Laboratory Report Number(s) Lone Tree Road (Deep) 10/5/15, 10/19/15, 6/13/16. Address Sample Date(s) Analyses Requested

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1 July 14, 216 Mr. Shaun Lehman MDEQ-OOGM Lansing District Office Constitution Hall 2 South 525 West Allegan Street Lansing, MI Re: Residential Well Sampling Hartland 36 Gas Plant SE/NE/NW Section 36, T3N-R6E Hartland Township, Livingston County, Michigan Dear Mr. Lehman: Per the request of Merit Energy Company (MEC), Environmental Consulting & Technology, Inc. (ECT) performed residential water supply well sampling in October 215, June 216, and July 216 in Hartland Township, Michigan. A total of fifteen water supply wells were sampled by personnel from ECT. The samples were submitted for the analyses noted in the below table to an independent/third party accredited laboratory. Laboratory analytical results were reported as not detected at the Reporting Limit for all analyses requested for all samples collected. Laboratory analytical reports are attached. Figure 1, attached, depicts the approximate locations of all sampled residential water supply wells. The following table indicates the addresses, dates, laboratory analyses requested, and laboratory report number for sampled wells: 3399 Veterans Drive Traverse City, MI (231) FAX (231) Address Sample Date(s) Analyses Requested Laboratory Report Number(s) 1339 Lone Tree Road (Deep) 1/5/15, 1/19/15, 6/13/16 Sulfolane 1, ethylene glycol 2, SVOCs 3, VOCs , , Lone Tree Road (Shallow) 1/3/15, 6/13/16 Sulfolane, ethylene , glycol, SVOCs, VOCs 9 Erin Lane 6/7/16 Sulfolane, DIPA 5, VOCs Erin Lane (Pole Bldg) 6/14/16 Sulfolane, DIPA, VOCs Cherry Blossom Lane 6/13/16 Sulfolane, DIPA, VOCs Cherry Blossom Lane 6/6/16 Sulfolane, DIPA, VOCs Sheila Lane 6/6/16 Sulfolane, DIPA, VOCs Jeni Lane 6/13/16 Sulfolane, DIPA, VOCs Jeni Lane 6 6/14/16 Sulfolane, DIPA, VOCs Jeni Lane 6/13/16 Sulfolane, DIPA, VOCs Jeni Lane 6/6/16 Sulfolane, DIPA, VOCS Pleasant Valley Road 6/13/16 Sulfolane, DIPA, VOCs Lone Tree Road 6/7/16 Sulfolane, DIPA, VOCs Lone Tree Road 6/7/16 Sulfolane, DIPA, VOCs Cherry Blossom Lane 7/7/16 Sulfolane, DIPA, VOCs Sulfolane analyzed by method SW D 2 Ethylene glycol analyzed by method SW815M 3 SVOCs: Semi-Volatile Organic Compounds analyzed by method SW D 4 VOCs: Volatile Organic Compounds analyzed by method SW826B 5 DIPA: Diisopropanolamine analyzed by method SW D 6 Due to a transcription error, 513 Jeni Lane is recorded in laboratory report as 731 Jeni Lane A copy of this letter has been sent to the Livingston County Department of Public Health and copies of each laboratory report have been sent to respective property owners. An Equal Opportunity/Affirmative Action Employer

2 Residential Well Sampling Hartland 36 Gas Plant July 14, 216 Page 2 Closing ECT sincerely appreciates the opportunity to provide our consulting services on this important project. Should you have questions or require additional information, please do not hesitate to contact me at your convenience at or jlewandowski@ectinc.com. Sincerely, ENVIRONMENTAL CONSULTING & TECHNOLOGY, INC. Jeremy S. Lewandowski Senior Engineer Dirk S. Mammen Principal Scientist CC: Matt Bolang Livingston County Department of Public Health Sean Craven Merit Energy Company Attachments: Figure 1 Sampled Residential Well Locations Laboratory Analytical Reports

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4 8-Oct-215 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: Hartland Gas Plant Work Order: Dear Sean, ALS Environmental received 24 samples on 6-Oct-215 8:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 31. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

5 ALS Group USA, Corp Date: 8-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received F-2 (18') Soil 1/2/215 15:5 1/6/215 8: F-3 (18') Soil 1/2/215 15:4 1/6/215 8: SS-18 (.5') Soil 1/2/215 17:5 1/6/215 8: SW-1 (8') Soil 1/5/215 15:3 1/6/215 8: SW-2 (8') Soil 1/5/215 15:35 1/6/215 8: SW-3 (7') Soil 1/5/215 15:4 1/6/215 8: SW-4 (1') Soil 1/5/215 15:45 1/6/215 8: F-1 (11') Soil 1/5/215 15:5 1/6/215 8: SS-9 (4') Soil 1/5/215 15:55 1/6/215 8: SS-9 (8') Soil 1/5/215 16: 1/6/215 8: SS-1 (2') Soil 1/5/215 16:5 1/6/215 8: SS-1 (1') Soil 1/5/215 16:1 1/6/215 8: SS-11 (2') Soil 1/5/215 16:12 1/6/215 8: SS-11 (4') Soil 1/5/215 16:14 1/6/215 8: SS-12 (4') Soil 1/5/215 16:16 1/6/215 8: SS-12 (6') Soil 1/5/215 16:18 1/6/215 8: SS-13 (4') Soil 1/5/215 16:2 1/6/215 8: SS-14 (2') Soil 1/5/215 16:22 1/6/215 8: SS-14 (4') Soil 1/5/215 16:24 1/6/215 8: SS-15 (6') Soil 1/5/215 16:26 1/6/215 8: SS-15 (1') Soil 1/5/215 16:28 1/6/215 8: SS-16 (2') Soil 1/5/215 16:3 1/6/215 8: SS-17 (2') Soil 1/5/215 16:32 1/6/215 8: W Water 1/5/215 14:25 1/6/215 8:3 Hold Sample Summary Page 1 of 1

6 ALS Group USA, Corp Date: 8-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W Lab ID: Collection Date: 1/5/215 2:25 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 1/6/15 Analyst: RM Sulfolane 1 µg/l 1 1/6/215 6:6 PM Surr: 2,4,6-Tribromophenol %REC 1 1/6/215 6:6 PM Surr: 2-Fluorobiphenyl %REC 1 1/6/215 6:6 PM Surr: 2-Fluorophenol %REC 1 1/6/215 6:6 PM Surr: 4-Terphenyl-d %REC 1 1/6/215 6:6 PM Surr: Nitrobenzene-d %REC 1 1/6/215 6:6 PM Surr: Phenol-d %REC 1 1/6/215 6:6 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 18 of 18

7 ALS Group USA, Corp Client: Merit Energy Work Order: Project: Hartland Gas Plant Date: 8-Oct-15 Batch ID: 7718 Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKW Units: µg/l Client ID: Run ID: SVMS8_1516A SeqNo: Analysis Date: 1/6/215 4:7 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_1516A SeqNo: Analysis Date: 1/6/215 4:47 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 1 of 5

8 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: 7728 Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKS Units: µg/kg Client ID: Run ID: SVMS8_1516A SeqNo: Analysis Date: 1/6/215 6:26 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 17 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSS Units: µg/kg Client ID: Run ID: SVMS8_1516A SeqNo: Analysis Date: 1/6/215 6:45 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units: µg/kg Client ID: SS-18 (.5') Run ID: SVMS8_1516A SeqNo: Analysis Date: 1/6/215 7:5 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 2 of 5

9 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: 7728 Instrument ID: SVMS8 Method: SW D MSD Sample ID: A MSD Units: µg/kg Client ID: SS-18 (.5') Run ID: SVMS8_1516A SeqNo: Analysis Date: 1/6/215 7:25 PM Prep Date: 1/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A A A A A A A A A A A A A A A A A QC Page: 3 of 5

10 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R Instrument ID: MOIST Method: E16.3M MBLK Sample ID: WBLKS-R Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: Run ID: MOIST_1516C SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Moisture.5 Limit Qual LCS Sample ID: LCS-R Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: Run ID: MOIST_1516C SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture DUP Sample ID: A DUP Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: SW-3 (7') Run ID: MOIST_1516C SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture DUP Sample ID: B DUP Units: % of sample Analysis Date: 1/6/215 5:3 PM Client ID: Run ID: MOIST_1516C SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture The following samples were analyzed in this batch: A A A A A A A A A A A A A A A QC Page: 4 of 5

11 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R Instrument ID: MOIST Method: E16.3M MBLK Sample ID: WBLKS-R Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Moisture.5 Limit Qual LCS Sample ID: LCS-R Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture DUP Sample ID: B DUP Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture DUP Sample ID: A DUP Units: % of sample Analysis Date: 1/7/215 1:41 PM Client ID: Run ID: MOIST_1517A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Moisture The following samples were analyzed in this batch: A A QC Page: 5 of 5

12 ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant WorkOrder: Date: 8-Oct-15 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported % of sample µg/kg-dry µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Percent of Sample Micrograms per Kilogram Dry Weight Micrograms per Liter QF Page 1 of 1

13 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 6-Oct-15 8:3 Work Order: Received by: NML Checklist completed by Diane Shaw Gary Byar 6-Oct-15 Reviewed by: esignature Date esignature 6-Oct-15 Date Matrices: Carrier name: Soil, water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2./2. c SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 1/6/215 8:54:55 AM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

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18 3-Oct-215 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: Hartland Gas Plant Work Order: Dear Sean, ALS Environmental received 1 sample on 2-Oct-215 1: AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 22. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

19 ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received W-1339 Deep Water 1/19/215 9:3 1/2/215 1: Hold Sample Summary Page 1 of 1

20 ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W-1339 Deep Lab ID: Collection Date: 1/19/215 9:3 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed ORGANIC COMPOUS BY GC-FID SW815M Analyst: KYM Ethylene glycol 5. mg/l 1 1/21/215 12:41 PM SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 1/23/15 Analyst: RS 2-Methylnaphthalene 5. µg/l 1 1/23/215 9:12 PM Acenaphthene 5. µg/l 1 1/23/215 9:12 PM Acenaphthylene 5. µg/l 1 1/23/215 9:12 PM Anthracene 5. µg/l 1 1/23/215 9:12 PM Benzo(a)anthracene 5. µg/l 1 1/23/215 9:12 PM Benzo(a)pyrene 5. µg/l 1 1/23/215 9:12 PM Benzo(b)fluoranthene 5. µg/l 1 1/23/215 9:12 PM Benzo(g,h,i)perylene 5. µg/l 1 1/23/215 9:12 PM Benzo(k)fluoranthene 5. µg/l 1 1/23/215 9:12 PM Chrysene 5. µg/l 1 1/23/215 9:12 PM Dibenzo(a,h)anthracene 5. µg/l 1 1/23/215 9:12 PM Fluoranthene 5. µg/l 1 1/23/215 9:12 PM Fluorene 5. µg/l 1 1/23/215 9:12 PM Indeno(1,2,3-cd)pyrene 5. µg/l 1 1/23/215 9:12 PM Naphthalene 5. µg/l 1 1/23/215 9:12 PM Phenanthrene 5. µg/l 1 1/23/215 9:12 PM Pyrene 5. µg/l 1 1/23/215 9:12 PM Surr: 2,4,6-Tribromophenol %REC 1 1/23/215 9:12 PM Surr: 2-Fluorobiphenyl %REC 1 1/23/215 9:12 PM Surr: 2-Fluorophenol %REC 1 1/23/215 9:12 PM Surr: 4-Terphenyl-d %REC 1 1/23/215 9:12 PM Surr: Nitrobenzene-d %REC 1 1/23/215 9:12 PM Surr: Phenol-d %REC 1 1/23/215 9:12 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,1-Trichloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,2-Trichloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 1/29/215 7:1 PM 1,1-Dichloroethane 1. µg/l 1 1/29/215 7:1 PM 1,1-Dichloroethene 1. µg/l 1 1/29/215 7:1 PM 1,2,3-Trichloropropane 1. µg/l 1 1/29/215 7:1 PM 1,2,4-Trichlorobenzene 1. µg/l 1 1/29/215 7:1 PM 1,2,4-Trimethylbenzene 1. µg/l 1 1/29/215 7:1 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 1/29/215 7:1 PM 1,2-Dibromoethane 1. µg/l 1 1/29/215 7:1 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 3

21 ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W-1339 Deep Lab ID: Collection Date: 1/19/215 9:3 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 2-Methylnaphthalene 4-Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1 µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 3

22 ALS Group USA, Corp Date: 3-Oct-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W-1339 Deep Lab ID: Collection Date: 1/19/215 9:3 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM 1/29/215 7:1 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 3 of 3

23 ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant Work Order: Date: 3-Oct-15 Case Narrative Batch R174943A The MS/MSD data for volatiles is not related tot his project's samples. No data requires qualification. Case Narrative Page 1 of 1

24 ALS Group USA, Corp Client: Merit Energy Work Order: Project: Hartland Gas Plant Date: 3-Oct-15 Batch ID: R Instrument ID: GC11 Method: SW815M MBLK Sample ID: MB-R R Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: Analysis Date: 1/21/215 11:1 A Prep Date: 1/21/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Ethylene glycol 5. Limit Qual LCS Sample ID: LCS-R R Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: Analysis Date: 1/21/215 1:7 A Prep Date: 1/21/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol MS Sample ID: A MS Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: Analysis Date: 1/21/215 1:16 A Prep Date: 1/21/215 DF: 2 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol MSD Sample ID: A MSD Units: mg/l Client ID: Run ID: GC11_15121A SeqNo: Analysis Date: 1/21/215 1:25 A Prep Date: 1/21/215 DF: 2 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol The following samples were analyzed in this batch: A QC Page: 1 of 13

25 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKW Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: Analysis Date: 1/23/215 3:37 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 5. Acenaphthene 5. Acenaphthylene 5. Anthracene 5. Benzo(a)anthracene 5. Benzo(a)pyrene 5. Benzo(b)fluoranthene 5. Benzo(g,h,i)perylene 5. Benzo(k)fluoranthene 5. Chrysene 5. Dibenzo(a,h)anthracene 5. Fluoranthene 5. Fluorene 5. Indeno(1,2,3-cd)pyrene 5. Naphthalene 5. Phenanthrene 5. Pyrene 5. Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 2 of 13

26 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: Analysis Date: 1/23/215 3:57 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 3 of 13

27 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D MS Sample ID: B MS Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: Analysis Date: 1/23/215 5:36 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 4 of 13

28 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D DUP Sample ID: B DUP Units: µg/l Client ID: Run ID: SVMS8_15123A SeqNo: Analysis Date: 1/23/215 6:15 P Prep Date: 1/23/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 5 of 13

29 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B MBLK Sample ID: VBLKW R174943A Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: Prep Date: Analysis Date: 1/29/215 12:12 P DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 6 of 13

30 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 7 of 13

31 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B LCS Sample ID: VLCSW R174943A Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: Prep Date: Analysis Date: 1/29/215 1:56 A DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 8 of 13

32 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 9 of 13

33 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B MS Sample ID: A MS Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: Prep Date: Analysis Date: 1/29/215 8:39 P DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 1 of 13

34 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 11 of 13

35 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B MSD Sample ID: A MSD Units: µg/l Client ID: Run ID: VMS8_15129A SeqNo: Prep Date: Analysis Date: 1/29/215 9:3 P DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 12 of 13

36 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R174943A Instrument ID: VMS8 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S The following samples were analyzed in this batch: A QC Page: 13 of 13

37 ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant WorkOrder: Date: 3-Oct-15 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l mg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter Milligrams per Liter QF Page 1 of 1

38 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 2-Oct-15 1: Work Order: Received by: DS Checklist completed by Diane Shaw Gary Byar 21-Oct-15 Reviewed by: esignature Date esignature 21-Oct-15 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 c SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 1/21/215 8:11:49 AM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

39

40 11-Nov-215 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: Hartland Gas Plant Work Order: Dear Sean, ALS Environmental received 5 samples on 31-Oct-215 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 27. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

41 ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received TMW-6 (65-7') Water 1/3/215 12:15 1/31/215 9: TMW-6 (55-6') Water 1/3/215 12:25 1/31/215 9: TMW-6 (45-5') Water 1/3/215 12:35 1/31/215 9: TMW-6 (35-4') Water 1/3/215 12:45 1/31/215 9: W-1339 Shallow Water 1/3/215 15:2 1/31/215 9:3 Hold Sample Summary Page 1 of 1

42 ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W-1339 Shallow Lab ID: Collection Date: 1/3/215 3:2 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed ORGANIC COMPOUS BY GC-FID SW815M Analyst: KYM Ethylene glycol 5. mg/l 1 11/9/215 9:34 AM SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 11/3/15 Analyst: RM 2-Methylnaphthalene 5. µg/l 1 11/4/215 9:19 PM Acenaphthene 5. µg/l 1 11/4/215 9:19 PM Acenaphthylene 5. µg/l 1 11/4/215 9:19 PM Anthracene 5. µg/l 1 11/4/215 9:19 PM Benzo(a)anthracene 5. µg/l 1 11/4/215 9:19 PM Benzo(a)pyrene 5. µg/l 1 11/4/215 9:19 PM Benzo(b)fluoranthene 5. µg/l 1 11/4/215 9:19 PM Benzo(g,h,i)perylene 5. µg/l 1 11/4/215 9:19 PM Benzo(k)fluoranthene 5. µg/l 1 11/4/215 9:19 PM Chrysene 5. µg/l 1 11/4/215 9:19 PM Dibenzo(a,h)anthracene 5. µg/l 1 11/4/215 9:19 PM Fluoranthene 5. µg/l 1 11/4/215 9:19 PM Fluorene 5. µg/l 1 11/4/215 9:19 PM Indeno(1,2,3-cd)pyrene 5. µg/l 1 11/4/215 9:19 PM Naphthalene 5. µg/l 1 11/4/215 9:19 PM Phenanthrene 5. µg/l 1 11/4/215 9:19 PM Pyrene 5. µg/l 1 11/4/215 9:19 PM Sulfolane 1 µg/l 1 11/4/215 9:19 PM Surr: 2,4,6-Tribromophenol %REC 1 11/4/215 9:19 PM Surr: 2-Fluorobiphenyl %REC 1 11/4/215 9:19 PM Surr: 2-Fluorophenol %REC 1 11/4/215 9:19 PM Surr: 4-Terphenyl-d %REC 1 11/4/215 9:19 PM Surr: Nitrobenzene-d %REC 1 11/4/215 9:19 PM Surr: Phenol-d %REC 1 11/4/215 9:19 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,1-Trichloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,2-Trichloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 11/1/215 7:27 AM 1,1-Dichloroethane 1. µg/l 1 11/1/215 7:27 AM 1,1-Dichloroethene 1. µg/l 1 11/1/215 7:27 AM 1,2,3-Trichloropropane 1. µg/l 1 11/1/215 7:27 AM 1,2,4-Trichlorobenzene 1. µg/l 1 11/1/215 7:27 AM 1,2,4-Trimethylbenzene 1. µg/l 1 11/1/215 7:27 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 11/1/215 7:27 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 5 of 7

43 ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W-1339 Shallow Lab ID: Collection Date: 1/3/215 3:2 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 2-Methylnaphthalene 4-Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1 µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 6 of 7

44 ALS Group USA, Corp Date: 11-Nov-15 Client: Merit Energy Project: Hartland Gas Plant Work Order: Sample ID: W-1339 Shallow Lab ID: Collection Date: 1/3/215 3:2 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM 11/1/215 7:27 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 7 of 7

45 ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant Work Order: Date: 11-Nov-15 Case Narrative Batch R175749A The MS/MSD data for volatiles is not related to this project's samples. No data requires qualification. Case Narrative Page 1 of 1

46 ALS Group USA, Corp Client: Merit Energy Work Order: Project: Hartland Gas Plant Date: 11-Nov-15 Batch ID: R Instrument ID: GC11 Method: SW815M MBLK Sample ID: MB-R R Units: mg/l Client ID: Run ID: GC11_15119A SeqNo: Analysis Date: 11/9/215 9:16 AM Prep Date: 11/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Ethylene glycol 5. Limit Qual LCS Sample ID: LCS-R R Units: mg/l Client ID: Run ID: GC11_15119A SeqNo: Analysis Date: 11/9/215 8:22 AM Prep Date: 11/6/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Ethylene glycol The following samples were analyzed in this batch: B QC Page: 1 of 13

47 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKW Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: Analysis Date: 11/4/215 1:44 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene 5. Acenaphthene 5. Acenaphthylene 5. Anthracene 5. Benzo(a)anthracene 5. Benzo(a)pyrene 5. Benzo(b)fluoranthene 5. Benzo(g,h,i)perylene 5. Benzo(k)fluoranthene 5. Chrysene 5. Dibenzo(a,h)anthracene 5. Fluoranthene 5. Fluorene 5. Indeno(1,2,3-cd)pyrene 5. Naphthalene 5. Phenanthrene 5. Pyrene 5. Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 2 of 13

48 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: 3553 Analysis Date: 11/4/215 2:4 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: Analysis Date: 11/4/215 3:5 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d J QC Page: 3 of 13

49 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D LCSD Sample ID: SLCSDW Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: Analysis Date: 11/4/215 3:26 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d J MS Sample ID: B MS Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: Analysis Date: 11/4/215 6:59 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 4 of 13

50 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: Instrument ID: SVMS8 Method: SW D MSD Sample ID: B MSD Units: µg/l Client ID: Run ID: SVMS8_15114A SeqNo: Analysis Date: 11/4/215 7:19 PM Prep Date: 11/3/215 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A A A A A QC Page: 5 of 13

51 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B MBLK Sample ID: VBLKW R175749A Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: Prep Date: Analysis Date: 11/9/215 11:42 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 6 of 13

52 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d J QC Page: 7 of 13

53 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B LCS Sample ID: VLCSW R175749A Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: Prep Date: Analysis Date: 11/9/215 1:5 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 8 of 13

54 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 9 of 13

55 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B MS Sample ID: A MS Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: Prep Date: Analysis Date: 11/1/215 8:44 A DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene S QC Page: 1 of 13

56 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 11 of 13

57 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B MSD Sample ID: A MSD Units: µg/l Client ID: Run ID: VMS6_15119B SeqNo: Prep Date: Analysis Date: 11/1/215 9:1 A DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 12 of 13

58 Client: Merit Energy Work Order: Project: Hartland Gas Plant Batch ID: R175749A Instrument ID: VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d The following samples were analyzed in this batch: B QC Page: 13 of 13

59 ALS Group USA, Corp Client: Merit Energy Project: Hartland Gas Plant WorkOrder: Date: 11-Nov-15 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l mg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter Milligrams per Liter QF Page 1 of 1

60 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 31-Oct-15 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 31-Oct-15 Reviewed by: esignature Date esignature 2-Nov-15 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 4.8/4.8 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 1/31/215 11:11:41 AM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

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63 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (1339 Lone Tree Rd - Deep) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 9. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

64 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Deep) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Lone Tree Rd - Deep Water 6/13/216 13:41 6/15/216 9:3 Hold Sample Summary Page 1 of 1

65 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Deep) Work Order: Sample ID: 1339 Lone Tree Rd - Deep Lab ID: Collection Date: 6/13/216 1:41 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Sulfolane 1 µg/l 1 6/16/216 11:5 PM Surr: 2,4,6-Tribromophenol %REC 1 6/16/216 11:5 PM Surr: 2-Fluorobiphenyl %REC 1 6/16/216 11:5 PM Surr: 2-Fluorophenol %REC 1 6/16/216 11:5 PM Surr: 4-Terphenyl-d %REC 1 6/16/216 11:5 PM Surr: Nitrobenzene-d %REC 1 6/16/216 11:5 PM Surr: Phenol-d %REC 1 6/16/216 11:5 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 1

66 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (1339 Lone Tree Rd - Deep) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 2

67 Client: Merit Energy Work Order: Project: ECT (1339 Lone Tree Rd - Deep) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Client ID: 1339 Lone Tree Rd - Deep Run ID: SVMS8_16616A Units:µg/L SeqNo: Analysis Date: 6/16/216 1:45 PM Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 2

68 ALS Group USA, Corp Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Deep) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

69 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 2:22:34 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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72 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (1339 Lone Tree Rd - Shallow) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 9. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

73 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Shallow) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Lone Tree Rd - Shallow Water 6/13/216 13:21 6/15/216 9:3 Hold Sample Summary Page 1 of 1

74 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Shallow) Work Order: Sample ID: 1339 Lone Tree Rd - Shallow Lab ID: Collection Date: 6/13/216 1:21 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Sulfolane 11 µg/l 1 6/16/216 1:25 PM Surr: 2,4,6-Tribromophenol %REC 1 6/16/216 1:25 PM Surr: 2-Fluorobiphenyl %REC 1 6/16/216 1:25 PM Surr: 2-Fluorophenol %REC 1 6/16/216 1:25 PM Surr: 4-Terphenyl-d %REC 1 6/16/216 1:25 PM Surr: Nitrobenzene-d %REC 1 6/16/216 1:25 PM Surr: Phenol-d %REC 1 6/16/216 1:25 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 1

75 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (1339 Lone Tree Rd - Shallow) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Client ID: 1339 Lone Tree Rd - Shallow Run ID: SVMS8_16616A Units:µg/L SeqNo: Analysis Date: 6/16/216 1:5 PM Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 2

76 Client: Merit Energy Work Order: Project: ECT (1339 Lone Tree Rd - Shallow) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 2

77 ALS Group USA, Corp Client: Merit Energy Project: ECT (1339 Lone Tree Rd - Shallow) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

78 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 2:2:41 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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81 1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (Hartland - 9 Erin Lane) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

82 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Erin Lane Water 6/7/216 8:36 6/8/216 9:3 Hold Sample Summary Page 1 of 1

83 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: Sample ID: 9 Erin Lane Lab ID: Collection Date: 6/7/216 8:36 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 59 µg/l 1 6/9/216 6:56 PM Sulfolane 12 µg/l 1 6/9/216 6:56 PM Surr: 2,4,6-Tribromophenol %REC 1 6/9/216 6:56 PM Surr: 2-Fluorobiphenyl %REC 1 6/9/216 6:56 PM Surr: 2-Fluorophenol %REC 1 6/9/216 6:56 PM Surr: 4-Terphenyl-d %REC 1 6/9/216 6:56 PM Surr: Nitrobenzene-d %REC 1 6/9/216 6:56 PM Surr: Phenol-d %REC 1 6/9/216 6:56 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 5:25 AM 1,1-Dichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,1-Dichloroethene 1. µg/l 1 6/9/216 5:25 AM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 5:25 AM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 5:25 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 5:25 AM 1,2-Dibromoethane 1. µg/l 1 6/9/216 5:25 AM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 1,2-Dichloroethane 1. µg/l 1 6/9/216 5:25 AM 1,2-Dichloropropane 1. µg/l 1 6/9/216 5:25 AM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 5:25 AM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 5:25 AM 2-Butanone 5. µg/l 1 6/9/216 5:25 AM 2-Hexanone 5. µg/l 1 6/9/216 5:25 AM 2-Methylnaphthalene 5. µg/l 1 6/9/216 5:25 AM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 5:25 AM Acetone 1 µg/l 1 6/9/216 5:25 AM Acrylonitrile 1. µg/l 1 6/9/216 5:25 AM Benzene 1. µg/l 1 6/9/216 5:25 AM Bromochloromethane 1. µg/l 1 6/9/216 5:25 AM Bromodichloromethane 1. µg/l 1 6/9/216 5:25 AM Bromoform 1. µg/l 1 6/9/216 5:25 AM Bromomethane 1. µg/l 1 6/9/216 5:25 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

84 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: Sample ID: 9 Erin Lane Lab ID: Collection Date: 6/7/216 8:36 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM 6/9/216 5:25 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

85 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) Work Order: Date: 1-Jun-16 Case Narrative Batch R189191a The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

86 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: B MS Client ID: 9 Erin Lane Run ID: SVMS8_1669A Units:µg/L SeqNo: Analysis Date: 6/9/216 6:36 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

87 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: 8717 Instrument ID SVMS8 Method: SW D DUP Sample ID: B DUP Units:µg/L Analysis Date: 6/9/216 7:16 PM Client ID: Run ID: SVMS8_1669A SeqNo:38721 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 2 of 1

88 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MBLK Sample ID: VBLKW R189191a Units:µg/L Analysis Date: 6/9/216 2:2 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

89 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

90 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B LCS Sample ID: VLCSW R189191a Units:µg/L Analysis Date: 6/9/216 1:12 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

91 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 6 of 1

92 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/9/216 1:53 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone , Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene SE S QC Page: 7 of 1

93 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S EO S QC Page: 8 of 1

94 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/9/216 11:18 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone 228 1, Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene SR SRE R S SR SR QC Page: 9 of 1

95 Client: Merit Energy Work Order: Project: ECT (Hartland - 9 Erin Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR SR SREO S SR The following samples were analyzed in this batch: A QC Page: 1 of 1

96 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland - 9 Erin Lane) WorkOrder: Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

97 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 3.6/3.6 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:32:23 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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100 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (9 Erin Lane Pole Building) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 1: AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 18. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

101 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Erin Lane Pole Building Water 6/14/216 8:25 6/15/216 1: Hold Sample Summary Page 1 of 1

102 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: Sample ID: 9 Erin Lane Pole Building Lab ID: Collection Date: 6/14/216 8:25 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 59 µg/l 1 6/17/216 3:28 AM Sulfolane 12 µg/l 1 6/17/216 3:28 AM Surr: 2,4,6-Tribromophenol %REC 1 6/17/216 3:28 AM Surr: 2-Fluorobiphenyl %REC 1 6/17/216 3:28 AM Surr: 2-Fluorophenol %REC 1 6/17/216 3:28 AM Surr: 4-Terphenyl-d %REC 1 6/17/216 3:28 AM Surr: Nitrobenzene-d %REC 1 6/17/216 3:28 AM Surr: Phenol-d %REC 1 6/17/216 3:28 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 6:42 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 6:42 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 6:42 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 6:42 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 6:42 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 6:42 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 6:42 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 6:42 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 6:42 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 6:42 PM 2-Butanone 5. µg/l 1 6/21/216 6:42 PM 2-Hexanone 5. µg/l 1 6/21/216 6:42 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 6:42 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 6:42 PM Acetone 1 µg/l 1 6/21/216 6:42 PM Acrylonitrile 1. µg/l 1 6/21/216 6:42 PM Benzene 1. µg/l 1 6/21/216 6:42 PM Bromochloromethane 1. µg/l 1 6/21/216 6:42 PM Bromodichloromethane 1. µg/l 1 6/21/216 6:42 PM Bromoform 1. µg/l 1 6/21/216 6:42 PM Bromomethane 1. µg/l 1 6/21/216 6:42 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

103 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: Sample ID: 9 Erin Lane Pole Building Lab ID: Collection Date: 6/14/216 8:25 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM 6/21/216 6:42 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

104 ALS Group USA, Corp Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) Work Order: Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

105 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

106 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 1

107 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

108 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

109 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

110 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

111 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

112 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

113 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

114 Client: Merit Energy Work Order: Project: ECT (9 Erin Lane Pole Building) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR S S The following samples were analyzed in this batch: B QC Page: 1 of 1

115 ALS Group USA, Corp Client: Merit Energy Project: ECT (9 Erin Lane Pole Building) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

116 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 1: Work Order: Received by: MEB Checklist completed by Meghan Broadbent Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: water Carrier name: UPS 16-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 6./6. SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 4:35:37 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

117

118 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (139 Cherry Blossom) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

119 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Cherry Blossom Water 6/13/216 17:39 6/15/216 9:3 Hold Sample Summary Page 1 of 1

120 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: Sample ID: 139 Cherry Blossom Lab ID: Collection Date: 6/13/216 5:39 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 53 µg/l 1 6/17/216 2:47 AM Sulfolane 11 µg/l 1 6/17/216 2:47 AM Surr: 2,4,6-Tribromophenol %REC 1 6/17/216 2:47 AM Surr: 2-Fluorobiphenyl %REC 1 6/17/216 2:47 AM Surr: 2-Fluorophenol %REC 1 6/17/216 2:47 AM Surr: 4-Terphenyl-d %REC 1 6/17/216 2:47 AM Surr: Nitrobenzene-d %REC 1 6/17/216 2:47 AM Surr: Phenol-d %REC 1 6/17/216 2:47 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 5:54 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 5:54 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 5:54 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 5:54 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 5:54 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 5:54 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 5:54 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 5:54 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 5:54 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 5:54 PM 2-Butanone 5. µg/l 1 6/21/216 5:54 PM 2-Hexanone 5. µg/l 1 6/21/216 5:54 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 5:54 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 5:54 PM Acetone 1 µg/l 1 6/21/216 5:54 PM Acrylonitrile 1. µg/l 1 6/21/216 5:54 PM Benzene 1. µg/l 1 6/21/216 5:54 PM Bromochloromethane 1. µg/l 1 6/21/216 5:54 PM Bromodichloromethane 1. µg/l 1 6/21/216 5:54 PM Bromoform 1. µg/l 1 6/21/216 5:54 PM Bromomethane 1. µg/l 1 6/21/216 5:54 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

121 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: Sample ID: 139 Cherry Blossom Lab ID: Collection Date: 6/13/216 5:39 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM 6/21/216 5:54 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

122 ALS Group USA, Corp Client: Merit Energy Project: ECT (139 Cherry Blossom) Work Order: Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

123 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

124 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 1

125 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

126 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

127 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

128 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

129 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

130 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

131 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

132 Client: Merit Energy Work Order: Project: ECT (139 Cherry Blossom) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR S S The following samples were analyzed in this batch: B QC Page: 1 of 1

133 ALS Group USA, Corp Client: Merit Energy Project: ECT (139 Cherry Blossom) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

134 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 3:2:37 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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137 1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (Hartland Cherry Blossom) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

138 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Cherry Blossom) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Cherry Blossom Water 6/6/216 7:26 6/8/216 9:3 Hold Sample Summary Page 1 of 1

139 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Cherry Blossom) Work Order: Sample ID: 1385 Cherry Blossom Lab ID: Collection Date: 6/6/216 7:26 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 7:57 PM Sulfolane 1 µg/l 1 6/9/216 7:57 PM Surr: 2,4,6-Tribromophenol %REC 1 6/9/216 7:57 PM Surr: 2-Fluorobiphenyl %REC 1 6/9/216 7:57 PM Surr: 2-Fluorophenol %REC 1 6/9/216 7:57 PM Surr: 4-Terphenyl-d %REC 1 6/9/216 7:57 PM Surr: Nitrobenzene-d %REC 1 6/9/216 7:57 PM Surr: Phenol-d %REC 1 6/9/216 7:57 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 6:15 AM 1,1-Dichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,1-Dichloroethene 1. µg/l 1 6/9/216 6:15 AM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 6:15 AM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 6:15 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 6:15 AM 1,2-Dibromoethane 1. µg/l 1 6/9/216 6:15 AM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 1,2-Dichloroethane 1. µg/l 1 6/9/216 6:15 AM 1,2-Dichloropropane 1. µg/l 1 6/9/216 6:15 AM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 6:15 AM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 6:15 AM 2-Butanone 5. µg/l 1 6/9/216 6:15 AM 2-Hexanone 5. µg/l 1 6/9/216 6:15 AM 2-Methylnaphthalene 5. µg/l 1 6/9/216 6:15 AM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 6:15 AM Acetone 1 µg/l 1 6/9/216 6:15 AM Acrylonitrile 1. µg/l 1 6/9/216 6:15 AM Benzene 1. µg/l 1 6/9/216 6:15 AM Bromochloromethane 1. µg/l 1 6/9/216 6:15 AM Bromodichloromethane 1. µg/l 1 6/9/216 6:15 AM Bromoform 1. µg/l 1 6/9/216 6:15 AM Bromomethane 1. µg/l 1 6/9/216 6:15 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

140 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Cherry Blossom) Work Order: Sample ID: 1385 Cherry Blossom Lab ID: Collection Date: 6/6/216 7:26 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM 6/9/216 6:15 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

141 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Cherry Blossom) Work Order: Date: 1-Jun-16 Case Narrative Batch R189191a The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

142 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: B MS Units:µg/L Analysis Date: 6/9/216 6:36 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

143 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: 8717 Instrument ID SVMS8 Method: SW D DUP Sample ID: B DUP Units:µg/L Analysis Date: 6/9/216 7:16 PM Client ID: Run ID: SVMS8_1669A SeqNo:38721 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 2 of 1

144 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MBLK Sample ID: VBLKW R189191a Units:µg/L Analysis Date: 6/9/216 2:2 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

145 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

146 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B LCS Sample ID: VLCSW R189191a Units:µg/L Analysis Date: 6/9/216 1:12 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

147 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 6 of 1

148 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/9/216 1:53 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone , Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene SE S QC Page: 7 of 1

149 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S EO S QC Page: 8 of 1

150 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/9/216 11:18 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone 228 1, Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene SR SRE R S SR SR QC Page: 9 of 1

151 Client: Merit Energy Work Order: Project: ECT (Hartland Cherry Blossom) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR SR SREO S SR The following samples were analyzed in this batch: A QC Page: 1 of 1

152 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Cherry Blossom) WorkOrder: Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

153 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 3.6/3.6 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:37:4 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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156 1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (Hartland Sheila Lane) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

157 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Sheila Lane) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Sheila Lane Water 6/6/216 17:56 6/8/216 9:3 Hold Sample Summary Page 1 of 1

158 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Sheila Lane) Work Order: Sample ID: Sheila Lane Lab ID: Collection Date: 6/6/216 5:56 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 8:38 PM Sulfolane 1 µg/l 1 6/9/216 8:38 PM Surr: 2,4,6-Tribromophenol %REC 1 6/9/216 8:38 PM Surr: 2-Fluorobiphenyl %REC 1 6/9/216 8:38 PM Surr: 2-Fluorophenol %REC 1 6/9/216 8:38 PM Surr: 4-Terphenyl-d %REC 1 6/9/216 8:38 PM Surr: Nitrobenzene-d %REC 1 6/9/216 8:38 PM Surr: Phenol-d %REC 1 6/9/216 8:38 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 2:51 PM 1,1-Dichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,1-Dichloroethene 1. µg/l 1 6/9/216 2:51 PM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 2:51 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 2:51 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 2:51 PM 1,2-Dibromoethane 1. µg/l 1 6/9/216 2:51 PM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 1,2-Dichloroethane 1. µg/l 1 6/9/216 2:51 PM 1,2-Dichloropropane 1. µg/l 1 6/9/216 2:51 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 2:51 PM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 2:51 PM 2-Butanone 5. µg/l 1 6/9/216 2:51 PM 2-Hexanone 5. µg/l 1 6/9/216 2:51 PM 2-Methylnaphthalene 5. µg/l 1 6/9/216 2:51 PM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 2:51 PM Acetone 1 µg/l 1 6/9/216 2:51 PM Acrylonitrile 1. µg/l 1 6/9/216 2:51 PM Benzene 1. µg/l 1 6/9/216 2:51 PM Bromochloromethane 1. µg/l 1 6/9/216 2:51 PM Bromodichloromethane 1. µg/l 1 6/9/216 2:51 PM Bromoform 1. µg/l 1 6/9/216 2:51 PM Bromomethane 1. µg/l 1 6/9/216 2:51 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

159 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Sheila Lane) Work Order: Sample ID: Sheila Lane Lab ID: Collection Date: 6/6/216 5:56 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM 6/9/216 2:51 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

160 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Sheila Lane) Work Order: Date: 1-Jun-16 Case Narrative Batch R Sample VLCSW The LCS recovery for volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were non-detect. No qualification is necessary for this analyte. Batch R The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

161 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: B MS Units:µg/L Analysis Date: 6/9/216 6:36 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

162 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: 8717 Instrument ID SVMS8 Method: SW D DUP Sample ID: B DUP Units:µg/L Analysis Date: 6/9/216 7:16 PM Client ID: Run ID: SVMS8_1669A SeqNo:38721 Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 2 of 1

163 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R Units:µg/L Analysis Date: 6/9/216 1:38 PM Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

164 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

165 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R Units:µg/L Analysis Date: 6/9/216 1:58 AM Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

166 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

167 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/9/216 8:55 PM Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

168 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

169 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/9/216 9:2 PM Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

170 Client: Merit Energy Work Order: Project: ECT (Hartland Sheila Lane) Batch ID: R Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S The following samples were analyzed in this batch: A QC Page: 1 of 1

171 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Sheila Lane) WorkOrder: Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

172 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.4/2.4 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:48:37 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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175 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (46 Jeni Lane) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

176 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Jeni Lane Water 6/13/216 15:31 6/15/216 9:3 Hold Sample Summary Page 1 of 1

177 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: Sample ID: 46 Jeni Lane Lab ID: Collection Date: 6/13/216 3:31 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/17/216 1:47 AM Sulfolane 1 µg/l 1 6/17/216 1:47 AM Surr: 2,4,6-Tribromophenol %REC 1 6/17/216 1:47 AM Surr: 2-Fluorobiphenyl %REC 1 6/17/216 1:47 AM Surr: 2-Fluorophenol %REC 1 6/17/216 1:47 AM Surr: 4-Terphenyl-d %REC 1 6/17/216 1:47 AM Surr: Nitrobenzene-d %REC 1 6/17/216 1:47 AM Surr: Phenol-d %REC 1 6/17/216 1:47 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 4:41 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 4:41 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 4:41 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 4:41 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 4:41 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 4:41 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 4:41 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 4:41 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 4:41 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 4:41 PM 2-Butanone 5. µg/l 1 6/21/216 4:41 PM 2-Hexanone 5. µg/l 1 6/21/216 4:41 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 4:41 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 4:41 PM Acetone 1 µg/l 1 6/21/216 4:41 PM Acrylonitrile 1. µg/l 1 6/21/216 4:41 PM Benzene 1. µg/l 1 6/21/216 4:41 PM Bromochloromethane 1. µg/l 1 6/21/216 4:41 PM Bromodichloromethane 1. µg/l 1 6/21/216 4:41 PM Bromoform 1. µg/l 1 6/21/216 4:41 PM Bromomethane 1. µg/l 1 6/21/216 4:41 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

178 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: Sample ID: 46 Jeni Lane Lab ID: Collection Date: 6/13/216 3:31 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM 6/21/216 4:41 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

179 ALS Group USA, Corp Client: Merit Energy Project: ECT (46 Jeni Lane) Work Order: Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

180 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

181 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 1

182 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

183 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

184 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

185 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

186 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

187 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

188 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

189 Client: Merit Energy Work Order: Project: ECT (46 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR S S The following samples were analyzed in this batch: B QC Page: 1 of 1

190 ALS Group USA, Corp Client: Merit Energy Project: ECT (46 Jeni Lane) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

191 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 2:24:54 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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194 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (731 Jeni Lane) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 1: AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

195 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Jenni Lane Water 6/14/216 7:35 6/15/216 1: Hold Sample Summary Page 1 of 1

196 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: Sample ID: 731 Jenni Lane Lab ID: Collection Date: 6/14/216 7:35 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/17/216 3:7 AM Sulfolane 1 µg/l 1 6/17/216 3:7 AM Surr: 2,4,6-Tribromophenol %REC 1 6/17/216 3:7 AM Surr: 2-Fluorobiphenyl %REC 1 6/17/216 3:7 AM Surr: 2-Fluorophenol %REC 1 6/17/216 3:7 AM Surr: 4-Terphenyl-d %REC 1 6/17/216 3:7 AM Surr: Nitrobenzene-d %REC 1 6/17/216 3:7 AM Surr: Phenol-d %REC 1 6/17/216 3:7 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 6:18 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 6:18 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 6:18 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 6:18 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 6:18 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 6:18 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 6:18 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 6:18 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 6:18 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 6:18 PM 2-Butanone 5. µg/l 1 6/21/216 6:18 PM 2-Hexanone 5. µg/l 1 6/21/216 6:18 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 6:18 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 6:18 PM Acetone 1 µg/l 1 6/21/216 6:18 PM Acrylonitrile 1. µg/l 1 6/21/216 6:18 PM Benzene 1. µg/l 1 6/21/216 6:18 PM Bromochloromethane 1. µg/l 1 6/21/216 6:18 PM Bromodichloromethane 1. µg/l 1 6/21/216 6:18 PM Bromoform 1. µg/l 1 6/21/216 6:18 PM Bromomethane 1. µg/l 1 6/21/216 6:18 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

197 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: Sample ID: 731 Jenni Lane Lab ID: Collection Date: 6/14/216 7:35 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM 6/21/216 6:18 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

198 ALS Group USA, Corp Client: Merit Energy Project: ECT (731 Jeni Lane) Work Order: Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

199 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

200 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 1

201 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

202 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

203 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

204 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

205 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

206 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

207 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

208 Client: Merit Energy Work Order: Project: ECT (731 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR S S The following samples were analyzed in this batch: B QC Page: 1 of 1

209 ALS Group USA, Corp Client: Merit Energy Project: ECT (731 Jeni Lane) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

210 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 1: Work Order: Received by: MEB Checklist completed by Meghan Broadbent Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: water Carrier name: UPS 16-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 6./6. SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 4:33:22 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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213 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (477 Jeni Lane) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

214 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Jeni Lane Water 6/13/216 16:1 6/15/216 9:3 Hold Sample Summary Page 1 of 1

215 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: Sample ID: 477 Jeni Lane Lab ID: Collection Date: 6/13/216 4:1 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/17/216 2:7 AM Sulfolane 1 µg/l 1 6/17/216 2:7 AM Surr: 2,4,6-Tribromophenol %REC 1 6/17/216 2:7 AM Surr: 2-Fluorobiphenyl %REC 1 6/17/216 2:7 AM Surr: 2-Fluorophenol %REC 1 6/17/216 2:7 AM Surr: 4-Terphenyl-d %REC 1 6/17/216 2:7 AM Surr: Nitrobenzene-d %REC 1 6/17/216 2:7 AM Surr: Phenol-d %REC 1 6/17/216 2:7 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 5:5 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 5:5 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 5:5 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 5:5 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 5:5 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 5:5 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 5:5 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 5:5 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 5:5 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 5:5 PM 2-Butanone 5. µg/l 1 6/21/216 5:5 PM 2-Hexanone 5. µg/l 1 6/21/216 5:5 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 5:5 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 5:5 PM Acetone 1 µg/l 1 6/21/216 5:5 PM Acrylonitrile 1. µg/l 1 6/21/216 5:5 PM Benzene 1. µg/l 1 6/21/216 5:5 PM Bromochloromethane 1. µg/l 1 6/21/216 5:5 PM Bromodichloromethane 1. µg/l 1 6/21/216 5:5 PM Bromoform 1. µg/l 1 6/21/216 5:5 PM Bromomethane 1. µg/l 1 6/21/216 5:5 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

216 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: Sample ID: 477 Jeni Lane Lab ID: Collection Date: 6/13/216 4:1 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM 6/21/216 5:5 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

217 ALS Group USA, Corp Client: Merit Energy Project: ECT (477 Jeni Lane) Work Order: Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

218 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

219 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 1

220 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

221 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

222 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

223 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

224 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

225 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

226 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

227 Client: Merit Energy Work Order: Project: ECT (477 Jeni Lane) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR S S The following samples were analyzed in this batch: B QC Page: 1 of 1

228 ALS Group USA, Corp Client: Merit Energy Project: ECT (477 Jeni Lane) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

229 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 3:15:3 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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232 1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (Hartland Jeni Lane) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

233 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Jeni Lane) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Jeni Lane Water 6/6/216 18:36 6/8/216 9:3 Hold Sample Summary Page 1 of 1

234 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Jeni Lane) Work Order: Sample ID: 495 Jeni Lane Lab ID: Collection Date: 6/6/216 6:36 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 7:37 PM Sulfolane 1 µg/l 1 6/9/216 7:37 PM Surr: 2,4,6-Tribromophenol %REC 1 6/9/216 7:37 PM Surr: 2-Fluorobiphenyl %REC 1 6/9/216 7:37 PM Surr: 2-Fluorophenol %REC 1 6/9/216 7:37 PM Surr: 4-Terphenyl-d %REC 1 6/9/216 7:37 PM Surr: Nitrobenzene-d %REC 1 6/9/216 7:37 PM Surr: Phenol-d %REC 1 6/9/216 7:37 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: BG 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 5:5 AM 1,1-Dichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,1-Dichloroethene 1. µg/l 1 6/9/216 5:5 AM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 5:5 AM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 5:5 AM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 5:5 AM 1,2-Dibromoethane 1. µg/l 1 6/9/216 5:5 AM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 1,2-Dichloroethane 1. µg/l 1 6/9/216 5:5 AM 1,2-Dichloropropane 1. µg/l 1 6/9/216 5:5 AM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 5:5 AM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 5:5 AM 2-Butanone 5. µg/l 1 6/9/216 5:5 AM 2-Hexanone 5. µg/l 1 6/9/216 5:5 AM 2-Methylnaphthalene 5. µg/l 1 6/9/216 5:5 AM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 5:5 AM Acetone 1 µg/l 1 6/9/216 5:5 AM Acrylonitrile 1. µg/l 1 6/9/216 5:5 AM Benzene 1. µg/l 1 6/9/216 5:5 AM Bromochloromethane 1. µg/l 1 6/9/216 5:5 AM Bromodichloromethane 1. µg/l 1 6/9/216 5:5 AM Bromoform 1. µg/l 1 6/9/216 5:5 AM Bromomethane 1. µg/l 1 6/9/216 5:5 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

235 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Jeni Lane) Work Order: Sample ID: 495 Jeni Lane Lab ID: Collection Date: 6/6/216 6:36 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM 6/9/216 5:5 AM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

236 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Jeni Lane) Work Order: Date: 1-Jun-16 Case Narrative Batch R189191a The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

237 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Date: 1-Jun-16 Batch ID: 8717 Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/9/216 3:25 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/9/216 3:45 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: B MS Units:µg/L Analysis Date: 6/9/216 6:36 PM Client ID: Run ID: SVMS8_1669A SeqNo: Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

238 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: 8717 Instrument ID SVMS8 Method: SW D DUP Sample ID: B DUP Client ID: 495 Jeni Lane Run ID: SVMS8_1669A Units:µg/L SeqNo:38721 Analysis Date: 6/9/216 7:16 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 2 of 1

239 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MBLK Sample ID: VBLKW R189191a Units:µg/L Analysis Date: 6/9/216 2:2 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

240 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

241 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B LCS Sample ID: VLCSW R189191a Units:µg/L Analysis Date: 6/9/216 1:12 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

242 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 6 of 1

243 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/9/216 1:53 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone , Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene SE S QC Page: 7 of 1

244 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S EO S QC Page: 8 of 1

245 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/9/216 11:18 AM Client ID: Run ID: VMS6_1668B SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone 228 1, Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene SR SRE R S SR SR QC Page: 9 of 1

246 Client: Merit Energy Work Order: Project: ECT (Hartland Jeni Lane) Batch ID: R189191a Instrument ID VMS6 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR SR SREO S SR The following samples were analyzed in this batch: A QC Page: 1 of 1

247 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Jeni Lane) WorkOrder: Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

248 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 8-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 3.6/3.6 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:34:43 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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251 23-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (869 N. Pleasant Valley) Work Order: Dear Sean, ALS Environmental received 1 sample on 15-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

252 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received N. Pleasant Valley Water 6/13/216 16:54 6/15/216 9:3 Hold Sample Summary Page 1 of 1

253 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: Sample ID: 869 N. Pleasant Valley Lab ID: Collection Date: 6/13/216 4:54 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/16/16 Analyst: RM Diisopropanolamine 54 µg/l 1 6/17/216 2:27 AM Sulfolane 11 µg/l 1 6/17/216 2:27 AM Surr: 2,4,6-Tribromophenol %REC 1 6/17/216 2:27 AM Surr: 2-Fluorobiphenyl %REC 1 6/17/216 2:27 AM Surr: 2-Fluorophenol %REC 1 6/17/216 2:27 AM Surr: 4-Terphenyl-d %REC 1 6/17/216 2:27 AM Surr: Nitrobenzene-d %REC 1 6/17/216 2:27 AM Surr: Phenol-d %REC 1 6/17/216 2:27 AM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,1-Trichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,2-Trichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/21/216 5:29 PM 1,1-Dichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,1-Dichloroethene 1. µg/l 1 6/21/216 5:29 PM 1,2,3-Trichloropropane 1. µg/l 1 6/21/216 5:29 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/21/216 5:29 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/21/216 5:29 PM 1,2-Dibromoethane 1. µg/l 1 6/21/216 5:29 PM 1,2-Dichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 1,2-Dichloroethane 1. µg/l 1 6/21/216 5:29 PM 1,2-Dichloropropane 1. µg/l 1 6/21/216 5:29 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/21/216 5:29 PM 1,3-Dichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 1,4-Dichlorobenzene 1. µg/l 1 6/21/216 5:29 PM 2-Butanone 5. µg/l 1 6/21/216 5:29 PM 2-Hexanone 5. µg/l 1 6/21/216 5:29 PM 2-Methylnaphthalene 5. µg/l 1 6/21/216 5:29 PM 4-Methyl-2-pentanone 1. µg/l 1 6/21/216 5:29 PM Acetone 1 µg/l 1 6/21/216 5:29 PM Acrylonitrile 1. µg/l 1 6/21/216 5:29 PM Benzene 1. µg/l 1 6/21/216 5:29 PM Bromochloromethane 1. µg/l 1 6/21/216 5:29 PM Bromodichloromethane 1. µg/l 1 6/21/216 5:29 PM Bromoform 1. µg/l 1 6/21/216 5:29 PM Bromomethane 1. µg/l 1 6/21/216 5:29 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

254 ALS Group USA, Corp Date: 23-Jun-16 Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: Sample ID: 869 N. Pleasant Valley Lab ID: Collection Date: 6/13/216 4:54 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM 6/21/216 5:29 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

255 ALS Group USA, Corp Client: Merit Energy Project: ECT (869 N. Pleasant Valley) Work Order: Date: 23-Jun-16 Case Narrative Batch R189964A Sample VLCSW The LCS recovery for Volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were nondetect. No qualification is necessary for this analyte. Batch R189964A The MS/MSD data for Volatiles is not related to this projects sample. No data requires qualification. Case Narrative Page 1 of 1

256 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Date: 23-Jun-16 Batch ID: Instrument ID SVMS8 Method: SW D MBLK Sample ID: SBLKW Units:µg/L Analysis Date: 6/16/216 7:57 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units:µg/L Analysis Date: 6/16/216 8:17 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: A MS Units:µg/L Analysis Date: 6/16/216 1:5 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

257 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: Instrument ID SVMS8 Method: SW D DUP Sample ID: A DUP Units:µg/L Analysis Date: 6/16/216 1:45 PM Client ID: Run ID: SVMS8_16616A SeqNo: Prep Date: 6/16/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: A QC Page: 2 of 1

258 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MBLK Sample ID: VBLKW R189964A Units:µg/L Analysis Date: 6/21/216 2:16 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

259 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

260 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B LCS Sample ID: VLCSW R189964A Units:µg/L Analysis Date: 6/21/216 1:3 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

261 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

262 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MS Sample ID: A MS Units:µg/L Analysis Date: 6/21/216 8:44 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

263 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

264 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B MSD Sample ID: A MSD Units:µg/L Analysis Date: 6/21/216 9:8 PM Client ID: Run ID: VMS1_16621A SeqNo: Prep Date: DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

265 Client: Merit Energy Work Order: Project: ECT (869 N. Pleasant Valley) Batch ID: R189964A Instrument ID VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d SR S S The following samples were analyzed in this batch: B QC Page: 1 of 1

266 ALS Group USA, Corp Client: Merit Energy Project: ECT (869 N. Pleasant Valley) WorkOrder: Date: 23-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit background or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

267 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 15-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 15-Jun-16 Reviewed by: esignature Date esignature Matrices: Water Carrier name: FedEx 15-Jun-16 Date Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.2/2.2 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/15/216 3:17:42 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction: SRC Page 1 of 1

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270 1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (Hartland Lone Tree Rd) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

271 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Lone Tree Rd Water 6/7/216 7:16 6/8/216 9:3 Hold Sample Summary Page 1 of 1

272 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Sample ID: Lone Tree Rd Lab ID: Collection Date: 6/7/216 7:16 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 58 µg/l 1 6/9/216 8:17 PM Sulfolane 12 µg/l 1 6/9/216 8:17 PM Surr: 2,4,6-Tribromophenol %REC 1 6/9/216 8:17 PM Surr: 2-Fluorobiphenyl %REC 1 6/9/216 8:17 PM Surr: 2-Fluorophenol %REC 1 6/9/216 8:17 PM Surr: 4-Terphenyl-d %REC 1 6/9/216 8:17 PM Surr: Nitrobenzene-d %REC 1 6/9/216 8:17 PM Surr: Phenol-d %REC 1 6/9/216 8:17 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 2:26 PM 1,1-Dichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,1-Dichloroethene 1. µg/l 1 6/9/216 2:26 PM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 2:26 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 2:26 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 2:26 PM 1,2-Dibromoethane 1. µg/l 1 6/9/216 2:26 PM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 1,2-Dichloroethane 1. µg/l 1 6/9/216 2:26 PM 1,2-Dichloropropane 1. µg/l 1 6/9/216 2:26 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 2:26 PM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 2:26 PM 2-Butanone 5. µg/l 1 6/9/216 2:26 PM 2-Hexanone 5. µg/l 1 6/9/216 2:26 PM 2-Methylnaphthalene 5. µg/l 1 6/9/216 2:26 PM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 2:26 PM Acetone 1 µg/l 1 6/9/216 2:26 PM Acrylonitrile 1. µg/l 1 6/9/216 2:26 PM Benzene 1. µg/l 1 6/9/216 2:26 PM Bromochloromethane 1. µg/l 1 6/9/216 2:26 PM Bromodichloromethane 1. µg/l 1 6/9/216 2:26 PM Bromoform 1. µg/l 1 6/9/216 2:26 PM Bromomethane 1. µg/l 1 6/9/216 2:26 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

273 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Sample ID: Lone Tree Rd Lab ID: Collection Date: 6/7/216 7:16 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM 6/9/216 2:26 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

274 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Date: 1-Jun-16 Case Narrative Batch R Sample VLCSW The LCS recovery for volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were non-detect. No qualification is necessary for this analyte. Batch R The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

275 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Date: 1-Jun-16 Batch ID: 8717 Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKW Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 3:25 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 3:45 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: B MS Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 6:36 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

276 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: 8717 Instrument ID: SVMS8 Method: SW D DUP Sample ID: B DUP Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 7:16 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 2 of 1

277 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B MBLK Sample ID: VBLKW R Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 1:38 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

278 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

279 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B LCS Sample ID: VLCSW R Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 1:58 AM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

280 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

281 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B MS Sample ID: A MS Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 8:55 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

282 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

283 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B MSD Sample ID: A MSD Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 9:2 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

284 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S The following samples were analyzed in this batch: A QC Page: 1 of 1

285 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) WorkOrder: Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

286 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature 8-Jun-16 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.4/2.4 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:41:25 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

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289 1-Jun-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: ECT (Hartland Lone Tree Rd) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jun-216 9:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 19. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

290 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Date Received Lone Tree Rd Water 6/7/216 7:54 6/8/216 9:3 Hold Sample Summary Page 1 of 1

291 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Sample ID: Lone Tree Rd Lab ID: Collection Date: 6/7/216 7:54 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 6/9/16 Analyst: RM Diisopropanolamine 5 µg/l 1 6/9/216 8:58 PM Sulfolane 1 µg/l 1 6/9/216 8:58 PM Surr: 2,4,6-Tribromophenol %REC 1 6/9/216 8:58 PM Surr: 2-Fluorobiphenyl %REC 1 6/9/216 8:58 PM Surr: 2-Fluorophenol %REC 1 6/9/216 8:58 PM Surr: 4-Terphenyl-d %REC 1 6/9/216 8:58 PM Surr: Nitrobenzene-d %REC 1 6/9/216 8:58 PM Surr: Phenol-d %REC 1 6/9/216 8:58 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,1-Trichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,2-Trichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 6/9/216 3:15 PM 1,1-Dichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,1-Dichloroethene 1. µg/l 1 6/9/216 3:15 PM 1,2,3-Trichloropropane 1. µg/l 1 6/9/216 3:15 PM 1,2,4-Trichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 1,2,4-Trimethylbenzene 1. µg/l 1 6/9/216 3:15 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 6/9/216 3:15 PM 1,2-Dibromoethane 1. µg/l 1 6/9/216 3:15 PM 1,2-Dichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 1,2-Dichloroethane 1. µg/l 1 6/9/216 3:15 PM 1,2-Dichloropropane 1. µg/l 1 6/9/216 3:15 PM 1,3,5-Trimethylbenzene 1. µg/l 1 6/9/216 3:15 PM 1,3-Dichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 1,4-Dichlorobenzene 1. µg/l 1 6/9/216 3:15 PM 2-Butanone 5. µg/l 1 6/9/216 3:15 PM 2-Hexanone 5. µg/l 1 6/9/216 3:15 PM 2-Methylnaphthalene 5. µg/l 1 6/9/216 3:15 PM 4-Methyl-2-pentanone 1. µg/l 1 6/9/216 3:15 PM Acetone 1 µg/l 1 6/9/216 3:15 PM Acrylonitrile 1. µg/l 1 6/9/216 3:15 PM Benzene 1. µg/l 1 6/9/216 3:15 PM Bromochloromethane 1. µg/l 1 6/9/216 3:15 PM Bromodichloromethane 1. µg/l 1 6/9/216 3:15 PM Bromoform 1. µg/l 1 6/9/216 3:15 PM Bromomethane 1. µg/l 1 6/9/216 3:15 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

292 ALS Group USA, Corp Date: 1-Jun-16 Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Sample ID: Lone Tree Rd Lab ID: Collection Date: 6/7/216 7:54 AM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM 6/9/216 3:15 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

293 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) Work Order: Date: 1-Jun-16 Case Narrative Batch R Sample VLCSW The LCS recovery for volatile compound Methyl Iodide was above the upper control limit. All the sample results in the batch were non-detect. No qualification is necessary for this analyte. Batch R The MS/MSD data for Volatiles is not related to this project's sample. No data requires qualification. Case Narrative Page 1 of 1

294 ALS Group USA, Corp Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Date: 1-Jun-16 Batch ID: 8717 Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKW Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 3:25 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 3:45 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d MS Sample ID: B MS Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 6:36 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d QC Page: 1 of 1

295 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: 8717 Instrument ID: SVMS8 Method: SW D DUP Sample ID: B DUP Units: µg/l Client ID: Run ID: SVMS8_1669A SeqNo: Analysis Date: 6/9/216 7:16 PM Prep Date: 6/9/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 53 3 Sulfolane 11 3 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 2 of 1

296 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B MBLK Sample ID: VBLKW R Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 1:38 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 3 of 1

297 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 4 of 1

298 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B LCS Sample ID: VLCSW R Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 1:58 AM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 5 of 1

299 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 6 of 1

300 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B MS Sample ID: A MS Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 8:55 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 7 of 1

301 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 8 of 1

302 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B MSD Sample ID: A MSD Units: µg/l Client ID: Run ID: VMS1_1669A SeqNo: Prep Date: Analysis Date: 6/9/216 9:2 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene QC Page: 9 of 1

303 Client: Merit Energy Work Order: Project: ECT (Hartland Lone Tree Rd) Batch ID: R Instrument ID: VMS1 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S The following samples were analyzed in this batch: A QC Page: 1 of 1

304 ALS Group USA, Corp Client: Merit Energy Project: ECT (Hartland Lone Tree Rd) WorkOrder: Date: 1-Jun-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and PQL, sample results may exhibit background or reag contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

305 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jun-16 9:3 Work Order: Received by: KRW Checklist completed by Keith Wierenga Gary Byar 8-Jun-16 Reviewed by: esignature Date esignature 8-Jun-16 Date Matrices: Carrier name: Water FedEx Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 2.4/2.4 C SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 6/8/216 2:55:5 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

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308 13-Jul-216 Sean Craven Merit Energy 151 Thomas Rd PO Box 91 Kalkaska, MI Re: Merit (13955 Cherry Blossom Ln) Work Order: Dear Sean, ALS Environmental received 1 sample on 8-Jul-216 1:3 AM for the analyses presented in the following report. The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Sample results are compliant with NELAP standard requirements and QC results achieved laboratory specifications. Any exceptions are noted in the Case Narrative, or noted with qualifiers in the report or QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained from ALS Environmental. Samples will be disposed in 3 days unless storage arrangements are made. The total number of pages in this report is 18. If you have any questions regarding this report, please feel free to contact me. Sincerely, Gary Byar Electronically approved by: Gary Byar Gary Byar Project Manager Certificate No: MI: 22 Report of Laboratory Analysis ADDRESS th Avenue Holland, Michigan PHONE (616) FAX (616) ALS GROUP USA, CORP Part of the ALS Laboratory Group A Campbell Brothers Limited Company

309 ALS Group USA, Corp Date: 13-Jul-16 Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: Work Order Sample Summary Lab Samp ID Client Sample ID Matrix Tag Number Collection Date Cherry Blossom Ln (Water Well) Date Received Water 7/7/216 14:3 7/8/216 1:3 Hold Sample Summary Page 1 of 1

310 ALS Group USA, Corp Date: 13-Jul-16 Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: Sample ID: Cherry Blossom Ln (Water Well) Lab ID: Collection Date: 7/7/216 2:3 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed SEMI-VOLATILE ORGANIC COMPOUS SW D Prep: SW351 / 7/11/16 Analyst: RM Diisopropanolamine 5 µg/l 1 7/12/216 1:36 PM Sulfolane 1 µg/l 1 7/12/216 1:36 PM Surr: 2,4,6-Tribromophenol %REC 1 7/12/216 1:36 PM Surr: 2-Fluorobiphenyl %REC 1 7/12/216 1:36 PM Surr: 2-Fluorophenol %REC 1 7/12/216 1:36 PM Surr: 4-Terphenyl-d %REC 1 7/12/216 1:36 PM Surr: Nitrobenzene-d %REC 1 7/12/216 1:36 PM Surr: Phenol-d %REC 1 7/12/216 1:36 PM VOLATILE ORGANIC COMPOUS SW826B Analyst: AK 1,1,1,2-Tetrachloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,1-Trichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,2,2-Tetrachloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,2-Trichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1,2-Trichlorotrifluoroethane 1. µg/l 1 7/12/216 5:44 PM 1,1-Dichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,1-Dichloroethene 1. µg/l 1 7/12/216 5:44 PM 1,2,3-Trichloropropane 1. µg/l 1 7/12/216 5:44 PM 1,2,4-Trichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 1,2,4-Trimethylbenzene 1. µg/l 1 7/12/216 5:44 PM 1,2-Dibromo-3-chloropropane 1. µg/l 1 7/12/216 5:44 PM 1,2-Dibromoethane 1. µg/l 1 7/12/216 5:44 PM 1,2-Dichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 1,2-Dichloroethane 1. µg/l 1 7/12/216 5:44 PM 1,2-Dichloropropane 1. µg/l 1 7/12/216 5:44 PM 1,3,5-Trimethylbenzene 1. µg/l 1 7/12/216 5:44 PM 1,3-Dichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 1,4-Dichlorobenzene 1. µg/l 1 7/12/216 5:44 PM 2-Butanone 5. µg/l 1 7/12/216 5:44 PM 2-Hexanone 5. µg/l 1 7/12/216 5:44 PM 2-Methylnaphthalene 5. µg/l 1 7/12/216 5:44 PM 4-Methyl-2-pentanone 1. µg/l 1 7/12/216 5:44 PM Acetone 1 µg/l 1 7/12/216 5:44 PM Acrylonitrile 1. µg/l 1 7/12/216 5:44 PM Benzene 1. µg/l 1 7/12/216 5:44 PM Bromochloromethane 1. µg/l 1 7/12/216 5:44 PM Bromodichloromethane 1. µg/l 1 7/12/216 5:44 PM Bromoform 1. µg/l 1 7/12/216 5:44 PM Bromomethane 1. µg/l 1 7/12/216 5:44 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 1 of 2

311 ALS Group USA, Corp Date: 13-Jul-16 Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: Sample ID: Cherry Blossom Ln (Water Well) Lab ID: Collection Date: 7/7/216 2:3 PM Matrix: WATER Analyses Result Qual Report Dilution Limit Units Factor Date Analyzed Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diethyl ether Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 5. µg/l 1 5. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 2. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 1. µg/l 1 3. µg/l %REC %REC %REC %REC 1 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM 7/12/216 5:44 PM See Qualifiers page for a list of qualifiers and their definitions. Analytical Results Page 2 of 2

312 ALS Group USA, Corp Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) Work Order: Date: 13-Jul-16 Case Narrative Batch R The MS/MSD data for volatiles is not related to this project's sample. No data requires qualification. Batch R The LCS recovery for volatile compounds 1,2 Dibromoethane and Methyl iodide was above the upper control limit. Sample results were non-detect for these compounds therefore no data requires qualification. Case Narrative Page 1 of 1

313 ALS Group USA, Corp Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Date: 13-Jul-16 Batch ID: 8841 Instrument ID: SVMS8 Method: SW D MBLK Sample ID: SBLKW Units: µg/l Client ID: Run ID: SVMS8_16712A SeqNo: Analysis Date: 7/12/216 12:32 PM Prep Date: 7/11/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine 5 Sulfolane 1 Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCS Sample ID: SLCSW Units: µg/l Client ID: Run ID: SVMS8_16712A SeqNo: Analysis Date: 7/12/216 12:53 PM Prep Date: 7/11/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d LCSD Sample ID: SLCSDW Units: µg/l Client ID: Run ID: SVMS8_16712A SeqNo: Analysis Date: 7/12/216 1:14 PM Prep Date: 7/11/216 DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual Diisopropanolamine Sulfolane Surr: 2,4,6-Tribromophenol Surr: 2-Fluorobiphenyl Surr: 2-Fluorophenol Surr: 4-Terphenyl-d Surr: Nitrobenzene-d Surr: Phenol-d The following samples were analyzed in this batch: B QC Page: 1 of 9

314 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B MBLK Sample ID: VBLKW R Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: Prep Date: Analysis Date: 7/12/216 1:21 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % 1,1,1,2-Tetrachloroethane 1. 1,1,1-Trichloroethane 1. 1,1,2,2-Tetrachloroethane 1. 1,1,2-Trichloroethane 1. 1,1,2-Trichlorotrifluoroethane 1. 1,1-Dichloroethane 1. 1,1-Dichloroethene 1. 1,2,3-Trichloropropane 1. 1,2,4-Trichlorobenzene 1. 1,2,4-Trimethylbenzene 1. 1,2-Dibromo-3-chloropropane 1. 1,2-Dibromoethane 1. 1,2-Dichlorobenzene 1. 1,2-Dichloroethane 1. 1,2-Dichloropropane 1. 1,3,5-Trimethylbenzene 1. 1,3-Dichlorobenzene 1. 1,4-Dichlorobenzene 1. 2-Butanone 5. 2-Hexanone 5. 2-Methylnaphthalene 5. 4-Methyl-2-pentanone 1. Acetone 1 Acrylonitrile 1. Benzene 1. Bromochloromethane 1. Bromodichloromethane 1. Bromoform 1. Bromomethane 1. Carbon disulfide 1. Carbon tetrachloride 1. Chlorobenzene 1. Chloroethane 1. Chloroform 1. Chloromethane 1. cis-1,2-dichloroethene 1. cis-1,3-dichloropropene 1. Dibromochloromethane 1. Dibromomethane 1. Dichlorodifluoromethane 1. Diethyl ether 1. Ethylbenzene 1. Limit Qual QC Page: 2 of 9

315 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B Hexachloroethane 1. Isopropylbenzene 1. m,p-xylene 2. Methyl iodide 1. Methyl tert-butyl ether 1. Methylene chloride 5. Naphthalene 5. n-propylbenzene 1. o-xylene 1. Styrene 1. Tetrachloroethene 1. Toluene 1. trans-1,2-dichloroethene 1. trans-1,3-dichloropropene 1. trans-1,4-dichloro-2-butene 2. Trichloroethene 1. Trichlorofluoromethane 1. Vinyl acetate 1. Vinyl chloride 1. Xylenes, Total 3. Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d QC Page: 3 of 9

316 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B LCS Sample ID: VLCSW R Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: Prep Date: Analysis Date: 7/12/216 12:6 PM DF: 1 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone Hexanone Methyl-2-pentanone Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene S QC Page: 4 of 9

317 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride Naphthalene n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S QC Page: 5 of 9

318 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B MS Sample ID: A MS Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: Prep Date: Analysis Date: 7/12/216 9:2 PM DF: 5 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone 73 2, Hexanone , Methyl-2-pentanone Acetone 778 5, Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene , S QC Page: 6 of 9

319 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride , Naphthalene 974 2, n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene 758 1, Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total , Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S S QC Page: 7 of 9

320 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B MSD Sample ID: A MSD Units: µg/l Client ID: Run ID: VMS9_16712A SeqNo: Prep Date: Analysis Date: 7/12/216 9:27 PM DF: 5 SPK Ref Control Ref Analyte Result PQL SPK Val Value %REC Limit Value % Limit Qual 1,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane ,2-Dibromoethane ,2-Dichlorobenzene ,2-Dichloroethane ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Butanone 767 2, Hexanone 83 2, Methyl-2-pentanone Acetone 87 5, Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachloroethane Isopropylbenzene m,p-xylene , S S QC Page: 8 of 9

321 Client: Merit Energy Work Order: Project: Merit (13955 Cherry Blossom Ln) Batch ID: R Instrument ID: VMS9 Method: SW826B Methyl iodide Methyl tert-butyl ether Methylene chloride 881 2, Naphthalene , n-propylbenzene o-xylene Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene trans-1,4-dichloro-2-butene 77 1, Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total , Surr: 1,2-Dichloroethane-d Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d S The following samples were analyzed in this batch: A QC Page: 9 of 9

322 ALS Group USA, Corp Client: Merit Energy Project: Merit (13955 Cherry Blossom Ln) WorkOrder: Date: 13-Jul-16 QUALIFIERS, ACRONYMS, UNITS Qualifier * a B E H J n O P R S U X Acronym DUP LCS LCSD LOD LOQ MBLK MDL MS MSD PQL TDL TNTC A D E SW Units Reported µg/l Description Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte is present at an estimated concentration between the MDL and Report Limit Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 4% above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL Analyte was detected in the Method Blank between the MDL and Reporting Limit, sample results may exhibit backgro or reagent contamination at the observed level. Description Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Limit of Detection (see MDL) Limit of Quantitation (see PQL) Method Blank Method Detection Limit Matrix Spike Matrix Spike Duplicate Practical Quantitation Limit Relative Percent Difference Target Detection Limit Too Numerous To Count APHA Standard Methods ASTM EPA SW-846 Update III Description Micrograms per Liter QF Page 1 of 1

323 ALS Group USA, Corp Sample Receipt Checklist Client Name: MERITENERGY Date/Time Received: 8-Jul-16 1:3 Work Order: Received by: DS Checklist completed by Diane Shaw Gary Byar 8-Jul-16 Reviewed by: esignature Date esignature 8-Jul-16 Date Matrices: Carrier name: Water UPS Shipping container/cooler in good condition? Yes No Not Present Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of custody present? Yes No Chain of custody signed when relinquished and received? Yes No Chain of custody agrees with sample labels? Yes No Samples in proper container/bottle? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No All samples received within holding time? Yes No Container/Temp Blank temperature in compliance? Yes No Sample(s) received on ice? Yes No Temperature(s)/Thermometer(s): 4.6/4.6 c SR2 Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? 7/8/216 1:35:5 PM Yes No No VOA vials submitted Water - ph acceptable upon receipt? Yes No N/A ph adjusted? Yes No N/A ph adjusted by: Login Notes: Client Contacted: Date Contacted: Person Contacted: Contacted By: Regarding: Comments: CorrectiveAction SRC Page 1 of 1

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