GOLDER. Golder Associates Inc. Al-1!1f;s. golder.com. June 22, Project No
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1 GOLDER June 22, 2018 Project No Canadian Pacific Plaza Attn: Aimee Zack 120 South 6th Street Suite 700 Minneapolis, MN RE: SHOREHAM YARD-SOUTHEAST PUMP & TREAT SYSTEM MCES SPECIAL DISCHARGE PERMIT 2289 SELF-MONITORING REPORT ELECTRONIC SUBMITTAL - MAY 2018 SAMPLE RESULTS INFORMATION Dear Aimee, Enclosed are copies of the Metropolitan Council Environmental Services (MCES) Self-Monitoring Report (SMR) and attachments submitted electronically to the MCES on June 22, 2018 for the Southeast Pump & Treat System. The enclosed documents include: Sampling s SMR - May, 2018 Analytical Data from Pace Analytical Services - May, 2018 ph Field Instrument Calibration Record If you have any questions regarding these submittals please contact the undersigned at Sincerely, Golder Associates. Al-1!1f;s Alan Phillips, GIT Project Geologist ~~ Barb Johnson, P.E. Associate adp CC: Claire Mackler, Golder Golder Associates West County Road B, Suite 105 Roseville, Minnesota, USA T: Golder and the G logo are trademarks of Golder Associates Corporation golder.com
2 Metropolitan Council Environmental Services Industrial Waste & Pollution Prevention Section 390 North Robert Street St. Paul, Minnesota Submittal ID: 6497 Submittal Date: 06/22/2018 Permit No: 2289 Monitoring Point: SP-01 Sampling s SMR MCES Industrial Discharge Permit holders must complete this form for each monitoring point specified in their permit. 1. Permittee: Canadian Pacific Railway Permit No: Site Address: 28th Ave NE & Central Ave NE, MINNEAPOLIS, MN Reporting Period: No Discharge/No Sampling Quarterly Reporters: Jan-Mar, 20 X Apr-Jun, 20 Jul-Sep, 20 Oct-Dec, 20 Semi-Annual Reporters: Jan-Jun, 20 Jul-Dec, 20 Annual Reporters: Jan-Dec, Proper Sampling: Were all samples collected and composited according to permit requirements? X Yes No 5. Proper Analysis: Were analyses conducted per permit requirements? X Yes No 6. Representative Discharge: Are the analytical results representative of the wastewater discharged during this monitoring event? X Yes No 7. Compliance Status: Compare the analytical results with the corresponding discharge limits in your Permit. Do any analytical results exceed the corresponding discharge limit(s) in your Permit? Yes X No 8. General comments regarding submission: 9. Certification Statement: I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties under law for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name (print): Barb Johnson Title: bsjohnson@golder.com Phone: Page 1 of 6
3 Sample s: Submit one result sheet for each sampling day per monitoring point. Enter daily values for each sampling event from one monitoring point, in accordance with requirements in the Industrial Discharge Permit (Section B). Daily and long-term values shall be compared to Discharge Limitations in Permit Section A.1 for compliance determinations. Attach all laboratory data sheets and supporting calculations. Flow Reading Start Date End Date Discharge Volume Units Comments 5/14/ :00 AM 5/14/ :59 PM 1045 GPD Estimated discharge on day of sampling event. Sample Start Date & Time: 05/14/ :20 Sample End Date & Time: 05/14/ :20 Daily Data Form Substance Analytical Unit Reporting Limits(mg/L) Analysis Method Sample Method Bottle Container Laboratory Name ph Instantaneous 6.3 S.U. SM 4500-H+ Grab - Single NA Other Acetone < 3 ug/l 3 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Allyl chloride < 2.2 ug/l 2.2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Benzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Bromobenzene < 0.23 ug/l 0.23 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Bromochloromethane < 0.34 ug/l 0.34 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Bromodichloromethane < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Bromoform < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Bromomethane < 2.4 ug/l 2.4 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Methyl Ethtyl Ketone < 3 ug/l 3 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services n-butylbenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services sec-butylbenzene < 2.2 ug/l 2.2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services tert-butylbenzene < 0.18 ug/l 0.18 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Carbon Tetrachloride < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Chlorobenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Chloroethane < 0.37 ug/l 0.37 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Chloroform < 2.5 ug/l 2.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Chloromethane < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 2-Chlorotoluene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 4-Chlorotoluene < 0.21 ug/l 0.21 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2-Dibromo-3- chloropropane < 2.2 ug/l 2.2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Dibromochloromethane < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Page 2 of 6
4 Daily Data Form Substance Analytical Unit Reporting Limits(mg/L) Analysis Method Sample Method Bottle Container Laboratory Name 1,2-Dibromoethane (EDB) < 0.18 ug/l 0.18 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Dibromomethane < 0.43 ug/l 0.43 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2-Dichlorobenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,3-Dichlorobenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,4-Dichlorobenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Dichlorodifluoromethan e < 0.22 ug/l 0.22 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1-Dichloroethane 41.7 ug/l 0.24 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2-Dichloroethane < 0.17 ug/l 0.17 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1-Dichloroethene 14.3 ug/l 0.41 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services cis-1,2-dichloroethene 23.5 ug/l 0.26 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Trans-1, 2- Dichloroethene < 0.26 ug/l 0.26 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Dichlorofluoromethane < 0.21 ug/l 0.21 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2-Dichloropropane < 0.23 ug/l 0.23 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,3-Dichloropropane < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 2,2-Dichloropropane < 0.48 ug/l 0.48 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1-Dichloropropene < 0.44 ug/l 0.44 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services cis-1,3-dichloropropene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Trans-1, 3- Dichloropropene < 0.23 ug/l 0.23 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Ethyl Ether < 2.2 ug/l 2.2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Ethyl Benzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Hexachlorobutadiene < 2.1 ug/l 2.1 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Isopropylbenzene (cumene) < 0.14 ug/l 0.14 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services p-isopropyltoluene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Methylene Chloride < 0.23 ug/l 0.23 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 4-Methyl-2-pentanone (MIBK) Methyl Tertiary Butyl Ether (MTBE) < 2.1 ug/l 2.1 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services < 0.17 ug/l 0.17 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Naphthalene < 2.5 ug/l 2.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services n-propylbenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Styrene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1,1,2- Tetrachloroethane < 0.18 ug/l 0.18 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Page 3 of 6
5 Daily Data Form Substance Analytical Unit Reporting Limits(mg/L) Analysis Method Sample Method Bottle Container Laboratory Name 1,1,2,2- Tetrachloroethane < 0.25 ug/l 0.25 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Tetrachloroethene 149 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Tetrahydrofuran < 2 ug/l 2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Toluene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2,3-Trichlorobenzene < 2.1 ug/l 2.1 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2,4-Trichlorobenzene < 2.2 ug/l 2.2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1,1-Trichloroethane 72.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1,2-Trichloroethane < 0.2 ug/l 0.2 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Trichloroethene 9.4 ug/l 0.33 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Trichlorofluoromethane < 0.18 ug/l 0.18 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2,3-Trichloropropane < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,1,2- Trichlorotrifluoroethane < 0.81 ug/l 0.81 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,2,4-Trimethylbenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services 1,3,5-Trimethylbenzene < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Vinyl Chloride < 0.18 ug/l 0.18 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services m&p-xylenes < 1 ug/l 1 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services o-xylenes < 0.5 ug/l 0.5 EPA 8260 Grab - Single Vial - 40 ml clear Pace Analytical Services Substance Sample Col. Method Sample Col. Method Reason Sample(s) Collected By Sample(s) Composited By Compositing Method Compositing Method Reason ph Instantaneous Manually Grab samples Other Acetone Manually Grab samples Other Allyl chloride Manually Grab samples Other Benzene Manually Grab samples Other Bromobenzene Manually Grab samples Other Bromochloromethane Manually Grab samples Other Bromodichloromethane Manually Grab samples Other Bromoform Manually Grab samples Other Bromomethane Manually Grab samples Other Methyl Ethtyl Ketone Manually Grab samples Other n-butylbenzene Manually Grab samples Other sec-butylbenzene Manually Grab samples Other tert-butylbenzene Manually Grab samples Other Carbon Tetrachloride Manually Grab samples Other Page 4 of 6
6 Chlorobenzene Manually Grab samples Other Chloroethane Manually Grab samples Other Chloroform Manually Grab samples Other Chloromethane Manually Grab samples Other 2-Chlorotoluene Manually Grab samples Other 4-Chlorotoluene Manually Grab samples Other 1,2-Dibromo-3- chloropropane Manually Grab samples Other Dibromochloromethane Manually Grab samples Other 1,2-Dibromoethane (EDB) Manually Grab samples Other Dibromomethane Manually Grab samples Other 1,2-Dichlorobenzene Manually Grab samples Other 1,3-Dichlorobenzene Manually Grab samples Other 1,4-Dichlorobenzene Manually Grab samples Other Dichlorodifluoromethan e Manually Grab samples Other 1,1-Dichloroethane Manually Grab samples Other 1,2-Dichloroethane Manually Grab samples Other 1,1-Dichloroethene Manually Grab samples Other cis-1,2-dichloroethene Manually Grab samples Other Trans-1, 2- Dichloroethene Manually Grab samples Other Dichlorofluoromethane Manually Grab samples Other 1,2-Dichloropropane Manually Grab samples Other 1,3-Dichloropropane Manually Grab samples Other 2,2-Dichloropropane Manually Grab samples Other 1,1-Dichloropropene Manually Grab samples Other cis-1,3-dichloropropene Manually Grab samples Other Trans-1, 3- Dichloropropene Manually Grab samples Other Ethyl Ether Manually Grab samples Other Ethyl Benzene Manually Grab samples Other Hexachlorobutadiene Manually Grab samples Other Isopropylbenzene (cumene) Manually Grab samples Other p-isopropyltoluene Manually Grab samples Other Methylene Chloride Manually Grab samples Other 4-Methyl-2-pentanone (MIBK) Methyl Tertiary Butyl Ether (MTBE) Manually Grab samples Other Manually Grab samples Other Naphthalene Manually Grab samples Other n-propylbenzene Manually Grab samples Other Styrene Manually Grab samples Other 1,1,1,2- Tetrachloroethane 1,1,2,2- Tetrachloroethane Manually Grab samples Other Manually Grab samples Other Page 5 of 6
7 Tetrachloroethene Manually Grab samples Other Tetrahydrofuran Manually Grab samples Other Toluene Manually Grab samples Other 1,2,3-Trichlorobenzene Manually Grab samples Other 1,2,4-Trichlorobenzene Manually Grab samples Other 1,1,1-Trichloroethane Manually Grab samples Other 1,1,2-Trichloroethane Manually Grab samples Other Trichloroethene Manually Grab samples Other Trichlorofluoromethane Manually Grab samples Other 1,2,3-Trichloropropane Manually Grab samples Other 1,1,2- Trichlorotrifluoroethane Manually Grab samples Other 1,2,4-Trimethylbenzene Manually Grab samples Other 1,3,5-Trimethylbenzene Manually Grab samples Other Vinyl Chloride Manually Grab samples Other m&p-xylenes Manually Grab samples Other o-xylenes Manually Grab samples Other Page 6 of 6
8 #=CL# LIMS USE: FR - ALISON ZOLL LIMS OBJECT ID: May 18, 2018 Alison Zoll Golder Associates. 744 Broad Street 25th Floor Newark, NJ RE: Project: CP-SHOREHAM YARD Pace Project No.: Dear Alison Zoll: Enclosed are the analytical results for sample(s) received by the laboratory on May 16, The results relate only to the samples included in this report. s reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Laurie Woelfel laurie.woelfel@pacelabs.com Project Manager Enclosures cc: Kat Smith, Golder without the written consent of. Page 1 of 18
9 #=CP# CERTIFICATIONS Project: Pace Project No.: CP-SHOREHAM YARD Green Bay Certification IDs 1241 Bellevue Street, Florida/NELAP Certification #: E87948 Illinois Certification #: Kentucky UST Certification #: 82 Louisiana Certification #: Minnesota Certification #: New York Certification #: North Dakota Certification #: R-150 Virginia VELAP ID: South Carolina Certification #: Texas Certification #: T Wisconsin Certification #: Wisconsin DATCP Certification #: USDA Soil Permit #: P Federal Fish & Wildlife Permit #: LE51774A-0 without the written consent of. Page 2 of 18
10 #=SS# SAMPLE SUMMARY Project: Pace Project No.: CP-SHOREHAM YARD Lab ID Sample ID Matrix Date Collected Date Received Water 05/14/18 08:00 05/16/18 08: SE EFFLUENT Water 05/14/18 14:20 05/16/18 08:45 without the written consent of. Page 3 of 18
11 #=SA# SAMPLE ANALYTE COUNT Project: Pace Project No.: CP-SHOREHAM YARD Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260 MDS 71 PASI-G SE EFFLUENT EPA 8260 MDS 71 PASI-G without the written consent of. Page 4 of 18
12 #=AR# ANALYTICAL RESULTS Project: CP-SHOREHAM YARD Pace Project No.: Sample: Lab ID: Collected: 05/14/18 08:00 Received: 05/16/18 08:45 Matrix: Water Parameters s Units PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Acetone <3.0 ug/l /17/18 13: Allyl chloride <2.2 ug/l /17/18 13: Benzene <0.50 ug/l /17/18 13: Bromobenzene <0.23 ug/l /17/18 13: Bromochloromethane <0.34 ug/l /17/18 13: Bromodichloromethane <0.50 ug/l /17/18 13: Bromoform <0.50 ug/l /17/18 13: Bromomethane <2.4 ug/l /17/18 13: Butanone (MEK) <3.0 ug/l /17/18 13: n-butylbenzene <0.50 ug/l /17/18 13: sec-butylbenzene <2.2 ug/l /17/18 13: tert-butylbenzene <0.18 ug/l /17/18 13: Carbon tetrachloride <0.50 ug/l /17/18 13: Chlorobenzene <0.50 ug/l /17/18 13: Chloroethane <0.37 ug/l /17/18 13: Chloroform <2.5 ug/l /17/18 13: Chloromethane <0.50 ug/l /17/18 13: Chlorotoluene <0.50 ug/l /17/18 13: Chlorotoluene <0.21 ug/l /17/18 13: ,2-Dibromo-3-chloropropane <2.2 ug/l /17/18 13: Dibromochloromethane <0.50 ug/l /17/18 13: ,2-Dibromoethane (EDB) <0.18 ug/l /17/18 13: Dibromomethane <0.43 ug/l /17/18 13: ,2-Dichlorobenzene <0.50 ug/l /17/18 13: ,3-Dichlorobenzene <0.50 ug/l /17/18 13: ,4-Dichlorobenzene <0.50 ug/l /17/18 13: Dichlorodifluoromethane <0.22 ug/l /17/18 13: ,1-Dichloroethane <0.24 ug/l /17/18 13: ,2-Dichloroethane <0.17 ug/l /17/18 13: ,1-Dichloroethene <0.41 ug/l /17/18 13: cis-1,2-dichloroethene <0.26 ug/l /17/18 13: trans-1,2-dichloroethene <0.26 ug/l /17/18 13: Dichlorofluoromethane <0.21 ug/l /17/18 13: ,2-Dichloropropane <0.23 ug/l /17/18 13: L1 1,3-Dichloropropane <0.50 ug/l /17/18 13: ,2-Dichloropropane <0.48 ug/l /17/18 13: ,1-Dichloropropene <0.44 ug/l /17/18 13: cis-1,3-dichloropropene <0.50 ug/l /17/18 13: trans-1,3-dichloropropene <0.23 ug/l /17/18 13: Diethyl ether (Ethyl ether) <2.2 ug/l /17/18 13: Ethylbenzene <0.50 ug/l /17/18 13: Hexachloro-1,3-butadiene <2.1 ug/l /17/18 13: Isopropylbenzene (Cumene) <0.14 ug/l /17/18 13: p-isopropyltoluene <0.50 ug/l /17/18 13: Methylene Chloride <0.23 ug/l /17/18 13: Methyl-2-pentanone (MIBK) <2.1 ug/l /17/18 13: Date: 05/18/ :00 PM without the written consent of. Page 5 of 18
13 #=AR# ANALYTICAL RESULTS Project: CP-SHOREHAM YARD Pace Project No.: Sample: Lab ID: Collected: 05/14/18 08:00 Received: 05/16/18 08:45 Matrix: Water Parameters s Units PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Methyl-tert-butyl ether <0.17 ug/l /17/18 13: Naphthalene <2.5 ug/l /17/18 13: n-propylbenzene <0.50 ug/l /17/18 13: Styrene <0.50 ug/l /17/18 13: ,1,1,2-Tetrachloroethane <0.18 ug/l /17/18 13: ,1,2,2-Tetrachloroethane <0.25 ug/l /17/18 13: Tetrachloroethene <0.50 ug/l /17/18 13: Tetrahydrofuran <2.0 ug/l /17/18 13: Toluene <0.50 ug/l /17/18 13: ,2,3-Trichlorobenzene <2.1 ug/l /17/18 13: ,2,4-Trichlorobenzene <2.2 ug/l /17/18 13: ,1,1-Trichloroethane <0.50 ug/l /17/18 13: ,1,2-Trichloroethane <0.20 ug/l /17/18 13: Trichloroethene <0.33 ug/l /17/18 13: Trichlorofluoromethane <0.18 ug/l /17/18 13: ,2,3-Trichloropropane <0.50 ug/l /17/18 13: ,1,2-Trichlorotrifluoroethane <0.81 ug/l /17/18 13: ,2,4-Trimethylbenzene <0.50 ug/l /17/18 13: ,3,5-Trimethylbenzene <0.50 ug/l /17/18 13: Vinyl chloride <0.18 ug/l /17/18 13: m&p-xylene <1.0 ug/l /17/18 13: o-xylene <0.50 ug/l /17/18 13: Surrogates 4-Bromofluorobenzene (S) 92 % /17/18 13: Dibromofluoromethane (S) 113 % /17/18 13: Toluene-d8 (S) 103 % /17/18 13: Date: 05/18/ :00 PM without the written consent of. Page 6 of 18
14 #=AR# ANALYTICAL RESULTS Project: CP-SHOREHAM YARD Pace Project No.: Sample: SE EFFLUENT Lab ID: Collected: 05/14/18 14:20 Received: 05/16/18 08:45 Matrix: Water Parameters s Units PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Acetone <3.0 ug/l /17/18 12: Allyl chloride <2.2 ug/l /17/18 12: Benzene <0.50 ug/l /17/18 12: Bromobenzene <0.23 ug/l /17/18 12: Bromochloromethane <0.34 ug/l /17/18 12: Bromodichloromethane <0.50 ug/l /17/18 12: Bromoform <0.50 ug/l /17/18 12: Bromomethane <2.4 ug/l /17/18 12: Butanone (MEK) <3.0 ug/l /17/18 12: n-butylbenzene <0.50 ug/l /17/18 12: sec-butylbenzene <2.2 ug/l /17/18 12: tert-butylbenzene <0.18 ug/l /17/18 12: Carbon tetrachloride <0.50 ug/l /17/18 12: Chlorobenzene <0.50 ug/l /17/18 12: Chloroethane <0.37 ug/l /17/18 12: Chloroform <2.5 ug/l /17/18 12: Chloromethane <0.50 ug/l /17/18 12: Chlorotoluene <0.50 ug/l /17/18 12: Chlorotoluene <0.21 ug/l /17/18 12: ,2-Dibromo-3-chloropropane <2.2 ug/l /17/18 12: Dibromochloromethane <0.50 ug/l /17/18 12: ,2-Dibromoethane (EDB) <0.18 ug/l /17/18 12: Dibromomethane <0.43 ug/l /17/18 12: ,2-Dichlorobenzene <0.50 ug/l /17/18 12: ,3-Dichlorobenzene <0.50 ug/l /17/18 12: ,4-Dichlorobenzene <0.50 ug/l /17/18 12: Dichlorodifluoromethane <0.22 ug/l /17/18 12: ,1-Dichloroethane 41.7 ug/l /17/18 12: ,2-Dichloroethane <0.17 ug/l /17/18 12: ,1-Dichloroethene 14.3 ug/l /17/18 12: cis-1,2-dichloroethene 23.5 ug/l /17/18 12: trans-1,2-dichloroethene <0.26 ug/l /17/18 12: Dichlorofluoromethane <0.21 ug/l /17/18 12: ,2-Dichloropropane <0.23 ug/l /17/18 12: L1 1,3-Dichloropropane <0.50 ug/l /17/18 12: ,2-Dichloropropane <0.48 ug/l /17/18 12: ,1-Dichloropropene <0.44 ug/l /17/18 12: cis-1,3-dichloropropene <0.50 ug/l /17/18 12: trans-1,3-dichloropropene <0.23 ug/l /17/18 12: Diethyl ether (Ethyl ether) <2.2 ug/l /17/18 12: Ethylbenzene <0.50 ug/l /17/18 12: Hexachloro-1,3-butadiene <2.1 ug/l /17/18 12: Isopropylbenzene (Cumene) <0.14 ug/l /17/18 12: p-isopropyltoluene <0.50 ug/l /17/18 12: Methylene Chloride <0.23 ug/l /17/18 12: Methyl-2-pentanone (MIBK) <2.1 ug/l /17/18 12: Date: 05/18/ :00 PM without the written consent of. Page 7 of 18
15 #=AR# ANALYTICAL RESULTS Project: CP-SHOREHAM YARD Pace Project No.: Sample: SE EFFLUENT Lab ID: Collected: 05/14/18 14:20 Received: 05/16/18 08:45 Matrix: Water Parameters s Units PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Methyl-tert-butyl ether <0.17 ug/l /17/18 12: Naphthalene <2.5 ug/l /17/18 12: n-propylbenzene <0.50 ug/l /17/18 12: Styrene <0.50 ug/l /17/18 12: ,1,1,2-Tetrachloroethane <0.18 ug/l /17/18 12: ,1,2,2-Tetrachloroethane <0.25 ug/l /17/18 12: Tetrachloroethene 149 ug/l /17/18 12: Tetrahydrofuran <2.0 ug/l /17/18 12: Toluene <0.50 ug/l /17/18 12: ,2,3-Trichlorobenzene <2.1 ug/l /17/18 12: ,2,4-Trichlorobenzene <2.2 ug/l /17/18 12: ,1,1-Trichloroethane 72.5 ug/l /17/18 12: ,1,2-Trichloroethane <0.20 ug/l /17/18 12: Trichloroethene 9.4 ug/l /17/18 12: Trichlorofluoromethane <0.18 ug/l /17/18 12: ,2,3-Trichloropropane <0.50 ug/l /17/18 12: ,1,2-Trichlorotrifluoroethane <0.81 ug/l /17/18 12: ,2,4-Trimethylbenzene <0.50 ug/l /17/18 12: ,3,5-Trimethylbenzene <0.50 ug/l /17/18 12: Vinyl chloride <0.18 ug/l /17/18 12: m&p-xylene <1.0 ug/l /17/18 12: o-xylene <0.50 ug/l /17/18 12: Surrogates 4-Bromofluorobenzene (S) 91 % /17/18 12: Dibromofluoromethane (S) 115 % /17/18 12: Toluene-d8 (S) 96 % /17/18 12: Date: 05/18/ :00 PM without the written consent of. Page 8 of 18
16 #=QC# QUALITY CONTROL DATA Project: Pace Project No.: CP-SHOREHAM YARD QC Batch: QC Batch Method: EPA 8260 Associated Lab Samples: , Analysis Method: Analysis Description: EPA MSV METHOD BLANK: Associated Lab Samples: , Parameter Units Blank Matrix: Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/l < /17/18 09:30 1,1,1-Trichloroethane ug/l < /17/18 09:30 1,1,2,2-Tetrachloroethane ug/l < /17/18 09:30 1,1,2-Trichloroethane ug/l < /17/18 09:30 1,1,2-Trichlorotrifluoroethane ug/l < /17/18 09:30 1,1-Dichloroethane ug/l < /17/18 09:30 1,1-Dichloroethene ug/l < /17/18 09:30 1,1-Dichloropropene ug/l < /17/18 09:30 1,2,3-Trichlorobenzene ug/l < /17/18 09:30 1,2,3-Trichloropropane ug/l < /17/18 09:30 1,2,4-Trichlorobenzene ug/l < /17/18 09:30 1,2,4-Trimethylbenzene ug/l < /17/18 09:30 1,2-Dibromo-3-chloropropane ug/l < /17/18 09:30 1,2-Dibromoethane (EDB) ug/l < /17/18 09:30 1,2-Dichlorobenzene ug/l < /17/18 09:30 1,2-Dichloroethane ug/l < /17/18 09:30 1,2-Dichloropropane ug/l < /17/18 09:30 1,3,5-Trimethylbenzene ug/l < /17/18 09:30 1,3-Dichlorobenzene ug/l < /17/18 09:30 1,3-Dichloropropane ug/l < /17/18 09:30 1,4-Dichlorobenzene ug/l < /17/18 09:30 2,2-Dichloropropane ug/l < /17/18 09:30 2-Butanone (MEK) ug/l < /17/18 09:30 2-Chlorotoluene ug/l < /17/18 09:30 4-Chlorotoluene ug/l < /17/18 09:30 4-Methyl-2-pentanone (MIBK) ug/l < /17/18 09:30 Acetone ug/l < /17/18 09:30 Allyl chloride ug/l < /17/18 09:30 Benzene ug/l < /17/18 09:30 Bromobenzene ug/l < /17/18 09:30 Bromochloromethane ug/l < /17/18 09:30 Bromodichloromethane ug/l < /17/18 09:30 Bromoform ug/l < /17/18 09:30 Bromomethane ug/l < /17/18 09:30 Carbon tetrachloride ug/l < /17/18 09:30 Chlorobenzene ug/l < /17/18 09:30 Chloroethane ug/l < /17/18 09:30 Chloroform ug/l < /17/18 09:30 Chloromethane ug/l < /17/18 09:30 cis-1,2-dichloroethene ug/l < /17/18 09:30 cis-1,3-dichloropropene ug/l < /17/18 09:30 Qualifiers s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 05/18/ :00 PM without the written consent of. Page 9 of 18
17 #=QC# QUALITY CONTROL DATA Project: Pace Project No.: CP-SHOREHAM YARD METHOD BLANK: Associated Lab Samples: , Parameter Units Blank Matrix: Water Reporting Limit MDL Analyzed Dibromochloromethane ug/l < /17/18 09:30 Dibromomethane ug/l < /17/18 09:30 Dichlorodifluoromethane ug/l < /17/18 09:30 Dichlorofluoromethane ug/l < /17/18 09:30 Diethyl ether (Ethyl ether) ug/l < /17/18 09:30 Ethylbenzene ug/l < /17/18 09:30 Hexachloro-1,3-butadiene ug/l < /17/18 09:30 Isopropylbenzene (Cumene) ug/l < /17/18 09:30 m&p-xylene ug/l < /17/18 09:30 Methyl-tert-butyl ether ug/l < /17/18 09:30 Methylene Chloride ug/l < /17/18 09:30 n-butylbenzene ug/l < /17/18 09:30 n-propylbenzene ug/l < /17/18 09:30 Naphthalene ug/l < /17/18 09:30 o-xylene ug/l < /17/18 09:30 p-isopropyltoluene ug/l < /17/18 09:30 sec-butylbenzene ug/l < /17/18 09:30 Styrene ug/l < /17/18 09:30 tert-butylbenzene ug/l < /17/18 09:30 Tetrachloroethene ug/l < /17/18 09:30 Tetrahydrofuran ug/l < /17/18 09:30 Toluene ug/l < /17/18 09:30 trans-1,2-dichloroethene ug/l < /17/18 09:30 trans-1,3-dichloropropene ug/l < /17/18 09:30 Trichloroethene ug/l < /17/18 09:30 Trichlorofluoromethane ug/l < /17/18 09:30 Vinyl chloride ug/l < /17/18 09:30 4-Bromofluorobenzene (S) % /17/18 09:30 Dibromofluoromethane (S) % /17/18 09:30 Toluene-d8 (S) % /17/18 09:30 Qualifiers LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS LCS % Rec % Rec Limits 1,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1,2-Trichlorotrifluoroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,4-Trichlorobenzene ug/l ,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l Qualifiers s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 05/18/ :00 PM without the written consent of. Page 10 of 18
18 #=QC# QUALITY CONTROL DATA Project: Pace Project No.: CP-SHOREHAM YARD LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS LCS % Rec % Rec Limits 1,2-Dichloroethane ug/l ,2-Dichloropropane ug/l L1 1,3-Dichlorobenzene ug/l ,4-Dichlorobenzene ug/l Benzene ug/l Bromodichloromethane ug/l Bromoform ug/l Bromomethane ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dichlorodifluoromethane ug/l Ethylbenzene ug/l Isopropylbenzene (Cumene) ug/l m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl chloride ug/l Bromofluorobenzene (S) % Dibromofluoromethane (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l < ,1,2-Trichloroethane ug/l < ,1,2-Trichlorotrifluoroethane ug/l < ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 05/18/ :00 PM without the written consent of. Page 11 of 18
19 #=QC# QUALITY CONTROL DATA Project: Pace Project No.: CP-SHOREHAM YARD MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,2,4-Trichlorobenzene ug/l < ,2-Dibromo-3- ug/l < chloropropane 1,2-Dibromoethane (EDB) ug/l < ,2-Dichlorobenzene ug/l < ,2-Dichloroethane ug/l < ,2-Dichloropropane ug/l < ,3-Dichlorobenzene ug/l < ,4-Dichlorobenzene ug/l < Benzene ug/l < Bromodichloromethane ug/l < Bromoform ug/l < Bromomethane ug/l < Carbon tetrachloride ug/l < Chlorobenzene ug/l < Chloroethane ug/l < Chloroform ug/l < Chloromethane ug/l < cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l < Dibromochloromethane ug/l < Dichlorodifluoromethane ug/l < Ethylbenzene ug/l < Isopropylbenzene (Cumene) ug/l < m&p-xylene ug/l < Methyl-tert-butyl ether ug/l < Methylene Chloride ug/l < o-xylene ug/l < Styrene ug/l < Tetrachloroethene ug/l Toluene ug/l < trans-1,2-dichloroethene ug/l < trans-1,3-dichloropropene ug/l < Trichloroethene ug/l Trichlorofluoromethane ug/l < Vinyl chloride ug/l < Bromofluorobenzene (S) % Dibromofluoromethane (S) % Toluene-d8 (S) % Qual s presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 05/18/ :00 PM without the written consent of. Page 12 of 18
20 #=QL# QUALIFIERS Project: Pace Project No.: CP-SHOREHAM YARD DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-G Pace Analytical Services - Green Bay ANALYTE QUALIFIERS L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. s may be biased high. Date: 05/18/ :00 PM without the written consent of. Page 13 of 18
21 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: CP-SHOREHAM YARD Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch EPA SE EFFLUENT EPA Date: 05/18/ :00 PM without the written consent of. Page 14 of 18
22 Company Name: Branch/location: Contact: Phone: Project Number: Project Name: CUSTOD preservation Codes A=None B=HCL C=H2S04 D=HN03 E=DI Water F=Methanol G=NaOH H::::Sodium Bisulfate Solution!::;;Sodium Thiosulfate J=Other UPPER MIDWEST REGION Miii: WI: Quote#: Mail To Contact: Mail To Company: Mail To Address: Page of Page 15 of 18 Project State: FILTERED? (YES/NO) Sampled By (Print}: PRESERVATION (CODE)* Invoice To Contact: Sampled By (Sign): Invoice To Company: PO#: Regulatory Program: Invoice To Address: Matrix Codes NOT needed on your sample A""Air 8 Biota C =Charcoal O=Oil SW = Surface Water Invoice To Phone: CUE NT COMMENTS LAB COMMENTS Use Only) Profile# Rush Turnaround Time Requested - Prelims TAT subject to approval/surcharge) Date Needed: (complete you want):
23 /,.1/i#r':,;:t' Document Name: Revised Date: 13Feb2018 Minneapolis Cooler Transfer Check List Page 1 of 1. Pace Analytical Document Number: Issuing Authority: F-MN-C-214-Rev.02 Pace Minnesota Quality Office Minneapolis Service Center Cooler Transfer Check List Client: L{of '7qf&3 Destination Lab: Received with Custody Seal: Custody Seal Intact: Yes Temp Read Corrected Temp Correction Factor Temperature C: to//) ~ +~ IR Gun: Samples on ice, cooling process has begun Rush/Short Hold: Nft Containers Intact: No Re-packed and Re-Iced: Temp Blank No Shipped By/Date: Lts;\ &Jf(~{( Notes: Page 16 of 18
24 l i Go/le,.-- All containers needing preservation have been checked and noted below: oyes ono ~A Client Name: Lab Lot# of ph paper: Sample Preservation Receipt Form Project # '-{ 0 { [{; C} /lo 3 Lab Std #ID of preservation (if ph adjusted): e Plastic ~ 1 I ;- -c;;~~;~~~ E Glass Vials i Jars <O I ~ ::J ::J ii; ::J :J: Cf) ::J ::J Cf) ::J "' ::J z ::J (.) z Cf) <C I- ::J :J: :ii c ::J LL I- 0 Pace... "I:!' "I:!' I() N M... N N M M M M en en en en en en LL LL I()..J > (!) a. a. a. a. a. a. a. (!) (!) ~ ~ ~ ~ ~ ~ g g g g (!) <( lab# a. z III III III III III III III III c c..., ~ ~ Cf) ~ Cl e 001 ;:;..... I :;: : c.: :. /. ~!f"' ''....:: ; : : <..,: 1. :.. : :. : :... N VI J: c. v 0 (/) ~.. : Initial when completed: ()') Ill J: c. ti N <( Ai c: N J: + c. I I 0 0 <11 ~ "7 'VI J: c. ("') 0 ~ 1241 Bellevue Street, Suite 9 : 2.5I5I i :. :! :.; :. :.. 1 :. ' : ''i.5/f//iq / 5/ :.... : : 004 :1 : :.....,..!. ;. :... : : > ; : >.. ::.. 11 : : { :: I : > '[ ${1;ifl''!. l1ji / 5I :..:... ; : h. :: ::..... :.. r i.... :. ::......: :,. I I5I10. : :.. : :.. :... ; i ;,... :.. : ~ : : :.. I r ::. r:~,,,>::. r ~:.. 't!f//:5 1: I5I10 I 010 :. J: :. :.. :. : / T.. '...(i" : :.... : ''7 i, I;. : f 3"\ 011 ':.~! I.?-:;.';> :;;'.:> /.i1{j 2.5I5I : I :. : : :. :.. : :. > :.... :... r: Z ; : : f ; c ;: :... 'j r. ::,' ; 2.~1r:.'f I5I10...; 014 : : :' :, :. 1' :...: : 1.1~ ;. ': :.. ~ :.!C,:'?>).!.:'; i:.:!s;/: : :... : <,. : : :.. '. '.. 1/.. 2.s I 5I10 :... ';.. '' : Ii. ' t!.;,.: :.. :,:!..:..;.. '/ Z::'.:>'1b'f10' I5I : ;..,.... ;.:. : :. ".; :..' 1:... :';. ' 1:/2 k2';s1t.~/ I5I10 : 020. i. : :; y :;<: Date/ Time: "O Q) (;) :;i ::0 <11 Qi = <11 ~ Volume (ml) 1, { : :: '>' :: :.'... :...,;7 r t?...;. ; : :i i'f ';\ ~i~ ~'.S.f 10. ~\ : :.. :.... Page 17 of 18 Exceptions to preservation chef. V~fcoliform, TOC, TOX, TOH, O&G, WI ORO, Phenolics, Other: Headspace in VOA Vials (>6mm) : oyes ;Ao on/a *If yes look in headspace column AGlU 1 liter amber glass BPlU 1 liter plastic unpres DG9A 40 ml amber ascorbic JGFU 4 oz amber jar unpres AGlH 1 liter amber glass HCl BP2N 500 ml plastic HN03 DG9T 40 ml amber Na Thio WGFU 4 oz clear jar unpres AG4S 125 ml amber glass H2S04 BP2Z 500 ml plastic NaOH, Znact VG9U 40 ml clear vial unpres WPFU 4 oz plastic jar unpres AG4U 120 ml amber glass unpres BP3U 250 ml plastic unpres VG9H 40 ml clear vial HCl AGSU 100 ml amber glass unpres BP3C 250 ml plastic NaOH VG9M 40 ml clear vial MeOH SPST 120 ml plastic Na Thiosulfate AG2S 500 ml amber glass H2S04 BP3N 250 ml plastic HN03 VG9D 40 ml clear vial DI ZPLC ziploc bag BG3U 250 ml clear glass unpres BP3S 250 ml plastic H2S04 GN: Page 1.. of z.. F-GB-C-046-Rev.02 (29Mar2018) Sample Preservation Receipt Form
25 µanalytlcat Document Name: Document Revised: 25Apr2018 Sample Condition Upon Receipt (SCUR) Document No.: Issuing Authority: 1241 Bellevue Street, Green Bay WI F-GB-C-031-Rev.07 Pace Green Bay Quality Office Client Name: Sample Condition Upon Receipt Form (SCUR) Go/Jer Project Courier: r CS Logistics r Fed Ex r Speedee r Client r; Pace Other: r UPS (1 Waltco Tracking#: ---~-~~~~-~~--~-~~~~~ Custody Seal on Cooler/Box Present: 17"yes r no Seals intact: Y yes r no Custody Seal on Samples Present: r yes r: no Seals intact: r yes r no Packing Material: ~Bubble WFc!/!!j j7 Bubble Bags r None r Other Thermometer Used SR - -, Type of Ice~ Blue Dry None Cooler Temperature Uncorr: d 5/corr: 3 ~ Temp Blank Present: rjyes pno Biological Tissue is Frozen: r yes r no Temp should be above freezing to 6 C. Biota Samples may be received at s o c. Chain of Custody Present: i/ves 0No ON/A 1. Chain of Custody Filled Out: iz{yes 0No ON/A 2. Chain of Custody Relinquished: [j{es 0No ON/A 3. Sampler Name & Signature on COC: Jzfves 0No ON/A 4. Samples Arrived within Hold Time:,...Jlfves 0No 5. - VOA Samples frozen upon receipt OYes 0No Date/Time: Short Hold Time Analysis (<72hr): 0Yes Jl/No 6. Rush Turn Around Time Requested: OYes iefno 7. Sufficient Volume: 8. For Analysis: es ONo MS/MSD: 0Yes l'.j'~o ON/A Correct Containers Used: Aves 0No 9. -Pace Containers Used: -Pace IR Containers Used: '6'ves 0No ON/A 0Yes ONo l'.'.lnta Containers Intact: r/ves ONo 10. Filtered volume received for Dissolved tests WO 0Yes ONo ~A 11. Sample Labels match COC: ON/A 12. -lndudes date/time/id/analysis Matrix: Trip Blank Present: ~Yes ONo ON/A 13. Trip Blank Custody Seals Present /l1es ONo ON/A #:I W0#: (77 Samples on ice, cooling process has begun :a~~~os~~) Pace Trip Blank Lot# (if purchased): Client Notification/ Resolution: If checked, see attached form for additional comments LJ Person Contacted: Date/Time: Comments/ Resolution: Initials: b Project Manager Review: Date: {j I (.e \ J. Paged-~ Page 18 of 18
26 GOLDER Page _l_of_l_ Field Instrument ph Calibration Records INSTRUMENT (MAKE/MODEL NO.) Sper Scientific/ STANDARD INFORMATION INSTRUMENT NO. Project Number:,;;;0~23;;..;;;;.6...;;..;;10;;..;;;; ;1~8 Project Name: GP-Shoreham Yard Standard Vendor: Field Environmental Instruments Prepared Date: NA Where Prepared: NA Purchase Date: Varies Expiration Date: Varies Grade: NIA Units: Standard Units Standard 4.0 c Lot# Ex~ Date 04/14/19 Standard 7.0 c Lot# Ex~ Date 09/01/19 Standard 10.0 c Lot# Ex~ Date 08/01/19 DATE TIME TEMP STD INSTRUMENT PASS/ CALIBRATED SAMPLER %DEV (mm/dd/yy} (hr: min} DEGC VALUE RESPONSE FAIL (YES, NO) INITIALS 2./ /'-f/18 rrso W.5 l.lj F y # ( /(f_ 2/1 '1 /I~ /'~T'6 t6.r ~-r.o Li.O C) f ~ 2-/ t ~ /\~ 160~ L~ y [OrO f {)c0 0 ~ t ff 3,//1//1 (~"->7 I '1. 5" 7.o p ~./Jf) ')//)//$ '' 11~ /''1. ) Y,u 'i, O v p i J-(J 3//'))/( ('11' 1~ - 0 t ~ ~0 ll0-0 0 f '\'. 1-1' ~/i6/1~ t n_o ~,s- 7,_0 7,o t> p v l +VJ '3/t6i1~ l)l) -~.o \_e) ~'-0 0 r \(,t-f ~/L4/(~ 1)3) 7. ) l O ~ CJ ~o~o 0 f I yf-fj ~n ~111 If '>Cf \Lo 7.o?.Q a- p '1 H 'i/l~//1 '2.cJ.1 \lo L(J' (J L( "o f '1 If# ~/l<j/f ( 2.Cf J'l 'I \ o. c) lo. d 0 f' I H ~I H\f t'( 1~ )(._ tr.o 7~0 7.. () 0 f' y H ~ 12-i/l f l '1 '10 tr.. o 'to ' p y Jff "\\~'\{Li l~ "'' 1'1.) Io.~ ff.o C) p y (11 5ft'1i Ii I. ti ~O 2-1.'(' 7J) 1 '1 0 6 {J y 411 1/f'\/{1 \ '-\ 3~ L '5"". O '1,() 'l,,d 0 fj 'L l1 }//'1,,., l ~\Ji 2S-O {0.0 l <9.. Q a y; ~ /rfj ' S/L~/16 Proo 2-t,1 7.0 p 7.. () 6 ~ t1-p IJ/l'/I~ l en>1 c\.() ~. () l..f1.0 0 f 'f ffi~ T/ll/fl /'f/l 2.0.') I <9. 0 lo.a " f r. ~ Acceptable calibration check is if the meter reads within +/- 0.2 ph units of the value of appropriate calibration standard. \\IVUN 1-V-FS I \Projects\Golder Projects\023 PROJECTS\ Shoreham Yard File Revicw\East Side Southeast P&T System\Data\2018\pH _Calibration Fonn.doc Golder Associates REV-2-03/07
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