CERTIFICATE OF ANALYSIS
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1 Your Project #: VILLAGE OF TAHSIS Your C.O.C. #: Attention:Mark DeGagne -35 Estevan Rd Nanaimo, BC CANADA V9S 3Y3 Report #: R24287 Version: - Final MAXXAM JOB #: B5B343 Received: 205/2/22, 5:45 Sample Matrix: Water # Samples Received: Analyses Chloride by Automated Colourimetry () Conductance - water () EPH in Water when PAH required () Nitrate + Nitrite (N) () Nitrite (N) by CFA () Nitrogen - Nitrate (as N) () PAH in Water by GC/MS (SIM) () Total LMW, HMW, Total PAH Calc () ph Water (, 5) Phenols (4-AAP) () Phenoxyalkyl acid Pesticides (2) Sulphate by Automated Colourimetry () Total Dissolved Solids (Filt. Residue) () EPH less PAH in Water by GC/FID () Tannin & Lignin (Total) () Carbon (Total Organic) (, 6) VOCs, VH, F, LH in Water by HS GC/MS () Volatile HC-BTEX () Glyphosate Water Subcontract (3) Pesticides in Water by LCMS Subcontract (4) RFA Water Subcontract (4) CERTIFICATE OF ANALYSIS Date Quantity Extracted Date Analyzed Laboratory Method N/A 205/2/29 BBY6SOP-000 N/A 205/2/29 BBY6SOP /2/ 205/2/3 BBY8SOP N/A 205/2/24 BBY6SOP-0000 N/A 205/2/24 BBY6SOP-0000 N/A 205/2/29 BBY6SOP /2/ 205/2/3 BBY8SOP-0002 N/A 206/0/04 BBY WI N/A 205/2/29 BBY6SOP N/A 205/2/29 BBY6SOP /0/06 206/0/06 CAL SOP-000 N/A 205/2/29 BBY6SOP /2/24 205/2/29 BBY6SOP N/A 206/0/04 BBY WI N/A 205/2/24 BRN SOP-0022 R.0 N/A 205/2/ BBY6SOP /2/24 205/2/24 BBY8SOP N/A 205/2/29 BBY WI /0/ 206/0/ CAM SOP /0/2 206/0/2 206/0/2 206/0/2 Analytical Method SM Cl- G m SM B m BCMOE EPH w 2/00 m SM NO3- I m SM NO3- I m SM NO3 I m EPA 8270d R4 m Auto Calc SM H+ B m SM D m EPA 85 R m SM SO42- E m SM C m Auto Calc SM-5550 B SM 22 5 C m EPA 8260c R3 m Auto Calc HPLC/FLD Reference Method suffix m indicates test methods incorporate validated modifications from specific reference methods to improve performance. * RPDs calculated using raw data. The rounding of final results may result in the apparent difference. () This test was performed by Maxxam Vancouver (2) This test was performed by Maxxam Calgary Environmental (3) This test was performed by Maxxam Ontario (From Burnaby) (4) This test was performed by Maxxam Montreal (From Burnaby) (5) The BC-MOE and APHA Standard Method require ph to be analysed within 5 minutes of sampling and therefore field analysis is required for compliance. All Laboratory ph analyses in this report are reported past the BC-MOE/APHA Standard Method holding time. (6) TOC present in the sample should be considered as non-purgeable TOC. Page of 4
2 Your Project #: VILLAGE OF TAHSIS Your C.O.C. #: Attention:Mark DeGagne -35 Estevan Rd Nanaimo, BC CANADA V9S 3Y3 Report #: R24287 Version: - Final MAXXAM JOB #: B5B343 Received: 205/2/22, 5:45 CERTIFICATE OF ANALYSIS Encryption Key Please direct all questions regarding this Certificate of Analysis to your Project Manager. Debbie Nordbruget, Project Manager DNordbruget@maxxam.ca Phone# (250) ==================================================================== This report has been generated and distributed using a secure automated process. Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section of ISO/IEC 7025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Total Cover Pages : 2 Page 2 of 4
3 Maxxam Job #: B5B343 RESULTS OF CHEMICAL ANALYSES OF WATER Maxxam ID Sampling Date COC Number Parameter Subcontract Parameter ANIONS Nitrite (N) Calculated Parameters Nitrate (N) Misc. Inorganics Total Organic Carbon (C) Anions Dissolved Sulphate (SO4) Dissolved Chloride (Cl) MISCELLANEOUS Tannins and Lignins Nutrients Nitrate plus Nitrite (N) Misc. Organics Phenols Physical Properties Conductivity ph Physical Properties Total Dissolved Solids N/A us/cm ph RDL = Reportable Detection Limit N/A = Not Applicable NW78 205/2/22 09: COMMUNITY WELL # ATTACHED < < < RDL N/A N/A 0 Page 3 of 4
4 Maxxam Job #: B5B343 RESULTS OF CHEMICAL ANALYSES OF WATER Maxxam ID Sampling Date COC Number Polycyclic Aromatics Low Molecular Weight PAH`s High Molecular Weight PAH`s Total PAH Naphthalene 2-Methylnaphthalene -Methylnaphthalene Quinoline Acenaphthylene Acenaphthene Fluorene Phenanthrene Anthracene Acridine Fluoranthene Pyrene Benzo(a)anthracene Chrysene Benzo(b&j)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Perylene Indeno(,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene Calculated Parameters LEPH (C0-C9 less PAH) HEPH (C9-C32 less PAH) Ext. Pet. Hydrocarbon EPH (C0-C9) EPH (C9-C32) Surrogate Recovery () O-TERPHENYL (sur.) D0-ANTHRACENE (sur.) D8-ACENAPHTHYLENE (sur.) D8-NAPHTHALENE (sur.) RDL = Reportable Detection Limit NW78 205/2/22 09: COMMUNITY WELL # <0.24 <0.24 <0.0 <0.0 <0.24 <0.00 <0.00 <0.00 <0.20 <0.20 <0.20 < RDL Page 4 of 4
5 Maxxam Job #: B5B343 RESULTS OF CHEMICAL ANALYSES OF WATER Maxxam ID Sampling Date COC Number D9-Acridine TERPHENYL-D4 (sur.) RDL = Reportable Detection Limit NW78 205/2/22 09: COMMUNITY WELL # 04 2 RDL Page 5 of 4
6 Maxxam Job #: B5B343 RESULTS OF CHEMICAL ANALYSES OF WATER Maxxam ID Sampling Date COC Number NW78 205/2/22 09: COMMUNITY WELL # RDL Volatiles VPH (VH6 to 0 - BTEX) Chloromethane Vinyl chloride Chloroethane Trichlorofluoromethane,,2Trichloro-,2,2Trifluoroethane Dichlorodifluoromethane,-dichloroethene Dichloromethane trans-,2-dichloroethene,-dichloroethane cis-,2-dichloroethene Chloroform,,-trichloroethane,2-dichloroethane Carbon tetrachloride Benzene Methyl-tert-butylether (MTBE),2-dichloropropane cis-,3-dichloropropene trans-,3-dichloropropene Bromomethane,,2-trichloroethane Trichloroethene Chlorodibromomethane,3-Butadiene Tetrachloroethene Bromodichloromethane Toluene Ethylbenzene m & p-xylene Bromoform Styrene o-xylene Xylenes (Total) <0 <.0 <.0 <4.0 <.0 <.0 <.0 <4.0 <.0 <.0 <.0 <.0 <5.0 <.0 < RDL = Reportable Detection Limit Page 6 of 4
7 Maxxam Job #: B5B343 RESULTS OF CHEMICAL ANALYSES OF WATER Maxxam ID Sampling Date COC Number NW78 205/2/22 09: COMMUNITY WELL # RDL,,,2-tetrachloroethane,,2,2-tetrachloroethane,2-dichlorobenzene,3-dichlorobenzene,4-dichlorobenzene Chlorobenzene Dibromomethane Bromobenzene VH C6-C0 Surrogate Recovery () <0. < ,4-Difluorobenzene (sur.) 4-Bromofluorobenzene (sur.) D4-,2-Dichloroethane (sur.) 04 9 RDL = Reportable Detection Limit Page 7 of 4
8 Maxxam Job #: B5B343 PHENOXYALKYL ACID PESTICIDES/HERBICIDES (WATER) Maxxam ID Sampling Date COC Number Phenoxyalkyl acid Pest. 3,5-dichlorobenzoic acid Dicamba MCPP MCPA Dichlorprop Bromoxynil 2,4-D Pentachlorophenol 2,4,5-TP 2,4,5-T Chloramben Dinoseb (DNBP) Bentazon 2,4-DB Picloram Diclofop-methyl Surrogate Recovery () 2,4,6-TRIBROMOPHENOL (sur.) RDL = Reportable Detection Limit NW78 205/2/22 09: COMMUNITY WELL # < RDL Page 8 of 4
9 Maxxam Job #: B5B343 GENERAL COMMENTS PHENOXYALKYL ACID PESTICIDES/HERBICIDES (WATER) Comments Sample NW78-02 Phenoxyalkyl acid Pesticides: Sample extracted past method-specified hold time. Results relate only to the items tested. Page 9 of 4
10 Maxxam Job #: B5B343 QUALITY ASSURAE REPORT Matrix Spike Spiked Blank Method Blank RPD QC Batch Parameter Date Recovery Recovery Value Value () 8533,4-Difluorobenzene (sur.) 205/2/ Bromofluorobenzene (sur.) 205/2/ D4-,2-Dichloroethane (sur.) 205/2/ D0-ANTHRACENE (sur.) 205/2/ D8-ACENAPHTHYLENE (sur.) 205/2/ D8-NAPHTHALENE (sur.) 205/2/ D9-Acridine 205/2/ TERPHENYL-D4 (sur.) 205/2/ O-TERPHENYL (sur.) 205/2/ ,4,6-TRIBROMOPHENOL (sur.) 206/0/ Total Dissolved Solids 205/2/ < Tannins and Lignins 205/2/ < ,,,2-tetrachloroethane 205/2/ ,,-trichloroethane 205/2/ ,,2,2-tetrachloroethane 205/2/ ,,2Trichloro-,2,2Trifluoroethane 205/2/ ,,2-trichloroethane 205/2/ ,-dichloroethane 205/2/ ,-dichloroethene 205/2/ ,2-dichlorobenzene 205/2/ ,2-dichloroethane 205/2/ ,2-dichloropropane 205/2/ ,3-Butadiene 205/2/24 < ,3-dichlorobenzene 205/2/ ,4-dichlorobenzene 205/2/ Benzene 205/2/ Bromobenzene 205/2/ Bromodichloromethane 205/2/ < Bromoform 205/2/ < Bromomethane 205/2/ < Carbon tetrachloride 205/2/ Chlorobenzene 205/2/ Page 0 of 4
11 Maxxam Job #: B5B343 QUALITY ASSURAE REPORT(CONT'D) Matrix Spike Spiked Blank Method Blank RPD QC Batch Parameter Date Recovery Recovery Value Value () 8533 Chlorodibromomethane 205/2/ < Chloroethane 205/2/ < Chloroform 205/2/ < Chloromethane 205/2/ < cis-,2-dichloroethene 205/2/ < cis-,3-dichloropropene 205/2/ < Dibromomethane 205/2/ < Dichlorodifluoromethane 205/2/ Dichloromethane 205/2/ Ethylbenzene 205/2/ m & p-xylene 205/2/ Methyl-tert-butylether (MTBE) 205/2/ < o-xylene 205/2/ Styrene 205/2/ Tetrachloroethene 205/2/ Toluene 205/2/ trans-,2-dichloroethene 205/2/ < trans-,3-dichloropropene 205/2/ < Trichloroethene 205/2/ Trichlorofluoromethane 205/2/ < VH C6-C0 205/2/ < Vinyl chloride 205/2/ Xylenes (Total) 205/2/ ph 205/2/ N/A Conductivity 205/2/ <.0 us/cm Nitrate plus Nitrite (N) 205/2/ Nitrite (N) 205/2/ < Phenols 205/2/ < Dissolved Chloride (Cl) 205/2/ Dissolved Sulphate (SO4) 205/2/ , RDL= Total Organic Carbon (C) 205/2/ Methylnaphthalene 206/0/ <0.0 Page of 4
12 Maxxam Job #: B5B343 QUALITY ASSURAE REPORT(CONT'D) Matrix Spike Spiked Blank Method Blank RPD QC Batch Parameter Date Recovery Recovery Value Value () Acenaphthene 206/0/ Acenaphthylene 206/0/ Acridine 206/0/ Anthracene Benzo(a)anthracene Benzo(a)pyrene 206/0/03 206/0/03 206/0/ < , RDL=0.00 < Benzo(b&j)fluoranthene 206/0/ Benzo(g,h,i)perylene 206/0/03 35 () Benzo(k)fluoranthene 206/0/ Chrysene 206/0/ Dibenz(a,h)anthracene 206/0/03 34 () Fluoranthene 206/0/ Fluorene 206/0/ Indeno(,2,3-cd)pyrene 206/0/03 36 () Naphthalene 206/0/ < Perylene 205/2/ Phenanthrene 206/0/ Pyrene 206/0/ Quinoline 206/0/ < EPH (C0-C9) 205/2/ < EPH (C9-C32) 205/2/ < ,4,5-T 206/0/ ,4,5-TP 206/0/ ,4-D 206/0/ ,4-DB 206/0/ ,5-dichlorobenzoic acid 206/0/ Bentazon 206/0/ Bromoxynil 206/0/ Chloramben 206/0/ Dicamba 206/0/ < Dichlorprop 206/0/ Page 2 of 4
13 Maxxam Job #: B5B343 QUALITY ASSURAE REPORT(CONT'D) QC Batch Parameter Diclofop-methyl Dinoseb (DNBP) MCPA MCPP Pentachlorophenol Picloram N/A = Not Applicable Date 206/0/06 206/0/06 206/0/06 206/0/06 206/0/06 206/0/06 Recovery Matrix Spike Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement. Recovery 43 Spiked Blank Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference Method Blank Spiked Blank: A blank matrix sample to which a known amount of the analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency. (Matrix Spike): The recovery in the matrix spike was not calculated. The relative difference between the concentration in the parent sample and the spiked amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than 2x that of the native sample concentration). () Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria. 28 Value Value () (Duplicate RPD): The duplicate RPD was not calculated. The concentration in the sample and/or duplicate was too low to permit a reliable RPD calculation (one or both samples < 5x RDL). RPD Page 3 of 4
14 Maxxam Job #: B5B343 VALIDATION SIGNATURE PAGE The analytical data and all QC contained in this report were reviewed and validated by the following individual(s). Andy Lu, Data Validation Coordinator Veronica Falk, Scientific Specialist Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section of ISO/IEC 7025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Page 4 of 4
CERTIFICATE OF ANALYSIS
Attention:Steve Allum 802 Drury Lane Burlington, ON L7R 4L3 Your Project #: LEAD Your C.O.C. #: na Report #: R4042481 Version: 1 - Final MAXXAM JOB #: B6C8371 Received: 2016/06/22, 08:00 Sample Matrix:
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