ANALYTICAL REPORT. Attn: Dan Spector

Transcription

1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. Benjamin Road Suite 0 Tampa, FL Tel: ()- TestAmerica Job I: 0-- Client Revision: For: Langan Engineering & Environmental Srvcs 0 NW th Court Suite 00 Miami Lakes, Florida 0 Attn: an Spector Authorized for release by: //0 :: PM Matt Jones, Project Manager I (0)- matt.jones@testamericainc.com esignee for Ken Hayes, Project Manager II ()0-0 ken.hayes@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

2 Table of Contents TestAmerica Job I: 0-- Cover Page Table of Contents Sample Summary Case Narrative efinitions/glossary etection Summary Client Sample Results QC Sample Results Internal Standard Summary QC Association Summary Lab Chronicle Method Summary Certification Summary Chain of Custody Receipt Checklists Page of //0

3 Sample Summary TestAmerica Job I: 0-- Lab Sample I Client Sample I Matrix Collected Received 0-- LMW-B 0// 0: 0// 0:0 0-- LMW-P 0// : 0// 0:0 0-- LMW-B 0// : 0// 0:0 0-- LMW-P 0// : 0// 0:0 0-- LMW-A 0// : 0// 0:0 Page of //0

4 Case Narrative Client: Langan Engineering & Environmental Srvcs TestAmerica Job I: 0-- Job I: 0-- Laboratory: Narrative Job Narrative 0-- Receipt The samples were received on //0 :0 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the coolers at receipt time were 0.º C, 0.º C, 0.º C,.º C and.º C. Laboratory Comments ue to system limitations Total Endosulfans and Total PCB's are not included in this report. The data for these summary analytes has been calculated by hand and entered into the accompanying E. GC/MS VOA Method 0B: The sample duplicate (UP) precision for was outside control limits. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. GC/MS Semi VOA Method 0 LL: The following analyte recovered outside control limits for the LCS associated with 0-0 and 0-0: Fluorene. This is not indicative of a systematic control problem because these were random marginal exceedances. Qualified results have been reported. Method 0 LL: The matrix spike / matrix spike duplicate (MS/MS) precision for 0-0 and 0-0 was outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory control sample duplicate (LCS/LCS) precision was within acceptance limits. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. GC Semi VOA Method B: The matrix spike / matrix spike duplicate / sample duplicate (MS/MS/UP) precision for preparation batch 0- was outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory control sample duplicate (LCS/LCS) precision was within acceptance limits. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. Metals No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Subcontract non-sister No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Organic Prep Method(s) 0C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MS) associated with analytical batch 00-. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. Page of //0

5 s GC/MS VOA U I GC/MS Semi VOA U I J GC Semi VOA U I IOXIN J I V Metals U I Glossary escription efinitions/glossary Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. escription Estimated value; value may not be accurate. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Indicates the analyte was detected in both the sample and method blank. escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. TestAmerica Job I: 0-- Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid ER uplicate error ratio (normalized absolute difference) ilution Factor L, RA, RE, IN Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision level concentration MA Minimum detectable activity EL Estimated etection Limit MC Minimum detectable concentration ML Method etection Limit ML Minimum Level (ioxin) NC Not Calculated N Not detected at the reporting limit (or ML or EL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) Page of //0

6 etection Summary TestAmerica Job I: 0-- Client Sample I: LMW-B Lab Sample I: 0-- Result ML EL TEF TEQ Method Prep Type,,,,,-HxC 0. J I pg/l B,,,,,-HxC 0.0 J I pg/l B Total Total HxC. J I. 0. pg/l B Total,,,,,,-HpC. V I pg/l B Total Total HpC. I V. 0. pg/l B Total OC V pg/l B Total Total TCF. J I. 0. pg/l B Total Total PeCF. J I. 0. pg/l B Total,,,,,-HxCF 0.00 J V I pg/l B Total Total HxCF. J I V. 0. pg/l B Total,,,,,,-HpCF. J V I pg/l B Total Total HpCF. J I V. 0. pg/l B Total OCF. V I pg/l B Total Result PQL ML Method Prep Type Acenaphthene ug/l 0 LL Total Anthracene ug/l 0 LL Benzo[a]anthracene 0.0 I ug/l 0 LL Benzo[a]pyrene 0.0 I ug/l 0 LL Benzo[b]fluoranthene 0.0 I ug/l 0 LL Chrysene 0.0 I ug/l 0 LL Fluoranthene ug/l 0 LL Fluorene. J ug/l 0 LL -Methylnaphthalene ug/l 0 LL -Methylnaphthalene ug/l 0 LL Naphthalene ug/l 0 LL Phenanthrene ug/l 0 LL Pyrene ug/l 0 LL Total Petroleum Hydrocarbons 00 0 ug/l FL-PRO (C-C0) Arsenic.. ug/l 00A Total Recoverable Barium 0.0. ug/l 00A Total Recoverable Lead ug/l 00A Total Recoverable Client Sample I: LMW-P Lab Sample I: 0-- Result ML EL TEF TEQ Method Prep Type Total TC 0. J I.0 0. pg/l B Total Total PeC 0. J I.0 0. pg/l B Total,,,,,-HxC 0. J I pg/l B Total Total HxC. J I.0 0. pg/l B Total,,,,,,-HpC. J V I pg/l B Total Total HpC 0. J I V.0 0. pg/l B Total OC V pg/l B Total Total TCF 0. J I.0 0. pg/l B Total Total PeCF. J I.0 0. pg/l B Total Total HxCF.0 J I.0 0. pg/l B Total,,,,,,-HpCF 0.0 J V I pg/l B Total Total HpCF. I J V.0 0. pg/l B Total This etection Summary does not include radiochemical test results. Page of //0

7 etection Summary TestAmerica Job I: 0-- Client Sample I: LMW-P (Continued) Lab Sample I: 0-- Result ML EL TEF TEQ Method Prep Type OCF. V I pg/l B Result PQL ML Method Prep Type Acenaphthene 0. I ug/l 0 LL Total Fluoranthene 0.0 I ug/l 0 LL Fluorene 0. I J ug/l 0 LL Phenanthrene 0.0 I ug/l 0 LL Pyrene 0.0 I ug/l 0 LL Arsenic... ug/l 00A Total Recoverable Barium 0.0. ug/l 00A Total Recoverable Lead ug/l 00A Total Recoverable Client Sample I: LMW-B Lab Sample I: 0-- Result ML EL TEF TEQ Method Prep Type,,,,-PeC 0. J V I pg/l B Total PeC 0. J V I. 0. pg/l B Total,,,,,-HxC. J I pg/l B Total,,,,,-HxC 0.0 J I pg/l B Total Total HxC. J I pg/l B Total,,,,,,-HpC. V pg/l B Total Total HpC V. 0. pg/l B Total OC V pg/l B Total,,,-TCF 0.0 J I pg/l B Total Total TCF.0 J I. 0. pg/l B Total Total PeCF 0. J I. 0. pg/l B Total,,,,,-HxCF 0.0 J I pg/l B Total Total HxCF. J I. 0. pg/l B Total,,,,,,-HpCF.0 V I pg/l B Total Total HpCF. J I V. 0. pg/l B Total OCF. J V I pg/l B Total Result PQL ML Method Prep Type Acetone I 0. ug/l 0B Total Chlorobenzene 0. I.0 0. ug/l 0B Isopropylbenzene 0. I.0 0. ug/l 0B Acenaphthene ug/l 0 LL Anthracene 0.00 I ug/l 0 LL Fluoranthene 0.00 I ug/l 0 LL Fluorene 0. I J ug/l 0 LL Phenanthrene 0. I ug/l 0 LL Pyrene 0.0 I ug/l 0 LL Total Petroleum Hydrocarbons 0 0 ug/l FL-PRO (C-C0) Arsenic. I.. ug/l 00A Total Recoverable Barium 0.0. ug/l 00A Total Recoverable Chromium. I.0. ug/l 00A Total Recoverable This etection Summary does not include radiochemical test results. Page of //0

8 etection Summary TestAmerica Job I: 0-- Client Sample I: LMW-B (Continued) Lab Sample I: 0-- Result PQL ML Method Prep Type Lead ug/l 00A Total Recoverable Client Sample I: LMW-P Lab Sample I: 0-- Result ML EL TEF TEQ Method Prep Type,,,-TC 0. J I pg/l B Total TC 0. J I. 0.0 pg/l B Total Total PeC. J I pg/l B Total,,,,,-HxC. J I pg/l B Total,,,,,-HxC. I pg/l B Total Total HxC. J I pg/l B Total,,,,,,-HpC V pg/l B Total Total HpC V 0.. pg/l B Total OC 0 V pg/l B Total Total TCF 0. I J. 0. pg/l B Total Total PeCF. J I pg/l B Total,,,,,-HxCF 0.00 J I pg/l B Total Total HxCF. J I pg/l B Total,,,,,,-HpCF. J V I pg/l B Total Total HpCF. J I V pg/l B Total OCF. V I pg/l B Total Result PQL ML Method Prep Type Acenaphthene 0. I ug/l 0 LL Total Fluoranthene 0.0 I ug/l 0 LL Fluorene 0.0 I J ug/l 0 LL Phenanthrene 0.0 I ug/l 0 LL Pyrene 0.0 I ug/l 0 LL Total Petroleum Hydrocarbons I 0 ug/l FL-PRO (C-C0) Barium 0.0. ug/l 00A Total Recoverable Lead ug/l 00A Total Recoverable Client Sample I: LMW-A Lab Sample I: 0-- Result ML EL TEF TEQ Method Prep Type Total PeC 0. J I. 0. pg/l B Total HxC 0. J I. 0. pg/l B Total,,,,,,-HpC. J V I pg/l B Total Total HpC. J I V. 0. pg/l B Total OC 0. V I pg/l B Total Total TCF. J I.0 0. pg/l B Total Total PeCF. J I. 0. pg/l B Total Total HxCF 0. J I. 0. pg/l B Total OCF 0. J V I pg/l B Total Result PQL ML Method Prep Type Arsenic.. ug/l 00A Total Total Recoverable This etection Summary does not include radiochemical test results. Page of //0

9 etection Summary TestAmerica Job I: 0-- Client Sample I: LMW-A (Continued) Lab Sample I: 0-- Result PQL ML Method Prep Type Barium.0. ug/l 00A Total Recoverable 0.0 Total Recoverable Lead 0. I. ug/l 00A This etection Summary does not include radiochemical test results. Page of //0

10 Client Sample I: LMW-B ate Collected: 0// 0: ate Received: 0// 0:0 Method: 0B - Volatile Organic Compounds (GC/MS) Result Client Sample Results PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Acetone. U 0. ug/l 0// :0 Benzene Bromobenzene Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane -Chlorotoluene -Chlorotoluene cis-,-ichloroethene cis-,-ichloropropene,-ibromo--chloropropane ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorobromomethane ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene Ethylbenzene Ethylene ibromide Hexachlorobutadiene -Hexanone Isopropylbenzene -Isopropyltoluene Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether m-xylene & p-xylene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene,,,-tetrachloroethane 0.0 U 0. U 0. U. U. U.0 U 0. U 0. U 0. U 0. U. U 0.0 U.0 U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U.0 U.0 U 0. U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// :0. ug/l 0// :0.0.0 ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// :0.0.0 ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0. ug/l 0// : ug/l 0// : ug/l 0// :0.0.0 ug/l 0// :0.0 ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0 Page of //0

11 Client Sample I: LMW-B ate Collected: 0// 0: ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0--,,,-Tetrachloroethane 0. U.0 0. ug/l 0// :0 Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene,,-trichlorobenzene,,-trichlorobenzene,,-trichloroethane,,-trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride Xylenes, Total 0.0 U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0. U 0.0 U ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0 -Bromofluorobenzene 0-0 0// :0 ibromofluoromethane 0-0 0// :0 Toluene-d (Surr) 0-0 0// :0 Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level Result PQL ML Acenaphthene ug/l 0// :0 0// : Acenaphthylene 0.0 U ug/l 0// :0 0// : Anthracene. Benzo[a]anthracene 0.0 I Benzo[a]pyrene 0.0 I Benzo[b]fluoranthene 0.0 I Benzo[g,h,i]perylene 0.00 U Benzo[k]fluoranthene Chrysene ibenz(a,h)anthracene 0.0 U 0.0 I 0.00 U Fluoranthene. Fluorene. J Indeno[,,-cd]pyrene 0.0 U -Methylnaphthalene. -Methylnaphthalene. Naphthalene 0. Phenanthrene. Pyrene ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : o-terphenyl (Surr) 0 0-0// :0 0// : Method: 0B - Organochlorine Pesticides by GC Result PQL ML Aldrin U ug/l 0// : 0// 0:0 alpha-bhc 0.00 U ug/l 0// : 0// 0:0 Page of //0

12 Client Sample I: LMW-B ate Collected: 0// 0: ate Received: 0// 0:0 Client Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- alpha-chlordane ug/l 0// : 0// 0:0 beta-bhc Chlordane (technical),'-,'-e,'-t delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene 0. U U 0. U ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0:0. 0. ug/l 0// : 0// 0:0 CB ecachlorobiphenyl 0-0// : 0// 0:0 ibutylchlorendate - 0// : 0// 0:0 Tetrachloro-m-xylene - 0// : 0// 0:0 Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Result PQL ML Bolstar 0.0 U ug/l 0// : 0// : Chlorpyrifos 0. U ug/l 0// : 0// : Coumaphos 0.0 U ug/l 0// : 0// : emeton, Total 0. U. 0. ug/l 0// : 0// : iazinon 0. U ug/l 0// : 0// : ichlorvos 0. U. 0. ug/l 0// : 0// : imethoate 0. U. 0. ug/l 0// : 0// : isulfoton 0. U. 0. ug/l 0// : 0// : EPN 0.0 U ug/l 0// : 0// : Ethyl Parathion 0.0 U ug/l 0// : 0// : Fensulfothion 0. U. 0. ug/l 0// : 0// : Guthion 0. U ug/l 0// : 0// : Malathion 0.0 U ug/l 0// : 0// : Merphos 0. U ug/l 0// : 0// : Methyl parathion 0. U ug/l 0// : 0// : Mevinphos 0. U. 0. ug/l 0// : 0// : Mocap 0. U ug/l 0// : 0// : Monochrotophos. U.. ug/l 0// : 0// : Naled 0. U. 0. ug/l 0// : 0// : Phorate 0. U ug/l 0// : 0// : Ronnel 0. U ug/l 0// : 0// : Sulfotepp 0.0 U ug/l 0// : 0// : Page of //0

13 Client Sample I: LMW-B ate Collected: 0// 0: ate Received: 0// 0:0 Client Sample Results TestAmerica Job I: 0-- Lab Sample I: 0-- Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued) Result PQL ML Tokuthion 0.0 U ug/l 0// : 0// : Trichloronate 0. U ug/l 0// : 0// : Triphenylphosphate (TPP) - 0// : 0// : Method: FL-PRO - Florida - Petroleum Range Organics (GC) Result PQL Total Petroleum Hydrocarbons (C-C0) ML 00 0 ug/l 0// : 0// :0 n-c 0-0// : 0// :0 o-terphenyl - 0// : 0// :0 Method: B - ioxins/furans, HRGC/HRMS (B) Result ML EL TEF TEQ,,,-TC N. 0. pg/l 0/0/ : 0/0/ : Total TC N. 0. pg/l 0/0/ : 0/0/ :,,,,-PeC N pg/l 0/0/ : 0/0/ : Total PeC N. 0. pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC 0. J I pg/l 0/0/ : 0/0/ :,,,,,-HxC 0.0 J I pg/l 0/0/ : 0/0/ : Total HxC. J I. 0. pg/l 0/0/ : 0/0/ :,,,,,,-HpC. V I pg/l 0/0/ : 0/0/ : Total HpC. I V. 0. pg/l 0/0/ : 0/0/ : OC V pg/l 0/0/ : 0/0/ :,,,-TCF N pg/l 0/0/ : 0/0/ : Total TCF. J I. 0. pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ : Total PeCF. J I. 0. pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF 0.00 J V I pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ : Total HxCF. J I V. 0. pg/l 0/0/ : 0/0/ :,,,,,,-HpCF. J V I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF N pg/l 0/0/ : 0/0/ : Total HpCF. J I V. 0. pg/l 0/0/ : 0/0/ : OCF. V I pg/l 0/0/ : 0/0/ : Total TEQ (EPA ) 0. Cl-,,,-TC - 0/0/ : 0/0/ : Internal Standard C-,,,-TC - 0/0/ : 0/0/ : C-,,,,-PeC - 0/0/ : 0/0/ : Page of //0

14 Client Sample I: LMW-B ate Collected: 0// 0: ate Received: 0// 0:0 Client Sample Results Method: B - ioxins/furans, HRGC/HRMS (B) (Continued) Internal Standard TestAmerica Job I: 0-- Lab Sample I: 0-- C-,,,,,-HxC - 0/0/ : 0/0/ : C-,,,,,-HxC - 0 0/0/ : 0/0/ : C-,,,,,,-HpC - 0 0/0/ : 0/0/ : C-OC 0-0/0/ : 0/0/ : C-,,,-TCF - 0/0/ : 0/0/ : C-,,,,-PeCF 0-0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF 0-0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF 0-0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-OCF - 0/0/ : 0/0/ : Method: 00A - Metals (ICP/MS) - Total Recoverable Result PQL Arsenic.. ug/l 0// 0: 0// : Barium 0.0. ug/l 0// 0: 0// : Cadmium 0.0 U ug/l 0// 0: 0// : Chromium. U Lead. Selenium.0 U Silver 0. U ML.0. ug/l 0// 0: 0// :. 0.0 ug/l 0// 0: 0// :..0 ug/l 0// 0: 0// :.0 0. ug/l 0// 0: 0// : Method: 0A - Mercury (CVAA) Result PQL ML Mercury 0.00 U ug/l 0// :0 0// : Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: 0-- Method: 0B - Volatile Organic Compounds (GC/MS) Result PQL ML Acetone. U 0. ug/l 0// : Benzene 0.0 U ug/l 0// : Bromobenzene 0. U.0 0. ug/l 0// : Bromoform 0. U.0 0. ug/l 0// : Bromomethane. U.0. ug/l 0// : -Butanone (MEK). U. ug/l 0// : Carbon disulfide.0 U.0.0 ug/l 0// : Carbon tetrachloride 0. U.0 0. ug/l 0// : Chlorobenzene 0. U.0 0. ug/l 0// : Chlorobromomethane 0. U.0 0. ug/l 0// : Chlorodibromomethane 0. U.0 0. ug/l 0// : Chloroethane. U.0. ug/l 0// : Chloroform 0.0 U ug/l 0// : Chloromethane.0 U.0.0 ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : Page of //0

15 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- -Chlorotoluene 0. U.0 0. ug/l 0// : cis-,-ichloroethene cis-,-ichloropropene,-ibromo--chloropropane ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorobromomethane ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene Ethylbenzene Ethylene ibromide Hexachlorobutadiene -Hexanone Isopropylbenzene -Isopropyltoluene Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether m-xylene & p-xylene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene,,,-tetrachloroethane,,,-tetrachloroethane Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene,,-trichlorobenzene,,-trichlorobenzene,,-trichloroethane,,-trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U.0 U.0 U 0. U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0. U.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0 ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : Page of //0

16 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Xylenes, Total 0.0 U ug/l 0// : -Bromofluorobenzene 0-0 0// : ibromofluoromethane 0-0 0// : Toluene-d (Surr) 0-0 0// : Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level Result PQL ML Acenaphthene 0. I ug/l 0// :0 0// :0 Acenaphthylene 0.0 U ug/l 0// :0 0// :0 Anthracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene ibenz(a,h)anthracene Fluoranthene Fluorene Indeno[,,-cd]pyrene -Methylnaphthalene -Methylnaphthalene Naphthalene Phenanthrene Pyrene 0.00 U 0.0 U 0.0 U 0.0 U 0.00 U 0.0 U 0.0 U 0.00 U 0.0 I 0. I J 0.0 U 0.00 U 0.0 U 0.00 U 0.0 I 0.0 I ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// :0 o-terphenyl (Surr) 0-0// :0 0// :0 Method: 0B - Organochlorine Pesticides by GC Result PQL ML Aldrin U ug/l 0// : 0// : alpha-bhc 0.00 U ug/l 0// : 0// : alpha-chlordane ug/l 0// : 0// : beta-bhc ug/l 0// : 0// : Chlordane (technical) 0. U ug/l 0// : 0// :,' ug/l 0// : 0// :,'-E ug/l 0// : 0// :,'-T ug/l 0// : 0// : delta-bhc ug/l 0// : 0// : ieldrin U ug/l 0// : 0// : Endosulfan I ug/l 0// : 0// : Endosulfan II ug/l 0// : 0// : Endosulfan sulfate ug/l 0// : 0// : Endrin ug/l 0// : 0// : Endrin aldehyde ug/l 0// : 0// : Endrin ketone ug/l 0// : 0// : gamma-bhc (Lindane) ug/l 0// : 0// : Page of //0

17 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- gamma-chlordane ug/l 0// : 0// : Heptachlor Heptachlor epoxide Methoxychlor Toxaphene 0. U ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :. 0. ug/l 0// : 0// : CB ecachlorobiphenyl 0-0// : 0// : ibutylchlorendate - 0// : 0// : Tetrachloro-m-xylene - 0// : 0// : Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Result PQL ML Bolstar 0.0 U ug/l 0// : 0// : Chlorpyrifos Coumaphos emeton, Total iazinon ichlorvos imethoate isulfoton EPN Ethyl Parathion Fensulfothion Guthion Malathion Merphos Methyl parathion Mevinphos Mocap Monochrotophos Naled Phorate Ronnel Sulfotepp Tokuthion Trichloronate 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0.0 U 0.00 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0.0 U 0. U.0 0. ug/l 0// : 0// : ug/l 0// : 0// :. 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// :. ug/l 0// : 0// :.0 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// : Triphenylphosphate (TPP) - 0// : 0// : Method: FL-PRO - Florida - Petroleum Range Organics (GC) Result PQL Total Petroleum Hydrocarbons (C-C0) ML U 0 ug/l 0// : 0// : n-c - 0// : 0// : o-terphenyl - 0// : 0// : Page of //0

18 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Method: B - ioxins/furans, HRGC/HRMS (B) Client Sample Results Result ML EL TEF TEQ TestAmerica Job I: 0-- Lab Sample I: 0--,,,-TC N.0 0. pg/l 0/0/ : 0/0/ : Total TC 0. J I.0 0. pg/l 0/0/ : 0/0/ :,,,,-PeC N pg/l 0/0/ : 0/0/ : Total PeC 0. J I.0 0. pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC 0. J I pg/l 0/0/ : 0/0/ : Total HxC. J I.0 0. pg/l 0/0/ : 0/0/ :,,,,,,-HpC. J V I pg/l 0/0/ : 0/0/ : Total HpC 0. J I V.0 0. pg/l 0/0/ : 0/0/ : OC V pg/l 0/0/ : 0/0/ :,,,-TCF N pg/l 0/0/ : 0/0/ : Total TCF 0. J I.0 0. pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ : Total PeCF. J I.0 0. pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ : Total HxCF.0 J I.0 0. pg/l 0/0/ : 0/0/ :,,,,,,-HpCF 0.0 J V I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF N pg/l 0/0/ : 0/0/ : Total HpCF. I J V.0 0. pg/l 0/0/ : 0/0/ : OCF. V I pg/l 0/0/ : 0/0/ : Total TEQ (EPA ) 0. Cl-,,,-TC - 0/0/ : 0/0/ : Internal Standard C-,,,-TC 0-0/0/ : 0/0/ : C-,,,,-PeC - 0/0/ : 0/0/ : C-,,,,,-HxC - 0/0/ : 0/0/ : C-,,,,,-HxC - 0 0/0/ : 0/0/ : C-,,,,,,-HpC - 0 0/0/ : 0/0/ : C-OC - 0/0/ : 0/0/ : C-,,,-TCF - 0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-OCF - 0/0/ : 0/0/ : Page of //0

19 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Method: 00A - Metals (ICP/MS) - Total Recoverable Result Client Sample Results PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Arsenic... ug/l 0// 0: 0// :00 Barium 0.0. ug/l 0// 0: 0// :00 Cadmium 0.0 U ug/l 0// 0: 0// :00 Chromium. U Lead. Selenium.0 U Silver Method: 0A - Mercury (CVAA) 0. U Result.0. ug/l 0// 0: 0// : ug/l 0// 0: 0// :00..0 ug/l 0// 0: 0// : ug/l 0// 0: 0// :00 PQL Mercury 0.00 U ug/l 0// :0 0// :0 Client Sample I: LMW-B ate Collected: 0// : ate Received: 0// 0:0 Method: 0B - Volatile Organic Compounds (GC/MS) Result PQL ML ML Lab Sample I: 0-- Acetone I 0. ug/l 0// : Benzene 0.0 U ug/l 0// : Bromobenzene Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane -Chlorotoluene -Chlorotoluene cis-,-ichloroethene cis-,-ichloropropene,-ibromo--chloropropane ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorobromomethane ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene 0. U 0. U. U. U.0 U 0. U 0. I 0. U 0. U. U 0.0 U.0 U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :. ug/l 0// :.0.0 ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// : ug/l 0// :.0.0 ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : Page of //0

20 Client Sample I: LMW-B ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Ethylbenzene 0. U.0 0. ug/l 0// : Ethylene ibromide Hexachlorobutadiene -Hexanone Isopropylbenzene -Isopropyltoluene Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether m-xylene & p-xylene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene,,,-tetrachloroethane,,,-tetrachloroethane Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene,,-trichlorobenzene,,-trichlorobenzene,,-trichloroethane,,-trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride Xylenes, Total 0.0 U 0. U. U 0. I 0. U.0 U.0 U 0. U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0. U 0.0 U ug/l 0// :.0 0. ug/l 0// :. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0 ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : -Bromofluorobenzene 0-0 0// : ibromofluoromethane 0-0 0// : Toluene-d (Surr) // : Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level Result PQL ML Acenaphthene ug/l 0// :0 0// :0 Acenaphthylene 0.0 U ug/l 0// :0 0// :0 Anthracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene 0.00 I 0.0 U 0.0 U 0.0 U 0.00 U 0.0 U 0.0 U ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// :0 Page 0 of //0

21 Client Sample I: LMW-B ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- ibenz(a,h)anthracene 0.00 U ug/l 0// :0 0// :0 Fluoranthene Fluorene Indeno[,,-cd]pyrene -Methylnaphthalene -Methylnaphthalene Naphthalene Phenanthrene Pyrene 0.00 I 0. I J 0.0 U 0.00 U 0.0 U 0.00 U 0. I 0.0 I ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// :0 o-terphenyl (Surr) 0-0// :0 0// :0 Method: 0B - Organochlorine Pesticides by GC Result PQL Aldrin U ug/l 0// : 0// : alpha-bhc alpha-chlordane beta-bhc Chlordane (technical),'-,'-e,'-t delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene U 0. U U 0. U ML ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// : CB ecachlorobiphenyl 0-0// : 0// : ibutylchlorendate - 0// : 0// : Tetrachloro-m-xylene - 0// : 0// : Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Result PQL ML Bolstar 0.00 U ug/l 0// : 0// 0: Chlorpyrifos Coumaphos emeton, Total iazinon 0. U 0.0 U 0. U 0. U ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: Page of //0

22 Client Sample I: LMW-B ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results TestAmerica Job I: 0-- Lab Sample I: 0-- Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued) Result PQL ML ichlorvos 0. U. 0. ug/l 0// : 0// 0: imethoate isulfoton EPN Ethyl Parathion Fensulfothion Guthion Malathion Merphos Methyl parathion Mevinphos Mocap Monochrotophos Naled Phorate Ronnel Sulfotepp Tokuthion Trichloronate 0.0 U 0. U 0.0 U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0.0 U 0. U. 0.0 ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0:.. ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: Triphenylphosphate (TPP) - 0// : 0// 0: Method: FL-PRO - Florida - Petroleum Range Organics (GC) Result PQL Total Petroleum Hydrocarbons (C-C0) ML 0 0 ug/l 0// : 0// : n-c - 0// : 0// : o-terphenyl - 0// : 0// : Method: B - ioxins/furans, HRGC/HRMS (B) Result ML EL TEF TEQ,,,-TC N. 0.0 pg/l 0/0/ : 0/0/ : Total TC N. 0.0 pg/l 0/0/ : 0/0/ :,,,,-PeC 0. J V I pg/l 0/0/ : 0/0/ : Total PeC 0. J V I. 0. pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC. J I pg/l 0/0/ : 0/0/ :,,,,,-HxC 0.0 J I pg/l 0/0/ : 0/0/ : Total HxC. J I pg/l 0/0/ : 0/0/ :,,,,,,-HpC. V pg/l 0/0/ : 0/0/ : Total HpC V. 0. pg/l 0/0/ : 0/0/ : OC V pg/l 0/0/ : 0/0/ :,,,-TCF 0.0 J I pg/l 0/0/ : 0/0/ : Total TCF.0 J I. 0. pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ : Total PeCF 0. J I. 0. pg/l 0/0/ : 0/0/ : Page of //0

23 Client Sample I: LMW-B ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: B - ioxins/furans, HRGC/HRMS (B) (Continued) Result ML EL TEF TEQ TestAmerica Job I: 0-- Lab Sample I: 0--,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF 0.0 J I pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ : Total HxCF. J I. 0. pg/l 0/0/ : 0/0/ :,,,,,,-HpCF.0 V I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF N pg/l 0/0/ : 0/0/ : Total HpCF. J I V. 0. pg/l 0/0/ : 0/0/ : OCF. J V I pg/l 0/0/ : 0/0/ : Total TEQ (EPA ). Cl-,,,-TC - 0/0/ : 0/0/ : Internal Standard C-,,,-TC - 0/0/ : 0/0/ : C-,,,,-PeC 0-0/0/ : 0/0/ : C-,,,,,-HxC - 0/0/ : 0/0/ : C-,,,,,-HxC - 0 0/0/ : 0/0/ : C-,,,,,,-HpC - 0 0/0/ : 0/0/ : C-OC 0-0/0/ : 0/0/ : C-,,,-TCF - 0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF 0-0/0/ : 0/0/ : C-,,,,,-HxCF 0-0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-OCF - 0/0/ : 0/0/ : Method: 00A - Metals (ICP/MS) - Total Recoverable Result PQL ML Arsenic. I.. ug/l 0// 0: 0// :0 Barium 0.0. ug/l 0// 0: 0// :0 Cadmium 0.0 U ug/l 0// 0: 0// :0 Chromium. I.0. ug/l 0// 0: 0// :0 Lead ug/l 0// 0: 0// :0 Selenium.0 U..0 ug/l 0// 0: 0// :0 Silver 0. U.0 0. ug/l 0// 0: 0// :0 Method: 0A - Mercury (CVAA) Result PQL ML Mercury 0.00 U ug/l 0// :0 0// :0 Page of //0

24 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Method: 0B - Volatile Organic Compounds (GC/MS) Result Client Sample Results PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Acetone. U 0. ug/l 0// :0 Benzene Bromobenzene Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane -Chlorotoluene -Chlorotoluene cis-,-ichloroethene cis-,-ichloropropene,-ibromo--chloropropane ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorobromomethane ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene Ethylbenzene Ethylene ibromide Hexachlorobutadiene -Hexanone Isopropylbenzene -Isopropyltoluene Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether m-xylene & p-xylene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene,,,-tetrachloroethane 0.0 U 0. U 0. U. U. U.0 U 0. U 0. U 0. U 0. U. U 0.0 U.0 U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U.0 U.0 U 0. U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// :0. ug/l 0// :0.0.0 ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// :0.0.0 ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0. ug/l 0// : ug/l 0// : ug/l 0// :0.0.0 ug/l 0// :0.0 ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0 Page of //0

25 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0--,,,-Tetrachloroethane 0. U.0 0. ug/l 0// :0 Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene,,-trichlorobenzene,,-trichlorobenzene,,-trichloroethane,,-trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride Xylenes, Total 0.0 U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0. U 0.0 U ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0.0. ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// : ug/l 0// :0 -Bromofluorobenzene 0-0 0// :0 ibromofluoromethane 0-0 0// :0 Toluene-d (Surr) 0-0 0// :0 Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level Result PQL ML Acenaphthene 0. I ug/l 0// :0 0// : Acenaphthylene 0.0 U ug/l 0// :0 0// : Anthracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene ibenz(a,h)anthracene Fluoranthene Fluorene Indeno[,,-cd]pyrene -Methylnaphthalene -Methylnaphthalene Naphthalene Phenanthrene Pyrene 0.00 U 0.0 U 0.0 U 0.0 U 0.00 U 0.0 U 0.0 U 0.00 U 0.0 I 0.0 I J 0.0 U 0.00 U 0.0 U 0.00 U 0.0 I 0.0 I ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : o-terphenyl (Surr) 0-0// :0 0// : Method: 0B - Organochlorine Pesticides by GC Result PQL ML Aldrin U ug/l 0// : 0// : alpha-bhc U ug/l 0// : 0// : Page of //0

26 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- alpha-chlordane ug/l 0// : 0// : beta-bhc Chlordane (technical),'-,'-e,'-t delta-bhc ieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene 0. U U 0. U ug/l 0// : 0// :.0 0. ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :.0 0. ug/l 0// : 0// : CB ecachlorobiphenyl 0-0// : 0// : ibutylchlorendate - 0// : 0// : Tetrachloro-m-xylene - 0// : 0// : Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Result PQL ML Bolstar 0.00 U ug/l 0// : 0// 0: Chlorpyrifos 0. U ug/l 0// : 0// 0: Coumaphos 0.0 U ug/l 0// : 0// 0: emeton, Total 0. U. 0. ug/l 0// : 0// 0: iazinon 0. U ug/l 0// : 0// 0: ichlorvos 0. U. 0. ug/l 0// : 0// 0: imethoate 0.0 U. 0.0 ug/l 0// : 0// 0: isulfoton 0. U. 0. ug/l 0// : 0// 0: EPN 0.0 U ug/l 0// : 0// 0: Ethyl Parathion 0.0 U ug/l 0// : 0// 0: Fensulfothion 0. U. 0. ug/l 0// : 0// 0: Guthion 0. U ug/l 0// : 0// 0: Malathion 0.0 U ug/l 0// : 0// 0: Merphos 0. U ug/l 0// : 0// 0: Methyl parathion 0. U ug/l 0// : 0// 0: Mevinphos 0. U. 0. ug/l 0// : 0// 0: Mocap 0. U ug/l 0// : 0// 0: Monochrotophos. U.. ug/l 0// : 0// 0: Naled 0. U. 0. ug/l 0// : 0// 0: Phorate 0. U ug/l 0// : 0// 0: Ronnel 0. U ug/l 0// : 0// 0: Sulfotepp 0.0 U ug/l 0// : 0// 0: Page of //0

27 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results TestAmerica Job I: 0-- Lab Sample I: 0-- Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued) Result PQL ML Tokuthion 0.0 U ug/l 0// : 0// 0: Trichloronate 0. U ug/l 0// : 0// 0: Triphenylphosphate (TPP) - 0// : 0// 0: Method: FL-PRO - Florida - Petroleum Range Organics (GC) Result PQL Total Petroleum Hydrocarbons (C-C0) ML I 0 ug/l 0// : 0// : n-c 0-0// : 0// : o-terphenyl - 0// : 0// : Method: B - ioxins/furans, HRGC/HRMS (B) Result ML EL TEF TEQ,,,-TC 0. J I pg/l 0/0/ : 0/0/ : Total TC 0. J I. 0.0 pg/l 0/0/ : 0/0/ :,,,,-PeC N pg/l 0/0/ : 0/0/ : Total PeC. J I pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC. J I pg/l 0/0/ : 0/0/ :,,,,,-HxC. I pg/l 0/0/ : 0/0/ : Total HxC. J I pg/l 0/0/ : 0/0/ :,,,,,,-HpC V pg/l 0/0/ : 0/0/ : Total HpC V 0.. pg/l 0/0/ : 0/0/ : OC 0 V pg/l 0/0/ : 0/0/ :,,,-TCF N pg/l 0/0/ : 0/0/ : Total TCF 0. I J. 0. pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ : Total PeCF. J I pg/l 0/0/ : 0/0/ :,,,,,-HxCF 0.00 J I pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ : Total HxCF. J I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF. J V I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF N pg/l 0/0/ : 0/0/ : Total HpCF. J I V pg/l 0/0/ : 0/0/ : OCF. V I pg/l 0/0/ : 0/0/ : Total TEQ (EPA ). Cl-,,,-TC - 0/0/ : 0/0/ : Internal Standard C-,,,-TC - 0/0/ : 0/0/ : C-,,,,-PeC - 0/0/ : 0/0/ : Page of //0

28 Client Sample I: LMW-P ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: B - ioxins/furans, HRGC/HRMS (B) (Continued) Internal Standard TestAmerica Job I: 0-- Lab Sample I: 0-- C-,,,,,-HxC 0-0/0/ : 0/0/ : C-,,,,,-HxC - 0 0/0/ : 0/0/ : C-,,,,,,-HpC - 0 0/0/ : 0/0/ : C-OC - 0/0/ : 0/0/ : C-,,,-TCF - 0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF 0-0/0/ : 0/0/ : C-,,,,,-HxCF 0-0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-OCF - 0/0/ : 0/0/ : Method: 00A - Metals (ICP/MS) - Total Recoverable Result PQL Arsenic. U.. ug/l 0// 0: 0// : Barium 0 Cadmium 0.0 U Chromium. U Lead. Selenium.0 U Silver 0. U ML.0. ug/l 0// 0: 0// : ug/l 0// 0: 0// :.0. ug/l 0// 0: 0// :. 0.0 ug/l 0// 0: 0// :..0 ug/l 0// 0: 0// :.0 0. ug/l 0// 0: 0// : Method: 0A - Mercury (CVAA) Result PQL ML Mercury 0.00 U ug/l 0// :0 0// : Client Sample I: LMW-A ate Collected: 0// : ate Received: 0// 0:0 Lab Sample I: 0-- Method: 0B - Volatile Organic Compounds (GC/MS) Result PQL ML Acetone. U 0. ug/l 0// : Benzene 0.0 U ug/l 0// : Bromobenzene 0. U.0 0. ug/l 0// : Bromoform 0. U.0 0. ug/l 0// : Bromomethane. U.0. ug/l 0// : -Butanone (MEK). U. ug/l 0// : Carbon disulfide.0 U.0.0 ug/l 0// : Carbon tetrachloride 0. U.0 0. ug/l 0// : Chlorobenzene 0. U.0 0. ug/l 0// : Chlorobromomethane 0. U.0 0. ug/l 0// : Chlorodibromomethane 0. U.0 0. ug/l 0// : Chloroethane. U.0. ug/l 0// : Chloroform 0.0 U ug/l 0// : Chloromethane.0 U.0.0 ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : Page of //0

29 Client Sample I: LMW-A ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- -Chlorotoluene 0. U.0 0. ug/l 0// : cis-,-ichloroethene cis-,-ichloropropene,-ibromo--chloropropane ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorobromomethane ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene Ethylbenzene Ethylene ibromide Hexachlorobutadiene -Hexanone Isopropylbenzene -Isopropyltoluene Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether m-xylene & p-xylene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene,,,-tetrachloroethane,,,-tetrachloroethane Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene,,-trichlorobenzene,,-trichlorobenzene,,-trichloroethane,,-trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U. U 0. U 0. U.0 U.0 U 0. U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0. U.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0 ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : Page of //0

30 Client Sample I: LMW-A ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Xylenes, Total 0.0 U ug/l 0// : -Bromofluorobenzene 0-0 0// : ibromofluoromethane 0-0 0// : Toluene-d (Surr) 0-0 0// : Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level Result PQL ML Acenaphthene 0.00 U ug/l 0// :0 0// :0 Acenaphthylene Anthracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene ibenz(a,h)anthracene Fluoranthene Fluorene Indeno[,,-cd]pyrene -Methylnaphthalene -Methylnaphthalene Naphthalene Phenanthrene Pyrene 0.0 U 0.00 U 0.0 U 0.0 U 0.0 U 0.00 U 0.0 U 0.0 U 0.00 U 0.0 U 0.00 J U 0.0 U 0.00 U 0.0 U 0.00 U 0.00 U 0.0 U ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// : ug/l 0// :0 0// :0 o-terphenyl (Surr) 0-0// :0 0// :0 Method: 0B - Organochlorine Pesticides by GC Result PQL ML Aldrin U ug/l 0// : 0// : alpha-bhc 0.00 U ug/l 0// : 0// : alpha-chlordane ug/l 0// : 0// : beta-bhc ug/l 0// : 0// : Chlordane (technical) 0. U ug/l 0// : 0// :,' ug/l 0// : 0// :,'-E ug/l 0// : 0// :,'-T ug/l 0// : 0// : delta-bhc ug/l 0// : 0// : ieldrin U ug/l 0// : 0// : Endosulfan I ug/l 0// : 0// : Endosulfan II ug/l 0// : 0// : Endosulfan sulfate ug/l 0// : 0// : Endrin ug/l 0// : 0// : Endrin aldehyde ug/l 0// : 0// : Endrin ketone ug/l 0// : 0// : gamma-bhc (Lindane) ug/l 0// : 0// : Page 0 of //0

31 Client Sample I: LMW-A ate Collected: 0// : ate Received: 0// 0:0 Client Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) Result PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- gamma-chlordane ug/l 0// : 0// : Heptachlor Heptachlor epoxide Methoxychlor Toxaphene 0. U ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :. 0. ug/l 0// : 0// : CB ecachlorobiphenyl 0-0// : 0// : ibutylchlorendate - 0// : 0// : Tetrachloro-m-xylene - 0// : 0// : Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Result PQL ML Bolstar 0.0 U ug/l 0// : 0// 0: Chlorpyrifos Coumaphos emeton, Total iazinon ichlorvos imethoate isulfoton EPN Ethyl Parathion Fensulfothion Guthion Malathion Merphos Methyl parathion Mevinphos Mocap Monochrotophos Naled Phorate Ronnel Sulfotepp Tokuthion Trichloronate 0. U 0.0 U 0. U 0. U 0. U 0. U 0. U 0.0 U 0.0 U 0. U 0. U 0.0 U 0. U 0. U 0. U 0. U. U 0. U 0. U 0. U 0.0 U 0.0 U 0. U ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0:.. ug/l 0// : 0// 0:. 0. ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: ug/l 0// : 0// 0: Triphenylphosphate (TPP) - 0// : 0// 0: Method: FL-PRO - Florida - Petroleum Range Organics (GC) Result PQL Total Petroleum Hydrocarbons (C-C0) ML U 0 ug/l 0// : 0// : n-c - 0// : 0// : o-terphenyl - 0// : 0// : Page of //0

32 Client Sample I: LMW-A ate Collected: 0// : ate Received: 0// 0:0 Method: B - ioxins/furans, HRGC/HRMS (B) Client Sample Results Result ML EL TEF TEQ TestAmerica Job I: 0-- Lab Sample I: 0--,,,-TC N pg/l 0/0/ : 0/0/ 0: Total TC N pg/l 0/0/ : 0/0/ 0:,,,,-PeC N pg/l 0/0/ : 0/0/ 0: Total PeC 0. J I. 0. pg/l 0/0/ : 0/0/ 0:,,,,,-HxC N pg/l 0/0/ : 0/0/ 0:,,,,,-HxC N pg/l 0/0/ : 0/0/ 0:,,,,,-HxC N pg/l 0/0/ : 0/0/ 0: Total HxC 0. J I. 0. pg/l 0/0/ : 0/0/ 0:,,,,,,-HpC. J V I pg/l 0/0/ : 0/0/ 0: Total HpC. J I V. 0. pg/l 0/0/ : 0/0/ 0: OC 0. V I pg/l 0/0/ : 0/0/ 0:,,,-TCF N pg/l 0/0/ : 0/0/ 0: Total TCF. J I.0 0. pg/l 0/0/ : 0/0/ 0:,,,,-PeCF N pg/l 0/0/ : 0/0/ 0:,,,,-PeCF N pg/l 0/0/ : 0/0/ 0: Total PeCF. J I. 0. pg/l 0/0/ : 0/0/ 0:,,,,,-HxCF N pg/l 0/0/ : 0/0/ 0:,,,,,-HxCF N pg/l 0/0/ : 0/0/ 0:,,,,,-HxCF N pg/l 0/0/ : 0/0/ 0:,,,,,-HxCF N pg/l 0/0/ : 0/0/ 0: Total HxCF 0. J I. 0. pg/l 0/0/ : 0/0/ 0:,,,,,,-HpCF N pg/l 0/0/ : 0/0/ 0:,,,,,,-HpCF N pg/l 0/0/ : 0/0/ 0: Total HpCF N. 0.0 pg/l 0/0/ : 0/0/ 0: OCF 0. J V I pg/l 0/0/ : 0/0/ 0: Total TEQ (EPA ) 0.0 Cl-,,,-TC - 0/0/ : 0/0/ 0: Internal Standard C-,,,-TC 0-0/0/ : 0/0/ 0: C-,,,,-PeC - 0/0/ : 0/0/ 0: C-,,,,,-HxC - 0/0/ : 0/0/ 0: C-,,,,,-HxC - 0 0/0/ : 0/0/ 0: C-,,,,,,-HpC - 0 0/0/ : 0/0/ 0: C-OC - 0/0/ : 0/0/ 0: C-,,,-TCF 0-0/0/ : 0/0/ 0: C-,,,,-PeCF - 0/0/ : 0/0/ 0: C-,,,,-PeCF - 0/0/ : 0/0/ 0: C-,,,,,-HxCF - 0/0/ : 0/0/ 0: C-,,,,,-HxCF - 0/0/ : 0/0/ 0: C-,,,,,-HxCF - 0/0/ : 0/0/ 0: C-,,,,,-HxCF - 0/0/ : 0/0/ 0: C-,,,,,,-HpCF - 0/0/ : 0/0/ 0: C-,,,,,,-HpCF - 0/0/ : 0/0/ 0: C-OCF - 0/0/ : 0/0/ 0: Page of //0

33 Client Sample I: LMW-A ate Collected: 0// : ate Received: 0// 0:0 Method: 00A - Metals (ICP/MS) - Total Recoverable Result Client Sample Results PQL ML TestAmerica Job I: 0-- Lab Sample I: 0-- Arsenic.. ug/l 0// 0: 0// : Barium.0. ug/l 0// 0: 0// : Cadmium 0.0 U ug/l 0// 0: 0// : Chromium Lead Selenium Silver Method: 0A - Mercury (CVAA). U 0. I.0 U 0. U Result.0. ug/l 0// 0: 0// :. 0.0 ug/l 0// 0: 0// :..0 ug/l 0// 0: 0// :.0 0. ug/l 0// 0: 0// : PQL Mercury 0.00 U ug/l 0// :0 0// : ML Page of //0

34 QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 0-/ Analysis Batch: MB MB Result PQL ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type: Acetone. U 0. ug/l 0// : Benzene Bromobenzene Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane -Chlorotoluene -Chlorotoluene cis-,-ichloroethene cis-,-ichloropropene,-ibromo--chloropropane ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorobromomethane ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene Ethylbenzene Ethylene ibromide Hexachlorobutadiene -Hexanone Isopropylbenzene -Isopropyltoluene Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether m-xylene & p-xylene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene 0.0 U ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// :. U.0. ug/l 0// :. U. ug/l 0// :.0 U.0.0 ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// :. U.0. ug/l 0// : 0.0 U ug/l 0// :.0 U.0.0 ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// :. U.0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0.0 U ug/l 0// : 0. U.0 0. ug/l 0// :. U.0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0.0 U ug/l 0// : 0. U.0 0. ug/l 0// :. U. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// :.0 U.0.0 ug/l 0// :.0 U.0 ug/l 0// : 0. U.0 0. ug/l 0// : 0.0 U ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0.0 U ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : Page of //0

35 QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MB 0-/ Analysis Batch: MB MB Result PQL ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type:,,,-Tetrachloroethane 0. U.0 0. ug/l 0// :,,,-Tetrachloroethane Tetrachloroethene Toluene trans-,-ichloroethene trans-,-ichloropropene,,-trichlorobenzene,,-trichlorobenzene,,-trichloroethane,,-trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride Xylenes, Total 0. U.0 0. ug/l 0// : 0.0 U ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// :. U.0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0. U.0 0. ug/l 0// : 0.0 U ug/l 0// : MB MB -Bromofluorobenzene 0-0 0// : ibromofluoromethane 0-0 0// : Toluene-d (Surr) 0-0 0// : Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Spike LCS LCS %Rec. Added Result %Rec Acetone 0 ug/l - Benzene.0. ug/l - Bromobenzene.0. ug/l 0-0 Bromoform.0. ug/l - 0 Bromomethane.0. ug/l - 0 -Butanone (MEK) 0. ug/l 0-0 Carbon disulfide.0.0 ug/l 0-0 Carbon tetrachloride.0. ug/l - Chlorobenzene.0. ug/l 0-0 Chlorobromomethane.0. ug/l 0-0 Chlorodibromomethane.0. ug/l 0-0 Chloroethane.0. ug/l - 0 Chloroform.0. ug/l - 0 Chloromethane.0. ug/l - 0 -Chlorotoluene.0. ug/l 0-0 -Chlorotoluene.0. ug/l 0-0 cis-,-ichloroethene.0. ug/l - 0 cis-,-ichloropropene.0. ug/l 0-0,-ibromo--Chloropropane.0.00 ug/l 0-0 ibromomethane.0. ug/l 0-0 Page of //0

36 QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 0-/ Analysis Batch: Spike Added LCS LCS Result TestAmerica Job I: 0-- Client Sample I: Lab Control Sample Prep Type:,-ichlorobenzene.0. ug/l 0-0,-ichlorobenzene.0. ug/l 0-0,-ichlorobenzene.0. ug/l 0-0 ichlorobromomethane.0. ug/l 0-0 ichlorodifluoromethane.0. ug/l -,-ichloroethane.0. ug/l - 0,-ichloroethane.0. ug/l 0-0,-ichloroethene.0. ug/l - 0,-ichloropropane.0. ug/l 0-0,-ichloropropane.0. ug/l 0-0,-ichloropropane.0. ug/l -,-ichloropropene.0. ug/l - Ethylbenzene.0. ug/l 0-0 Ethylene ibromide.0. ug/l - 0 Hexachlorobutadiene.0. ug/l - -Hexanone 0 0. ug/l 0 - Isopropylbenzene.0. ug/l - 0 -Isopropyltoluene.0. ug/l - Methylene Chloride.0. ug/l - 0 -Methyl--pentanone (MIBK) 0 0. ug/l - Methyl tert-butyl ether.0. ug/l - 0 n-butylbenzene.0. ug/l - N-Propylbenzene.0. ug/l - 0 o-xylene.0. ug/l - 0 sec-butylbenzene.0. ug/l - Styrene.0. ug/l - tert-butylbenzene.0.0 ug/l - 0,,,-Tetrachloroethane.0. ug/l 0-0,,,-Tetrachloroethane.0.0 ug/l 0-0 Tetrachloroethene.0. ug/l 0 - Toluene.0. ug/l 0 - trans-,-ichloroethene.0. ug/l - trans-,-ichloropropene.0. ug/l - 0,,-Trichlorobenzene.0. ug/l -,,-Trichlorobenzene.0. ug/l - 0,,-Trichloroethane.0.0 ug/l 0 -,,-Trichloroethane.0.0 ug/l 0-0 Trichloroethene.0. ug/l - Trichlorofluoromethane.0. ug/l -,,-Trichloropropane.0. ug/l - 0,,-Trimethylbenzene.0.0 ug/l 0 -,,-Trimethylbenzene.0. ug/l - Vinyl chloride.0. ug/l - %Rec %Rec. LCS LCS -Bromofluorobenzene 0-0 ibromofluoromethane 0-0 Toluene-d (Surr) 0-0 Page of //0

37 QC Sample Results Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level TestAmerica Job I: 0-- Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: 0 MB MB Result PQL Acenaphthene 0.00 U ug/l 0// :0 0// : Acenaphthylene Anthracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene ibenz(a,h)anthracene Fluoranthene Fluorene Indeno[,,-cd]pyrene -Methylnaphthalene -Methylnaphthalene Naphthalene Phenanthrene Pyrene ML 0.0 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.00 U ug/l 0// :0 0// : 0.0 U ug/l 0// :0 0// : MB MB o-terphenyl (Surr) 0-0// :0 0// : Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: 0 Spike LCS LCS %Rec. Added Result %Rec Acenaphthene.00. ug/l 0 - Acenaphthylene.00. ug/l - Anthracene.00. ug/l - Benzo[a]anthracene.00. ug/l - Benzo[a]pyrene.00. ug/l - Benzo[b]fluoranthene.00. ug/l - 0 Benzo[g,h,i]perylene.00. ug/l - Benzo[k]fluoranthene.00.0 ug/l - Chrysene.00. ug/l - ibenz(a,h)anthracene.00. ug/l - Fluoranthene.00. ug/l - Fluorene.00. ug/l 0 - Indeno[,,-cd]pyrene.00. ug/l - -Methylnaphthalene.00. ug/l - -Methylnaphthalene.00. ug/l - Naphthalene.00. ug/l - Phenanthrene.00. ug/l - Pyrene.00. ug/l 0 - Page of //0

38 QC Sample Results TestAmerica Job I: 0-- Method: 0 LL - Semivolatile Organic Compounds by GC/MS - Low Level (Continued) Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: 0 LCS LCS o-terphenyl (Surr) 0 - Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: Prep Batch: 0 Spike LCS LCS %Rec. RP Added Result Acenaphthene.00. ug/l 0-0 Acenaphthylene.00. ug/l - 0 Anthracene.00.0 ug/l - 0 Benzo[a]anthracene.00. ug/l - Benzo[a]pyrene.00.0 ug/l - 0 Benzo[b]fluoranthene.00. ug/l - 0 Benzo[g,h,i]perylene.00. ug/l - Benzo[k]fluoranthene.00. ug/l - Chrysene.00. ug/l - ibenz(a,h)anthracene.00. ug/l - 0 Fluoranthene.00. ug/l 0 - Fluorene.00. J ug/l - Indeno[,,-cd]pyrene.00.0 ug/l - -Methylnaphthalene.00. ug/l - 0 -Methylnaphthalene.00. ug/l 0-0 Naphthalene.00.0 ug/l - 0 Phenanthrene.00.0 ug/l - Pyrene.00. ug/l 0 - %Rec RP Limit LCS LCS o-terphenyl (Surr) 0 - Method: 0B - Organochlorine Pesticides by GC Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB Result PQL Aldrin U ug/l 0// : 0// :0 alpha-bhc alpha-chlordane beta-bhc Chlordane (technical),'-,'-e,'-t delta-bhc ieldrin Endosulfan I ML U ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : U ug/l 0// : 0// : ug/l 0// : 0// :0 Page of //0

39 QC Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) TestAmerica Job I: 0-- Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB Result PQL Endosulfan II ug/l 0// : 0// :0 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane) gamma-chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene ML ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// : ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 MB MB CB ecachlorobiphenyl 0-0// : 0// :0 ibutylchlorendate - 0// : 0// :0 Tetrachloro-m-xylene 0-0// : 0// :0 Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Added Result Aldrin ug/l - alpha-bhc ug/l - alpha-chlordane ug/l - beta-bhc ug/l -,' ug/l 0 -,'-E ug/l -,'-T ug/l - delta-bhc ug/l - ieldrin ug/l 0 - Endosulfan I ug/l - Endosulfan II ug/l - Endosulfan sulfate ug/l - Endrin ug/l - Endrin aldehyde ug/l - Endrin ketone ug/l 0 - gamma-bhc (Lindane) ug/l - gamma-chlordane ug/l - Heptachlor ug/l 0 - Heptachlor epoxide ug/l - Methoxychlor I ug/l - %Rec LCS LCS CB ecachlorobiphenyl 0 - ibutylchlorendate - Tetrachloro-m-xylene - Page of //0

40 QC Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) TestAmerica Job I: 0-- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS %Rec. RP Added Result Aldrin ug/l - alpha-bhc ug/l - 0 alpha-chlordane ug/l - 0 beta-bhc ug/l -,' ug/l - 0,'-E ug/l -,'-T ug/l - 0 delta-bhc ug/l - ieldrin ug/l - 0 Endosulfan I ug/l - 0 Endosulfan II ug/l 0 - Endosulfan sulfate ug/l - 0 Endrin ug/l - 0 Endrin aldehyde ug/l - Endrin ketone ug/l 0 - gamma-bhc (Lindane) ug/l - gamma-chlordane ug/l - Heptachlor ug/l - Heptachlor epoxide ug/l - Methoxychlor I ug/l - %Rec RP Limit LCS LCS CB ecachlorobiphenyl 0 - ibutylchlorendate - Tetrachloro-m-xylene 0 - Lab Sample I: 0-- MS Client Sample I: LMW-P Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS %Rec. Result Added Result Aldrin U ug/l - alpha-bhc 0.00 U ug/l - 0 alpha-chlordane ug/l 0-0 beta-bhc ug/l 0 -,' ug/l 0-0,'-E ug/l 0-0,'-T ug/l - 0 delta-bhc ug/l - ieldrin U ug/l 0 - Endosulfan I ug/l - 0 Endosulfan II ug/l - 0 Endosulfan sulfate ug/l 0 - Endrin ug/l - 0 Endrin aldehyde ug/l - Endrin ketone ug/l - gamma-bhc (Lindane) ug/l - gamma-chlordane ug/l 0-0 %Rec Page 0 of //0

41 QC Sample Results Method: 0B - Organochlorine Pesticides by GC (Continued) TestAmerica Job I: 0-- Lab Sample I: 0-- MS Client Sample I: LMW-P Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS %Rec. Result Added Result Heptachlor ug/l - Heptachlor epoxide ug/l 0-0 Methoxychlor I ug/l - MS MS CB ecachlorobiphenyl 0 - ibutylchlorendate - Tetrachloro-m-xylene - Lab Sample I: 0-- MS Client Sample I: LMW-P Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS %Rec. RP Result Added Result Aldrin U ug/l - 0 alpha-bhc 0.00 U ug/l alpha-chlordane ug/l beta-bhc ug/l 0-0,' ug/l 0-0 0,'-E ug/l 0-0 0,'-T ug/l delta-bhc ug/l - 0 ieldrin U ug/l 0-0 Endosulfan I ug/l Endosulfan II ug/l Endosulfan sulfate ug/l 0-0 Endrin ug/l Endrin aldehyde ug/l - 0 Endrin ketone ug/l - 0 gamma-bhc (Lindane) ug/l 0 - gamma-chlordane ug/l Heptachlor ug/l - 0 Heptachlor epoxide ug/l Methoxychlor I ug/l 0-0 %Rec %Rec RP Limit MS MS CB ecachlorobiphenyl 0 - ibutylchlorendate - Tetrachloro-m-xylene - Page of //0

42 QC Sample Results TestAmerica Job I: 0-- Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB Result PQL Bolstar 0.0 U ug/l 0// : 0// :0 Chlorpyrifos Coumaphos emeton, Total iazinon ichlorvos imethoate isulfoton EPN Ethyl Parathion Fensulfothion Guthion Malathion Merphos Methyl parathion Mevinphos Mocap Monochrotophos Naled Phorate Ronnel Sulfotepp Tokuthion Trichloronate ML 0. U.0 0. ug/l 0// : 0// :0 0.0 U ug/l 0// : 0// :0 0. U. 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0.0 U ug/l 0// : 0// : U ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0.0 U ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U ug/l 0// : 0// :0. U. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 0.0 U ug/l 0// : 0// :0 0.0 U ug/l 0// : 0// :0 0. U.0 0. ug/l 0// : 0// :0 MB MB Triphenylphosphate (TPP) - 0// : 0// :0 Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Added Result %Rec Bolstar.0. ug/l 0-0 Chlorpyrifos.0.0 ug/l 0-0 Coumaphos.0. ug/l 0-0 emeton, Total.00.0 ug/l iazinon.0. ug/l - ichlorvos.0. I ug/l 0-0 EPN.0. ug/l 0-0 Ethyl Parathion.0. ug/l - Fensulfothion.0. I ug/l 0-0 Guthion.0.0 ug/l 0-0 Malathion.0. ug/l 0-0 Methyl parathion.0. ug/l - 0 Mevinphos.0. I ug/l Page of //0

43 QC Sample Results TestAmerica Job I: 0-- Method: B - Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique (Continued) Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Added Result Mocap.0. ug/l Monochrotophos.0. I ug/l - 0 Naled.0. ug/l 0-0 Phorate.0. ug/l 0-0 Ronnel.0. ug/l - Tokuthion.0. ug/l Trichloronate.0.0 ug/l 0-0 LCS LCS Triphenylphosphate (TPP) - Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS %Rec. RP Added Result Bolstar.0. ug/l Chlorpyrifos.0. ug/l Coumaphos.0. ug/l emeton, Total.00. ug/l iazinon.0. ug/l - 0 ichlorvos.0. I ug/l EPN.0. ug/l Ethyl Parathion.0.0 ug/l - 0 Fensulfothion.0. I ug/l Guthion.0. ug/l Malathion.0. ug/l Methyl parathion.0.0 ug/l Mevinphos.0. I ug/l Mocap.0. ug/l Monochrotophos.0. I ug/l Naled.0.0 ug/l Phorate.0. ug/l Ronnel.0. ug/l - 0 Tokuthion.0. ug/l Trichloronate.0. ug/l %Rec %Rec RP Limit LCS LCS Triphenylphosphate (TPP) - Page of //0

44 QC Sample Results Method: FL-PRO - Florida - Petroleum Range Organics (GC) TestAmerica Job I: 0-- Lab Sample I: MB 00-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: MB MB Total Petroleum Hydrocarbons (C-C0) Result PQL ML U 0 ug/l 0// : 0// : MB MB n-c - 0// : 0// : o-terphenyl - 0// : 0// : Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: Spike LCS LCS %Rec. Total Petroleum Hydrocarbons (C-C0) LCS LCS Added n-c - Result 00 0 ug/l - o-terphenyl - Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: 0 Prep Batch: Spike LCS LCS %Rec. RP Total Petroleum Hydrocarbons (C-C0) LCS LCS Added n-c - Result %Rec 00 0 ug/l - 0 o-terphenyl - %Rec RP Limit Method: B - ioxins/furans, HRGC/HRMS (B) Lab Sample I: HG000000B Analysis Batch: MB MB,,,-TC Result ML EL TEF TEQ N Client Sample I: Method Blank Prep Type: Total Prep Batch: _P pg/l 0/0/ : 0/0/ : Total TC N pg/l 0/0/ : 0/0/ :,,,,-PeC 0. J I pg/l 0/0/ : 0/0/ : Total PeC 0. J I pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ :,,,,,-HxC N pg/l 0/0/ : 0/0/ : Total HxC N pg/l 0/0/ : 0/0/ :,,,,,,-HpC. J I pg/l 0/0/ : 0/0/ : Total HpC. J I pg/l 0/0/ : 0/0/ : Page of //0

45 QC Sample Results Method: B - ioxins/furans, HRGC/HRMS (B) (Continued) Lab Sample I: HG000000B Analysis Batch: MB MB OC Result ML EL TEF TEQ. J I TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type: Total Prep Batch: _P pg/l 0/0/ : 0/0/ :,,,-TCF N pg/l 0/0/ : 0/0/ : Total TCF N.0 0. pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ :,,,,-PeCF N pg/l 0/0/ : 0/0/ : Total PeCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ :,,,,,-HxCF 0. J I pg/l 0/0/ : 0/0/ :,,,,,-HxCF N pg/l 0/0/ : 0/0/ : Total HxCF 0. J I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF 0. J I pg/l 0/0/ : 0/0/ :,,,,,,-HpCF 0. J I pg/l 0/0/ : 0/0/ : Total HpCF 0. J I pg/l 0/0/ : 0/0/ : OCF. I pg/l 0/0/ : 0/0/ : Total TEQ MB MB Cl-,,,-TC - 0/0/ : 0/0/ : Internal Standard MB MB 0. C-,,,-TC - 0/0/ : 0/0/ : C-,,,,-PeC 0-0/0/ : 0/0/ : C-,,,,,-HxC - 0/0/ : 0/0/ : C-,,,,,-HxC - 0 0/0/ : 0/0/ : C-,,,,,,-HpC - 0 0/0/ : 0/0/ : C-OC - 0/0/ : 0/0/ : C-,,,-TCF - 0/0/ : 0/0/ : C-,,,,-PeCF 0-0/0/ : 0/0/ : C-,,,,-PeCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF 0-0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,-HxCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-,,,,,,-HpCF - 0/0/ : 0/0/ : C-OCF - 0/0/ : 0/0/ : Lab Sample I: HG000000C Client Sample I: Lab Control Sample Prep Type: Total Analysis Batch: Prep Batch: _P Spike LCS LCS %Rec. Added Result %Rec,,,-TC 00 0 pg/l -,,,,-PeC 00 0 V pg/l 0 -,,,,,-HxC 00 0 pg/l 0 -,,,,,-HxC pg/l 0 - Page of //0

46 QC Sample Results Method: B - ioxins/furans, HRGC/HRMS (B) (Continued) Lab Sample I: HG000000C Analysis Batch: Spike Added LCS LCS Result TestAmerica Job I: 0-- Client Sample I: Lab Control Sample Prep Type: Total Prep Batch: _P %Rec.,,,,,-HxC 00 pg/l -,,,,,,-HpC 00 V pg/l 0-0 OC 000 V pg/l -,,,-TCF 00 0 pg/l -,,,,-PeCF 00 pg/l 0 -,,,,-PeCF 00 0 pg/l -,,,,,-HxCF 00 pg/l -,,,,,-HxCF 00 pg/l - 0,,,,,-HxCF 00 V pg/l 0 -,,,,,-HxCF 00 pg/l - 0,,,,,,-HpCF 00 V pg/l -,,,,,,-HpCF 00 V pg/l - OCF V pg/l - LCS LCS Cl-,,,-TC - Internal Standard LCS LCS C-,,,-TC 0 - C-,,,,-PeC - C-,,,,,-HxC - C-,,,,,-HxC - C-,,,,,,-HpC - C-OC - C-,,,-TCF - C-,,,,-PeCF - C-,,,,-PeCF - C-,,,,,-HxCF - 0 C-,,,,,-HxCF - C-,,,,,-HxCF - C-,,,,,-HxCF - 0 C-,,,,,,-HpCF - C-,,,,,,-HpCF 0 - C-OCF - %Rec Method: 00A - Metals (ICP/MS) Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis Batch: Prep Batch: MB MB Result PQL Arsenic. U.. ug/l 0// 0: 0// :0 Barium Cadmium Chromium Lead ML. U.0. ug/l 0// 0: 0// :0 0.0 U ug/l 0// 0: 0// :0. U.0. ug/l 0// 0: 0// :0 0.0 U. 0.0 ug/l 0// 0: 0// :0 Page of //0

47 Method: 00A - Metals (ICP/MS) (Continued) QC Sample Results TestAmerica Job I: 0-- Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis Batch: Prep Batch: MB MB Result PQL Selenium.0 U..0 ug/l 0// 0: 0// :0 Silver ML 0. U.0 0. ug/l 0// 0: 0// :0 Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Added Result Arsenic 0 ug/l - Barium 0 ug/l - Cadmium ug/l - Chromium 0 ug/l - Lead 00 0 ug/l - Selenium 0 ug/l - Silver 0.0. ug/l - Method: 0A - Mercury (CVAA) Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB Result PQL Mercury 0.00 U ug/l 0// :0 0// :0 ML %Rec Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS %Rec. Added Result %Rec Mercury.0. ug/l 0-0 Lab Sample I: 0-- MS Client Sample I: LMW-B Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS %Rec. Result Added Result %Rec Mercury 0.00 U.00.0 ug/l 0-0 Lab Sample I: 0-- MS Client Sample I: LMW-B Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS %Rec. RP Result Added Result %Rec RP Limit Mercury 0.00 U.00.0 ug/l Page of //0

48 Internal Standards Summary Method: B - ioxins/furans, HRGC/HRMS (B) TestAmerica Job I: 0-- Percent Internal Standard Recovery (Acceptance ) Prep Type: Total TC,,,,-Pe,,,,-H,,,,-H,,,,,- C-OC TCF,,,,-Pe Lab Sample I Client Sample I (-) (-) (-) (-0) (-0) (-) (-) (-) 0-- LMW-B LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A HG000000B Method Blank Percent Internal Standard Recovery (Acceptance ) PeCF,,,,-H HxCF HxCF HxCF,,,,,-,,,,,- C-OCF Lab Sample I Client Sample I (-) (-) (-) (-) (-) (-) (-) (-) 0-- LMW-B LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A HG000000B Internal Standard Legend TC = C-,,,-TC Method Blank C-,,,,-PeC = C-,,,,-PeC C-,,,,,-HxC = C-,,,,,-HxC C-,,,,,-HxC = C-,,,,,-HxC C-,,,,,,-HpC = C-,,,,,,-HpC C-OC = C-OC TCF = C-,,,-TCF C-,,,,-PeCF = C-,,,,-PeCF PeCF = C-,,,,-PeCF C-,,,,,-HxCF = C-,,,,,-HxCF HxCF = C-,,,,,-HxCF HxCF = C-,,,,,-HxCF HxCF = C-,,,,,-HxCF C-,,,,,,-HpCF = C-,,,,,,-HpCF C-,,,,,,-HpCF = C-,,,,,,-HpCF C-OCF = C-OCF Method: B - ioxins/furans, HRGC/HRMS (B) Prep Type: Total Percent Internal Standard Recovery (Acceptance ) TC,,,,-Pe,,,,-H,,,,-H,,,,,- C-OC TCF,,,,-Pe Lab Sample I Client Sample I (0-) (-) (-) (-) (-) (-) (-) (-) HG000000C Lab Control Sample Percent Internal Standard Recovery (Acceptance ) PeCF,,,,-H HxCF HxCF HxCF,,,,,-,,,,,- C-OCF Lab Sample I Client Sample I (-) (-0) (-) (-) (-0) (-) (0-) (-) HG000000C Lab Control Sample Internal Standard Legend TC = C-,,,-TC C-,,,,-PeC = C-,,,,-PeC Page of //0

49 C-,,,,,-HxC = C-,,,,,-HxC C-,,,,,-HxC = C-,,,,,-HxC C-,,,,,,-HpC = C-,,,,,,-HpC C-OC = C-OC TCF = C-,,,-TCF C-,,,,-PeCF = C-,,,,-PeCF PeCF = C-,,,,-PeCF C-,,,,,-HxCF = C-,,,,,-HxCF HxCF = C-,,,,,-HxCF HxCF = C-,,,,,-HxCF HxCF = C-,,,,,-HxCF C-,,,,,,-HpCF = C-,,,,,,-HpCF C-,,,,,,-HpCF = C-,,,,,,-HpCF C-OCF = C-OCF Internal Standards Summary TestAmerica Job I: 0-- Page of //0

50 GC/MS VOA Analysis Batch: QC Association Summary TestAmerica Job I: 0-- Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0B 0-- LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-/ Lab Control Sample MB 0-/ Method Blank GC/MS Semi VOA Prep Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0C 0-- LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-0/-A Lab Control Sample LCS 0-0/-A Lab Control Sample up MB 0-0/-A Method Blank Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0 LL LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-0/-A Lab Control Sample LCS 0-0/-A Lab Control Sample up MB 0-0/-A Method Blank 0B 0B 0B 0B 0B 0B 0C 0C 0C 0C 0C 0C 0C 0 LL 0 0 LL 0 0 LL 0 0 LL 0 0 LL 0 0 LL 0 0 LL 0 GC Semi VOA Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0C 0-- LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-/-A Lab Control Sample LCS 0-/-A Lab Control Sample up MB 0-/-A Method Blank Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B B 0-- LMW-P 0-- LMW-B 0C 0C 0C 0C 0C 0C 0C B B Page 0 of //0

51 GC Semi VOA (Continued) Analysis Batch: (Continued) QC Association Summary TestAmerica Job I: 0-- Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-P B 0-- LMW-A LCS 0-/-A Lab Control Sample LCS 0-/-A Lab Control Sample up MB 0-/-A Method Blank Prep Batch: B B B B Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0-- LMW-P 0-- MS LMW-P 0-- MS LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-/-A Lab Control Sample LCS 0-/-A Lab Control Sample up MB 0-/-A Method Blank Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0B 0-- MS LMW-P 0-- MS LMW-P LCS 0-/-A Lab Control Sample LCS 0-/-A Lab Control Sample up MB 0-/-A Method Blank 0B 0B 0B 0B 0B Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0B 0-- LMW-P 0-- LMW-A Analysis Batch: 0 0B 0B Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-P 0B Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0C 0-- LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 00-/-A Lab Control Sample LCS 00-/-A Lab Control Sample up MB 00-/-A Method Blank 0C 0C 0C 0C 0C 0C 0C Page of //0

52 GC Semi VOA (Continued) Analysis Batch: 0 QC Association Summary TestAmerica Job I: 0-- Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B FL-PRO 0-- LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 00-/-A Lab Control Sample LCS 00-/-A Lab Control Sample up MB 00-/-A Method Blank Specialty Organics Analysis Batch: FL-PRO FL-PRO FL-PRO FL-PRO FL-PRO FL-PRO FL-PRO Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B Total B 0-- LMW-P Total 0-- LMW-B Total 0-- LMW-P Total 0-- LMW-A Total HG000000B Method Blank Total HG000000C Lab Control Sample Total Prep Batch: _P Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B Total 0-- LMW-P Total 0-- LMW-B Total 0-- LMW-P Total 0-- LMW-A Total HG000000B Method Blank Total HG000000C Lab Control Sample Total B B B B B B Metals Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0A 0-- MS LMW-B 0-- MS LMW-B 0-- LMW-P 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-/-A Lab Control Sample MB 0-/-A Method Blank Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B 0A 0-- MS LMW-B 0-- MS LMW-B 0A 0A 0A 0A 0A 0A 0A 0A 0A 0A Page of //0

53 Metals (Continued) Analysis Batch: (Continued) QC Association Summary TestAmerica Job I: 0-- Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-P 0A 0-- LMW-B 0-- LMW-P 0-- LMW-A LCS 0-/-A Lab Control Sample MB 0-/-A Method Blank Prep Batch: 0A 0A 0A 0A 0A Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B Total Recoverable 00A 0-- LMW-P Total Recoverable 0-- LMW-B Total Recoverable 0-- LMW-P Total Recoverable 0-- LMW-A Total Recoverable LCS 0-/-A Lab Control Sample Total Recoverable MB 0-/-A Method Blank Total Recoverable Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- LMW-B Total Recoverable 00A 0-- LMW-P Total Recoverable 0-- LMW-B Total Recoverable 0-- LMW-P Total Recoverable 0-- LMW-A Total Recoverable LCS 0-/-A Lab Control Sample Total Recoverable MB 0-/-A Method Blank Total Recoverable 00A 00A 00A 00A 00A 00A 00A 00A 00A 00A 00A 00A Page of //0

54 Lab Chronicle Client: Langan Engineering & Environmental Srvcs TestAmerica Job I: 0-- Client Sample I: LMW-B Lab Sample I: 0-- ate Collected: 0// 0: ate Received: 0// 0:0 Prep Type Total Total Total Recoverable Total Recoverable Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// :0 ECC TAL TAM Prep 0C 0 0// :0 QMC TAL TAL Analysis 0 LL 0// : JMF TAL TAL Prep 0// : R TAL TAL Analysis 0B 0// 0:0 CWA TAL TAL Prep 0C 0// : QMC TAL TAL Analysis B 0// : MLT TAL TAL Prep 0C 0// : KH TAL PEN Analysis FL-PRO 0 0// :0 IR TAL PEN Prep _P 0/0/ : TAL KNX Analysis B 0/0/ : MA TAL KNX Prep 00A 0// 0: BJB TAL SAV Analysis 00A 0// : BWR TAL SAV Prep 0A 0// :0 JKL TAL SAV Analysis 0A 0// : JKL TAL SAV Client Sample I: LMW-P Lab Sample I: 0-- ate Collected: 0// : ate Received: 0// 0:0 Lab Prep Type Total Total Total Recoverable Total Recoverable Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// : ECC TAL TAM Prep 0C 0 0// :0 QMC TAL TAL Analysis 0 LL 0// :0 JMF TAL TAL Prep 0// : R TAL TAL Analysis 0B 0 0// : CWA TAL TAL Prep 0C 0// : QMC TAL TAL Analysis B 0// : MLT TAL TAL Prep 0C 0// : KH TAL PEN Analysis FL-PRO 0 0// : IR TAL PEN Prep _P 0/0/ : TAL KNX Analysis B 0/0/ : MA TAL KNX Prep 00A 0// 0: BJB TAL SAV Analysis 00A 0// :00 BWR TAL SAV Prep 0A 0// :0 JKL TAL SAV Analysis 0A 0// :0 JKL TAL SAV Lab Client Sample I: LMW-B Lab Sample I: 0-- ate Collected: 0// : ate Received: 0// 0:0 Prep Type Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// : ECC TAL TAM Lab Page of //0

55 Lab Chronicle Client: Langan Engineering & Environmental Srvcs TestAmerica Job I: 0-- Client Sample I: LMW-B Lab Sample I: 0-- ate Collected: 0// : ate Received: 0// 0:0 Prep Type Total Total Total Recoverable Total Recoverable Batch Type Batch Method Run ilution Factor Batch Number or Analyst Prep 0C 0 0// :0 QMC TAL TAL Analysis 0 LL 0// :0 JMF TAL TAL Prep 0// : R TAL TAL Analysis 0B 0// : CWA TAL TAL Prep 0C 0// : QMC TAL TAL Analysis B 0// 0: MLT TAL TAL Prep 0C 0// : KH TAL PEN Analysis FL-PRO 0 0// : IR TAL PEN Prep _P 0/0/ : TAL KNX Analysis B 0/0/ : MA TAL KNX Prep 00A 0// 0: BJB TAL SAV Analysis 00A 0// :0 BWR TAL SAV Prep 0A 0// :0 JKL TAL SAV Analysis 0A 0// :0 JKL TAL SAV Client Sample I: LMW-P Lab Sample I: 0-- ate Collected: 0// : ate Received: 0// 0:0 Prep Type Total Total Total Recoverable Total Recoverable Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// :0 ECC TAL TAM Prep 0C 0 0// :0 QMC TAL TAL Analysis 0 LL 0// : JMF TAL TAL Prep 0// : R TAL TAL Analysis 0B 0// : CWA TAL TAL Prep 0C 0// : QMC TAL TAL Analysis B 0// 0: MLT TAL TAL Prep 0C 0// : KH TAL PEN Analysis FL-PRO 0 0// : IR TAL PEN Prep _P 0/0/ : TAL KNX Analysis B 0/0/ : MA TAL KNX Prep 00A 0// 0: BJB TAL SAV Analysis 00A 0// : BWR TAL SAV Prep 0A 0// :0 JKL TAL SAV Analysis 0A 0// : JKL TAL SAV Lab Lab Client Sample I: LMW-A Lab Sample I: 0-- ate Collected: 0// : ate Received: 0// 0:0 Prep Type Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// : ECC TAL TAM Prep 0C 0 0// :0 QMC TAL TAL Lab Page of //0

56 Lab Chronicle Client: Langan Engineering & Environmental Srvcs TestAmerica Job I: 0-- Client Sample I: LMW-A Lab Sample I: 0-- ate Collected: 0// : ate Received: 0// 0:0 Prep Type Total Total Total Recoverable Total Recoverable Batch Type Laboratory References: Batch Method Run ilution Factor Batch Number or Analyst Analysis 0 LL 0// :0 JMF TAL TAL Prep 0// : R TAL TAL Analysis 0B 0// : CWA TAL TAL Prep 0C 0// : QMC TAL TAL Analysis B 0// 0: MLT TAL TAL Prep 0C 0// : KH TAL PEN Analysis FL-PRO 0 0// : IR TAL PEN Prep _P 0/0/ : TAL KNX Analysis B 0/0/ 0: MA TAL KNX Prep 00A 0// 0: BJB TAL SAV Analysis 00A 0// : BWR TAL SAV Prep 0A 0// :0 JKL TAL SAV Analysis 0A 0// : JKL TAL SAV TAL KNX = TestAmerica Knoxville, Middlebrook Pike, Knoxville, TN, TEL ()-000 TAL PEN = TestAmerica Pensacola, McLemore rive, Pensacola, FL, TEL (0)-0 TAL SAV = TestAmerica Savannah, LaRoche Avenue, Savannah, GA 0, TEL ()- TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- TAL TAM =, Benjamin Road, Suite 0, Tampa, FL, TEL ()- Lab Page of //0

57 Method Summary TestAmerica Job I: 0-- Method Method escription Protocol Laboratory 0B Volatile Organic Compounds (GC/MS) SW TAL TAM 0 LL Semivolatile Organic Compounds by GC/MS - Low Level SW TAL TAL 0B Organochlorine Pesticides by GC SW TAL TAL B Organophosphorous Compounds by Gas Chromatography, Capillary Column Technique SW TAL TAL FL-PRO Florida - Petroleum Range Organics (GC) FL-EP TAL PEN B ioxins/furans, HRGC/HRMS (B) EPA- TAL KNX 00A Metals (ICP/MS) SW TAL SAV 0A Mercury (CVAA) SW TAL SAV Protocol References: EPA- = EPA- FL-EP = State Of Florida epartment Of Environmental Protection, Florida Administrative Code. SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL KNX = TestAmerica Knoxville, Middlebrook Pike, Knoxville, TN, TEL ()-000 TAL PEN = TestAmerica Pensacola, McLemore rive, Pensacola, FL, TEL (0)-0 TAL SAV = TestAmerica Savannah, LaRoche Avenue, Savannah, GA 0, TEL ()- TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- TAL TAM =, Benjamin Road, Suite 0, Tampa, FL, TEL ()- Page of //0

58 Certification Summary Client: Langan Engineering & Environmental Srvcs TestAmerica Job I: 0-- Laboratory: The certifications listed below are applicable to this report. Authority Program EPA Region Certification I Expiration ate Florida NELAP E 0-0- Laboratory: TestAmerica Knoxville All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Arkansas EQ State Program California State Program 0-0- Colorado State Program N/A 0-- Connecticut State Program PH Florida NELAP E 0-0- Georgia State Program Hawaii State Program N/A 0-- Kansas NELAP E- -- Kentucky (W) State Program 0 -- L-A-B o ELAP L 0-- Louisiana NELAP 0-0- Louisiana (W) NELAP LA00 -- Maryland State Program 0-- Michigan State Program 0-- Nevada State Program TN New Jersey NELAP TN New York NELAP 0-- North Carolina (W) State Program 0-- North Carolina (WW/SW) State Program -- Ohio VAP State Program CL Oklahoma State Program 0-- Pennsylvania NELAP South Carolina State Program Tennessee State Program Texas NELAP T00-TX 0-- USA Federal P Utah NELAP QUAN 0-- Virginia NELAP Washington State Program C 0-- West Virginia (W) State Program C -- West Virginia EP State Program 0-0- Wisconsin State Program Laboratory: TestAmerica Pensacola All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Alabama State Program Arizona State Program AZ0 0-- Arkansas EQ State Program Florida NELAP E 0-0- Georgia State Program N/A 0-0- Illinois NELAP Iowa State Program 0-- Kansas NELAP E- 0-- * * Certification renewal pending - certification considered valid. Page of //0

59 Certification Summary Client: Langan Engineering & Environmental Srvcs TestAmerica Job I: 0-- Laboratory: TestAmerica Pensacola (Continued) All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Kentucky (UST) State Program 0-0- Kentucky (WW) State Program * Louisiana NELAP Maryland State Program 0-0- Massachusetts State Program M-FL Michigan State Program 0-0- New Jersey NELAP FL North Carolina (WW/SW) State Program -- * Oklahoma State Program 0-- Pennsylvania NELAP Rhode Island State Program LAO * South Carolina State Program Tennessee State Program TN Texas NELAP T USA Federal P Virginia NELAP West Virginia EP State Program 0-0- Laboratory: TestAmerica Savannah The certifications listed below are applicable to this report. Authority Program EPA Region Certification I Expiration ate Florida NELAP E Laboratory: TestAmerica Tallahassee Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification I Expiration ate Florida NELAP E The following analytes are included in this report, but are not certified under this certification: Analysis Method Prep Method Matrix B 0C emeton, Total * Certification renewal pending - certification considered valid. Page of //0

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