ Date Prepared: 03/09/ Analysis Batch: Prep Batch: N/A Units: mg/l Instrument ID: SEA041 Lab File ID: GX D Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: PRIMARY Analyte Spike Amount Result % Rec. Limit Qual Gasoline Surrogate % Rec Acceptance Limits 4-Bromofluorobenzene (Surr) Trifluorotoluene (Surr) Ethylbenzene-d Fluorobenzene (Surr) Toluene-d8 (Surr) Calculations are performed before rounding to avoid round-off errors in calculated results. Page 10 of 15

11 Quality Control Results Client: IRST Job Number: Matrix Spike - Batch: Method: NWTPH-Gx Preparation: 5030B Lab Sample ID: Client Matrix: Water Dilution: 50 Date Analyzed: 03/09/ Date Prepared: 03/09/ Analysis Batch: Prep Batch: N/A Units: mg/l Instrument ID: SEA041 Lab File ID: GX D Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: PRIMARY Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual Gasoline Calculations are performed before rounding to avoid round-off errors in calculated results. Page 11 of 15

12 Quality Control Results Client: IRST Job Number: Lab Control Spike - Batch: Method: 1010 Preparation: N/A Lab Sample ID: LCS /1 Client Matrix: Solid Dilution: 1.0 Date Analyzed: 03/19/ Date Prepared: N/A Analysis Batch: Prep Batch: N/A Units: Degrees F Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: No Equipment Assigned N/A Analyte Spike Amount Result % Rec. Limit Qual Flashpoint Calculations are performed before rounding to avoid round-off errors in calculated results. Page 12 of 15

13 DATA REPORTING QUALIFIERS Client: IRST Job Number: Lab Section Qualifier Description GC/MS VOA J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. GC VOA B J Compound was found in the blank and sample. Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Page 13 of 15

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15 LOGIN SAMPLE RECEIPT CHECK LIST Client: IRST Job Number: Login Number: 5165 Question T/F/NA Comment Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. NA client dropped off in SR Cooler Temperature is acceptable. NA Cooler Temperature is recorded. NA COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. NA If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Page 15 of 15

ANALYTICAL REPORT. Job Number: Job Description: Old Douglas Harbor. For: PND Engineers, Inc West 36th Ave. Anchorage, AK 99503

ANALYTICAL REPORT. Job Number: Job Description: Old Douglas Harbor. For: PND Engineers, Inc West 36th Ave. Anchorage, AK 99503 ANALYTICAL REPORT Job Number: 580-5385-2 Job Description: Old Douglas Harbor For: PND Engineers, Inc. 1506 West 36th Ave. Anchorage, AK 99503 Attention: Ms. Jennifer Lundberg Katie Downie Project Manager