APPENDIX D Laboratory Analytical Reports
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1 Allied Aviation Initial Abatement Report, Arlington, VA December 4, 2015 Amec Foster Wheeler Project APPENDIX D Laboratory Analytical Reports
2 #=CL# LIMS USE: FR - JOHN MITTAUER LIMS OBJECT ID: November 05, 2015 John Mittauer Amec Foster Wheeler Albemarle Point Place Suite 115 Chantilly, VA RE: Dear John Mittauer: Enclosed are the analytical results for sample(s) received by the laboratory on November 03, The results relate only to the samples included in this report. s reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Page 1 of 20
3 #=CP# CERTIFICATIONS Charlotte Certification IDs 9800 Kincey Ave. Ste 100, North Carolina Drinking Water Certification #: North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: Page 2 of 20
4 #=SS# SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received 001 FOUR MILE - A Water 10/31/15 09:30 11/03/15 09: FOUR MILE - B Water 10/31/15 09:35 11/03/15 09: FOUR MILE - C Water 10/31/15 09:45 11/03/15 09: FOUR MILE - D Water 10/31/15 09:55 11/03/15 09: FOUR MILE - E Water 10/31/15 10:05 11/03/15 09: OUTFALL 18 BOOM Water 10/31/15 10:45 11/03/15 09:30 Page 3 of 20
5 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory 001 FOUR MILE - A EPA 8015 Modified BJL EPA 5030/8015 Mod. ZDO EPA 8270 RES 21 PASI-C EPA 8260 NB 9 PASI-C 002 FOUR MILE - B EPA 8015 Modified BJL EPA 5030/8015 Mod. ZDO EPA 8270 RES 21 PASI-C EPA 8260 NB 9 PASI-C 003 FOUR MILE - C EPA 8015 Modified BJL EPA 5030/8015 Mod. ZDO EPA 8270 RES 21 PASI-C EPA 8260 NB 9 PASI-C 004 FOUR MILE - D EPA 8015 Modified BJL EPA 5030/8015 Mod. ZDO EPA 8270 RES 21 PASI-C EPA 8260 NB 9 PASI-C 005 FOUR MILE - E EPA 8015 Modified BJL EPA 5030/8015 Mod. ZDO EPA 8270 RES 21 PASI-C EPA 8260 NB 9 PASI-C 006 OUTFALL 18 BOOM EPA 8015 Modified BJL EPA 5030/8015 Mod. ZDO EPA 8270 RES 21 PASI-C EPA 8260 NB 9 PASI-C Page 4 of 20
6 #=AR# ANALYTICAL RESULTS Sample: FOUR MILE - A Lab ID: 001 Collected: 10/31/15 09:30 Received: 11/03/15 09:30 Matrix: Water Report s s Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510 Diesel Range Organics(C10- ND mg/l /04/15 09:30 11/04/15 17:56 C28) n-pentacosane (S) 93 % /04/15 09:30 11/04/15 17: Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod. Gas Range Organics (C6-C10) J mg/l /03/15 21:05 4-Bromofluorobenzene (S) 92 % /03/15 21: MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/l /04/15 10:30 11/04/15 15: Acenaphthylene ND ug/l /04/15 10:30 11/04/15 15: Anthracene ND ug/l /04/15 10:30 11/04/15 15: Benzo(a)anthracene ND ug/l /04/15 10:30 11/04/15 15: Benzo(a)pyrene ND ug/l /04/15 10:30 11/04/15 15: Benzo(b)fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Benzo(g,h,i)perylene ND ug/l /04/15 10:30 11/04/15 15: Benzo(k)fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Chrysene ND ug/l /04/15 10:30 11/04/15 15: Dibenz(a,h)anthracene ND ug/l /04/15 10:30 11/04/15 15: Fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Fluorene ND ug/l /04/15 10:30 11/04/15 15: Indeno(1,2,3-cd)pyrene ND ug/l /04/15 10:30 11/04/15 15: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 15: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 15: Naphthalene ND ug/l /04/15 10:30 11/04/15 15: Phenanthrene ND ug/l /04/15 10:30 11/04/15 15: Pyrene ND ug/l /04/15 10:30 11/04/15 15: Nitrobenzene-d5 (S) 27 % /04/15 10:30 11/04/15 15: Fluorobiphenyl (S) 27 % /04/15 10:30 11/04/15 15: Terphenyl-d14 (S) 42 % /04/15 10:30 11/04/15 15: MSV Low Level Analytical Method: EPA 8260 Benzene ND ug/l /04/15 20: Ethylbenzene ND ug/l /04/15 20: Toluene ND ug/l /04/15 20: Xylene (Total) ND ug/l /04/15 20: m&p-xylene ND ug/l /04/15 20: o-xylene ND ug/l /04/15 20: Bromofluorobenzene (S) 100 % /04/15 20: ,2-Dichloroethane-d4 (S) 118 % /04/15 20: Toluene-d8 (S) 103 % /04/15 20: Page 5 of 20
7 #=AR# ANALYTICAL RESULTS Sample: FOUR MILE - B Lab ID: 002 Collected: 10/31/15 09:35 Received: 11/03/15 09:30 Matrix: Water Report s s Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510 Diesel Range Organics(C10- ND mg/l /04/15 09:30 11/04/15 18:20 C28) n-pentacosane (S) 70 % /04/15 09:30 11/04/15 18: Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod. Gas Range Organics (C6-C10) J mg/l /03/15 21:27 4-Bromofluorobenzene (S) 94 % /03/15 21: MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/l /04/15 10:30 11/04/15 15: Acenaphthylene ND ug/l /04/15 10:30 11/04/15 15: Anthracene ND ug/l /04/15 10:30 11/04/15 15: Benzo(a)anthracene ND ug/l /04/15 10:30 11/04/15 15: Benzo(a)pyrene ND ug/l /04/15 10:30 11/04/15 15: Benzo(b)fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Benzo(g,h,i)perylene ND ug/l /04/15 10:30 11/04/15 15: Benzo(k)fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Chrysene ND ug/l /04/15 10:30 11/04/15 15: Dibenz(a,h)anthracene ND ug/l /04/15 10:30 11/04/15 15: Fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Fluorene ND ug/l /04/15 10:30 11/04/15 15: Indeno(1,2,3-cd)pyrene ND ug/l /04/15 10:30 11/04/15 15: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 15: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 15: Naphthalene ND ug/l /04/15 10:30 11/04/15 15: Phenanthrene ND ug/l /04/15 10:30 11/04/15 15: Pyrene ND ug/l /04/15 10:30 11/04/15 15: Nitrobenzene-d5 (S) 67 % /04/15 10:30 11/04/15 15: Fluorobiphenyl (S) 64 % /04/15 10:30 11/04/15 15: Terphenyl-d14 (S) 51 % /04/15 10:30 11/04/15 15: MSV Low Level Analytical Method: EPA 8260 Benzene ND ug/l /04/15 20: Ethylbenzene ND ug/l /04/15 20: Toluene ND ug/l /04/15 20: Xylene (Total) ND ug/l /04/15 20: m&p-xylene ND ug/l /04/15 20: o-xylene ND ug/l /04/15 20: Bromofluorobenzene (S) 100 % /04/15 20: ,2-Dichloroethane-d4 (S) 117 % /04/15 20: Toluene-d8 (S) 104 % /04/15 20: Page 6 of 20
8 #=AR# ANALYTICAL RESULTS Sample: FOUR MILE - C Lab ID: 003 Collected: 10/31/15 09:45 Received: 11/03/15 09:30 Matrix: Water Report s s Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510 Diesel Range Organics(C10- ND mg/l /04/15 09:30 11/04/15 18:20 C28) n-pentacosane (S) 71 % /04/15 09:30 11/04/15 18: Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod. Gas Range Organics (C6-C10) J mg/l /03/15 21:50 4-Bromofluorobenzene (S) 91 % /03/15 21: MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/l /04/15 10:30 11/04/15 15: Acenaphthylene ND ug/l /04/15 10:30 11/04/15 15: Anthracene ND ug/l /04/15 10:30 11/04/15 15: Benzo(a)anthracene ND ug/l /04/15 10:30 11/04/15 15: Benzo(a)pyrene ND ug/l /04/15 10:30 11/04/15 15: Benzo(b)fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Benzo(g,h,i)perylene ND ug/l /04/15 10:30 11/04/15 15: Benzo(k)fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Chrysene ND ug/l /04/15 10:30 11/04/15 15: Dibenz(a,h)anthracene ND ug/l /04/15 10:30 11/04/15 15: Fluoranthene ND ug/l /04/15 10:30 11/04/15 15: Fluorene ND ug/l /04/15 10:30 11/04/15 15: Indeno(1,2,3-cd)pyrene ND ug/l /04/15 10:30 11/04/15 15: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 15: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 15: Naphthalene ND ug/l /04/15 10:30 11/04/15 15: Phenanthrene ND ug/l /04/15 10:30 11/04/15 15: Pyrene ND ug/l /04/15 10:30 11/04/15 15: Nitrobenzene-d5 (S) 80 % /04/15 10:30 11/04/15 15: Fluorobiphenyl (S) 75 % /04/15 10:30 11/04/15 15: Terphenyl-d14 (S) 66 % /04/15 10:30 11/04/15 15: MSV Low Level Analytical Method: EPA 8260 Benzene ND ug/l /04/15 21: Ethylbenzene ND ug/l /04/15 21: Toluene ND ug/l /04/15 21: Xylene (Total) ND ug/l /04/15 21: m&p-xylene ND ug/l /04/15 21: o-xylene 0.38J ug/l /04/15 21: Bromofluorobenzene (S) 99 % /04/15 21: ,2-Dichloroethane-d4 (S) 119 % /04/15 21: Toluene-d8 (S) 103 % /04/15 21: Page 7 of 20
9 #=AR# ANALYTICAL RESULTS Sample: FOUR MILE - D Lab ID: 004 Collected: 10/31/15 09:55 Received: 11/03/15 09:30 Matrix: Water Report s s Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510 Diesel Range Organics(C10- ND mg/l /04/15 09:30 11/04/15 18:43 C28) n-pentacosane (S) 80 % /04/15 09:30 11/04/15 18: Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod. Gas Range Organics (C6-C10) 0.021J mg/l /03/15 22:12 4-Bromofluorobenzene (S) 94 % /03/15 22: MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/l /04/15 10:30 11/04/15 16: Acenaphthylene ND ug/l /04/15 10:30 11/04/15 16: Anthracene ND ug/l /04/15 10:30 11/04/15 16: Benzo(a)anthracene ND ug/l /04/15 10:30 11/04/15 16: Benzo(a)pyrene ND ug/l /04/15 10:30 11/04/15 16: Benzo(b)fluoranthene ND ug/l /04/15 10:30 11/04/15 16: Benzo(g,h,i)perylene ND ug/l /04/15 10:30 11/04/15 16: Benzo(k)fluoranthene ND ug/l /04/15 10:30 11/04/15 16: Chrysene ND ug/l /04/15 10:30 11/04/15 16: Dibenz(a,h)anthracene ND ug/l /04/15 10:30 11/04/15 16: Fluoranthene ND ug/l /04/15 10:30 11/04/15 16: Fluorene ND ug/l /04/15 10:30 11/04/15 16: Indeno(1,2,3-cd)pyrene ND ug/l /04/15 10:30 11/04/15 16: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 16: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 16: Naphthalene ND ug/l /04/15 10:30 11/04/15 16: Phenanthrene ND ug/l /04/15 10:30 11/04/15 16: Pyrene ND ug/l /04/15 10:30 11/04/15 16: Nitrobenzene-d5 (S) 76 % /04/15 10:30 11/04/15 16: Fluorobiphenyl (S) 77 % /04/15 10:30 11/04/15 16: Terphenyl-d14 (S) 65 % /04/15 10:30 11/04/15 16: MSV Low Level Analytical Method: EPA 8260 Benzene ND ug/l /04/15 21: Ethylbenzene ND ug/l /04/15 21: Toluene ND ug/l /04/15 21: Xylene (Total) ND ug/l /04/15 21: m&p-xylene ND ug/l /04/15 21: o-xylene 0.36J ug/l /04/15 21: Bromofluorobenzene (S) 101 % /04/15 21: ,2-Dichloroethane-d4 (S) 118 % /04/15 21: Toluene-d8 (S) 103 % /04/15 21: Page 8 of 20
10 #=AR# ANALYTICAL RESULTS Sample: FOUR MILE - E Lab ID: 005 Collected: 10/31/15 10:05 Received: 11/03/15 09:30 Matrix: Water Report s s Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510 Diesel Range Organics(C10- ND mg/l /04/15 09:30 11/04/15 18:43 C28) n-pentacosane (S) 94 % /04/15 09:30 11/04/15 18: Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod. Gas Range Organics (C6-C10) 0.014J mg/l /03/15 22:35 4-Bromofluorobenzene (S) 91 % /03/15 22: MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/l /04/15 10:30 11/04/15 16: Acenaphthylene ND ug/l /04/15 10:30 11/04/15 16: Anthracene ND ug/l /04/15 10:30 11/04/15 16: Benzo(a)anthracene ND ug/l /04/15 10:30 11/04/15 16: Benzo(a)pyrene ND ug/l /04/15 10:30 11/04/15 16: Benzo(b)fluoranthene ND ug/l /04/15 10:30 11/04/15 16: Benzo(g,h,i)perylene ND ug/l /04/15 10:30 11/04/15 16: Benzo(k)fluoranthene ND ug/l /04/15 10:30 11/04/15 16: Chrysene ND ug/l /04/15 10:30 11/04/15 16: Dibenz(a,h)anthracene ND ug/l /04/15 10:30 11/04/15 16: Fluoranthene ND ug/l /04/15 10:30 11/04/15 16: Fluorene ND ug/l /04/15 10:30 11/04/15 16: Indeno(1,2,3-cd)pyrene ND ug/l /04/15 10:30 11/04/15 16: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 16: Methylnaphthalene ND ug/l /04/15 10:30 11/04/15 16: Naphthalene ND ug/l /04/15 10:30 11/04/15 16: Phenanthrene ND ug/l /04/15 10:30 11/04/15 16: Pyrene ND ug/l /04/15 10:30 11/04/15 16: Nitrobenzene-d5 (S) 74 % /04/15 10:30 11/04/15 16: Fluorobiphenyl (S) 72 % /04/15 10:30 11/04/15 16: Terphenyl-d14 (S) 65 % /04/15 10:30 11/04/15 16: MSV Low Level Analytical Method: EPA 8260 Benzene ND ug/l /04/15 21: Ethylbenzene ND ug/l /04/15 21: Toluene ND ug/l /04/15 21: Xylene (Total) ND ug/l /04/15 21: m&p-xylene ND ug/l /04/15 21: o-xylene ND ug/l /04/15 21: Bromofluorobenzene (S) 101 % /04/15 21: ,2-Dichloroethane-d4 (S) 120 % /04/15 21: Toluene-d8 (S) 103 % /04/15 21: Page 9 of 20
11 #=AR# ANALYTICAL RESULTS Sample: OUTFALL 18 BOOM Lab ID: 006 Collected: 10/31/15 10:45 Received: 11/03/15 09:30 Matrix: Water Report s s Limit MDL DF Prepared Analyzed CAS No. Qual 8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3510 Diesel Range Organics(C mg/l /04/15 09:30 11/04/15 19:07 C28) n-pentacosane (S) 75 % /04/15 09:30 11/04/15 19: Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod. Gas Range Organics (C6-C10) 0.016J mg/l /03/15 22:57 4-Bromofluorobenzene (S) 93 % /03/15 22: MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/l /04/15 10:30 11/04/15 17: Acenaphthylene ND ug/l /04/15 10:30 11/04/15 17: Anthracene ND ug/l /04/15 10:30 11/04/15 17: Benzo(a)anthracene ND ug/l /04/15 10:30 11/04/15 17: Benzo(a)pyrene ND ug/l /04/15 10:30 11/04/15 17: Benzo(b)fluoranthene ND ug/l /04/15 10:30 11/04/15 17: Benzo(g,h,i)perylene ND ug/l /04/15 10:30 11/04/15 17: Benzo(k)fluoranthene ND ug/l /04/15 10:30 11/04/15 17: Chrysene ND ug/l /04/15 10:30 11/04/15 17: Dibenz(a,h)anthracene ND ug/l /04/15 10:30 11/04/15 17: Fluoranthene ND ug/l /04/15 10:30 11/04/15 17: Fluorene ND ug/l /04/15 10:30 11/04/15 17: Indeno(1,2,3-cd)pyrene ND ug/l /04/15 10:30 11/04/15 17: Methylnaphthalene 13.5 ug/l /04/15 10:30 11/04/15 17: Methylnaphthalene 15.9 ug/l /04/15 10:30 11/04/15 17: Naphthalene 4.6J ug/l /04/15 10:30 11/04/15 17: Phenanthrene ND ug/l /04/15 10:30 11/04/15 17: Pyrene ND ug/l /04/15 10:30 11/04/15 17: Nitrobenzene-d5 (S) 79 % /04/15 10:30 11/04/15 17: Fluorobiphenyl (S) 79 % /04/15 10:30 11/04/15 17: Terphenyl-d14 (S) 80 % /04/15 10:30 11/04/15 17: MSV Low Level Analytical Method: EPA 8260 Benzene ND ug/l /04/15 21: Ethylbenzene ND ug/l /04/15 21: Toluene ND ug/l /04/15 21: Xylene (Total) ND ug/l /04/15 21: m&p-xylene 0.75J ug/l /04/15 21: o-xylene 0.52J ug/l /04/15 21: Bromofluorobenzene (S) 99 % /04/15 21: ,2-Dichloroethane-d4 (S) 120 % /04/15 21: Toluene-d8 (S) 103 % /04/15 21: Page 10 of 20
12 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: GCV/10039 EPA 5030/8015 Mod. Analysis Method: Analysis Description: EPA 5030/8015 Mod. Gasoline Range Organics Associated Lab Samples: 001, 002, 003, 004, 005, 006 METHOD BLANK: Associated Lab Samples: 001, 002, 003, 004, 005, 006 Blank Matrix: Water Reporting Limit MDL Analyzed Gas Range Organics (C6-C10) mg/l 0.014J /03/15 17:12 4-Bromofluorobenzene (S) % /03/15 17:12 LABORATORY CONTROL SAMPLE: Spike Conc. LCS LCS Limits Gas Range Organics (C6-C10) mg/l Bromofluorobenzene (S) % MATRIX SPIKE SAMPLE: Spike Conc. MS MS Limits Gas Range Organics (C6-C10) mg/l ND Bromofluorobenzene (S) % SAMPLE DUPLICATE: Dup Gas Range Organics (C6-C10) mg/l ND 0.011J 30 4-Bromofluorobenzene (S) % RPD Max RPD s presented on this page are in the units indicated by the "" column except where an alternate unit is presented to the right of the result. Page 11 of 20
13 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MSV/34136 EPA 8260 Analysis Method: Analysis Description: EPA MSV Low Level Associated Lab Samples: 001, 002, 003, 004, 005, 006 METHOD BLANK: Associated Lab Samples: 001, 002, 003, 004, 005, 006 Blank Matrix: Water Reporting Limit MDL Analyzed Benzene ug/l ND /04/15 12:09 Ethylbenzene ug/l ND /04/15 12:09 m&p-xylene ug/l ND /04/15 12:09 o-xylene ug/l ND /04/15 12:09 Toluene ug/l ND /04/15 12:09 Xylene (Total) ug/l ND /04/15 12:09 1,2-Dichloroethane-d4 (S) % /04/15 12:09 4-Bromofluorobenzene (S) % /04/15 12:09 Toluene-d8 (S) % /04/15 12:09 LABORATORY CONTROL SAMPLE: Spike Conc. LCS LCS Limits Benzene ug/l Ethylbenzene ug/l m&p-xylene ug/l o-xylene ug/l Toluene ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % MATRIX SPIKE SAMPLE: Spike Conc. MS MS Limits Benzene ug/l ND Ethylbenzene ug/l m&p-xylene ug/l ND o-xylene ug/l ND Toluene ug/l ND ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % s presented on this page are in the units indicated by the "" column except where an alternate unit is presented to the right of the result. Page 12 of 20
14 #=QC# QUALITY CONTROL DATA SAMPLE DUPLICATE: Dup Benzene ug/l Ethylbenzene ug/l ND ND 30 m&p-xylene ug/l o-xylene ug/l Toluene ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % RPD Max RPD s presented on this page are in the units indicated by the "" column except where an alternate unit is presented to the right of the result. Page 13 of 20
15 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: OEXT/38811 EPA 3510 Analysis Method: Analysis Description: EPA 8015 Modified 8015 GCS Associated Lab Samples: 001, 002, 003, 004, 005, 006 METHOD BLANK: Associated Lab Samples: 001, 002, 003, 004, 005, 006 Blank Matrix: Water Reporting Limit MDL Analyzed Diesel Range Organics(C10-C28) mg/l 0.18J /03/15 16:48 n-pentacosane (S) % /03/15 16:48 LABORATORY CONTROL SAMPLE: Spike Conc. LCS LCS Limits Diesel Range Organics(C10-C28) mg/l n-pentacosane (S) % MATRIX SPIKE SAMPLE: Spike Conc. MS MS Limits Diesel Range Organics(C10-C28) mg/l n-pentacosane (S) % SAMPLE DUPLICATE: Dup Diesel Range Organics(C10-C28) mg/l D6 n-pentacosane (S) % RPD Max RPD s presented on this page are in the units indicated by the "" column except where an alternate unit is presented to the right of the result. Page 14 of 20
16 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: OEXT/38851 EPA 3510 Analysis Method: Analysis Description: EPA Water MSSV Associated Lab Samples: 001, 002, 003, 004, 005, 006 METHOD BLANK: Associated Lab Samples: 001, 002, 003, 004, 005, 006 Blank Matrix: Water Reporting Limit MDL Analyzed 1-Methylnaphthalene ug/l ND /04/15 13:52 2-Methylnaphthalene ug/l ND /04/15 13:52 Acenaphthene ug/l ND /04/15 13:52 Acenaphthylene ug/l ND /04/15 13:52 Anthracene ug/l ND /04/15 13:52 Benzo(a)anthracene ug/l ND /04/15 13:52 Benzo(a)pyrene ug/l ND /04/15 13:52 Benzo(b)fluoranthene ug/l ND /04/15 13:52 Benzo(g,h,i)perylene ug/l ND /04/15 13:52 Benzo(k)fluoranthene ug/l ND /04/15 13:52 Chrysene ug/l ND /04/15 13:52 Dibenz(a,h)anthracene ug/l ND /04/15 13:52 Fluoranthene ug/l ND /04/15 13:52 Fluorene ug/l ND /04/15 13:52 Indeno(1,2,3-cd)pyrene ug/l ND /04/15 13:52 Naphthalene ug/l ND /04/15 13:52 Phenanthrene ug/l ND /04/15 13:52 Pyrene ug/l ND /04/15 13:52 2-Fluorobiphenyl (S) % /04/15 13:52 Nitrobenzene-d5 (S) % /04/15 13:52 Terphenyl-d14 (S) % /04/15 13:52 LABORATORY CONTROL SAMPLE & LCSD: Spike Conc LCS LCSD LCS LCSD Limits RPD 1-Methylnaphthalene ug/l Methylnaphthalene ug/l Acenaphthene ug/l Acenaphthylene ug/l Anthracene ug/l Benzo(a)anthracene ug/l Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l Benzo(k)fluoranthene ug/l Chrysene ug/l Dibenz(a,h)anthracene ug/l Fluoranthene ug/l Fluorene ug/l Indeno(1,2,3-cd)pyrene ug/l Max RPD s presented on this page are in the units indicated by the "" column except where an alternate unit is presented to the right of the result. Page 15 of 20
17 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE & LCSD: Spike Conc LCS LCSD LCS LCSD Limits RPD Naphthalene ug/l Phenanthrene ug/l Pyrene ug/l Fluorobiphenyl (S) % Nitrobenzene-d5 (S) % Terphenyl-d14 (S) % Max RPD s presented on this page are in the units indicated by the "" column except where an alternate unit is presented to the right of the result. Page 16 of 20
18 #=QL# QUALIFIERS DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a ph of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. Page 17 of 20
19 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 001 FOUR MILE - A EPA 3510 OEXT/38811 EPA 8015 Modified GCSV/ FOUR MILE - B EPA 3510 OEXT/38811 EPA 8015 Modified GCSV/ FOUR MILE - C EPA 3510 OEXT/38811 EPA 8015 Modified GCSV/ FOUR MILE - D EPA 3510 OEXT/38811 EPA 8015 Modified GCSV/ FOUR MILE - E EPA 3510 OEXT/38811 EPA 8015 Modified GCSV/ OUTFALL 18 BOOM EPA 3510 OEXT/38811 EPA 8015 Modified GCSV/ FOUR MILE - A EPA 5030/8015 Mod. GCV/ FOUR MILE - B EPA 5030/8015 Mod. GCV/ FOUR MILE - C EPA 5030/8015 Mod. GCV/ FOUR MILE - D EPA 5030/8015 Mod. GCV/ FOUR MILE - E EPA 5030/8015 Mod. GCV/ OUTFALL 18 BOOM EPA 5030/8015 Mod. GCV/ FOUR MILE - A EPA 3510 OEXT/38851 EPA 8270 MSSV/ FOUR MILE - B EPA 3510 OEXT/38851 EPA 8270 MSSV/ FOUR MILE - C EPA 3510 OEXT/38851 EPA 8270 MSSV/ FOUR MILE - D EPA 3510 OEXT/38851 EPA 8270 MSSV/ FOUR MILE - E EPA 3510 OEXT/38851 EPA 8270 MSSV/ OUTFALL 18 BOOM EPA 3510 OEXT/38851 EPA 8270 MSSV/ FOUR MILE - A EPA 8260 MSV/ FOUR MILE - B EPA 8260 MSV/ FOUR MILE - C EPA 8260 MSV/ FOUR MILE - D EPA 8260 MSV/ FOUR MILE - E EPA 8260 MSV/ OUTFALL 18 BOOM EPA 8260 MSV/34136 Page 18 of 20
20 Page 19 of 20
21 Page 20 of 20
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