BIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: Cascade Thornapple River Assoc. Project: Water Analysis Lab Order:
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3 Date: 31-Jul-18 Work Order Sample Summary Lab Sample ID Client Sample ID Matrix Collection Date Date Received A Dam & Burger Water 7/25/2018 7/25/ A 48th & RR Water 7/25/2018 7/25/2018 Page 1 of 1
4 Date: 31-Jul-18 CASE NARRATIVE Samples are routinely analyzed using methods outlined in the following references: (SW) Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846, 3rd Ed. (E) Methods for Chemical Analysis of Water and Wastes, EPA-600/ (A) Standard Methods for the Examination of Water and Wastewater, APHA, 18th Ed. (D) Annual Book of ASTM Standards. Specific methods utilized for this project are provided in the analytical report and are identified by the reference document abbreviation ( ) followed by the method number. All QA/QC and sample analyses met method, laboratory and/or regulatory data quality objectives unless otherwise specified below. No data qualifications required. Page 1 of 1
5 Lab Sample ID: A Client Sample ID: Dam & Burger Anions by Ion Chromatography 1. Nitrogen, Nitrate (As N) E mg/l 1 RHS 7/26/ Nitrogen, Nitrite (As N) E mg/l 1 RHS 7/26/2018 Total Mercury by CVAA 1. Mercury SW7470A < µg/l 1 RHS 7/26/2018 Total Metal(s) by ICP 1. Arsenic SW6010B < µg/l 1 RHS 7/27/ Barium SW6010B < µg/l 1 RHS 7/27/ Cadmium SW6010B < µg/l 1 RHS 7/27/ Chromium SW6010B < µg/l 1 RHS 7/27/ Copper SW6010B < µg/l 1 RHS 7/27/ Lead SW6010B < µg/l 1 RHS 7/27/ Magnesium SW6010B 25,000 1,000 µg/l 1 RHS 7/27/ Manganese SW6010B < µg/l 1 RHS 7/27/ Nickel SW6010B < µg/l 1 RHS 7/27/ Selenium SW6010B < µg/l 1 RHS 7/27/ Silver SW6010B < µg/l 1 RHS 7/27/ Zinc SW6010B < µg/l 1 RHS 7/27/ of 6
6 Lab Sample ID: A Client Sample ID: Dam & Burger Volatiles by GC/MS 1. 1,1,1,2-Tetrachloroethane SW8260B < ,1,1-Trichloroethane SW8260B < ,1,2,2-Tetrachloroethane SW8260B < ,1,2-Trichloroethane SW8260B < ,1-Dichloroethane SW8260B < ,1-Dichloroethene SW8260B < ,1-Dichloropropene SW8260B < ,2,3-Trichlorobenzene SW8260B < ,2,3-Trichloropropane SW8260B < ,2,4-Trichlorobenzene SW8260B < ,2,4-Trimethylbenzene SW8260B < ,2-Dibromo-3-chloropropane SW8260B < ,2-Dibromoethane SW8260B < ,2-Dichlorobenzene SW8260B < ,2-Dichloroethane SW8260B < ,2-Dichloropropane SW8260B < ,3,5-Trimethylbenzene SW8260B < ,3-Dichlorobenzene SW8260B < ,3-Dichloropropane SW8260B < ,4-Dichlorobenzene SW8260B < ,2-Dichloropropane SW8260B < Butanone SW8260B < µg/l 1 ATD 7/26/ Chlorotoluene SW8260B < Hexanone SW8260B < µg/l 1 ATD 7/26/ Chlorotoluene SW8260B < Isopropyltoluene SW8260B < Methyl-2-pentanone SW8260B < µg/l 1 ATD 7/26/ Acetone SW8260B < µg/l 1 ATD 7/26/ Benzene SW8260B < Bromobenzene SW8260B < Bromochloromethane SW8260B < Bromodichloromethane SW8260B < Bromoform SW8260B < Bromomethane SW8260B < Carbon disulfide SW8260B < µg/l 1 ATD 7/26/ Carbon tetrachloride SW8260B < Chlorobenzene SW8260B < Chloroethane SW8260B < Chloroform SW8260B < Chloromethane SW8260B < of 6
7 Lab Sample ID: A Client Sample ID: Dam & Burger 41. cis-1,2-dichloroethene SW8260B < cis-1,3-dichloropropene SW8260B < Dibromochloromethane SW8260B < Dibromomethane SW8260B < Dichlorodifluoromethane SW8260B < Diethyl ether SW8260B < µg/l 1 ATD 7/26/ Ethylbenzene SW8260B < Hexachlorobutadiene SW8260B < Hexachloroethane SW8260B < Iodomethane SW8260B < Isopropylbenzene SW8260B < m,p-xylene SW8260B < µg/l 1 ATD 7/26/ Methyl tert-butyl ether SW8260B < µg/l 1 ATD 7/26/ Methylene chloride SW8260B < n-butylbenzene SW8260B < n-propylbenzene SW8260B < o-xylene SW8260B < sec-butylbenzene SW8260B < Styrene SW8260B < tert-butylbenzene SW8260B < Tetrachloroethene SW8260B < Toluene SW8260B < trans-1,2-dichloroethene SW8260B < trans-1,3-dichloropropene SW8260B < trans-1,4-dichloro-2-butene SW8260B < Trichloroethene SW8260B < Trichlorofluoromethane SW8260B < Vinyl chloride SW8260B < 1.0 Coliform by Membrane Filtration 1. Escherichia Coli H10029 < CFU/100 ml 1 SCL 7/25/2018 Ammonia Nitrogen 1. Nitrogen, Ammonia (As N) E350.3 < mg/l 1 RHS 7/30/2018 Phorphorus by UV/VIS Spec. 1. Phosphorus, Total (As P) E mg/l 1 RHS 7/30/2018 Total Inorganic Nitrogen 1. Total Inorganic Nitrogen NA mg/l 1 RHS 7/30/ of 6
8 Lab Sample ID: A Client Sample ID: 48th & RR Anions by Ion Chromatography 1. Nitrogen, Nitrate (As N) E mg/l 1 RHS 7/26/ Nitrogen, Nitrite (As N) E mg/l 1 RHS 7/26/2018 Total Mercury by CVAA 1. Mercury SW7470A < µg/l 1 RHS 7/26/2018 Total Metal(s) by ICP 1. Arsenic SW6010B < µg/l 1 RHS 7/27/ Barium SW6010B < µg/l 1 RHS 7/27/ Cadmium SW6010B < µg/l 1 RHS 7/27/ Chromium SW6010B < µg/l 1 RHS 7/27/ Copper SW6010B < µg/l 1 RHS 7/27/ Lead SW6010B < µg/l 1 RHS 7/27/ Magnesium SW6010B 23,000 1,000 µg/l 1 RHS 7/27/ Manganese SW6010B < µg/l 1 RHS 7/27/ Nickel SW6010B < µg/l 1 RHS 7/27/ Selenium SW6010B < µg/l 1 RHS 7/27/ Silver SW6010B < µg/l 1 RHS 7/27/ Zinc SW6010B < µg/l 1 RHS 7/27/ of 6
9 Lab Sample ID: A Client Sample ID: 48th & RR Volatiles by GC/MS 1. 1,1,1,2-Tetrachloroethane SW8260B < ,1,1-Trichloroethane SW8260B < ,1,2,2-Tetrachloroethane SW8260B < ,1,2-Trichloroethane SW8260B < ,1-Dichloroethane SW8260B < ,1-Dichloroethene SW8260B < ,1-Dichloropropene SW8260B < ,2,3-Trichlorobenzene SW8260B < ,2,3-Trichloropropane SW8260B < ,2,4-Trichlorobenzene SW8260B < ,2,4-Trimethylbenzene SW8260B < ,2-Dibromo-3-chloropropane SW8260B < ,2-Dibromoethane SW8260B < ,2-Dichlorobenzene SW8260B < ,2-Dichloroethane SW8260B < ,2-Dichloropropane SW8260B < ,3,5-Trimethylbenzene SW8260B < ,3-Dichlorobenzene SW8260B < ,3-Dichloropropane SW8260B < ,4-Dichlorobenzene SW8260B < ,2-Dichloropropane SW8260B < Butanone SW8260B < µg/l 1 ATD 7/27/ Chlorotoluene SW8260B < Hexanone SW8260B < µg/l 1 ATD 7/27/ Chlorotoluene SW8260B < Isopropyltoluene SW8260B < Methyl-2-pentanone SW8260B < µg/l 1 ATD 7/27/ Acetone SW8260B < µg/l 1 ATD 7/27/ Benzene SW8260B < Bromobenzene SW8260B < Bromochloromethane SW8260B < Bromodichloromethane SW8260B < Bromoform SW8260B < Bromomethane SW8260B < Carbon disulfide SW8260B < µg/l 1 ATD 7/27/ Carbon tetrachloride SW8260B < Chlorobenzene SW8260B < Chloroethane SW8260B < Chloroform SW8260B < Chloromethane SW8260B < of 6
10 Lab Sample ID: A Client Sample ID: 48th & RR 41. cis-1,2-dichloroethene SW8260B < cis-1,3-dichloropropene SW8260B < Dibromochloromethane SW8260B < Dibromomethane SW8260B < Dichlorodifluoromethane SW8260B < Diethyl ether SW8260B < µg/l 1 ATD 7/27/ Ethylbenzene SW8260B < Hexachlorobutadiene SW8260B < Hexachloroethane SW8260B < Iodomethane SW8260B < Isopropylbenzene SW8260B < m,p-xylene SW8260B < µg/l 1 ATD 7/27/ Methyl tert-butyl ether SW8260B < µg/l 1 ATD 7/27/ Methylene chloride SW8260B < n-butylbenzene SW8260B < n-propylbenzene SW8260B < o-xylene SW8260B < sec-butylbenzene SW8260B < Styrene SW8260B < tert-butylbenzene SW8260B < Tetrachloroethene SW8260B < Toluene SW8260B < trans-1,2-dichloroethene SW8260B < trans-1,3-dichloropropene SW8260B < trans-1,4-dichloro-2-butene SW8260B < Trichloroethene SW8260B < Trichlorofluoromethane SW8260B < Vinyl chloride SW8260B < 1.0 Coliform by Membrane Filtration 1. Escherichia Coli H10029 < CFU/100 ml 1 SCL 7/25/2018 Ammonia Nitrogen 1. Nitrogen, Ammonia (As N) E350.3 < mg/l 1 RHS 7/30/2018 Phorphorus by UV/VIS Spec. 1. Phosphorus, Total (As P) E mg/l 1 RHS 7/30/2018 Total Inorganic Nitrogen 1. Total Inorganic Nitrogen NA mg/l 1 RHS 7/30/ of 6
11 7/31/2018 Client: Cascade Thornapple River Assoc. ANALYTICAL DETAIL REPORT Sample ID Client Sample ID Matrix Date TCLP/SPLP Test Name Sampled Prep Date Analysis Date Date QC Batch Analytical Batch A Dam & Burger Water Ammonia Nitrogen 7/25/2018 R /30/2018 POTENTIAL_180730D Dam & Burger Water Anions by Ion Chromatography 7/25/2018 R /26/2018 IC_A_180726A Dam & Burger Water Coliform by Membrane 7/25/2018 Filtration R /25/2018 SCW_180725A Dam & Burger Water Phorphorus by UV/VIS Spec. 7/25/2018 R /30/2018 SPEC_A_180730A Dam & Burger Water Total Inorganic Nitrogen 7/25/2018 R /30/2018 IC_A_180726A Dam & Burger Water Total Mercury by CVAA 7/25/2018 7/26/ /26/2018 MTL_D_HY_180726A Dam & Burger Water Total Metal(s) by ICP 7/25/2018 7/27/ /27/2018 MTL_G_ICP_180727A Dam & Burger Water Volatiles by GC/MS 7/25/2018 R /26/2018 GCMS_Q_180726A A 48th & RR Water Ammonia Nitrogen 7/25/2018 R /30/2018 POTENTIAL_180730D 48th & RR Water Anions by Ion Chromatography 7/25/2018 R /26/2018 IC_A_180726A 48th & RR Water Coliform by Membrane 7/25/2018 Filtration R /25/2018 SCW_180725A 48th & RR Water Phorphorus by UV/VIS Spec. 7/25/2018 R /30/2018 SPEC_A_180730A 48th & RR Water Total Inorganic Nitrogen 7/25/2018 R /30/2018 IC_A_180726A 48th & RR Water Total Mercury by CVAA 7/25/2018 7/26/ /26/2018 MTL_D_HY_180726A 48th & RR Water Total Metal(s) by ICP 7/25/2018 7/27/ /27/2018 MTL_G_ICP_180727A 48th & RR Water Volatiles by GC/MS 7/25/2018 R /27/2018 GCMS_Q_180726A Page: 1 of 1
BIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: CTRA Project: 6454 T Lab Order: A 6454 Aqueous 3/1/2013.
Date: 08-Mar-13 Work Order Sample Summary Lab Sample ID Client Sample ID Matrix Collection Date Date Received 1303004-01A 6454 Aqueous 3/1/2013 3/1/2013 Page 1 of 1 Date: 08-Mar-13 CASE NARRATIVE Samples
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