ANALYTICAL REPORT. Attn: Thomas W Hensel

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release by: //0 ::0 PM Marty Edwards, Manager of Project Management (0)-0 marty.edwards@testamericainc.

1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Foster Creighton Drive Nashville, TN 0 Tel: ()-0 TestAmerica Job ID: 0-- Client Revision: For: AMEC Foster Wheeler E & I, Inc Cogdill Road Knoxville, Tennessee Attn: Thomas W Hensel Authorized for release by: //0 ::0 PM Marty Edwards, Manager of Project Management (0)-0 marty.edwards@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

2 Table of Contents TestAmerica Job ID: 0-- Cover Page Table of Contents Sample Summary Case Narrative Definitions Detection Summary Client Sample Results QC Association QC Sample Results Chronicle Method Summary Certification Summary Chain of Custody Receipt Checklists Page of //0

3 Sample Summary TestAmerica Job ID: 0-- Lab Sample ID Client Sample ID Matrix Collected Received 0-- Denso Well Water 0/0/: 0/0/0: 0-- Macamber Well Water 0/0/ 0: 0/0/ 0: 0-- Trip Blank Water 0/0/ 0:00 0/0/ 0: Page of //0

4 Case Narrative Client: AMEC Foster Wheeler E & I, Inc TestAmerica Job ID: 0-- Job ID: 0-- Laboratory: Narrative Comments No additional comments. Job Narrative 0-- Receipt The samples were received on //0 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 0.º C. GC/MS VOA Method 0B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with analytical batch 0-. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Revised Report The deliverables were revised to report a lower detection limit (MDL). Page of //0

5 Glossary Definitions/Glossary TestAmerica Job ID: 0-- Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) Page of //0

6 Detection Summary TestAmerica Job ID: 0-- Client Sample ID: Denso Well Lab Sample ID: 0-- No Detections. Client Sample ID: Macamber Well Lab Sample ID: 0-- No Detections. Client Sample ID: Trip Blank Lab Sample ID: 0-- No Detections. This Detection Summary does not include radiochemical test results. Page of //0

7 Client Sample ID: Denso Well Date Collected: 0/0/: Date Received: 0/0/0: Method: 0B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 0-- Lab Sample ID: 0-- Matrix: Water Analyzed Acrylonitrile < ug/l 0/0/ : Surrogate %Recovery Qualifier Limits -Bromofluorobenzene (Surr) 0-0 0/0/ : Unit D Analyzed,-Dichloroethane-d (Surr) 0-0 0/0/: Dibromofluoromethane (Surr) 0-0 0/0/: Toluene-d (Surr) 0-0 0/0/: Dil Fac Dil Fac Page of //0

8 Client Sample ID: Macamber Well Date Collected: 0/0/0: Date Received: 0/0/0: Method: 0B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 0-- Lab Sample ID: 0-- Matrix: Water Analyzed Acrylonitrile < ug/l 0/0/ : Surrogate %Recovery Qualifier Limits -Bromofluorobenzene (Surr) 0-0 0/0/ : Unit D Analyzed,-Dichloroethane-d (Surr) 0-0 0/0/: Dibromofluoromethane (Surr) 0-0 0/0/: Toluene-d (Surr) 0-0 0/0/: Dil Fac Dil Fac Page of //0

9 Client Sample ID: Trip Blank Date Collected: 0/0/0:00 Date Received: 0/0/0: Method: 0B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier Client Sample Results RL MDL TestAmerica Job ID: 0-- Lab Sample ID: 0-- Matrix: Water Analyzed Acrylonitrile < ug/l 0/0/ : Surrogate %Recovery Qualifier Limits -Bromofluorobenzene (Surr) 0-0 0/0/ : Unit D Analyzed,-Dichloroethane-d (Surr) 0-0 0/0/: Dibromofluoromethane (Surr) 0-0 0/0/: Toluene-d (Surr) 0-0 0/0/: Dil Fac Dil Fac Page of //0

10 GC/MS VOA Analysis Batch: QC Association Summary TestAmerica Job ID: 0-- Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 0-- Denso Well Total/NA Water 0B 0-- Macamber Well Total/NA 0-- Trip Blank Total/NA LCS 0-/ Lab Control Sample Total/NA LCSD 0-/ Lab Control Sample Dup Total/NA MB 0-/ Method Blank Total/NA Water Water Water Water Water 0B 0B 0B 0B 0B Page of //0

11 QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 0-/ Matrix: Water Analysis Batch: Analyte MB MB Result Qualifier RL MDL TestAmerica Job ID: 0-- Client Sample ID: Method Blank Prep Type: Total/NA Analyzed Acrylonitrile < ug/l 0/0/ 0: Surrogate %Recovery MB MB Qualifier Limits -Bromofluorobenzene (Surr) 0-0 0/0/ 0: Unit D Analyzed,-Dichloroethane-d (Surr) 0-0 0/0/0: Dibromofluoromethane (Surr) 0-0 0/0/0: Toluene-d (Surr) 0-0 0/0/0: Lab Sample ID: LCS 0-/ Matrix: Water Analysis Batch: Analyte Spike Added LCS LCS Result Qualifier Dil Fac Dil Fac Client Sample ID: Lab Control Sample Prep Type: Total/NA Acrylonitrile 00 0 ug/l - 0 Surrogate %Recovery LCS LCS Qualifier Limits -Bromofluorobenzene (Surr) 0-0,-Dichloroethane-d (Surr) 0-0 Dibromofluoromethane (Surr) 0-0 Toluene-d (Surr) 0-0 Unit D %Rec %Rec. Limits Lab Sample ID: LCSD 0-/ Matrix: Water Analysis Batch: Analyte Spike Added LCSD LCSD Result Qualifier Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Acrylonitrile 00 ug/l - 0 Surrogate LCSD LCSD %Recovery Qualifier Limits -Bromofluorobenzene (Surr) 0-0,-Dichloroethane-d (Surr) Dibromofluoromethane (Surr) 0-0 Toluene-d (Surr) 0-0 Unit D %Rec %Rec. Limits RPD RPD Limit Page of //0

12 Lab Chronicle Client: AMEC Foster Wheeler E & I, Inc TestAmerica Job ID: 0-- Client Sample ID: Denso Well Lab Sample ID: 0-- Date Collected: 0/0/: Matrix: Water Date Received: 0/0/0: Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyzed Analyst Total/NA Analysis 0B ml ml 0/0/: MJH TAL NSH Final Batch Number Client Sample ID: Macamber Well Lab Sample ID: 0-- Date Collected: 0/0/0: Matrix: Water Date Received: 0/0/0: Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyzed Analyst Total/NA Analysis 0B ml ml 0/0/: MJH TAL NSH Final Batch Number Client Sample ID: Trip Blank Lab Sample ID: 0-- Date Collected: 0/0/0:00 Matrix: Water Date Received: 0/0/0: Prep Type Batch Type Batch Method Run Dil Factor Initial Amount Amount or Analyzed Analyst Total/NA Analysis 0B ml ml 0/0/: MJH TAL NSH Laboratory References: TAL NSH =, 0 Foster Creighton Drive, Nashville, TN 0, TEL ()-0 Final Batch Number Lab Lab Lab Page of //0

13 Method Summary TestAmerica Job ID: 0-- Method Method Description Protocol Laboratory 0B Volatile Organic Compounds (GC/MS) SW TAL NSH Protocol References: SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL NSH =, 0 Foster Creighton Drive, Nashville, TN 0, TEL ()-0 Page of //0

14 Certification Summary Client: AMEC Foster Wheeler E & I, Inc TestAmerica Job ID: 0-- Laboratory: All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification ID Expiration Date ALA ALA NA: NELAP & ALA -- ALA ISO/IEC Alaska (UST) State Program UST-0 -- Arizona State Program AZ Arkansas DEQ State Program California State Program -- Connecticut State Program PH Florida NELAP E 0-0- Georgia State Program N/A 0-0- Illinois NELAP Iowa State Program 0-0- Kansas NELAP E- -- Kentucky (UST) State Program 0-0- Kentucky (WW) State Program Louisiana NELAP Maryland State Program 0-- Massachusetts State Program M-TN Minnesota NELAP Mississippi State Program N/A 0-0- * Montana (UST) State Program NA 0--0 Nevada State Program TN New Hampshire NELAP -0- New Jersey NELAP TN 0-0- New York NELAP 0-- North Carolina (WW/SW) State Program -- North Dakota State Program R * Ohio VAP State Program CL00 -- Oklahoma State Program 0-- Oregon NELAP TN Pennsylvania NELAP Rhode Island State Program LAO00-0- South Carolina State Program 00 (00) 0-- South Carolina (DW) State Program 00 (00) -- Tennessee State Program Texas NELAP T USDA Federal S- -0- Utah NELAP TN * Virginia NELAP Washington State Program C 0-- * West Virginia DEP State Program 0-- Wisconsin State Program Wyoming (UST) ALA.0 -- Laboratory: TestAmerica Pensacola All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification ID Expiration Date Alabama State Program * Arizona State Program AZ0 0-- Arkansas DEQ State Program * Certification renewal pending - certification considered valid. Page of //0

15 Certification Summary Client: AMEC Foster Wheeler E & I, Inc TestAmerica Job ID: 0-- Laboratory: TestAmerica Pensacola (Continued) All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification ID Expiration Date Florida NELAP E 0-0- Georgia State Program N/A 0-0- Illinois NELAP Iowa State Program 0-- Kansas NELAP E- 0-- * Kentucky (UST) State Program 0-0- * Kentucky (WW) State Program Louisiana NELAP * Maryland State Program 0-0- Massachusetts State Program M-FL Michigan State Program 0-0- * New Jersey NELAP FL * North Carolina (WW/SW) State Program -- Oklahoma State Program 0-- Pennsylvania NELAP Rhode Island State Program LAO South Carolina State Program * Tennessee State Program TN * Texas NELAP T USDA Federal P Virginia NELAP West Virginia DEP State Program 0-0- * Certification renewal pending - certification considered valid. Page of //0

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18 Login Sample Receipt Checklist Client: AMEC Foster Wheeler E & I, Inc Job Number: 0-- Login Number: List Source: List Number: Creator: McBride, Mike Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. N/A N/A N/A Page of //0

ANALYTICAL REPORT. Attn: Richard Boelter

ANALYTICAL REPORT. Attn: Richard Boelter ANALYTICAL REPORT TestAmerica Laboratories, Inc. 0 Community Drive Suite South Burlington, VT 00 Tel: (0)0-0 TestAmerica Job ID: 00-0- TestAmerica Sample Delivery Group: 00-0 Client For: ARCADIS U.S. Inc