March 6, Mr. John Meyer DRI Coordinator Tampa Bay Regional Planning Council 4000 Gateway Center Blvd. Pinellas Park, FL 33782

Transcription

1 Cardno ENTRIX March, 0 Mr. John Meyer RI Coordinator Tampa Bay Regional Planning Council 000 Gateway Center Blvd. Pinellas Park, FL 0 Crescent Park rive Riverview, FL USA Phone 00 Toll-free 00 Fax Michele Crary Pasco County Government Center Planning and evelopment ept. Citizens r., Suite 0 New Port Richey, FL Tricia Neasman RI Review Coordinator SWFWM Broad Street Brooksville, FL 0 Mary Ellen Edwards Florida epartment of Environmental Protection 0 N. Telecom Parkway Temple Terrace, FL -0 RE: Wesley Chapel Lakes (RI No. ) Annual Quality and Wetland Hydroperiod Monitoring s (0) To Whom It May Concern: Please find attached the water quality and wetland hydroperiod monitoring report of 0. The raw data for the surface and groundwater quality sampling is attached. ue to the lack of flow through the creek system sampling for the surface water was collected using the shallow well. issolved oxygen, iron and alkalinity were the only parameters that exceeded the applicable Class III water quality standard. Low dissolved oxygen can be expected in the summer months when warmer waters have less ability to hold oxygen as well as within groundwater. The slightly higher iron concentrations tend to occur when sampling from a groundwater source. Low alkalinity is not uncommon in ephemeral conveyances that are dominated by rainfall. Australia Belgium Canada Ecuador Indonesia Kenya New Zealand Papua New Guinea Peru ed Arab Emirates ed Kingdom ed States Operations in 0 countries

2 Wesley Chapel Lakes RI No. Annual Quality and Wetland Hydroperiod Monitoring s (0) The parameters raise no concern over continued development activities at the Wesley Chapel site. All other parameters analyzed during this assessment were within normal, expected ranges with no exceedances of applicable Class III standards. Please let us know if you have any questions or comments relative to the report. Sincerely, John A. Goolsby, CEP Senor Project Scientist For Cardno ENTRIX Timothy L. Neldner, PWS Senior Consultant for Cardno ENTRIX JAG/mmm/cab Enc: cc: Wesley Chapel Lakes Surface Quality Monitoring 0-0 Monitoring Report Mike ady w/ Meadow Pointe IV Holdings Lee Arnold w/ Maxcy evelopment Group Maggie McCullagh/Cardno ENTRIX

3 Wesley Chapel Lakes Surface Quality Monitoring 0-0 Monitoring Report

4 Wesley Chapel Lakes 0-0 Monitoring Report ocument Information for Maxcy evelopment/meadow Pointe IV Holdings Project Name Wesley Chapel Lakes Project Number / Project Manager John Goolsby ate March 0 for: Mr. Mike ady Meadow Pointe IV Holdings Park Place Blvd., Suite 00 Clearwater, FL Mr. Lee Arnold Maxcy evelopment Group Colwell Ave., Suite 0 Tampa, FL by: Maggie M. McCullagh Environmental Specialist Jason E. Jendrucko Staff Scientist aniel G. Hammond Senior Project Scientist Cardno ENTRIX 0 Crescent Park rive Riverview, FL

5 Wesley Chapel Lakes 0-0 Monitoring Report Table of Contents Introduction...- Monitoring Protocol...-. Monitoring Stations Monitoring Schedule and Conditions... - Parameters...- s...- iscussion...- Appendix Appendix A Lab ata Sheets Tables Table Field and Lab s, Wesley Chapel Lakes, Pasco County, Florida... - Table Piezometer and Staff Gauge s, Wesley Chapel Lakes, Pasco County, FL, October 0 and 0 February Figures Figure Quality & Level Monitoring... -

6 Wesley Chapel Lakes 0-0 Monitoring Report Introduction Cardno ENTRIX was retained by Wesley Chapel Lakes to conduct surface water monitoring at the Wesley Chapel Lakes development site. Pasco County issued evelopment Order No. - which contained various requirements for the project. The project site is located south of the County Road in Pasco County, Florida. The following report presents the water quality results for the 0 monitoring year with the wet season results from 0 and the dry season results from 0. Monitoring Protocol. Monitoring Stations Sampling occurs at two locations inside the Meadow Pointe community at the northern most point of the property where stormwater enters the site (Inflow) and the southernmost point of the property where stormwater exits the site (Outfall) (Figure ). The Inflow station was known as SW- and W- and the Outfall station was known as SW- and W- in years past. In addition, six shallow well piezometers are monitored for water levels throughout the site (see Figure ).. Monitoring Schedule and Conditions According to the approved Monitoring Plan, two surface water quality monitoring events are scheduled to be conducted every year: one event during the dry season (January May) and one event during the wet season (June September). Monitoring is to continue until two years after build out. Sampling is conducted in the surface water conveyance when sufficient water is observed to cause flow at each monitoring station. This report presents the water quality results for the 0 monitoring year with the wet season results from 0 and the dry season results from 0. Parameters Field measurements and grab samples are collected following a rainfall event sufficient to cause flow at the monitoring station for the following parameters: Temperature Conductivity Turbidity ph issolved oxygen A grab sample is collected, preserved on site, and transported to the laboratory for analysis of the following parameters: Fecal Coliform Biochemical Oxygen emand Chromium Color Total Suspended Solids Nitrite Oil and Grease Lead Nitrate Chlorine Total Phosphorus Chloride Iron Total Organic Carbon Copper Volatile Organics* Orthophosphate Sulfate Semi-volatile Organics* Alkalinity *every other year only Sampling is conducted according to Florida epartment of Environmental Protection (EP) Standard Operating Procedures (SOP). Laboratory analysis is performed by a facility possessing NELAC accreditation. March 0 Cardno ENTRIX - Wesley_Chapel_0_Report

7 ! P-! P-! Infall! P-! P-! P-! Level Monitors! Quality Monitors Outfall P-! 0,000,000 Feet 0 00,00 Meters This map and all data contained within are supplied as is with no warranty. Cardno ENTRIX, Inc. expressly disclaims responsibility for damages or liability from any claims that may arise out of the use or misuse of this map. It is the sole responsibility of the user to determine if the data on this map meets the user s needs. This map was not created as survey data, nor should it be used as such. It is the user s responsibility to obtain proper survey data, prepared by a licensed surveyor, where required by law. Figure. Quality & Level Monitoring Wesley Chapel Lakes Pasco County, Florida ÊImage: 00 Sec,, Twp S Rng 0 E 0 Crescent Park rive Riverview, FL - x.com ph. () -00 fx () -00 Coordinate System: NA UTM Zone N feet ate: 0/0/0 Rev. ate: 0/0/0 PM: JJ GIS Analyst: ACW Map ocument: piezometers_000_acw.mxd Project Number: -00 PF ocument: piezometers_000_acw.pdf Plot Size:. x

8 Wesley Chapel Lakes 0-0 Monitoring Report s s of field measurements and laboratory analyses are provided in Tables and. Laboratory data sheets are attached as Appendix A. Cardno ENTRIX sampled during the wet season on October 0 and 0 February 0 the results are presented below. Table Field and Lab s, Wesley Chapel Lakes, Pasco County, Florida Paramete r Temperatu re ( C) issolved Oxygen (mg/l) ph (std s) Conductivi ty (ms/cm) Turbidity (NTU) Salinity (ppt) Oil and Grease Class III Standard Wet Season event 0//0 ry Season event 0/0/0 Outfall Inflow Outfall Inflow SW- W- SW- W- SW- W- SW- W- N/A shall not be <.0 mg/l shall not be <.0 or >. Shall not be increased more than 0% above background or to, whichever is greater above natural background conditions N/A Shall not be >.0 U (.) U (.) U (.). I. I 0. I. I 0. I Chloride N/A 0 0 Chlorine (Residual) 0.0 U (.0) U (.0) U (.0) U (.0) U (.0) U (.00) U (.0) U (.0) Sulfate N/A 0. I. 0 U (.). I U (.) Nitrate N/A U (0.0) U (0.0) U (0.0) U (0.0) U (.0) U (.0) U (.0) U (.0) Nitrite N/A U (0.0) U (0.0) U (0.0) U (0.0) U (.0) U (.0) U (.0) U (.0) Nitrate+Nit rite Phosphoru s N/A U (0.0) U (0.0) U (0.0) U (0.0) U (.0) U (.0) U (.0) U (.0) N/A 0. I I 0.0 I 0.0 I I Color N/A March 0 Cardno ENTRIX - Wesley_Chapel_0_Report

9 Wesley Chapel Lakes 0 Monitoring Report Paramete r Biochemic al Oxygen emand Class III Standard Shall not be increased to exceed values which would cause dissolved oxygen to be depressed below the limit Wet Season event 0//0 ry Season event 0/0/0 Outfall Inflow Outfall Inflow SW- W- SW- W- SW- W- SW- W- U (.0) U (.0) U (.0) U (.0) U (.0) U (.0) U (.0) Total issolved Solids Total Suspende d Solids Total Coliform Fecal Coliform N/A N/A..... #CFU/00mL #CFU/00mL 0 U (.0) U (.0) U (.0) U (.0) Total Alkalinity Shall not be depressed below Iron.0 mg/l I.. U (0.00) Chromium Copper Lead Cr(III) e(0.[ln H]+0.) µg/l Cu e(0.[lnh] -.0) µg/l Pb e(.[lnh]-.0) µg/l U(.0) U(.0) U(.0) U (.0). I.0 I. I U (.0) U (.) U (.) U (.) U (.) U (.). I U (.) U (.) U (.0) U (.0) U (.0) U (.0) U (.0) U (.0) U (.0). I Total Organic Carbon 0.0 ml. 0. I... For the following parameters only detections will be listed Volatile Organics Semi- Volatile Organics Various U U U U U U U U Various U U U U * * * * Bis(-ethylhexyl) phthalate 0. IV. IV 0. IV. IV U - Undetected Value listed is the laboratory method detection limit (ML). I - Indicates result was detected between the method detection limit and the practical quantitation limit () V - Indicates the analyte was detected in both the sample and the associated method blank Piezometer and staff gauge measurements were collected on October 0 and 0 February 0 for stations P- through P- and are presented in Table. March 0 Cardno ENTRIX - Wesley_Chapel_0_Report

10 Wesley Chapel Lakes 0 Monitoring Report Table Piezometer and Staff Gauge s, Wesley Chapel Lakes, Pasco County, FL, October 0 and 0 February 0. Station Piezometer reading (ft, NGV)* Staff Gauge Reading (ft) -Oct- -Feb- -Oct- -Feb- P out of water P out of water P out of water P-.. out of water out of water P-... (NGV) out of water P-.. N/A N/A *- reading estimated since pipe height unknown iscussion Cardno ENTRIX conducted surface water quality monitoring at the Wesley Chapel Lakes development site in accordance with the evelopment Order. ue to lack of flow in the system the dry season surface water sampling was obtained through the shallow well. This report presents the results the water quality results for the 0 monitoring year with the wet season results from 0 and the dry season results from 0. issolved oxygen, alkalinity and iron were the only parameters that exceeded the applicable Class III water quality standard throughout the monitoring period. Low dissolved oxygen can be expected in the summer months when warmer waters have less ability to hold oxygen. Low dissolved oxygen was expected during the dry season due to sampling having to occur through the shallow well. Low alkalinity is not uncommon in ephemeral conveyances that are dominated by rainfall and is expected to be lower in the shallow well. Iron exceeded the Class III standard in the deep well during the wet season and at all stations during the dry season with the exception of the deep well at the inflow. High iron results are not uncommon when sampling groundwater. These parameters do not raise any concern over continued development activities at the Wesley Chapel site. For the semi-volatile organics, Bis (-ethylhexyl) phthalate was detected, this does not raise a concern due to the fact that the parameter was also detected in the method blank. All other parameters analyzed during this assessment were within normal, expected ranges with no exceedances of applicable Class III standards. March 0 Cardno ENTRIX - Wesley_Chapel_0_Report

11 Wesley Chapel Lakes APPENIX A LAB ATA SHEETS

12 ANALYTICAL REPORT TestAmerica Laboratories, Inc. Benjamin Road Suite 00 Tampa, FL Tel: ()- TestAmerica Job I: 0-0- Client For: Cardno ENTRIX. 0 Crescent Park rive Riverview, Florida Attn: Mr. aniel Hammond 0 Authorized for release by: //0 :0:0 PM Nancy Robertson Project Manager II nancy.robertson@testamericainc.com esignee for Amy Atkins Project Manager I amy.atkins@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

13 Table of Contents TestAmerica Job I: 0-0- Cover Page Table of Contents efinitions/glossary Case Narrative etection Summary Client Sample s Surrogate Summary QC Sample s QC Association Summary Lab Chronicle Certification Summary Method Summary Sample Summary Chain of Custody Receipt Checklists Page of //0

14 s GC/MS VOA U GC/MS Semi VOA U J J I HPLC/IC I U Metals U J I General Chemistry I U Biology U escription Indicates that the compound was analyzed for but not detected. escription Indicates that the compound was analyzed for but not detected. efinitions/glossary Estimated value; value may not be accurate. Surrogate recovery outside of criteria. Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. escription The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Indicates that the compound was analyzed for but not detected. escription Indicates that the compound was analyzed for but not detected. Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. escription The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Indicates that the compound was analyzed for but not detected. escription Indicates that the compound was analyzed for but not detected. TestAmerica Job I: Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid L, RA, RE, IN Indicates a ilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample EL Estimated etection Limit EPA ed States Environmental Protection Agency ML Method etection Limit ML Minimum Level (ioxin) N Not detected at the reporting limit (or ML or EL if shown) Practical Quantitation Limit QC Quality Control RL Reporting Limit RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) Page of //0

15 Case Narrative Client: Cardno ENTRIX. TestAmerica Job I: 0-0- Job I: 0-0- Laboratory: Narrative Job Narrative 0-0- Receipt The samples were received on 0//0 : PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the coolers at receipt time were.º C,.º C,.º C and.º C. GC/MS Semi VOA Method 0C: The matrix spike (MS) recoveries for batch 0 were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method 0C: Surrogate recovery for the following sample was outside of acceptance limits: W-Outfall (0-0-). There was insufficient sample to perform a re-extraction; therefore, the data have been reported. Batch: 0. Method 0C: The laboratory control sample (LCS) for batch 0 exceeded control limits for the following analyte:,'-ichlorobenzidine.,'-ichlorobenzidine has been identified as a poor performing analyte when analyzed using this method; therefore, re-extraction was not performed. The LCS was re-run for verification. These results have been reported and qualified. Method 0C: The laboratory control sample (LCS) for batch 0 recovered outside acceptance limits for Hexachlorobutadiene and Hexachloroethane. The LCS was re-run for verification. There was insufficient sample to perform a re-extraction; therefore, the data have been reported. Method 0C: The matrix spike (MS) recoveries for batch 0 were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. 0 Method 0C: Surrogate recoveries were outside control limits for the following samples: SW-Inflow (0-0-), SW-Outfall (0-0-). The samples were reported from a re-extracted batch. The surrogates confirmed failure from the original batch. Matrix interference is suspected. The data have been qualified and reported. Batch: 0. Metals Method 00. Rev.: The matrix spike / matrix spike duplicate (MS/MS) recovery for batch 0 was outside control limits for Iron with parent sample result times greater than spike added. The associated laboratory control sample (LCS) recovery met acceptance criteria. Analytical batch 0. (0-0- MS), (0-0- MS) General Chemistry Method.: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch 000 were outside control limits for NO MW-P (0-0-). The associated laboratory control sample (LCS) recovery met acceptance criteria. Method SM B: The results for the following samples were outside the ideal range of 0-0 colonies per plate as defined by Standard Methods B: W-Inflow (0-0-), W-Outfall (0-0-) The colonies were clearly readable; therefore, the results have been reported. Batch 00 Method SM : Sample (0-0- U), SW-Inflow (0-0-) was performed at a dilution of based on sample location. This dilution did not fall within the ideal range of 0-0 colonies as defined by Standard Methods. Batch 0 Method SM : Batch 0 first and second level confirmations were >0% per method. SW-Inflow (0-0-) No other analytical or quality issues were noted. Page of //0

16 etection Summary TestAmerica Job I: 0-0- Client Sample I: W-Inflow Lab Sample I: 0-0- ML il Fac Method Prep Type Sulfate mg/l 00.0 Chloride mg/l 00.0 Iron 0.00 I mg/l 00. Rev. Total Recoverable HEM (Oil and Grease). I.0. mg/l A Phosphorus 0.0 I mg/l. Total Organic Carbon 0. I mg/l 00 Color PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids mg/l SM 0 Coliform, Total CFU/00mL SM B Client Sample I: SW-Inflow Lab Sample I: 0-0- ML il Fac Method Prep Type Sulfate mg/l 00.0 Chloride mg/l 00.0 Iron mg/l 00. Rev. Total Recoverable Phosphorus 0. I mg/l. Total Organic Carbon mg/l 00 Color PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity.0.0 mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids..0.0 mg/l SM 0 Biochemical Oxygen emand mg/l SM 0B Coliform, Total CFU/00mL 00 SM B Coliform, Fecal.0.0 CFU/00mL SM 0 Client Sample I: W-Outfall Lab Sample I: 0-0- ML il Fac Method Prep Type Sulfate 0. I mg/l 00.0 Chloride mg/l 00.0 Iron mg/l 00. Rev. Total Recoverable Phosphorus mg/l. Total Organic Carbon mg/l 00 Color PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids..0.0 mg/l SM 0 Coliform, Total CFU/00mL SM B Coliform, Fecal.0.0 CFU/00mL SM Client Sample I: SW-Outfall Lab Sample I: 0-0- ML il Fac Method Prep Type Sulfate mg/l 00.0 Chloride mg/l 00.0 Page of //0

17 etection Summary TestAmerica Job I: 0-0- Client Sample I: SW-Outfall (Continued) Lab Sample I: 0-0- ML il Fac Method Prep Type Iron mg/l 00. Rev. Total Recoverable Phosphorus 0. I mg/l. Total Organic Carbon mg/l 00 Color PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity.0.0 mg/l SM 0B Total issolved Solids.0.0 mg/l SM 0C Total Suspended Solids mg/l SM 0 Coliform, Total CFU/00mL 00 SM B Coliform, Fecal CFU/00mL SM Client Sample I: Trip Blank Lab Sample I: 0-0- No etections 0 Page of //0

18 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Inflow ate Collected: 0// 0:0 ate Received: 0// : Lab Sample I: 0-0- Method: 0B - Volatile Organic Compounds (GC/MS) ML il Fac Benzene 0.0 U ug/l 0// : Bromobenzene 0. U.0 0. ug/l 0// : Chlorobromomethane 0. U.0 0. ug/l 0// : ichlorobromomethane 0. U.0 0. ug/l 0// : Bromoform 0. U.0 0. ug/l 0// : Bromomethane. U.0. ug/l 0// : n-butylbenzene 0. U.0 0. ug/l 0// : sec-butylbenzene 0. U.0 0. ug/l 0// : tert-butylbenzene 0. U.0 0. ug/l 0// : Carbon tetrachloride 0. U.0 0. ug/l 0// : Chlorobenzene 0. U.0 0. ug/l 0// : Chloroethane. U.0. ug/l 0// : Chloroform 0.0 U ug/l 0// : Chloromethane.0 U.0.0 ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : Chlorodibromomethane 0. U.0 0. ug/l 0// :,-ibromo--chloropropane. U.0. ug/l 0// : Ethylene ibromide 0.0 U ug/l 0// : ibromomethane 0. U.0 0. ug/l 0// :,-ichlorobenzene 0. U.0 0. ug/l 0// :,-ichlorobenzene 0. U.0 0. ug/l 0// :,-ichlorobenzene 0. U.0 0. ug/l 0// : ichlorodifluoromethane. U.0. ug/l 0// :,-ichloroethane 0. U.0 0. ug/l 0// :,-ichloroethane 0. U.0 0. ug/l 0// :,-ichloroethene 0. U.0 0. ug/l 0// : cis-,-ichloroethene 0. U.0 0. ug/l 0// : trans-,-ichloroethene 0. U.0 0. ug/l 0// :,-ichloropropane 0. U.0 0. ug/l 0// :,-ichloropropane 0. U.0 0. ug/l 0// :,-ichloropropane 0. U.0 0. ug/l 0// :,-ichloropropene 0. U.0 0. ug/l 0// : cis-,-ichloropropene 0. U.0 0. ug/l 0// : trans-,-ichloropropene 0. U.0 0. ug/l 0// : Ethylbenzene 0. U.0 0. ug/l 0// : Hexachlorobutadiene 0.0 U ug/l 0// : Isopropylbenzene 0. U.0 0. ug/l 0// : -Isopropyltoluene 0. U.0 0. ug/l 0// : Methylene Chloride.0 U.0.0 ug/l 0// : Naphthalene. U.0. ug/l 0// : N-Propylbenzene 0. U.0 0. ug/l 0// : Styrene 0. U.0 0. ug/l 0// :,,,-Tetrachloroethane 0. U.0 0. ug/l 0// :,,,-Tetrachloroethane 0. U.0 0. ug/l 0// : Tetrachloroethene 0.0 U ug/l 0// : Toluene 0. U.0 0. ug/l 0// :,,-Trichlorobenzene 0. U.0 0. ug/l 0// :,,-Trichlorobenzene 0. U.0 0. ug/l 0// :,,-Trichloroethane 0. U.0 0. ug/l 0// :,,-Trichloroethane 0. U.0 0. ug/l 0// : 0 Page of //0

19 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Inflow ate Collected: 0// 0:0 ate Received: 0// : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- Trichloroethene 0.0 U ug/l 0// : Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U Surrogate %Recovery il Fac.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : 0. ug/l 0// : 0. ug/l 0// : 0. ug/l 0// :.0.0 ug/l 0// : 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : Toluene-d (Surr) // : -Bromofluorobenzene 0-0 0// : ibromofluoromethane // : Method: 0C - Semivolatile Organic Compounds (GC/MS),-ichlorobenzene. U. ug/l 0/0/ : 0// : N-Nitrosodimethylamine. U Phenol. U,-ichlorobenzene. U Hexachloroethane 0. U Bis(-chloroethyl)ether. U,-ichlorobenzene. U N-Nitrosodi-n-propylamine. U Nitrobenzene. U Hexachlorobutadiene. U,,-Trichlorobenzene. U Isophorone. U Naphthalene. U Bis(-chloroethoxy)methane. U Hexachlorocyclopentadiene. U -Chloronaphthalene. U Acenaphthylene.0 U Acenaphthene. U imethyl phthalate. U,-initrotoluene 0.0 U Fluorene. U -Chlorophenyl phenyl ether.0 U,-initrotoluene.0 U iethyl phthalate. U N-Nitrosodiphenylamine. U Hexachlorobenzene. U -Bromophenyl phenyl ether. U Phenanthrene. U Anthracene. U ML il Fac il Fac. ug/l 0/0/ : 0// :.. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.0 ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0.0 ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.0 ug/l 0/0/ : 0// :.0 ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0 Page of //0

20 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Inflow ate Collected: 0// 0:0 ate Received: 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- i-n-butyl phthalate. U. ug/l 0/0/ : 0// : Fluoranthene. U Pyrene. U Butyl benzyl phthalate. U Bis(-ethylhexyl) phthalate. U Chrysene. U Benzo[a]anthracene. U,'-ichlorobenzidine. U i-n-octyl phthalate. U Benzo[b]fluoranthene. U Benzo[k]fluoranthene. U Benzo[a]pyrene. U Indeno[,,-cd]pyrene. U ibenz(a,h)anthracene. U Benzo[g,h,i]perylene. U -Chlorophenol. U -Nitrophenol. U,-imethylphenol.0 U,-ichlorophenol.0 U,,-Trichlorophenol. U -Chloro--methylphenol. U,-initrophenol. U,-initro--methylphenol. U Pentachlorophenol. U -Nitrophenol. U Benzyl alcohol. U -Methylphenol. U Benzoic acid U -Chloroaniline. U -Methylnaphthalene. U,,-Trichlorophenol. U -Nitroaniline. U -Nitroaniline. U ibenzofuran. U -Nitroaniline. U & Methylphenol. U -Methylnaphthalene. U,'-oxybis[-chloropropane]. U il Fac. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.0 ug/l 0/0/ : 0// :.0 ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0 Surrogate %Recovery -Fluorophenol - 0/0/ : 0// : Nitrobenzene-d - 0 0/0/ : 0// : -Fluorobiphenyl - 0/0/ : 0// : Terphenyl-d - 0/0/ : 0// :,,-Tribromophenol - 0/0/ : 0// : Phenol-d (Surr) 0-0/0/ : 0// : il Fac Method: Anions, Ion Chromatography ML il Fac Sulfate mg/l 0// 0: Chloride mg/l 0// 0: Page of //0

21 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Inflow ate Collected: 0// 0:0 ate Received: 0// : Method: 00. Rev. - Metals (ICP) - Total Recoverable ML Lab Sample I: 0-0- Chromium U mg/l 0// 0: 0// : Copper 0.00 U Iron 0.00 I Lead U General Chemistry il Fac mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : HEM (Oil and Grease). I.0. mg/l 0// 0: 0// 0: Nitrate Nitrite as N 0.0 U Nitrite as N 0.0 U Nitrate as N 0.0 U Phosphorus Total Organic Carbon 0.0 I 0. I Color.0 ph at time of analysis. Alkalinity 0 Total issolved Solids 0 Total Suspended Solids.0 Chlorine, Total Residual.0 U Biochemical Oxygen emand.0 U General Chemistry - issolved ML il Fac mg/l 0// : mg/l 0// : mg/l 0// : mg/l 0// 0: 0// : mg/l 0// :.0.0 PCU 0// 0:0.0.0 SU 0// 0:0.0.0 mg/l 0// : 0 0 mg/l 0// 0:.0.0 mg/l 0// 0:.0.0 mg/l 0// 0:0.0.0 mg/l 0// 0: Orthophosphate 0.0 U mg/l 0// : ML il Fac 0 Method: SM B - Coliforms, Total (Membrane Filter) ML il Fac Coliform, Total CFU/00mL 0// : Method: SM - Coliforms, Fecal (Membrane Filter) ML il Fac Coliform, Fecal.0 U.0.0 CFU/00mL 0// : Client Sample I: SW-Inflow ate Collected: 0// 0:0 ate Received: 0// : Lab Sample I: 0-0- Method: 0C - Semivolatile Organic Compounds (GC/MS) ML il Fac,-ichlorobenzene. U.. ug/l 0/0/ : 0// :0 N-Nitrosodimethylamine. U.. ug/l 0/0/ : 0// :0 Phenol. U.. ug/l 0/0/ : 0// :0,-ichlorobenzene. U.. ug/l 0/0/ : 0// :0 Hexachloroethane 0. U. 0. ug/l 0/0/ : 0// :0 Bis(-chloroethyl)ether. U.. ug/l 0/0/ : 0// :0,-ichlorobenzene. U.. ug/l 0/0/ : 0// :0 N-Nitrosodi-n-propylamine. U.. ug/l 0/0/ : 0// :0 Nitrobenzene. U.. ug/l 0/0/ : 0// :0 Hexachlorobutadiene 0. U. 0. ug/l 0/0/ : 0// :0,,-Trichlorobenzene. U.. ug/l 0/0/ : 0// :0 Isophorone. U.. ug/l 0/0/ : 0// :0 Naphthalene. U.. ug/l 0/0/ : 0// :0 Page 0 of //0

22 Client Sample s TestAmerica Job I: 0-0- Client Sample I: SW-Inflow ate Collected: 0// 0:0 ate Received: 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- Bis(-chloroethoxy)methane. U.. ug/l 0/0/ : 0// :0 Hexachlorocyclopentadiene. U -Chloronaphthalene. U Acenaphthylene. U Acenaphthene. U imethyl phthalate. U,-initrotoluene 0.0 U Fluorene. U -Chlorophenyl phenyl ether. U,-initrotoluene 0. U iethyl phthalate. U N-Nitrosodiphenylamine. U Hexachlorobenzene. U -Bromophenyl phenyl ether. U Phenanthrene. U Anthracene 0. U i-n-butyl phthalate. U Fluoranthene. U Pyrene. U Butyl benzyl phthalate. U Bis(-ethylhexyl) phthalate. U Chrysene. U Benzo[a]anthracene. U,'-ichlorobenzidine. U i-n-octyl phthalate. U Benzo[b]fluoranthene. U Benzo[k]fluoranthene. U Benzo[a]pyrene 0. U Indeno[,,-cd]pyrene. U ibenz(a,h)anthracene 0. U Benzo[g,h,i]perylene. U -Chlorophenol.0 U -Nitrophenol. U,-imethylphenol. U,-ichlorophenol. U,,-Trichlorophenol. U -Chloro--methylphenol. U,-initrophenol.0 U,-initro--methylphenol. U Pentachlorophenol. U -Nitrophenol.0 U Benzyl alcohol. U -Methylphenol. U Benzoic acid U -Chloroaniline.0 U -Methylnaphthalene. U,,-Trichlorophenol.0 U -Nitroaniline. U -Nitroaniline. U ibenzofuran. U -Nitroaniline. U il Fac.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// : ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0. 0. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0. 0. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0. 0. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0. 0. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0..0 ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.0 ug/l 0/0/ : 0// :0. ug/l 0/0/ : 0// :0. ug/l 0/0/ : 0// :0.0 ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0 ug/l 0/0/ : 0// :0.0 ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0..0 ug/l 0/0/ : 0// :0. ug/l 0/0/ : 0// :0. ug/l 0/0/ : 0// :0.. ug/l 0/0/ : 0// :0. ug/l 0/0/ : 0// :0 0 Page of //0

23 Client Sample s TestAmerica Job I: 0-0- Client Sample I: SW-Inflow ate Collected: 0// 0:0 ate Received: 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- & Methylphenol. U.. ug/l 0/0/ : 0// :0 -Methylnaphthalene. U,'-oxybis[-chloropropane].0 U Surrogate %Recovery il Fac.. ug/l 0/0/ : 0// :0..0 ug/l 0/0/ : 0// :0 -Fluorophenol - 0/0/ : 0// :0 Nitrobenzene-d - 0 0/0/ : 0// :0 -Fluorobiphenyl - 0/0/ : 0// :0 Terphenyl-d 0 J - 0/0/ : 0// :0,,-Tribromophenol - 0/0/ : 0// :0 Phenol-d (Surr) - 0/0/ : 0// :0 Method: Anions, Ion Chromatography Sulfate mg/l 0// 0: Chloride Method: 00. Rev. - Metals (ICP) - Total Recoverable ML il Fac il Fac mg/l 0// 0: Chromium U mg/l 0// 0: 0// : Copper 0.00 U Iron 0. Lead U ML il Fac mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : 0 General Chemistry ML il Fac HEM (Oil and Grease). U.. mg/l 0// 0: 0// 0: Nitrate Nitrite as N 0.0 U mg/l 0// : Nitrite as N 0.0 U mg/l 0// : Nitrate as N 0.0 U mg/l 0// : Phosphorus 0. I mg/l 0// 0: 0// : Total Organic Carbon mg/l 0// :0 Color PCU 0// 0:0 ph at time of analysis..0.0 SU 0// 0:0 Alkalinity.0.0 mg/l 0// : Total issolved Solids mg/l 0// 0: Total Suspended Solids..0.0 mg/l 0// 0: Chlorine, Total Residual.0 U.0.0 mg/l 0// 0:0 Biochemical Oxygen emand mg/l 0// 0: General Chemistry - issolved ML il Fac Orthophosphate 0.0 U mg/l 0// : Method: SM B - Coliforms, Total (Membrane Filter) ML il Fac Coliform, Total CFU/00mL 0// : 00 Method: SM - Coliforms, Fecal (Membrane Filter) ML il Fac Coliform, Fecal.0.0 CFU/00mL 0// : Page of //0

24 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Outfall ate Collected: 0// :00 ate Received: 0// : Method: 0B - Volatile Organic Compounds (GC/MS) ML Lab Sample I: 0-0- Benzene 0.0 U ug/l 0// : Bromobenzene 0. U Chlorobromomethane 0. U ichlorobromomethane 0. U Bromoform 0. U Bromomethane. U n-butylbenzene 0. U sec-butylbenzene 0. U tert-butylbenzene 0. U Carbon tetrachloride 0. U Chlorobenzene 0. U Chloroethane. U Chloroform 0.0 U Chloromethane.0 U -Chlorotoluene 0. U -Chlorotoluene 0. U Chlorodibromomethane 0. U,-ibromo--Chloropropane. U Ethylene ibromide 0.0 U ibromomethane 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U ichlorodifluoromethane. U,-ichloroethane 0. U,-ichloroethane 0. U,-ichloroethene 0. U cis-,-ichloroethene 0. U trans-,-ichloroethene 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropene 0. U cis-,-ichloropropene 0. U trans-,-ichloropropene 0. U Ethylbenzene 0. U Hexachlorobutadiene 0.0 U Isopropylbenzene 0. U -Isopropyltoluene 0. U Methylene Chloride.0 U Naphthalene. U N-Propylbenzene 0. U Styrene 0. U,,,-Tetrachloroethane 0. U,,,-Tetrachloroethane 0. U Tetrachloroethene 0.0 U Toluene 0. U,,-Trichlorobenzene 0. U,,-Trichlorobenzene 0. U,,-Trichloroethane 0. U,,-Trichloroethane 0. U il Fac.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// : ug/l 0// :.0.0 ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : 0 Page of //0

25 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Outfall ate Collected: 0// :00 ate Received: 0// : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- Trichloroethene 0.0 U ug/l 0// : Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U Surrogate %Recovery il Fac.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : 0. ug/l 0// : 0. ug/l 0// : 0. ug/l 0// :.0.0 ug/l 0// : 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : Toluene-d (Surr) // : -Bromofluorobenzene 0-0 0// : ibromofluoromethane // : Method: 0C - Semivolatile Organic Compounds (GC/MS),-ichlorobenzene. U.. ug/l 0// 0:0 0// : N-Nitrosodimethylamine. U Phenol. U,-ichlorobenzene. U Hexachloroethane 0. U J Bis(-chloroethyl)ether. U,-ichlorobenzene. U N-Nitrosodi-n-propylamine. U Nitrobenzene. U Hexachlorobutadiene 0. U J,,-Trichlorobenzene. U Isophorone. U Naphthalene. U Bis(-chloroethoxy)methane. U Hexachlorocyclopentadiene. U -Chloronaphthalene. U Acenaphthylene. U Acenaphthene. U imethyl phthalate. U,-initrotoluene 0.0 U Fluorene. U -Chlorophenyl phenyl ether. U,-initrotoluene 0. U iethyl phthalate. U N-Nitrosodiphenylamine. U Hexachlorobenzene. U -Bromophenyl phenyl ether. U Phenanthrene. U Anthracene 0. U ML il Fac il Fac.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0.0 ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0. ug/l 0// 0:0 0// : 0 Page of //0

26 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Outfall ate Collected: 0// :00 ate Received: 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- i-n-butyl phthalate. U.. ug/l 0// 0:0 0// : Fluoranthene. U Pyrene. U Butyl benzyl phthalate. U Bis(-ethylhexyl) phthalate. U Chrysene. U Benzo[a]anthracene. U,'-ichlorobenzidine. U J i-n-octyl phthalate. U Benzo[b]fluoranthene. U Benzo[k]fluoranthene. U Benzo[a]pyrene 0. U Indeno[,,-cd]pyrene. U ibenz(a,h)anthracene 0. U Benzo[g,h,i]perylene. U -Chlorophenol.0 U -Nitrophenol. U,-imethylphenol. U,-ichlorophenol. U,,-Trichlorophenol. U -Chloro--methylphenol. U,-initrophenol.0 U,-initro--methylphenol. U Pentachlorophenol. U -Nitrophenol.0 U Benzyl alcohol. U -Methylphenol. U Benzoic acid U -Chloroaniline.0 U -Methylnaphthalene. U,,-Trichlorophenol.0 U -Nitroaniline. U -Nitroaniline. U ibenzofuran. U -Nitroaniline. U & Methylphenol. U -Methylnaphthalene. U,'-oxybis[-chloropropane].0 U il Fac.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. 0. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :..0 ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.0 ug/l 0// 0:0 0// :. ug/l 0// 0:0 0// :. ug/l 0// 0:0 0// :.0 ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// : ug/l 0// 0:0 0// :.0 ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :..0 ug/l 0// 0:0 0// :. ug/l 0// 0:0 0// :. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :.. ug/l 0// 0:0 0// :..0 ug/l 0// 0:0 0// : 0 Surrogate %Recovery -Fluorophenol - 0// 0:0 0// : Nitrobenzene-d 0-0 0// 0:0 0// : -Fluorobiphenyl - 0// 0:0 0// : Terphenyl-d J - 0// 0:0 0// :,,-Tribromophenol - 0// 0:0 0// : Phenol-d (Surr) - 0// 0:0 0// : il Fac Method: Anions, Ion Chromatography ML il Fac Sulfate 0. I mg/l 0// 0: Chloride mg/l 0// 0: Page of //0

27 Client Sample s TestAmerica Job I: 0-0- Client Sample I: W-Outfall ate Collected: 0// :00 ate Received: 0// : Method: 00. Rev. - Metals (ICP) - Total Recoverable ML Lab Sample I: 0-0- Chromium U mg/l 0// 0: 0// : Copper 0.00 U Iron. Lead U General Chemistry il Fac mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : HEM (Oil and Grease). U.. mg/l 0// 0: 0// 0: Nitrate Nitrite as N 0.0 U Nitrite as N 0.0 U Nitrate as N 0.0 U Phosphorus 0. Total Organic Carbon. Color 0 ph at time of analysis. Alkalinity 0 Total issolved Solids 0 Total Suspended Solids. Chlorine, Total Residual.0 U Biochemical Oxygen emand.0 U General Chemistry - issolved ML il Fac mg/l 0// : mg/l 0// : mg/l 0// : mg/l 0// 0: 0// : mg/l 0// : 0 0 PCU 0// 0:0.0.0 SU 0// 0:0.0.0 mg/l 0// : 0 0 mg/l 0// 0:.0.0 mg/l 0// 0:.0.0 mg/l 0// 0:0.0.0 mg/l 0// 0: Orthophosphate 0.0 U mg/l 0// : ML il Fac 0 Method: SM B - Coliforms, Total (Membrane Filter) ML il Fac Coliform, Total CFU/00mL 0// : Method: SM - Coliforms, Fecal (Membrane Filter) ML il Fac Coliform, Fecal.0.0 CFU/00mL 0// : Client Sample I: SW-Outfall ate Collected: 0// :0 ate Received: 0// : Lab Sample I: 0-0- Method: 0C - Semivolatile Organic Compounds (GC/MS) ML il Fac,-ichlorobenzene. U. ug/l 0/0/ : 0// : N-Nitrosodimethylamine. U. ug/l 0/0/ : 0// : Phenol. U.. ug/l 0/0/ : 0// :,-ichlorobenzene. U. ug/l 0/0/ : 0// : Hexachloroethane 0. U 0. ug/l 0/0/ : 0// : Bis(-chloroethyl)ether. U. ug/l 0/0/ : 0// :,-ichlorobenzene. U. ug/l 0/0/ : 0// : N-Nitrosodi-n-propylamine.0 U.0 ug/l 0/0/ : 0// : Nitrobenzene.0 U.0 ug/l 0/0/ : 0// : Hexachlorobutadiene. U. ug/l 0/0/ : 0// :,,-Trichlorobenzene. U. ug/l 0/0/ : 0// : Isophorone. U. ug/l 0/0/ : 0// : Naphthalene. U. ug/l 0/0/ : 0// : Page of //0

28 Client Sample s TestAmerica Job I: 0-0- Client Sample I: SW-Outfall ate Collected: 0// :0 ate Received: 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- Bis(-chloroethoxy)methane. U. ug/l 0/0/ : 0// : Hexachlorocyclopentadiene. U -Chloronaphthalene. U Acenaphthylene. U Acenaphthene. U imethyl phthalate. U,-initrotoluene 0. U Fluorene. U -Chlorophenyl phenyl ether. U,-initrotoluene 0. U iethyl phthalate. U N-Nitrosodiphenylamine. U Hexachlorobenzene. U -Bromophenyl phenyl ether. U Phenanthrene. U Anthracene. U i-n-butyl phthalate. U Fluoranthene. U Pyrene. U Butyl benzyl phthalate. U Bis(-ethylhexyl) phthalate. U Chrysene. U Benzo[a]anthracene. U,'-ichlorobenzidine. U i-n-octyl phthalate. U Benzo[b]fluoranthene. U Benzo[k]fluoranthene. U Benzo[a]pyrene.0 U Indeno[,,-cd]pyrene. U ibenz(a,h)anthracene. U Benzo[g,h,i]perylene. U -Chlorophenol. U -Nitrophenol. U,-imethylphenol. U,-ichlorophenol. U,,-Trichlorophenol.0 U -Chloro--methylphenol. U,-initrophenol. U,-initro--methylphenol. U Pentachlorophenol. U -Nitrophenol. U Benzyl alcohol. U -Methylphenol. U Benzoic acid U -Chloroaniline. U -Methylnaphthalene. U,,-Trichlorophenol. U -Nitroaniline. U -Nitroaniline. U ibenzofuran. U -Nitroaniline. U il Fac. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :..0 ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :.0 ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : 0 Page of //0

29 Client Sample s TestAmerica Job I: 0-0- Client Sample I: SW-Outfall ate Collected: 0// :0 ate Received: 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- & Methylphenol. U. ug/l 0/0/ : 0// : -Methylnaphthalene. U,'-oxybis[-chloropropane]. U Surrogate %Recovery il Fac. ug/l 0/0/ : 0// :. ug/l 0/0/ : 0// : -Fluorophenol - 0/0/ : 0// : Nitrobenzene-d - 0 0/0/ : 0// : -Fluorobiphenyl - 0/0/ : 0// : Terphenyl-d 0 J - 0/0/ : 0// :,,-Tribromophenol - 0/0/ : 0// : Phenol-d (Surr) - 0/0/ : 0// : Method: Anions, Ion Chromatography Sulfate mg/l 0// :0 Chloride Method: 00. Rev. - Metals (ICP) - Total Recoverable ML il Fac il Fac mg/l 0// :0 Chromium U mg/l 0// 0: 0// : Copper 0.00 U Iron 0. Lead U ML il Fac mg/l 0// 0: 0// : mg/l 0// 0: 0// : mg/l 0// 0: 0// : 0 General Chemistry ML il Fac HEM (Oil and Grease). U.. mg/l 0// 0: 0// 0: Nitrate Nitrite as N 0.0 U mg/l 0// : Nitrite as N 0.0 U mg/l 0// : Nitrate as N 0.0 U mg/l 0// : Phosphorus 0. I mg/l 0// 0: 0// : Total Organic Carbon mg/l 0// : Color PCU 0// 0:0 ph at time of analysis..0.0 SU 0// 0:0 Alkalinity.0.0 mg/l 0// : Total issolved Solids.0.0 mg/l 0// 0: Total Suspended Solids mg/l 0// 0: Chlorine, Total Residual.0 U.0.0 mg/l 0// 0:0 Biochemical Oxygen emand.0 U.0.0 mg/l 0// 0: General Chemistry - issolved ML il Fac Orthophosphate 0.0 U mg/l 0// : Method: SM B - Coliforms, Total (Membrane Filter) ML il Fac Coliform, Total CFU/00mL 0// : 00 Method: SM - Coliforms, Fecal (Membrane Filter) ML il Fac Coliform, Fecal CFU/00mL 0// : Page of //0

30 Client Sample s TestAmerica Job I: 0-0- Client Sample I: Trip Blank ate Collected: 0// 00:00 ate Received: 0// : Method: 0B - Volatile Organic Compounds (GC/MS) ML Lab Sample I: 0-0- Benzene 0.0 U ug/l 0// : Bromobenzene 0. U Chlorobromomethane 0. U ichlorobromomethane 0. U Bromoform 0. U Bromomethane. U n-butylbenzene 0. U sec-butylbenzene 0. U tert-butylbenzene 0. U Carbon tetrachloride 0. U Chlorobenzene 0. U Chloroethane. U Chloroform 0.0 U Chloromethane.0 U -Chlorotoluene 0. U -Chlorotoluene 0. U Chlorodibromomethane 0. U,-ibromo--Chloropropane. U Ethylene ibromide 0.0 U ibromomethane 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U ichlorodifluoromethane. U,-ichloroethane 0. U,-ichloroethane 0. U,-ichloroethene 0. U cis-,-ichloroethene 0. U trans-,-ichloroethene 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropene 0. U cis-,-ichloropropene 0. U trans-,-ichloropropene 0. U Ethylbenzene 0. U Hexachlorobutadiene 0.0 U Isopropylbenzene 0. U -Isopropyltoluene 0. U Methylene Chloride.0 U Naphthalene. U N-Propylbenzene 0. U Styrene 0. U,,,-Tetrachloroethane 0. U,,,-Tetrachloroethane 0. U Tetrachloroethene 0.0 U Toluene 0. U,,-Trichlorobenzene 0. U,,-Trichlorobenzene 0. U,,-Trichloroethane 0. U,,-Trichloroethane 0. U il Fac.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// : ug/l 0// :.0.0 ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : 0 Page of //0

31 Client Sample s TestAmerica Job I: 0-0- Client Sample I: Trip Blank ate Collected: 0// 00:00 ate Received: 0// : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-0- Trichloroethene 0.0 U ug/l 0// : Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U Surrogate %Recovery il Fac.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : 0. ug/l 0// : 0. ug/l 0// : 0. ug/l 0// :.0.0 ug/l 0// : 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : Toluene-d (Surr) // : -Bromofluorobenzene 0-0 0// : ibromofluoromethane // : il Fac 0 Page 0 of //0

32 Surrogate Summary TestAmerica Job I: 0-0- Method: 0B - Volatile Organic Compounds (GC/MS) Prep Type: Percent Surrogate Recovery (Acceptance ) TOL BFB BFM Lab Sample I Client Sample I (0-0) (0-0) (0-0) 0-0- W-Inflow W-Outfall Trip Blank 0 00 LCS 0-0/ Lab Control Sample MB 0-0/ Method Blank 0 0 Surrogate Legend TOL = Toluene-d (Surr) BFB = -Bromofluorobenzene BFM = ibromofluoromethane Method: 0B - Volatile Organic Compounds (GC/MS) Prep Type: TCLP Percent Surrogate Recovery (Acceptance ) TOL BFB BFM Lab Sample I Client Sample I (0-0) (0-0) (0-0) 0-0-B- U uplicate B- MS Matrix Spike 00 Surrogate Legend TOL = Toluene-d (Surr) BFB = -Bromofluorobenzene BFM = ibromofluoromethane 0 Method: 0C - Semivolatile Organic Compounds (GC/MS) Prep Type: FP NBZ FBP TPH TBP PHL Lab Sample I Client Sample I (-) (-0) (-) (-) (-) (-) 0-0- W-Inflow 0-0- SW-Inflow 0-0- W-Outfall 0-0- SW-Outfall A MS 0-0-E--A U 0-0-F--A U 0-0-F--A MS LCS 0-0/-A LCS 0-0/-A MB 0-0/-A MB 0-0/-A Surrogate Legend FP = -Fluorophenol NBZ = Nitrobenzene-d FBP = -Fluorobiphenyl TPH = Terphenyl-d TBP =,,-Tribromophenol PHL = Phenol-d (Surr) Matrix Spike uplicate uplicate Matrix Spike Lab Control Sample Lab Control Sample Method Blank Method Blank Percent Surrogate Recovery (Acceptance ) 0 0 J 0 J 0 J 0 0 J 0 0 Page of //0

33 Method: 0B - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 0-0/ Analysis Batch: 0 MB MB QC Sample s ML TestAmerica Job I: 0-0- Client Sample I: Method Blank Prep Type: Benzene 0.0 U ug/l 0// 0: Bromobenzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane n-butylbenzene sec-butylbenzene tert-butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane -Chlorotoluene -Chlorotoluene Chlorodibromomethane,-ibromo--Chloropropane Ethylene ibromide ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene cis-,-ichloroethene trans-,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene cis-,-ichloropropene trans-,-ichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene -Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene,,,-Tetrachloroethane,,,-Tetrachloroethane Tetrachloroethene Toluene,,-Trichlorobenzene,,-Trichlorobenzene il Fac 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0.0 U ug/l 0// 0:.0 U.0.0 ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:.0 U.0.0 ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0 Page of //0

34 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MB 0-0/ Analysis Batch: 0 MB MB ML TestAmerica Job I: 0-0- Client Sample I: Method Blank Prep Type:,,-Trichloroethane 0. U.0 0. ug/l 0// 0:,,-Trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride o-xylene Acetone -Butanone (MEK) -Methyl--pentanone (MIBK) Carbon disulfide -Hexanone Methyl tert-butyl ether m-xylene & p-xylene Surrogate il Fac 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0.0 U ug/l 0// 0:. U 0. ug/l 0// 0:. U 0. ug/l 0// 0:. U 0. ug/l 0// 0:.0 U.0.0 ug/l 0// 0:. U 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: MB %Recovery MB Toluene-d (Surr) // 0: -Bromofluorobenzene 0-0 0// 0: ibromofluoromethane // 0: il Fac 0 Lab Sample I: LCS 0-0/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Spike LCS LCS Added %Rec Benzene ug/l 0 - Bromobenzene 0.0. ug/l 0-0 Chlorobromomethane ug/l ichlorobromomethane ug/l 0-0 Bromoform 0.0. ug/l - 0 Bromomethane 0.0. ug/l - 0 n-butylbenzene 0.0. ug/l - sec-butylbenzene ug/l 0 - tert-butylbenzene 0.0. ug/l - 0 Carbon tetrachloride 0.0. ug/l - Chlorobenzene 0.0. ug/l 0-0 Chloroethane ug/l 00-0 Chloroform 0.0. ug/l - 0 Chloromethane 0.0. ug/l - 0 -Chlorotoluene 0.0. ug/l 0-0 -Chlorotoluene 0.0. ug/l 0-0 Chlorodibromomethane 0.0. ug/l 0-0,-ibromo--Chloropropane ug/l 0-0 Ethylene ibromide 0.0. ug/l - 0 ibromomethane 0.0. ug/l 0 0-0,-ichlorobenzene ug/l 0-0,-ichlorobenzene 0.0. ug/l 0-0 Page of //0

35 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 0-0/ Analysis Batch: 0 Spike Added TestAmerica Job I: 0-0- Client Sample I: Lab Control Sample Prep Type:,-ichlorobenzene 0.0. ug/l 0-0 LCS LCS %Rec ichlorodifluoromethane 0.0. ug/l 0 -,-ichloroethane 0.0. ug/l - 0,-ichloroethane 0.0. ug/l 0-0,-ichloroethene 0.0. ug/l - 0 cis-,-ichloroethene 0.0. ug/l - 0 trans-,-ichloroethene 0.0. ug/l -,-ichloropropane 0.0. ug/l 0-0,-ichloropropane 0.0. ug/l 0-0,-ichloropropane 0.0. ug/l -,-ichloropropene 0.0. ug/l - cis-,-ichloropropene 0.0. ug/l 0-0 trans-,-ichloropropene ug/l 0-0 Ethylbenzene 0.0. ug/l 0-0 Hexachlorobutadiene 0.0. ug/l - Isopropylbenzene 0.0. ug/l - 0 -Isopropyltoluene ug/l - Methylene Chloride 0.0. ug/l - 0 Naphthalene 0.0. ug/l N-Propylbenzene 0.0. ug/l - 0 Styrene 0.0. ug/l -,,,-Tetrachloroethane 0.0. ug/l 0-0,,,-Tetrachloroethane ug/l 0-0 Tetrachloroethene 0.0. ug/l 0 - Toluene ug/l 0 0 -,,-Trichlorobenzene 0.0. ug/l -,,-Trichlorobenzene ug/l 0-0,,-Trichloroethane 0.0. ug/l -,,-Trichloroethane 0.0. ug/l 0-0 Trichloroethene 0.0. ug/l - Trichlorofluoromethane 0.0. ug/l -,,-Trichloropropane 0.0. ug/l - 0,,-Trimethylbenzene 0.0. ug/l 0 -,,-Trimethylbenzene 0.0. ug/l - Vinyl chloride 0.0. ug/l 0 - o-xylene 0.0. ug/l - 0 Acetone 0.0. ug/l - -Butanone (MEK) 0.0. ug/l - 0 -Methyl--pentanone (MIBK) 0.0. ug/l - Carbon disulfide 0.0. ug/l Hexanone 0.0. ug/l 0 - Methyl tert-butyl ether 0.0. ug/l Surrogate LCS %Recovery LCS Toluene-d (Surr) Bromofluorobenzene 0-0 ibromofluoromethane Page of //0

36 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: 0-0-B- MS Analysis Batch: 0 Sample Sample Spike Added TestAmerica Job I: 0-0- Benzene.0 U 00 ug/l - MS MS %Rec Bromobenzene. U 00 0 ug/l Chlorobromomethane. U 00 ug/l ichlorobromomethane. U 00 ug/l Bromoform. U 00 ug/l - 0 Bromomethane U 00 ug/l - 0 n-butylbenzene. U 00 ug/l - sec-butylbenzene. U 00 ug/l - tert-butylbenzene. U 00 ug/l - 0 Carbon tetrachloride. U 00 ug/l - Chlorobenzene. U 00 0 ug/l Chloroethane U 00 0 ug/l 0-0 Chloroform.0 U 00 0 ug/l 0-0 Chloromethane 0 U 00 0 ug/l 0-0 -Chlorotoluene. U 00 ug/l 0-0 -Chlorotoluene. U 00 0 ug/l Chlorodibromomethane. U 00 0 ug/l 0 0-0,-ibromo--Chloropropane U 00 ug/l 0-0 Ethylene ibromide.0 U 00 ug/l 0-0 ibromomethane. U 00 ug/l 0-0,-ichlorobenzene. U 00 0 ug/l 0 0-0,-ichlorobenzene. U 00 ug/l 0 0-0,-ichlorobenzene. U 00 0 ug/l ichlorodifluoromethane U 00 ug/l -,-ichloroethane. U 00 ug/l - 0,-ichloroethane. U 00 0 ug/l 0 0-0,-ichloroethene. U 00 0 ug/l 0-0 cis-,-ichloroethene. U 00 ug/l - 0 trans-,-ichloroethene. U 00 ug/l -,-ichloropropane. U 00 ug/l 0-0,-ichloropropane. U 00 0 ug/l 0 0-0,-ichloropropane. U 00 ug/l -,-ichloropropene. U 00 ug/l - cis-,-ichloropropene. U 00 ug/l 0-0 trans-,-ichloropropene. U 00 ug/l - 0 Ethylbenzene. U 00 0 ug/l Hexachlorobutadiene.0 U 00 ug/l - Isopropylbenzene. U 00 ug/l - 0 -Isopropyltoluene. U 00 0 ug/l 0 - Methylene Chloride 0 U 00 ug/l - 0 Naphthalene U 00 ug/l N-Propylbenzene. U 00 ug/l - 0 Styrene. U 00 0 ug/l 0 -,,,-Tetrachloroethane. U 00 0 ug/l 0 0-0,,,-Tetrachloroethane. U 00 0 ug/l Tetrachloroethene.0 U 00 0 ug/l 0 - Toluene. U 00 ug/l 0 -,,-Trichlorobenzene. U 00 ug/l -,,-Trichlorobenzene. U 00 ug/l 0-0 Client Sample I: Matrix Spike Prep Type: TCLP 0 Page of //0

37 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: 0-0-B- MS Analysis Batch: 0 Sample Sample Spike Added TestAmerica Job I: 0-0-,,-Trichloroethane. U 00 ug/l - MS MS %Rec,,-Trichloroethane. U 00 0 ug/l Trichloroethene.0 U 00 0 ug/l 00 - Trichlorofluoromethane U 00 ug/l 0 -,,-Trichloropropane. U 00 0 ug/l 0-0,,-Trimethylbenzene. U 00 0 ug/l 0 0 -,,-Trimethylbenzene. U 00 ug/l - Vinyl chloride.0 U 00 ug/l 0 - o-xylene.0 U 00 ug/l 00-0 Acetone U 00 ug/l - -Butanone (MEK) U 00 ug/l - 0 -Methyl--pentanone (MIBK) U 00 0 ug/l 0 - Carbon disulfide 0 U 00 ug/l 0-0 -Hexanone U 00 ug/l 0 - Methyl tert-butyl ether. U 00 ug/l - 0 Surrogate Toluene-d (Surr) 0-0 MS %Recovery MS -Bromofluorobenzene 0-0 ibromofluoromethane Client Sample I: Matrix Spike Prep Type: TCLP 0 Lab Sample I: 0-0-B- U Client Sample I: uplicate Prep Type: TCLP Analysis Batch: 0 Sample Sample U U RP RP Limit Benzene.0 U.0 U ug/l NC 0 Bromobenzene. U. U ug/l NC 0 Chlorobromomethane. U. U ug/l NC 0 ichlorobromomethane. U. U ug/l NC 0 Bromoform. U. U ug/l NC 0 Bromomethane U U ug/l NC 0 n-butylbenzene. U. U ug/l NC 0 sec-butylbenzene. U. U ug/l NC 0 tert-butylbenzene. U. U ug/l NC 0 Carbon tetrachloride. U. U ug/l NC 0 Chlorobenzene. U. U ug/l NC 0 Chloroethane U U ug/l NC 0 Chloroform.0 U.0 U ug/l NC 0 Chloromethane 0 U 0 U ug/l NC 0 -Chlorotoluene. U. U ug/l NC 0 -Chlorotoluene. U. U ug/l NC 0 Chlorodibromomethane. U. U ug/l NC 0,-ibromo--Chloropropane U U ug/l NC 0 Ethylene ibromide.0 U.0 U ug/l NC 0 ibromomethane. U. U ug/l NC 0,-ichlorobenzene. U. U ug/l NC 0,-ichlorobenzene. U. U ug/l NC 0,-ichlorobenzene. U. U ug/l NC 0 Page of //0

38 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: 0-0-B- U Analysis Batch: 0 Sample Sample TestAmerica Job I: 0-0- Client Sample I: uplicate Prep Type: TCLP ichlorodifluoromethane U U ug/l NC 0 U U,-ichloroethane. U. U ug/l NC 0,-ichloroethane. U. U ug/l NC 0,-ichloroethene. U. U ug/l NC 0 cis-,-ichloroethene. U. U ug/l NC 0 trans-,-ichloroethene. U. U ug/l NC 0,-ichloropropane. U. U ug/l NC 0,-ichloropropane. U. U ug/l NC 0,-ichloropropane. U. U ug/l NC 0,-ichloropropene. U. U ug/l NC 0 cis-,-ichloropropene. U. U ug/l NC 0 trans-,-ichloropropene. U. U ug/l NC 0 Ethylbenzene. U. U ug/l NC 0 Hexachlorobutadiene.0 U.0 U ug/l NC 0 Isopropylbenzene. U. U ug/l NC 0 -Isopropyltoluene. U. U ug/l NC 0 Methylene Chloride 0 U 0 U ug/l NC 0 Naphthalene U U ug/l NC 0 N-Propylbenzene. U. U ug/l NC 0 Styrene. U. U ug/l NC 0,,,-Tetrachloroethane. U. U ug/l NC 0,,,-Tetrachloroethane. U. U ug/l NC 0 Tetrachloroethene.0 U.0 U ug/l NC 0 Toluene. U. U ug/l NC 0,,-Trichlorobenzene. U. U ug/l NC 0,,-Trichlorobenzene. U. U ug/l NC 0,,-Trichloroethane. U. U ug/l NC 0,,-Trichloroethane. U. U ug/l NC 0 Trichloroethene.0 U.0 U ug/l NC 0 Trichlorofluoromethane U U ug/l NC 0,,-Trichloropropane. U. U ug/l NC 0,,-Trimethylbenzene. U. U ug/l NC 0,,-Trimethylbenzene. U. U ug/l NC 0 Vinyl chloride.0 U.0 U ug/l NC 0 o-xylene.0 U.0 U ug/l NC 0 Acetone U U ug/l NC 0 -Butanone (MEK) U U ug/l NC 0 -Methyl--pentanone (MIBK) U U ug/l NC 0 Carbon disulfide 0 U 0 U ug/l NC 0 -Hexanone U U ug/l NC 0 Methyl tert-butyl ether. U. U ug/l NC 0 m-xylene & p-xylene.0 U.0 U ug/l NC 0 RP RP Limit 0 Surrogate Toluene-d (Surr) U %Recovery U -Bromofluorobenzene 0-0 ibromofluoromethane Page of //0

39 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) TestAmerica Job I: 0-0- Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: 0 MB MB,-ichlorobenzene. U 0. ug/l 0// 0:0 0// : N-Nitrosodimethylamine Phenol,-ichlorobenzene Hexachloroethane Bis(-chloroethyl)ether,-ichlorobenzene N-Nitrosodi-n-propylamine Nitrobenzene Hexachlorobutadiene,,-Trichlorobenzene Isophorone Naphthalene Bis(-chloroethoxy)methane Hexachlorocyclopentadiene -Chloronaphthalene Acenaphthylene Acenaphthene imethyl phthalate,-initrotoluene Fluorene -Chlorophenyl phenyl ether,-initrotoluene iethyl phthalate N-Nitrosodiphenylamine Hexachlorobenzene -Bromophenyl phenyl ether Phenanthrene Anthracene i-n-butyl phthalate Fluoranthene Pyrene Butyl benzyl phthalate Bis(-ethylhexyl) phthalate Chrysene Benzo[a]anthracene,'-ichlorobenzidine i-n-octyl phthalate Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[a]pyrene Indeno[,,-cd]pyrene ibenz(a,h)anthracene Benzo[g,h,i]perylene -Chlorophenol -Nitrophenol,-imethylphenol,-ichlorophenol,,-Trichlorophenol ML il Fac. U 0. ug/l 0// 0:0 0// :. U.0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : 0. U 0 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :.0 U 0.0 ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :.0 U 0.0 ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : 0. U 0 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : 0. U 0 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U.0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :.0 U 0.0 ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U.0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : 0. U.0 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :.0 U 0.0 ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : 0 Page of //0

40 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: 0 MB MB -Chloro--methylphenol. U 0. ug/l 0// 0:0 0// :,-initrophenol,-initro--methylphenol Pentachlorophenol -Nitrophenol Benzyl alcohol -Methylphenol Benzoic acid -Chloroaniline -Methylnaphthalene,,-Trichlorophenol -Nitroaniline -Nitroaniline ibenzofuran -Nitroaniline & Methylphenol -Methylnaphthalene,'-oxybis[-chloropropane] Surrogate ML il Fac. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : U 0 ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// :. U 0. ug/l 0// 0:0 0// : MB %Recovery MB -Fluorophenol 0-0// 0:0 0// : Nitrobenzene-d - 0 0// 0:0 0// : -Fluorobiphenyl - 0// 0:0 0// : Terphenyl-d - 0// 0:0 0// :,,-Tribromophenol - 0// 0:0 0// : Phenol-d (Surr) - 0// 0:0 0// : il Fac 0 Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: 0 Spike LCS LCS Added %Rec,-ichlorobenzene 00. ug/l - 0 N-Nitrosodimethylamine 00. ug/l - 0 Phenol ug/l 0-0,-ichlorobenzene 00.0 ug/l - 0 Hexachloroethane 00. J ug/l - 0 Bis(-chloroethyl)ether 00. ug/l -,-ichlorobenzene 00. ug/l - 0 N-Nitrosodi-n-propylamine 00. ug/l - 0 Nitrobenzene 00. ug/l - 0 Hexachlorobutadiene 00. J ug/l - 0,,-Trichlorobenzene 00.0 ug/l - 0 Isophorone 00. ug/l - 0 Naphthalene 00. ug/l 0-0 Bis(-chloroethoxy)methane 00. ug/l - Hexachlorocyclopentadiene 00. ug/l 0-0 -Chloronaphthalene ug/l 0-0 Acenaphthylene 00. ug/l - 0 Page of //0

41 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: 0 Spike LCS LCS Added %Rec Acenaphthene 00.0 ug/l - 0 imethyl phthalate 00. ug/l -,-initrotoluene 00. ug/l - Fluorene 00. ug/l - 0 -Chlorophenyl phenyl ether 00. ug/l -,-initrotoluene 00. ug/l - iethyl phthalate 00. ug/l 0 - N-Nitrosodiphenylamine 00. ug/l - Hexachlorobenzene 00. ug/l - -Bromophenyl phenyl ether 00. ug/l - 0 Phenanthrene 00. ug/l - 0 Anthracene 00. ug/l - i-n-butyl phthalate 00. ug/l 0-0 Fluoranthene 00. ug/l - 0 Pyrene 00. ug/l - 0 Butyl benzyl phthalate 00. ug/l - Bis(-ethylhexyl) phthalate 00. ug/l - Chrysene 00. ug/l Benzo[a]anthracene 00. ug/l - 0,'-ichlorobenzidine 00. I J ug/l 0-0 i-n-octyl phthalate 00. ug/l - Benzo[b]fluoranthene 00. ug/l 0-0 Benzo[k]fluoranthene ug/l 0-0 Benzo[a]pyrene 00. ug/l - 0 Indeno[,,-cd]pyrene ug/l - 0 ibenz(a,h)anthracene 00. ug/l - 0 Benzo[g,h,i]perylene 00. ug/l - 0 -Chlorophenol 00. ug/l 0-0 -Nitrophenol 00. ug/l -,-imethylphenol 00. ug/l - 0,-ichlorophenol 00. ug/l 0 -,,-Trichlorophenol 00. ug/l - -Chloro--methylphenol 00. ug/l - 0,-initrophenol 00. ug/l 0-0,-initro--methylphenol 00. ug/l 0 - Pentachlorophenol 00. ug/l 0 - -Nitrophenol 00. ug/l - 0 Benzyl alcohol 00. ug/l - 0 -Methylphenol 00. ug/l Benzoic acid 00. ug/l 0-0 -Chloroaniline 00. I ug/l 0-0 -Methylnaphthalene 00. ug/l - 0,,-Trichlorophenol 00. ug/l - 0 -Nitroaniline 00. ug/l - 0 -Nitroaniline 00. I ug/l 0-0 ibenzofuran 00. ug/l - -Nitroaniline 00. ug/l - 0 & Methylphenol 00 ug/l - 0 -Methylnaphthalene 00. ug/l 0 -,'-oxybis[-chloropropane] 00. ug/l Page 0 of //0

42 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: 0 Surrogate LCS %Recovery LCS -Fluorophenol - Nitrobenzene-d 0-0 -Fluorobiphenyl - Terphenyl-d -,,-Tribromophenol - Phenol-d (Surr) - Lab Sample I: 0-0-F--A MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec,-ichlorobenzene. U.. ug/l - 0 N-Nitrosodimethylamine. U.. ug/l - 0 Phenol. U.. ug/l - 0,-ichlorobenzene. U J.. J ug/l - 0 Hexachloroethane 0. U J.. J ug/l - 0 Bis(-chloroethyl)ether. U.. ug/l -,-ichlorobenzene. U J.. J ug/l - 0 N-Nitrosodi-n-propylamine. U J.. J ug/l - 0 Nitrobenzene. U J.. J ug/l 0-0 Hexachlorobutadiene 0. U J.. ug/l - 0,,-Trichlorobenzene. U.. ug/l - 0 Isophorone. U J.. J ug/l - 0 Naphthalene. U J.. J ug/l - 0 Bis(-chloroethoxy)methane. U J.. J ug/l - Hexachlorocyclopentadiene. U.. ug/l 0-0 -Chloronaphthalene. U.. ug/l - 0 Acenaphthylene. U.. ug/l - 0 Acenaphthene. U.. ug/l 0-0 imethyl phthalate. U J.. J ug/l -,-initrotoluene 0. U J.. J ug/l - Fluorene. U.. ug/l - 0 -Chlorophenyl phenyl ether. U.. ug/l -,-initrotoluene 0. U J.. J ug/l - iethyl phthalate. U J.. J ug/l N-Nitrosodiphenylamine. U.. ug/l - Hexachlorobenzene. U.. ug/l - -Bromophenyl phenyl ether. U.. ug/l - 0 Phenanthrene. U.. ug/l - 0 Anthracene 0. U.. ug/l - i-n-butyl phthalate. U.. ug/l 0-0 Fluoranthene. U.. ug/l - 0 Pyrene. U.. ug/l - 0 Butyl benzyl phthalate. U.. ug/l - Bis(-ethylhexyl) phthalate. U.. ug/l - Chrysene. U.. ug/l 0-0 Benzo[a]anthracene. U.. ug/l - 0,'-ichlorobenzidine. U J.. I ug/l Page of //0

43 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: 0-0-F--A MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec i-n-octyl phthalate. U. 0. ug/l - Benzo[b]fluoranthene. U.. ug/l 0-0 Benzo[k]fluoranthene. U.. ug/l - 0 Benzo[a]pyrene 0. U..0 ug/l - 0 Indeno[,,-cd]pyrene. U.. ug/l - 0 ibenz(a,h)anthracene 0. U..0 ug/l - 0 Benzo[g,h,i]perylene. U.. ug/l - 0 -Chlorophenol.0 U J.. J ug/l 0-0 -Nitrophenol. U J.. J ug/l -,-imethylphenol. U J. 0. J ug/l - 0,-ichlorophenol. U J.. J ug/l 0 -,,-Trichlorophenol. U J.. J ug/l - -Chloro--methylphenol. U J.. J ug/l - 0,-initrophenol.0 U.. I ug/l 0-0,-initro--methylphenol. U.. I ug/l - Pentachlorophenol. U.. ug/l Nitrophenol.0 U..0 I ug/l - 0 Benzyl alcohol. U.. ug/l - 0 -Methylphenol. U J.. J ug/l 0-0 Benzoic acid U.. I ug/l 0-0 -Chloroaniline.0 U.. I ug/l 0-0 -Methylnaphthalene. U.. ug/l - 0,,-Trichlorophenol.0 U J.. J ug/l 0-0 -Nitroaniline. U J.. I J ug/l - 0 -Nitroaniline. U.. I ug/l - 0 ibenzofuran. U..0 ug/l - -Nitroaniline. U.. I ug/l - 0 & Methylphenol. U J. J ug/l - 0 -Methylnaphthalene. U.. ug/l 0 -,'-oxybis[-chloropropane].0 U.. ug/l Surrogate -Fluorophenol - MS %Recovery MS Nitrobenzene-d - 0 -Fluorobiphenyl - Terphenyl-d J -,,-Tribromophenol - Phenol-d (Surr) - Lab Sample I: 0-0-E--A U Client Sample I: uplicate Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample U U RP,-ichlorobenzene. U. U ug/l NC N-Nitrosodimethylamine. U. U ug/l NC Phenol. U. U ug/l NC,-ichlorobenzene. U. U ug/l NC Hexachloroethane 0. U J 0. U J ug/l NC RP Limit Page of //0

44 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: 0-0-E--A U Client Sample I: uplicate Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample U U RP Bis(-chloroethyl)ether. U. U ug/l NC,-ichlorobenzene. U. U ug/l NC N-Nitrosodi-n-propylamine. U. U ug/l NC Nitrobenzene. U. U ug/l NC Hexachlorobutadiene 0. U J 0. U J ug/l NC,,-Trichlorobenzene. U. U ug/l NC Isophorone. U. U ug/l NC Naphthalene. U. U ug/l NC Bis(-chloroethoxy)methane.0 U. U ug/l NC Hexachlorocyclopentadiene. U. U ug/l NC -Chloronaphthalene. U. U ug/l NC Acenaphthylene. U. U ug/l NC Acenaphthene. U. U ug/l NC imethyl phthalate. U. U ug/l NC,-initrotoluene 0. U 0.0 U ug/l NC Fluorene. U. U ug/l NC -Chlorophenyl phenyl ether. U. U ug/l NC,-initrotoluene 0. U 0. U ug/l NC iethyl phthalate. U. U ug/l NC N-Nitrosodiphenylamine. U. U ug/l NC Hexachlorobenzene. U. U ug/l NC -Bromophenyl phenyl ether. U. U ug/l NC Phenanthrene. U. U ug/l NC Anthracene 0. U 0. U ug/l NC i-n-butyl phthalate. U. U ug/l NC Fluoranthene. U. U ug/l NC Pyrene. U. U ug/l NC Butyl benzyl phthalate. U. U ug/l NC Bis(-ethylhexyl) phthalate. U. U ug/l NC Chrysene. U. U ug/l NC Benzo[a]anthracene. U. U ug/l NC,'-ichlorobenzidine. U J. U J ug/l NC i-n-octyl phthalate. U. U ug/l NC Benzo[b]fluoranthene. U. U ug/l NC Benzo[k]fluoranthene. U. U ug/l NC Benzo[a]pyrene 0. U 0. U ug/l NC Indeno[,,-cd]pyrene. U. U ug/l NC ibenz(a,h)anthracene 0. U 0. U ug/l NC Benzo[g,h,i]perylene. U. U ug/l NC -Chlorophenol. U.0 U ug/l NC -Nitrophenol. U. U ug/l NC,-imethylphenol. U. U ug/l NC,-ichlorophenol. U. U ug/l NC,,-Trichlorophenol. U. U ug/l NC -Chloro--methylphenol. U. U ug/l NC,-initrophenol. U.0 U ug/l NC,-initro--methylphenol. U. U ug/l NC Pentachlorophenol. U. U ug/l NC -Nitrophenol. U.0 U ug/l NC Benzyl alcohol. U. U ug/l NC RP Limit 0 Page of //0

45 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: 0-0-E--A U Client Sample I: uplicate Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample U U RP -Methylphenol. U. U ug/l NC Benzoic acid U U ug/l NC -Chloroaniline. U.0 U ug/l NC -Methylnaphthalene. U. U ug/l NC,,-Trichlorophenol. U.0 U ug/l NC -Nitroaniline. U. U ug/l NC -Nitroaniline. U. U ug/l NC ibenzofuran. U. U ug/l NC -Nitroaniline. U. U ug/l NC & Methylphenol. U. U ug/l NC -Methylnaphthalene. U. U ug/l NC,'-oxybis[-chloropropane]. U.0 U ug/l NC Surrogate -Fluorophenol - U %Recovery U Nitrobenzene-d - 0 -Fluorobiphenyl - Terphenyl-d -,,-Tribromophenol - Phenol-d (Surr) - RP Limit 0 Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: 0 MB MB,-ichlorobenzene. U 0. ug/l 0/0/ : 0// : N-Nitrosodimethylamine Phenol,-ichlorobenzene Hexachloroethane Bis(-chloroethyl)ether,-ichlorobenzene N-Nitrosodi-n-propylamine Nitrobenzene Hexachlorobutadiene,,-Trichlorobenzene Isophorone Naphthalene Bis(-chloroethoxy)methane Hexachlorocyclopentadiene -Chloronaphthalene Acenaphthylene Acenaphthene imethyl phthalate,-initrotoluene Fluorene -Chlorophenyl phenyl ether,-initrotoluene ML il Fac. U 0. ug/l 0/0/ : 0// :. U.0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// : 0. U 0 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :.0 U 0.0 ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :.0 U 0.0 ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// : 0. U 0 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// : 0. U 0 0. ug/l 0/0/ : 0// : Page of //0

46 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: 0 MB MB iethyl phthalate. U 0. ug/l 0/0/ : 0// : N-Nitrosodiphenylamine Hexachlorobenzene -Bromophenyl phenyl ether Phenanthrene Anthracene i-n-butyl phthalate Fluoranthene Pyrene Butyl benzyl phthalate Bis(-ethylhexyl) phthalate Chrysene Benzo[a]anthracene,'-ichlorobenzidine i-n-octyl phthalate Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[a]pyrene Indeno[,,-cd]pyrene ibenz(a,h)anthracene Benzo[g,h,i]perylene -Chlorophenol -Nitrophenol,-imethylphenol,-ichlorophenol,,-Trichlorophenol -Chloro--methylphenol,-initrophenol,-initro--methylphenol Pentachlorophenol -Nitrophenol Benzyl alcohol -Methylphenol Benzoic acid -Chloroaniline -Methylnaphthalene,,-Trichlorophenol -Nitroaniline -Nitroaniline ibenzofuran -Nitroaniline & Methylphenol -Methylnaphthalene,'-oxybis[-chloropropane] ML il Fac. U 0. ug/l 0/0/ : 0// :. U.0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :.0 U 0.0 ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U.0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// : 0. U.0 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :.0 U 0.0 ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// : U 0 ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// :. U 0. ug/l 0/0/ : 0// : 0 Surrogate MB %Recovery MB -Fluorophenol - 0/0/ : 0// : Nitrobenzene-d - 0 0/0/ : 0// : -Fluorobiphenyl - 0/0/ : 0// : il Fac Page of //0

47 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: 0 Surrogate MB %Recovery MB Terphenyl-d - 0/0/ : 0// :,,-Tribromophenol - 0/0/ : 0// : Phenol-d (Surr) - 0/0/ : 0// : Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: 0 Spike LCS LCS Added %Rec,-ichlorobenzene 00. ug/l 0-0 N-Nitrosodimethylamine 00. ug/l - 0 Phenol 00. ug/l - 0,-ichlorobenzene ug/l - 0 Hexachloroethane ug/l 0-0 Bis(-chloroethyl)ether 00. ug/l -,-ichlorobenzene 00. ug/l - 0 N-Nitrosodi-n-propylamine 00. ug/l - 0 Nitrobenzene 00. ug/l - 0 Hexachlorobutadiene 00. ug/l - 0,,-Trichlorobenzene ug/l 0-0 Isophorone 00.0 ug/l - 0 Naphthalene 00. ug/l - 0 Bis(-chloroethoxy)methane 00. ug/l - Hexachlorocyclopentadiene 00. ug/l 0-0 -Chloronaphthalene ug/l - 0 Acenaphthylene 00. ug/l - 0 Acenaphthene 00.0 ug/l - 0 imethyl phthalate 00. ug/l -,-initrotoluene 00. ug/l - Fluorene 00. ug/l - 0 -Chlorophenyl phenyl ether 00. ug/l -,-initrotoluene 00. ug/l - iethyl phthalate 00. ug/l 0 - N-Nitrosodiphenylamine 00. ug/l - Hexachlorobenzene 00. ug/l - -Bromophenyl phenyl ether 00.0 ug/l - 0 Phenanthrene 00. ug/l - 0 Anthracene 00. ug/l - i-n-butyl phthalate 00. ug/l 0-0 Fluoranthene 00. ug/l - 0 Pyrene 00. ug/l - 0 Butyl benzyl phthalate 00. ug/l - Bis(-ethylhexyl) phthalate 00. ug/l - Chrysene 00.0 ug/l 0-0 Benzo[a]anthracene 00. ug/l - 0,'-ichlorobenzidine 00. ug/l 0-0 i-n-octyl phthalate 00. ug/l - Benzo[b]fluoranthene 00. ug/l 0-0 Benzo[k]fluoranthene 00. ug/l - 0 il Fac 0 Page of //0

48 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: 0 Spike LCS LCS Added %Rec Benzo[a]pyrene 00. ug/l - 0 Indeno[,,-cd]pyrene 00. ug/l - 0 ibenz(a,h)anthracene 00. ug/l - 0 Benzo[g,h,i]perylene 00. ug/l - 0 -Chlorophenol 00. ug/l Nitrophenol 00. ug/l -,-imethylphenol 00.0 ug/l - 0,-ichlorophenol 00. ug/l 0 -,,-Trichlorophenol 00. ug/l - -Chloro--methylphenol 00. ug/l - 0,-initrophenol 00. ug/l 0-0,-initro--methylphenol 00. ug/l - Pentachlorophenol 00. ug/l 0 - -Nitrophenol 00.0 I ug/l - 0 Benzyl alcohol 00. ug/l - 0 -Methylphenol 00. ug/l 0-0 Benzoic acid I ug/l Chloroaniline 00. I ug/l 0-0 -Methylnaphthalene 00.0 ug/l - 0,,-Trichlorophenol ug/l 0-0 -Nitroaniline 00. ug/l - 0 -Nitroaniline 00. ug/l - 0 ibenzofuran 00. ug/l - -Nitroaniline 00. ug/l - 0 & Methylphenol 00 ug/l - 0 -Methylnaphthalene 00. ug/l 0 -,'-oxybis[-chloropropane] 00.0 ug/l Surrogate LCS %Recovery LCS -Fluorophenol - Nitrobenzene-d - 0 -Fluorobiphenyl - Terphenyl-d -,,-Tribromophenol - Phenol-d (Surr) - Lab Sample I: A MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec,-ichlorobenzene.0 U.. ug/l - 0 N-Nitrosodimethylamine. U.. ug/l - 0 Phenol. U.. ug/l - 0,-ichlorobenzene. U.. ug/l - 0 Hexachloroethane 0. U.. ug/l - 0 Bis(-chloroethyl)ether. U.. ug/l -,-ichlorobenzene.0 U. 0. ug/l - 0 N-Nitrosodi-n-propylamine. U.. ug/l - 0 Page of //0

49 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: A MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec Nitrobenzene. U.. ug/l 0-0 Hexachlorobutadiene 0. U.. ug/l - 0,,-Trichlorobenzene. U..0 ug/l - 0 Isophorone. U..0 ug/l - 0 Naphthalene. U.. ug/l - 0 Bis(-chloroethoxy)methane. U.. ug/l 0 - Hexachlorocyclopentadiene. U.. ug/l 0-0 -Chloronaphthalene. U.. ug/l - 0 Acenaphthylene. U.. ug/l - 0 Acenaphthene. U.. ug/l - 0 imethyl phthalate. U.. ug/l -,-initrotoluene 0. U.. ug/l - Fluorene. U.. ug/l - 0 -Chlorophenyl phenyl ether. U.. ug/l -,-initrotoluene 0. U.. ug/l - iethyl phthalate. U.. ug/l 0 - N-Nitrosodiphenylamine. U.. ug/l 0 - Hexachlorobenzene. U.. ug/l - -Bromophenyl phenyl ether. U.. ug/l - 0 Phenanthrene. U. 0.0 ug/l - 0 Anthracene 0. U..0 ug/l - i-n-butyl phthalate. U.. ug/l 0-0 Fluoranthene. U.. ug/l - 0 Pyrene. U.. ug/l - 0 Butyl benzyl phthalate. U.. ug/l - Bis(-ethylhexyl) phthalate. U.. ug/l - Chrysene. U.. ug/l 0-0 Benzo[a]anthracene. U. 0. ug/l - 0,'-ichlorobenzidine. U.. ug/l 0-0 i-n-octyl phthalate. U. 0. ug/l - Benzo[b]fluoranthene. U.. ug/l 0-0 Benzo[k]fluoranthene. U.. ug/l - 0 Benzo[a]pyrene 0. U.. ug/l - 0 Indeno[,,-cd]pyrene. U..0 ug/l - 0 ibenz(a,h)anthracene 0. U.. ug/l - 0 Benzo[g,h,i]perylene.0 U.. ug/l - 0 -Chlorophenol.0 U.. ug/l 0-0 -Nitrophenol. U.. ug/l -,-imethylphenol. U J.. J ug/l - 0,-ichlorophenol. U.. ug/l 0 0 -,,-Trichlorophenol. U.. ug/l - -Chloro--methylphenol. U..0 ug/l - 0,-initrophenol. U.. I ug/l 0-0,-initro--methylphenol. U.. ug/l - Pentachlorophenol. U.. ug/l 0 - -Nitrophenol. U.. I ug/l - 0 Benzyl alcohol. U.. ug/l - 0 -Methylphenol. U.. ug/l 0-0 Benzoic acid U.. I ug/l 0-0 -Chloroaniline.0 U..0 I ug/l Page of //0

50 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: A MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec -Methylnaphthalene. U.. ug/l - 0,,-Trichlorophenol.0 U.. ug/l - 0 -Nitroaniline. U.. ug/l - 0 -Nitroaniline. U.. I ug/l - 0 ibenzofuran. U.. ug/l - -Nitroaniline. U.. ug/l 0-0 & Methylphenol. U J 0. J ug/l 0-0 -Methylnaphthalene. U.. ug/l 0 -,'-oxybis[-chloropropane].0 U..0 ug/l 0-0 Surrogate -Fluorophenol - MS %Recovery MS Nitrobenzene-d - 0 -Fluorobiphenyl 0 - Terphenyl-d -,,-Tribromophenol - Phenol-d (Surr) 0 - Lab Sample I: 0-0-F--A U Client Sample I: uplicate Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample U U RP,-ichlorobenzene. U.0 U ug/l NC N-Nitrosodimethylamine. U. U ug/l NC Phenol. U. U ug/l NC,-ichlorobenzene. U. U ug/l NC Hexachloroethane 0. U 0. U ug/l NC Bis(-chloroethyl)ether. U. U ug/l NC,-ichlorobenzene. U.0 U ug/l NC N-Nitrosodi-n-propylamine. U. U ug/l NC Nitrobenzene. U. U ug/l NC Hexachlorobutadiene 0. U 0. U ug/l NC,,-Trichlorobenzene. U. U ug/l NC Isophorone. U. U ug/l NC Naphthalene. U. U ug/l NC Bis(-chloroethoxy)methane. U. U ug/l NC Hexachlorocyclopentadiene. U. U ug/l NC -Chloronaphthalene. U. U ug/l NC Acenaphthylene. U. U ug/l NC Acenaphthene. U. U ug/l NC imethyl phthalate. U. U ug/l NC,-initrotoluene 0. U 0. U ug/l NC Fluorene. U. U ug/l NC -Chlorophenyl phenyl ether. U. U ug/l NC,-initrotoluene 0. U 0. U ug/l NC iethyl phthalate. U. U ug/l NC N-Nitrosodiphenylamine. U. U ug/l NC Hexachlorobenzene. U. U ug/l NC RP Limit 0 Page of //0

51 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-0- Lab Sample I: 0-0-F--A U Client Sample I: uplicate Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample U U RP -Bromophenyl phenyl ether. U. U ug/l NC Phenanthrene. U. U ug/l NC Anthracene 0. U 0. U ug/l NC i-n-butyl phthalate. U. U ug/l NC Fluoranthene. U. U ug/l NC Pyrene. U. U ug/l NC Butyl benzyl phthalate. U. U ug/l NC Bis(-ethylhexyl) phthalate. U. U ug/l NC Chrysene. U. U ug/l NC Benzo[a]anthracene. U. U ug/l NC,'-ichlorobenzidine. U. U ug/l NC i-n-octyl phthalate. U. U ug/l NC Benzo[b]fluoranthene. U. U ug/l NC Benzo[k]fluoranthene. U. U ug/l NC Benzo[a]pyrene 0. U 0. U ug/l NC Indeno[,,-cd]pyrene. U. U ug/l NC ibenz(a,h)anthracene 0. U 0. U ug/l NC Benzo[g,h,i]perylene. U.0 U ug/l NC -Chlorophenol.0 U.0 U ug/l NC -Nitrophenol. U. U ug/l NC,-imethylphenol. U. U ug/l NC,-ichlorophenol. U. U ug/l NC,,-Trichlorophenol. U. U ug/l NC -Chloro--methylphenol. U. U ug/l NC,-initrophenol.0 U. U ug/l NC,-initro--methylphenol. U. U ug/l NC Pentachlorophenol. U. U ug/l NC -Nitrophenol.0 U. U ug/l NC Benzyl alcohol. U. U ug/l NC -Methylphenol. U. U ug/l NC Benzoic acid U U ug/l NC -Chloroaniline.0 U.0 U ug/l NC -Methylnaphthalene. U. U ug/l NC,,-Trichlorophenol.0 U.0 U ug/l NC -Nitroaniline. U. U ug/l NC -Nitroaniline. U. U ug/l NC ibenzofuran. U. U ug/l NC -Nitroaniline. U. U ug/l NC & Methylphenol. U. U ug/l NC -Methylnaphthalene. U. U ug/l NC,'-oxybis[-chloropropane].0 U.0 U ug/l NC RP Limit 0 Surrogate -Fluorophenol - U %Recovery U Nitrobenzene-d - 0 -Fluorobiphenyl - Terphenyl-d -,,-Tribromophenol - Phenol-d (Surr) - Page 0 of //0

52 Method: Anions, Ion Chromatography Lab Sample I: MB 0-00/ Analysis Batch: 00 MB MB QC Sample s ML TestAmerica Job I: 0-0- Client Sample I: Method Blank Prep Type: Sulfate 0.0 U mg/l 0// 0: Chloride Lab Sample I: LCS 0-00/ Analysis Batch: 00 il Fac 0.0 U mg/l 0// 0: Spike Added Client Sample I: Lab Control Sample Prep Type: Sulfate mg/l LCS LCS %Rec Chloride mg/l Lab Sample I: 0-0- MS Analysis Batch: 00 Sample Sample Spike Added Sulfate mg/l MS MS %Rec Chloride mg/l Lab Sample I: 0-0- MS Analysis Batch: 00 Sample Sample Spike Added Client Sample I: W-Inflow Prep Type: Client Sample I: W-Inflow Prep Type: Sulfate mg/l MS MS %Rec Chloride mg/l RP RP Limit 0 Method: 00. Rev. - Metals (ICP) Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis Batch: 0 Prep Batch: 0 MB MB Chromium U mg/l 0// 0: 0// : Copper Iron Lead ML il Fac 0.00 U mg/l 0// 0: 0// : 0.00 U mg/l 0// 0: 0// : U mg/l 0// 0: 0// : Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis Batch: 0 Prep Batch: 0 Spike LCS LCS Added %Rec Chromium mg/l Copper mg/l Iron.00.0 mg/l Lead.00.0 mg/l Page of //0

53 Method: 00. Rev. - Metals (ICP) (Continued) QC Sample s TestAmerica Job I: 0-0- Lab Sample I: 0-0-E--B MS Client Sample I: Matrix Spike Prep Type: Total Recoverable Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec Chromium U mg/l 0-0 Copper mg/l Iron 0 J.00.0 J mg/l 0-0 Lead mg/l 0-0 Lab Sample I: 0-0-E--C MS Client Sample I: Matrix Spike uplicate Prep Type: Total Recoverable Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS RP Added %Rec Chromium U mg/l Copper mg/l Iron 0 J.00. J mg/l Lead mg/l Method: A - HEM and SGT-HEM Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 0 Prep Batch: 0 MB MB HEM (Oil and Grease).0 U.0.0 mg/l 0// 0: 0// 0: ML RP Limit il Fac 0 Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 0 Prep Batch: 0 Spike LCS LCS Added %Rec HEM (Oil and Grease) 0.0. mg/l - Lab Sample I: 0-0- MS Client Sample I: W-Inflow Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample Spike MS MS Added %Rec HEM (Oil and Grease). I.. mg/l - Lab Sample I: 0-0- U Client Sample I: W-Outfall Prep Type: Analysis Batch: 0 Prep Batch: 0 Sample Sample U U RP RP Limit HEM (Oil and Grease). U. U mg/l NC Page of //0

54 Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 0-000/ Analysis Batch: 000 MB MB QC Sample s ML TestAmerica Job I: 0-0- Client Sample I: Method Blank Prep Type: Nitrate Nitrite as N 0.0 U mg/l 0// : Nitrite as N Nitrate as N Lab Sample I: LCS 0-000/ Analysis Batch: 000 il Fac 0.0 U mg/l 0// : 0.0 U mg/l 0// : Spike Added Client Sample I: Lab Control Sample Prep Type: Nitrate Nitrite as N mg/l 0-0 LCS LCS %Rec Nitrite as N I mg/l 0-0 Lab Sample I: 0-0-F- MS ^0 Analysis Batch: 000 Sample Sample Spike Added Nitrate Nitrite as N 0.0. mg/l 0-0 MS MS %Rec Nitrite as N.0 U mg/l Lab Sample I: 0-0-F- MS ^0 Analysis Batch: 000 Sample Sample Spike Added Client Sample I: Matrix Spike Prep Type: Client Sample I: Matrix Spike uplicate Prep Type: Nitrate Nitrite as N 0.0. mg/l MS MS %Rec Nitrite as N.0 U.00.0 mg/l RP RP Limit 0 Method:. - Phosphorus, Orthophosphate Lab Sample I: MB 0-0/-A Client Sample I: Method Blank Prep Type: issolved Analysis Batch: 0 MB MB ML il Fac Orthophosphate 0.0 U mg/l 0// : Lab Sample I: LCS 0-0/-A Client Sample I: Lab Control Sample Prep Type: issolved Analysis Batch: 0 Spike LCS LCS Added %Rec Orthophosphate mg/l Lab Sample I: 0-0- MS Client Sample I: W-Inflow Prep Type: issolved Analysis Batch: 0 Sample Sample Spike MS MS Added %Rec Orthophosphate 0.0 U mg/l Page of //0

55 QC Sample s Method:. - Phosphorus, Orthophosphate (Continued) Lab Sample I: 0-0- MS Analysis Batch: 0 Sample Sample Spike Added TestAmerica Job I: 0-0- Client Sample I: W-Inflow Prep Type: issolved Orthophosphate 0.0 U mg/l Method:. - Phosphorus, Total MS MS %Rec Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB Phosphorus 0.0 U mg/l 0// 0: 0// : ML Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS Added %Rec Phosphorus.00.0 mg/l Lab Sample I: 0-00-B--B MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS Added %Rec Phosphorus 0.0 I.00. mg/l RP RP Limit il Fac 0 Lab Sample I: 0-00-B--C MS Client Sample I: Matrix Spike uplicate Prep Type: Analysis Batch: Prep Batch: Sample Sample Spike MS MS RP Added %Rec RP Limit Phosphorus 0.0 I.00.0 mg/l Lab Sample I: 0-0-B--B U Client Sample I: uplicate Prep Type: Analysis Batch: Prep Batch: Sample Sample U U RP RP Limit Phosphorus mg/l 0 Method: 00 - Organic Carbon, Total (TOC) Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis Batch: MB MB ML il Fac Total Organic Carbon 0.0 U mg/l 0// : Page of //0

56 Method: 00 - Organic Carbon, Total (TOC) (Continued) Lab Sample I: LCS 0-/ Analysis Batch: QC Sample s Spike Added TestAmerica Job I: 0-0- Client Sample I: Lab Control Sample Prep Type: Total Organic Carbon mg/l Lab Sample I: 0-0- MS Analysis Batch: Sample Sample Spike Added LCS LCS %Rec Total Organic Carbon 0. I 0.0. mg/l Lab Sample I: 0-0- MS Analysis Batch: Sample Sample Spike Added MS MS %Rec Client Sample I: W-Inflow Prep Type: Client Sample I: W-Inflow Prep Type: Total Organic Carbon 0. I 0.0. mg/l Method: SM 0B - Color, Colorimetric Lab Sample I: MB 0-00/ Analysis Batch: 00 MB MB MS MS %Rec ML RP RP Limit Client Sample I: Method Blank Prep Type: Color.0 U.0.0 PCU 0// 0:0 ph at time of analysis il Fac..0.0 SU 0// 0:0 0 Lab Sample I: LCS 0-00/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 00 Spike LCS LCS Added %Rec Color PCU Lab Sample I: 0-0- U Client Sample I: SW-Outfall Prep Type: Analysis Batch: 00 Sample Sample U U RP RP Limit Color 0 0 PCU 0 0 ph at time of analysis.. SU 0. Method: SM 0B - Alkalinity Lab Sample I: MB 0-0/ Client Sample I: Method Blank Prep Type: Analysis Batch: 0 MB MB ML il Fac Alkalinity.0 U.0.0 mg/l 0// : Page of //0

57 Method: SM 0B - Alkalinity (Continued) Lab Sample I: LCS 0-0/ Analysis Batch: 0 QC Sample s Spike Added TestAmerica Job I: 0-0- Client Sample I: Lab Control Sample Prep Type: Alkalinity mg/l 0-0 Lab Sample I: 0-0- U Analysis Batch: 0 Sample Sample LCS LCS %Rec Client Sample I: W-Inflow Prep Type: Alkalinity 0 0 mg/l 0 Method: SM 0C - Solids, Total issolved (TS) Lab Sample I: MB 0-0/ Analysis Batch: 0 MB MB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Total issolved Solids.0 U.0.0 mg/l 0// 0: Lab Sample I: LCS 0-0/ Analysis Batch: 0 Spike Added il Fac Client Sample I: Lab Control Sample Prep Type: Total issolved Solids mg/l 0-0 LCS LCS %Rec 0 Lab Sample I: 0-0- U Client Sample I: W-Outfall Prep Type: Analysis Batch: 0 Sample Sample U U RP RP Limit Total issolved Solids 0 mg/l 0 Method: SM 0 - Solids, Total Suspended (TSS) Lab Sample I: MB 0-00/ Client Sample I: Method Blank Prep Type: Analysis Batch: 00 MB MB ML il Fac Total Suspended Solids.0 U.0.0 mg/l 0// 0: Lab Sample I: LCS 0-00/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 00 Spike LCS LCS Added %Rec Total Suspended Solids 00. mg/l 0-0 Page of //0

58 QC Sample s Method: SM 0 - Solids, Total Suspended (TSS) (Continued) Lab Sample I: 0-0- U Analysis Batch: 00 Sample Sample TestAmerica Job I: 0-0- Client Sample I: SW-Outfall Prep Type: Total Suspended Solids.0.0 mg/l 0 Method: SM 00 Cl B - Chlorine, Total Residual Lab Sample I: MB 0-0/ Analysis Batch: 0 MB MB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Chlorine, Total Residual.0 U.0.0 mg/l 0// 0:0 Lab Sample I: 0-0-A- U Analysis Batch: 0 Sample Sample il Fac Client Sample I: uplicate Prep Type: Chlorine, Total Residual.0 U.0 U mg/l NC 0 Method: SM 0B - BO, -ay Lab Sample I: SCB 0-00/ SCB Analysis Batch: 00 SCB SCB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Biochemical Oxygen emand.0 U.0.0 mg/l 0// 0: il Fac 0 Lab Sample I: USB 0-00/ USB Client Sample I: Method Blank Prep Type: Analysis Batch: 00 USB USB ML il Fac Biochemical Oxygen emand.0 U.0.0 mg/l 0// 0: Lab Sample I: LCS 0-00/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 00 Spike LCS LCS Added %Rec Biochemical Oxygen emand mg/l - Lab Sample I: 0-0- U Client Sample I: SW-Outfall Prep Type: Analysis Batch: 00 Sample Sample U U RP RP Limit Biochemical Oxygen emand.0 U.0 U mg/l NC 0 Page of //0

59 Method: SM B - Coliforms, Total (Membrane Filter) Lab Sample I: MB 0-00/ Analysis Batch: 00 MB MB QC Sample s ML TestAmerica Job I: 0-0- Client Sample I: Method Blank Prep Type: Coliform, Total.0 U.0.0 CFU/00mL 0// : Lab Sample I: 0-0- U Analysis Batch: 00 Sample Sample il Fac Client Sample I: SW-Inflow Prep Type: Coliform, Total CFU/00mL 0 Method: SM - Coliforms, Fecal (Membrane Filter) Lab Sample I: MB 0-0/ Analysis Batch: 0 MB MB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Coliform, Fecal.0 U.0.0 CFU/00mL 0// : Lab Sample I: 0-0- U Analysis Batch: 0 Sample Sample il Fac Client Sample I: SW-Inflow Prep Type: Coliform, Fecal.0 CFU/00mL 0 U U RP RP Limit 0 Page of //0

60 QC Association Summary TestAmerica Job I: 0-0- GC/MS VOA Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0-B- U uplicate TCLP 0B 0-0-B- MS Matrix Spike TCLP 0B 0-0- W-Inflow 0B 0-0- W-Outfall 0B 0-0- Trip Blank 0B LCS 0-0/ Lab Control Sample 0B MB 0-0/ Method Blank 0B GC/MS Semi VOA Prep Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Outfall 0C 0-0-E--A U uplicate 0C 0-0-F--A MS Matrix Spike 0C LCS 0-0/-A Lab Control Sample 0C MB 0-0/-A Method Blank 0C Prep Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow 0C 0-0- SW-Inflow 0C 0-0- SW-Outfall 0C A MS Matrix Spike 0C 0-0-F--A U uplicate 0C LCS 0-0/-A Lab Control Sample 0C MB 0-0/-A Method Blank 0C 0 Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Outfall 0C E--A U uplicate 0C F--A MS Matrix Spike 0C 0 LCS 0-0/-A Lab Control Sample 0C 0 MB 0-0/-A Method Blank 0C 0 Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow 0C SW-Inflow 0C SW-Outfall 0C A MS Matrix Spike 0C F--A U uplicate 0C 0 LCS 0-0/-A Lab Control Sample 0C 0 MB 0-0/-A Method Blank 0C 0 HPLC/IC Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow 0-0- MS W-Inflow Page of //0

61 QC Association Summary TestAmerica Job I: 0-0- HPLC/IC (Continued) Analysis Batch: 00 (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- MS W-Inflow SW-Inflow W-Outfall SW-Outfall 00.0 LCS 0-00/ Lab Control Sample 00.0 MB 0-00/ Method Blank 00.0 Metals Prep Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0-E--B MS Matrix Spike Total Recoverable E--C MS Matrix Spike uplicate Total Recoverable W-Inflow Total Recoverable SW-Inflow Total Recoverable W-Outfall Total Recoverable SW-Outfall Total Recoverable 00. LCS 0-0/-A Lab Control Sample Total Recoverable 00. MB 0-0/-A Method Blank Total Recoverable 00. Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0-E--B MS Matrix Spike Total Recoverable 00. Rev E--C MS Matrix Spike uplicate Total Recoverable 00. Rev W-Inflow Total Recoverable 00. Rev SW-Inflow Total Recoverable 00. Rev W-Outfall Total Recoverable 00. Rev SW-Outfall Total Recoverable 00. Rev. 0 LCS 0-0/-A Lab Control Sample Total Recoverable 00. Rev. 0 MB 0-0/-A Method Blank Total Recoverable 00. Rev. 0 0 General Chemistry Analysis Batch: 000 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0-F- MS ^0 Matrix Spike 0-0-F- MS ^0 Matrix Spike uplicate 0-0- W-Inflow 0-0- SW-Inflow 0-0- W-Outfall 0-0- SW-Outfall LCS 0-000/ Lab Control Sample MB 0-000/ Method Blank Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow 0-0- SW-Inflow 0-0- W-Outfall 0-0- SW-Outfall 0-0- U SW-Outfall LCS 0-00/ Lab Control Sample SM 0 SM 0 SM 0 SM 0 SM 0 SM 0 Page 0 of //0

62 QC Association Summary TestAmerica Job I: 0-0- General Chemistry (Continued) Analysis Batch: 00 (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch MB 0-00/ Method Blank SM 0 Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow SM 0B 0-0- SW-Inflow SM 0B 0-0- W-Outfall SM 0B 0-0- SW-Outfall SM 0B 0-0- U SW-Outfall SM 0B LCS 0-00/ Lab Control Sample SM 0B SCB 0-00/ SCB Method Blank SM 0B USB 0-00/ USB Method Blank SM 0B Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow SM 0C 0-0- SW-Inflow SM 0C 0-0- W-Outfall SM 0C 0-0- U W-Outfall SM 0C 0-0- SW-Outfall SM 0C LCS 0-0/ Lab Control Sample SM 0C MB 0-0/ Method Blank SM 0C Analysis Batch: 0 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow SM 0B 0-0- U W-Inflow SM 0B 0-0- SW-Inflow SM 0B 0-0- W-Outfall SM 0B 0-0- SW-Outfall SM 0B LCS 0-0/ Lab Control Sample SM 0B MB 0-0/ Method Blank SM 0B Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow SM 0B 0-0- SW-Inflow SM 0B 0-0- W-Outfall SM 0B 0-0- SW-Outfall SM 0B 0-0- U SW-Outfall SM 0B LCS 0-00/ Lab Control Sample SM 0B MB 0-00/ Method Blank SM 0B Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow issolved MS W-Inflow issolved MS W-Inflow issolved SW-Inflow issolved W-Outfall issolved SW-Outfall issolved. LCS 0-0/-A Lab Control Sample issolved. Page of //0

63 QC Association Summary TestAmerica Job I: 0-0- General Chemistry (Continued) Analysis Batch: 0 (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch MB 0-0/-A Method Blank issolved. Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0-A- U uplicate SM 00 Cl B 0-0- W-Inflow SM 00 Cl B 0-0- SW-Inflow SM 00 Cl B 0-0- W-Outfall SM 00 Cl B 0-0- SW-Outfall SM 00 Cl B MB 0-0/ Method Blank SM 00 Cl B Prep Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow A 0-0- MS W-Inflow A 0-0- SW-Inflow A 0-0- W-Outfall A 0-0- U W-Outfall A 0-0- SW-Outfall A LCS 0-0/-A Lab Control Sample A MB 0-0/-A Method Blank A Analysis Batch: 0 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow A MS W-Inflow A SW-Inflow A W-Outfall A U W-Outfall A SW-Outfall A 0 LCS 0-0/-A Lab Control Sample A 0 MB 0-0/-A Method Blank A 0 Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-00-B--B MS Matrix Spike igestion 0-00-B--C MS Matrix Spike uplicate igestion 0-0-B--B U uplicate igestion 0-0- W-Inflow igestion 0-0- SW-Inflow igestion 0-0- W-Outfall igestion 0-0- SW-Outfall igestion LCS 0-/-A Lab Control Sample igestion MB 0-/-A Method Blank igestion Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-00-B--B MS Matrix Spike B--C MS Matrix Spike uplicate. 0-0-B--B U uplicate W-Inflow SW-Inflow. Page of //0

64 QC Association Summary TestAmerica Job I: 0-0- General Chemistry (Continued) Analysis Batch: (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Outfall SW-Outfall. LCS 0-/-A Lab Control Sample. MB 0-/-A Method Blank. Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow MS W-Inflow MS W-Inflow SW-Inflow W-Outfall SW-Outfall 00 LCS 0-/ Lab Control Sample 00 MB 0-/ Method Blank 00 Biology Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow SM B 0-0- SW-Inflow SM B 0-0- U SW-Inflow SM B 0-0- W-Outfall SM B 0-0- SW-Outfall SM B MB 0-00/ Method Blank SM B 0 Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0- W-Inflow SM 0-0- SW-Inflow SM 0-0- U SW-Inflow SM 0-0- W-Outfall SM 0-0- SW-Outfall SM MB 0-0/ Method Blank SM Page of //0

65 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-0- Client Sample I: W-Inflow Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// : Prep Type Total Recoverable Total Recoverable issolved Batch Type Batch Method Run ilution Factor or Analyst Analysis 0B 0 0// : EC TAL TAM Batch Number Prep 0C 0 0/0/ : AG TAL TAM Analysis 0C 0 0// : SCC TAL TAM Analysis // 0: KW TAL TAM Prep // 0: GF TAL TAM Analysis 00. Rev. 0 0// : GF TAL TAM Analysis // : KW TAL TAM Analysis SM // 0: TO TAL TAM Analysis SM 0B 00 0// 0: AG TAL TAM Analysis SM 0C 0 0// 0: TO TAL TAM Analysis SM 0B 0 0// : RWF TAL TAM Analysis SM 0B 00 0// 0:0 AG TAL TAM Analysis. 0 0// : RWF TAL TAM Analysis SM 00 Cl B 0 0// 0:0 RWF TAL TAM Prep A 0 0// 0: SC TAL TAM Analysis A 0 0// 0: SC TAL TAM Prep igestion 0// 0: MAP TAL SAV Analysis. 0// : JR TAL SAV Analysis 00 0// : JR TAL SAV Analysis SM B 00 RWF TAL TAM (Start) (End) 0// : 0// : Analysis SM 0 RWF TAL TAM (Start) (End) 0// : 0// :0 Lab 0 Client Sample I: SW-Inflow Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// : Prep Type Total Recoverable Total Recoverable issolved Batch Type Batch Method Run ilution Factor or Analyst Prep 0C 0 0/0/ : AG TAL TAM Batch Number Analysis 0C 0 0// :0 SCC TAL TAM Analysis // 0: KW TAL TAM Prep // 0: GF TAL TAM Analysis 00. Rev. 0 0// : GF TAL TAM Analysis // : KW TAL TAM Analysis SM // 0: TO TAL TAM Analysis SM 0B 00 0// 0: AG TAL TAM Analysis SM 0C 0 0// 0: TO TAL TAM Analysis SM 0B 0 0// : RWF TAL TAM Analysis SM 0B 00 0// 0:0 AG TAL TAM Analysis. 0 0// : RWF TAL TAM Lab Page of //0

66 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-0- Client Sample I: SW-Inflow Lab Sample I: 0-0- ate Collected: 0// 0:0 ate Received: 0// : Prep Type Batch Type Batch Method Run ilution Factor or Analyst Analysis SM 00 Cl B 0 0// 0:0 RWF TAL TAM Batch Number Prep A 0 0// 0: SC TAL TAM Analysis A 0 0// 0: SC TAL TAM Prep igestion 0// 0: MAP TAL SAV Analysis. 0// : JR TAL SAV Analysis 00 0// :0 JR TAL SAV Analysis SM B RWF TAL TAM (Start) (End) 0// : 0// : Analysis SM 0 RWF TAL TAM (Start) (End) 0// : 0// :0 Client Sample I: W-Outfall Lab Sample I: 0-0- ate Collected: 0// :00 ate Received: 0// : Prep Type Batch Type Batch Method Run ilution Factor or Analyst Analysis 0B 0 0// : EC TAL TAM Batch Number Lab Lab 0 Total Recoverable Total Recoverable issolved Prep 0C 0 0// 0:0 AG TAL TAM Analysis 0C 0 0// : SCC TAL TAM Analysis // 0: KW TAL TAM Prep // 0: GF TAL TAM Analysis 00. Rev. 0 0// : GF TAL TAM Analysis // : KW TAL TAM Analysis SM // 0: TO TAL TAM Analysis SM 0B 00 0// 0: AG TAL TAM Analysis SM 0C 0 0// 0: TO TAL TAM Analysis SM 0B 0 0// : RWF TAL TAM Analysis SM 0B 00 0// 0:0 AG TAL TAM Analysis. 0 0// : RWF TAL TAM Analysis SM 00 Cl B 0 0// 0:0 RWF TAL TAM Prep A 0 0// 0: SC TAL TAM Analysis A 0 0// 0: SC TAL TAM Prep igestion 0// 0: MAP TAL SAV Analysis. 0// : JR TAL SAV Analysis 00 0// : JR TAL SAV Analysis SM B 00 RWF TAL TAM (Start) 0// : (End) 0// : Analysis SM 0 RWF TAL TAM (Start) 0// : (End) 0// :0 Page of //0

67 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-0- Client Sample I: SW-Outfall Lab Sample I: 0-0- ate Collected: 0// :0 ate Received: 0// : Prep Type Total Recoverable Total Recoverable issolved Batch Type Batch Method Run ilution Factor or Analyst Prep 0C 0 0/0/ : AG TAL TAM Batch Number Analysis 0C 0 0// : SCC TAL TAM Analysis // :0 KW TAL TAM Prep // 0: GF TAL TAM Analysis 00. Rev. 0 0// : GF TAL TAM Analysis // : KW TAL TAM Analysis SM // 0: TO TAL TAM Analysis SM 0B 00 0// 0: AG TAL TAM Analysis SM 0C 0 0// 0: TO TAL TAM Analysis SM 0B 0 0// : RWF TAL TAM Analysis SM 0B 00 0// 0:0 AG TAL TAM Analysis. 0 0// : RWF TAL TAM Analysis SM 00 Cl B 0 0// 0:0 RWF TAL TAM Prep A 0 0// 0: SC TAL TAM Analysis A 0 0// 0: SC TAL TAM Prep igestion 0// 0: MAP TAL SAV Analysis. 0// : JR TAL SAV Analysis 00 0// : JR TAL SAV Analysis SM B RWF TAL TAM (Start) (End) 0// : 0// : Analysis SM 0 RWF TAL TAM (Start) (End) 0// : 0// :0 Lab 0 Client Sample I: Trip Blank Lab Sample I: 0-0- ate Collected: 0// 00:00 ate Received: 0// : Prep Type Batch Type Batch Method Run ilution Factor or Analyst Analysis 0B 0 0// : EC TAL TAM Batch Number Lab Laboratory References: TAL SAV = TestAmerica Savannah, 0 LaRoche Avenue, Savannah, GA 0, TEL ()- TAL TAM =, Benjamin Road, Suite 00, Tampa, FL, TEL ()- Page of //0

68 Certification Summary Client: Cardno ENTRIX. TestAmerica Job I: 0-0- Laboratory: All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Alabama State Program Florida NELAC E 0-0- Georgia State Program 0-0- USA Federal P Laboratory: TestAmerica Savannah All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate ALA o ELAP ALA ISO/IEC Alabama State Program Alaska (UST) State Program 0 UST Arkansas EQ State Program California NELAC CA 0-- Colorado State Program N/A -- Connecticut State Program PH Florida NELAC E GA ept. of Agriculture State Program N/A -- Georgia State Program N/A 0-0- Georgia State Program Guam State Program 0-00r 0-- Hawaii State Program N/A 0-0- Illinois NELAC Indiana State Program N/A 0-0- Iowa State Program 0-0- Kentucky State Program Kentucky (UST) State Program 0-- Louisiana NELAC Louisiana NELAC LA Maine State Program GA Maryland State Program 0 -- Massachusetts State Program M-GA Michigan State Program 0-0- Mississippi State Program N/A 0-0- Montana State Program CERT00 -- Nebraska State Program TestAmerica-Savannah 0-0- New Jersey NELAC GA 0-0- New Mexico State Program N/A 0-0- New York NELAC North Carolina ENR State Program -- North Carolina HHS State Program Oklahoma State Program 0-- Pennsylvania NELAC Puerto Rico State Program GA Rhode Island State Program LAO00-0- South Carolina State Program Tennessee State Program TN Texas NELAC T00-0-TX -0- USA Federal SAV Vermont State Program 0 -- Virginia NELAC Washington State Program 0 C Page of //0

69 Certification Summary Client: Cardno ENTRIX. TestAmerica Job I: 0-0- Laboratory: TestAmerica Savannah (Continued) All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate West Virginia State Program 0C -- West Virginia EP State Program 0-0- Wisconsin State Program Wyoming State Program TMS-Q Page of //0

70 Method Summary TestAmerica Job I: 0-0- Method Method escription Protocol Laboratory 0B Volatile Organic Compounds (GC/MS) SW TAL TAM 0C Semivolatile Organic Compounds (GC/MS) SW TAL TAM 00.0 Anions, Ion Chromatography MCAWW TAL TAM 00. Rev. Metals (ICP) EPA TAL TAM A HEM and SGT-HEM A TAL TAM. Nitrogen, Nitrate-Nitrite MCAWW TAL TAM. Phosphorus, Orthophosphate MCAWW TAL TAM. Phosphorus, Total EPA TAL SAV 00 Organic Carbon, Total (TOC) SW TAL SAV SM 0B Color, Colorimetric SM TAL TAM SM 0B Alkalinity SM TAL TAM SM 0C Solids, Total issolved (TS) SM TAL TAM SM 0 Solids, Total Suspended (TSS) SM TAL TAM SM 00 Cl B Chlorine, Total Residual SM TAL TAM SM 0B BO, -ay SM TAL TAM SM B Coliforms, Total (Membrane Filter) SM TAL TAM SM Coliforms, Fecal (Membrane Filter) SM TAL TAM Protocol References: A = EPA---00 EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. Laboratory References: TAL SAV = TestAmerica Savannah, 0 LaRoche Avenue, Savannah, GA 0, TEL ()- TAL TAM =, Benjamin Road, Suite 00, Tampa, FL, TEL ()- 0 Page of //0

71 Sample Summary TestAmerica Job I: 0-0- Lab Sample I Client Sample I Matrix Collected Received 0-0- W-Inflow 0// 0:0 0// : 0-0- SW-Inflow 0// 0:0 0// : 0-0- W-Outfall 0// :00 0// : 0-0- SW-Outfall 0// :0 0// : 0-0- Trip Blank 0// 00:00 0// : 0 Page 0 of //0

72 0 Page of //0

73 Login Sample Receipt Checklist Client: Cardno ENTRIX. Job Number: 0-0- Login Number: 0 List Number: Creator: McNulty, Carol Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. N/A N/A List Source: 0 Page of //0

74 Login Sample Receipt Checklist Client: Cardno ENTRIX. Job Number: 0-0- Login Number: 0 List Number: Creator: Conner, Keaton Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey meter. The cooler's custody seal, if present, is intact. Sample custody seals, if present, are intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the containers received and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified. There is sufficient vol. for all requested analyses, incl. any requested MS/MSs Containers requiring zero headspace have no headspace or bubble is <mm (/"). Multiphasic samples are not present. Samples do not require splitting or compositing. Residual Chlorine Checked. N/A N/A N/A List Source: TestAmerica Savannah List Creation: 0// 0: AM 0 Page of //0

75 ANALYTICAL REPORT TestAmerica Laboratories, Inc. Benjamin Road Suite 00 Tampa, FL Tel: ()- TestAmerica Job I: 0-- Client For: Cardno ENTRIX. 0 Crescent Park rive Riverview, Florida Attn: Mr. aniel Hammond 0 Authorized for release by: //0 :: PM Nancy Robertson Project Manager II nancy.robertson@testamericainc.com esignee for Amy Atkins Project Manager I amy.atkins@testamericainc.com The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. s relate only to the items tested and the sample(s) as received by the laboratory.

76 Table of Contents TestAmerica Job I: 0-- Cover Page Table of Contents Sample Summary Case Narrative efinitions/glossary etection Summary Client Sample s QC Sample s QC Association Summary Lab Chronicle Method Summary Certification Summary Chain of Custody Receipt Checklists Page of //0

77 Sample Summary TestAmerica Job I: 0-- Lab Sample I Client Sample I Matrix Collected Received 0-- SW-IN 0/0/ 0: 0/0/ : 0-- W-IN 0/0/ 0:0 0/0/ : 0-- SW-OUT 0/0/ : 0/0/ : 0-- W-OUT 0/0/ :0 0/0/ : 0-- Trip Blank 0/0/ 00:00 0/0/ : 0 Page of //0

78 Case Narrative Client: Cardno ENTRIX. TestAmerica Job I: 0-- Job I: 0-- Laboratory: Narrative Job Narrative 0-- Receipt The samples were received on //0 : PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the coolers at receipt time were.0º C,.º C,.0º C and.0º C. GC/MS VOA Method 0B: The matrix spike (MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. GC/MS Semi VOA Method 0C: The method blank for batch contained bis(-ethylhexyl)phthalate above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. The samples are flagged with V. General Chemistry Method.: The matrix spike / matrix spike duplicate (MS/MS) recoveries for batch were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. (0-- MS), (0-- MS) No other analytical or quality issues were noted. 0 Page of //0

79 s GC/MS VOA U I J GC/MS Semi VOA U I V Metals U I General Chemistry I J U Biology U escription Indicates that the compound was analyzed for but not detected. efinitions/glossary The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Indicates the analyte was detected in both the sample and the associated method blank. escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. escription The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. Indicates that the compound was analyzed for but not detected. escription Indicates that the compound was analyzed for but not detected. TestAmerica Job I: Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid ER uplicate error ratio (normalized absolute difference) L, RA, RE, IN Indicates a ilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision level concentration EL Estimated etection Limit EPA ed States Environmental Protection Agency MA Minimum detectable activity MC Minimum detectable concentration ML Method etection Limit ML Minimum Level (ioxin) N Not detected at the reporting limit (or ML or EL if shown) Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) Page of //0

80 etection Summary TestAmerica Job I: 0-- Client Sample I: SW-IN Lab Sample I: 0-- ML il Fac Method Prep Type Bis(-ethylhexyl) phthalate 0. I V 0 0. ug/l Chromium 0.00 I mg/l 00. Rev. Total Recoverable Iron mg/l 00. Rev. Total Recoverable HEM (Oil & Grease). I. 0. mg/l A 0C Chloride.0.0 mg/l 00.0 Sulfate. I.0. mg/l 00.0 Nitrogen, Kjeldahl mg/l. Phosphorus mg/l. Total Organic Carbon mg/l 00 Color PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity..0.0 mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids..0.0 mg/l SM 0 Coliform, Total CFU/00mL 0 SM B Client Sample I: W-IN Lab Sample I: 0-- ML il Fac Method Prep Type Bis(-ethylhexyl) phthalate. I V 0 0. ug/l Lead 0.00 I mg/l 00. Rev. Total Recoverable HEM (Oil & Grease) 0. I. 0. mg/l A 0C Chloride mg/l 00.0 Nitrogen, Kjeldahl 0. I mg/l. Phosphorus 0.0 I mg/l. Total Organic Carbon mg/l 00 Color PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids mg/l SM 0 Coliform, Total CFU/00mL 0 SM B 0 Client Sample I: SW-OUT Lab Sample I: 0-- ML il Fac Method Prep Type Bis(-ethylhexyl) phthalate 0. I V 0 0. ug/l 0C Chromium 0.00 I mg/l 00. Rev. Total Recoverable Iron mg/l 00. Rev. Total Recoverable HEM (Oil & Grease). I.0 0. mg/l A Chloride mg/l 00.0 Sulfate 0.0. mg/l 00.0 Nitrogen, Kjeldahl mg/l. Phosphorus 0.0 I mg/l. Total Organic Carbon mg/l 00 Color PCU 0 SM 0B ph at time of analysis..0.0 SU 0 SM 0B This etection Summary does not include radiochemical test results. Page of //0

81 etection Summary TestAmerica Job I: 0-- Client Sample I: SW-OUT (Continued) Lab Sample I: 0-- ML il Fac Method Prep Type Alkalinity.0.0 mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids..0.0 mg/l SM 0 Coliform, Total CFU/00mL 0 SM B Client Sample I: W-OUT Lab Sample I: 0-- ML il Fac Method Prep Type Bis(-ethylhexyl) phthalate. I V. 0. ug/l Chromium I mg/l 00. Rev. Total Recoverable Copper 0.00 I mg/l 00. Rev. Total Recoverable Iron mg/l 00. Rev. Total Recoverable HEM (Oil & Grease) 0. I. 0. mg/l A 0C Chloride.0.0 mg/l 00.0 Nitrogen, Kjeldahl mg/l. Phosphorus mg/l. Total Organic Carbon mg/l 00 Color.0.0 PCU SM 0B ph at time of analysis..0.0 SU SM 0B Alkalinity mg/l SM 0B Total issolved Solids mg/l SM 0C Total Suspended Solids..0.0 mg/l SM 0 Coliform, Total CFU/00mL 0 SM B Coliform, Fecal CFU/00mL SM 0 Client Sample I: Trip Blank Lab Sample I: 0-- No etections This etection Summary does not include radiochemical test results. Page of //0

82 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-IN ate Collected: 0/0/ 0: ate Received: 0/0/ : Lab Sample I: 0-- Method: 0B - Volatile Organic Compounds (GC/MS) ML il Fac Benzene 0.0 U ug/l 0// 0: Bromobenzene 0. U.0 0. ug/l 0// 0: Chlorobromomethane 0. U.0 0. ug/l 0// 0: ichlorobromomethane 0. U.0 0. ug/l 0// 0: Bromoform 0. U.0 0. ug/l 0// 0: Bromomethane. U.0. ug/l 0// 0: n-butylbenzene 0. U.0 0. ug/l 0// 0: sec-butylbenzene 0. U.0 0. ug/l 0// 0: tert-butylbenzene 0. U.0 0. ug/l 0// 0: Carbon tetrachloride 0. U.0 0. ug/l 0// 0: Chlorobenzene 0. U.0 0. ug/l 0// 0: Chloroethane. U.0. ug/l 0// 0: Chloroform 0.0 U ug/l 0// 0: Chloromethane.0 U.0.0 ug/l 0// 0: -Chlorotoluene 0. U.0 0. ug/l 0// 0: -Chlorotoluene 0. U.0 0. ug/l 0// 0: Chlorodibromomethane 0. U.0 0. ug/l 0// 0:,-ibromo--Chloropropane. U.0. ug/l 0// 0: Ethylene ibromide 0.0 U ug/l 0// 0: ibromomethane 0. U.0 0. ug/l 0// 0:,-ichlorobenzene 0. U.0 0. ug/l 0// 0:,-ichlorobenzene 0. U.0 0. ug/l 0// 0:,-ichlorobenzene 0. U.0 0. ug/l 0// 0: ichlorodifluoromethane. U.0. ug/l 0// 0:,-ichloroethane 0. U.0 0. ug/l 0// 0:,-ichloroethane 0. U.0 0. ug/l 0// 0:,-ichloroethene 0. U.0 0. ug/l 0// 0: cis-,-ichloroethene 0. U.0 0. ug/l 0// 0: trans-,-ichloroethene 0. U.0 0. ug/l 0// 0:,-ichloropropane 0. U.0 0. ug/l 0// 0:,-ichloropropane 0. U.0 0. ug/l 0// 0:,-ichloropropane 0. U.0 0. ug/l 0// 0:,-ichloropropene 0. U.0 0. ug/l 0// 0: cis-,-ichloropropene 0. U.0 0. ug/l 0// 0: trans-,-ichloropropene 0. U.0 0. ug/l 0// 0: Ethylbenzene 0. U.0 0. ug/l 0// 0: Hexachlorobutadiene 0.0 U ug/l 0// 0: Isopropylbenzene 0. U.0 0. ug/l 0// 0: -Isopropyltoluene 0. U.0 0. ug/l 0// 0: Methylene Chloride.0 U.0.0 ug/l 0// 0: Naphthalene. U.0. ug/l 0// 0: N-Propylbenzene 0. U.0 0. ug/l 0// 0: Styrene 0. U.0 0. ug/l 0// 0:,,,-Tetrachloroethane 0. U.0 0. ug/l 0// 0:,,,-Tetrachloroethane 0. U.0 0. ug/l 0// 0: Tetrachloroethene 0.0 U ug/l 0// 0: Toluene 0. U.0 0. ug/l 0// 0:,,-Trichlorobenzene 0. U.0 0. ug/l 0// 0:,,-Trichlorobenzene 0. U.0 0. ug/l 0// 0: 0 Page of //0

83 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-IN ate Collected: 0/0/ 0: ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0--,,-Trichloroethane 0. U.0 0. ug/l 0// 0:,,-Trichloroethane 0. U Trichloroethene 0.0 U Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U Surrogate %Recovery il Fac.0 0. ug/l 0// 0: ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0: ug/l 0// 0: 0. ug/l 0// 0: 0. ug/l 0// 0: 0. ug/l 0// 0:.0.0 ug/l 0// 0: 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0: Toluene-d (Surr) // 0: -Bromofluorobenzene // 0: ibromofluoromethane // 0: il Fac 0 Method: 0C - Semivolatile Organic Compounds (GC/MS) ML il Fac,,-Trichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :,-ichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :,-ichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :,-ichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :,'-oxybis[-chloropropane] 0. U 0 0. ug/l 0/0/ :0 0// :,,-Trichlorophenol. U 0. ug/l 0/0/ :0 0// :,,-Trichlorophenol 0. U 0 0. ug/l 0/0/ :0 0// :,-ichlorophenol 0. U 0 0. ug/l 0/0/ :0 0// :,-imethylphenol 0. U 0 0. ug/l 0/0/ :0 0// :,-initrophenol. U 0. ug/l 0/0/ :0 0// :,-initrotoluene. U 0. ug/l 0/0/ :0 0// :,-initrotoluene 0. U 0 0. ug/l 0/0/ :0 0// : -Chloronaphthalene 0.0 U ug/l 0/0/ :0 0// : -Chlorophenol 0. U 0 0. ug/l 0/0/ :0 0// : -Methylnaphthalene 0. U 0 0. ug/l 0/0/ :0 0// : -Methylphenol 0. U 0 0. ug/l 0/0/ :0 0// : -Nitroaniline 0. U 0 0. ug/l 0/0/ :0 0// : -Nitrophenol 0. U 0 0. ug/l 0/0/ :0 0// : & Methylphenol 0. U 0 0. ug/l 0/0/ :0 0// :,'-ichlorobenzidine 0. U 0 0. ug/l 0/0/ :0 0// : -Nitroaniline. U 0. ug/l 0/0/ :0 0// :,-initro--methylphenol 0. U 0 0. ug/l 0/0/ :0 0// : -Bromophenyl phenyl ether. U 0. ug/l 0/0/ :0 0// : -Chloro--methylphenol. U 0. ug/l 0/0/ :0 0// : -Chloroaniline 0. U 0 0. ug/l 0/0/ :0 0// : -Chlorophenyl phenyl ether 0. U 0 0. ug/l 0/0/ :0 0// : Page of //0

84 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-IN ate Collected: 0/0/ 0: ate Received: 0/0/ : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- -Nitroaniline. U 0. ug/l 0/0/ :0 0// : -Nitrophenol. U Acenaphthene 0.0 U Acenaphthylene 0. U Anthracene. U Benzidine. U Benzo[a]anthracene 0. U Benzo[a]pyrene.0 U Benzo[b]fluoranthene 0. U Benzo[g,h,i]perylene. U Benzo[k]fluoranthene. U Benzoic acid. U Benzyl alcohol 0. U Bis(-chloroethoxy)methane 0. U Bis(-chloroethyl)ether 0. U Bis(-ethylhexyl) phthalate 0. I V Butyl benzyl phthalate 0. U Chrysene 0. U ibenz(a,h)anthracene. U ibenzofuran 0.0 U iethyl phthalate. U imethyl phthalate. U i-n-butyl phthalate. U i-n-octyl phthalate 0. U Fluoranthene. U Fluorene. U Hexachlorobenzene. U Hexachlorobutadiene 0. U Hexachlorocyclopentadiene 0. U Hexachloroethane 0. U Indeno[,,-cd]pyrene. U Isophorone 0. U Naphthalene 0. U Nitrobenzene 0. U N-Nitrosodimethylamine. U N-Nitrosodi-n-propylamine 0. U N-Nitrosodiphenylamine. U Pentachlorophenol. U Phenanthrene. U Phenol 0. U Pyrene.0 U il Fac 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0.0 ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0.0 ug/l 0/0/ :0 0// : 0 Surrogate %Recovery,,-Tribromophenol - 0/0/ :0 0// : -Fluorobiphenyl - 0/0/ :0 0// : -Fluorophenol - 0 0/0/ :0 0// : Nitrobenzene-d 0-0/0/ :0 0// : Phenol-d - 0 0/0/ :0 0// : Terphenyl-d 0-0 0/0/ :0 0// : il Fac Page 0 of //0

85 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-IN ate Collected: 0/0/ 0: ate Received: 0/0/ : Method: 00. Rev. - Metals (ICP) - Total Recoverable ML Lab Sample I: 0-- Chromium 0.00 I mg/l 0/0/ 0: 0// : Copper 0.00 U Iron. Lead U General Chemistry il Fac mg/l 0/0/ 0: 0// : mg/l 0/0/ 0: 0// : mg/l 0/0/ 0: 0// : HEM (Oil & Grease). I. 0. mg/l 0// : Chloride Sulfate. I Nitrogen, Kjeldahl. Nitrate Nitrite as N 0.0 U Nitrite as N 0.0 U Nitrate as N 0.0 U Phosphorus 0. Total Organic Carbon Color 0 ph at time of analysis. Alkalinity. Total issolved Solids 0 Total Suspended Solids. Chlorine, Total Residual.0 U Biochemical Oxygen emand.0 U ML il Fac.0.0 mg/l 0// :.0. mg/l 0// : mg/l 0// : 0// : mg/l 0/0/ 0: mg/l 0/0/ 0: mg/l 0/0/ 0: mg/l 0// : 0// : mg/l 0// :0 0 0 PCU 0/0/ 0:0.0.0 SU 0/0/ 0:0.0.0 mg/l 0/0/ 0:.0.0 mg/l 0/0/ 0:.0.0 mg/l 0/0/ 0:.0.0 mg/l 0/0/ 0: mg/l 0/0/ 0: 0 General Chemistry - issolved ML il Fac Orthophosphate 0.0 U mg/l 0/0/ :0 Method: SM B - Coliforms, Total (Membrane Filter) ML il Fac Coliform, Total CFU/00mL 0/0/ : 0 Method: SM - Coliforms, Fecal (Membrane Filter) ML il Fac Coliform, Fecal.0 U.0.0 CFU/00mL 0/0/ : Client Sample I: W-IN ate Collected: 0/0/ 0:0 ate Received: 0/0/ : Lab Sample I: 0-- Method: 0B - Volatile Organic Compounds (GC/MS) ML il Fac Benzene 0.0 U ug/l 0// 0: Bromobenzene 0. U.0 0. ug/l 0// 0: Chlorobromomethane 0. U.0 0. ug/l 0// 0: ichlorobromomethane 0. U.0 0. ug/l 0// 0: Bromoform 0. U.0 0. ug/l 0// 0: Bromomethane. U.0. ug/l 0// 0: n-butylbenzene 0. U.0 0. ug/l 0// 0: sec-butylbenzene 0. U.0 0. ug/l 0// 0: tert-butylbenzene 0. U.0 0. ug/l 0// 0: Page of //0

86 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-IN ate Collected: 0/0/ 0:0 ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- Carbon tetrachloride 0. U.0 0. ug/l 0// 0: Chlorobenzene 0. U Chloroethane. U Chloroform 0.0 U Chloromethane.0 U -Chlorotoluene 0. U -Chlorotoluene 0. U Chlorodibromomethane 0. U,-ibromo--Chloropropane. U Ethylene ibromide 0.0 U ibromomethane 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U ichlorodifluoromethane. U,-ichloroethane 0. U,-ichloroethane 0. U,-ichloroethene 0. U cis-,-ichloroethene 0. U trans-,-ichloroethene 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropene 0. U cis-,-ichloropropene 0. U trans-,-ichloropropene 0. U Ethylbenzene 0. U Hexachlorobutadiene 0.0 U Isopropylbenzene 0. U -Isopropyltoluene 0. U Methylene Chloride.0 U Naphthalene. U N-Propylbenzene 0. U Styrene 0. U,,,-Tetrachloroethane 0. U,,,-Tetrachloroethane 0. U Tetrachloroethene 0.0 U Toluene 0. U,,-Trichlorobenzene 0. U,,-Trichlorobenzene 0. U,,-Trichloroethane 0. U,,-Trichloroethane 0. U Trichloroethene 0.0 U Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U il Fac.0 0. ug/l 0// 0:.0. ug/l 0// 0: ug/l 0// 0:.0.0 ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0. ug/l 0// 0: ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0.0 ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0: ug/l 0// 0: 0 Page of //0

87 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-IN ate Collected: 0/0/ 0:0 ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- Acetone. U 0. ug/l 0// 0: -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U Surrogate %Recovery il Fac 0. ug/l 0// 0: 0. ug/l 0// 0:.0.0 ug/l 0// 0: 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0: Toluene-d (Surr) // 0: -Bromofluorobenzene // 0: ibromofluoromethane // 0: Method: 0C - Semivolatile Organic Compounds (GC/MS),,-Trichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :0,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,'-oxybis[-chloropropane] 0. U,,-Trichlorophenol. U,,-Trichlorophenol 0. U,-ichlorophenol 0. U,-imethylphenol 0. U,-initrophenol. U,-initrotoluene. U,-initrotoluene 0. U -Chloronaphthalene 0.0 U -Chlorophenol 0. U -Methylnaphthalene 0. U -Methylphenol 0. U -Nitroaniline 0. U -Nitrophenol 0. U & Methylphenol 0. U,'-ichlorobenzidine 0. U -Nitroaniline. U,-initro--methylphenol 0. U -Bromophenyl phenyl ether. U -Chloro--methylphenol. U -Chloroaniline 0. U -Chlorophenyl phenyl ether 0. U -Nitroaniline. U -Nitrophenol. U Acenaphthene 0.0 U Acenaphthylene 0. U Anthracene. U Benzidine. U Benzo[a]anthracene 0. U Benzo[a]pyrene.0 U Benzo[b]fluoranthene 0. U ML il Fac il Fac 0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0.0 ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0 Page of //0

88 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-IN ate Collected: 0/0/ 0:0 ate Received: 0/0/ : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- Benzo[g,h,i]perylene. U 0. ug/l 0/0/ :0 0// :0 Benzo[k]fluoranthene. U Benzoic acid. U Benzyl alcohol 0. U Bis(-chloroethoxy)methane 0. U Bis(-chloroethyl)ether 0. U Bis(-ethylhexyl) phthalate. I V Butyl benzyl phthalate 0. U Chrysene 0. U ibenz(a,h)anthracene. U ibenzofuran 0.0 U iethyl phthalate. U imethyl phthalate. U i-n-butyl phthalate. U i-n-octyl phthalate 0. U Fluoranthene. U Fluorene. U Hexachlorobenzene. U Hexachlorobutadiene 0. U Hexachlorocyclopentadiene 0. U Hexachloroethane 0. U Indeno[,,-cd]pyrene. U Isophorone 0. U Naphthalene 0. U Nitrobenzene 0. U N-Nitrosodimethylamine. U N-Nitrosodi-n-propylamine 0. U N-Nitrosodiphenylamine. U Pentachlorophenol. U Phenanthrene. U Phenol 0. U Pyrene.0 U il Fac 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// :0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// :0 0.0 ug/l 0/0/ :0 0// :0 0 Surrogate %Recovery,,-Tribromophenol - 0/0/ :0 0// :0 -Fluorobiphenyl - 0/0/ :0 0// :0 -Fluorophenol - 0 0/0/ :0 0// :0 Nitrobenzene-d 0-0/0/ :0 0// :0 Phenol-d - 0 0/0/ :0 0// :0 Terphenyl-d /0/ :0 0// :0 il Fac Method: 00. Rev. - Metals (ICP) - Total Recoverable ML il Fac Chromium U mg/l 0/0/ 0: 0// : Copper 0.00 U mg/l 0/0/ 0: 0// : Iron 0.00 U mg/l 0/0/ 0: 0// : Lead 0.00 I mg/l 0/0/ 0: 0// : Page of //0

89 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-IN ate Collected: 0/0/ 0:0 ate Received: 0/0/ : General Chemistry ML Lab Sample I: 0-- HEM (Oil & Grease) 0. I. 0. mg/l 0// : Chloride 0 Sulfate. U Nitrogen, Kjeldahl 0. I Nitrate Nitrite as N 0.0 U Nitrite as N 0.0 U Nitrate as N 0.0 U Phosphorus 0.0 I Total Organic Carbon. Color.0 ph at time of analysis. Alkalinity 0 Total issolved Solids 0 Total Suspended Solids.0 Chlorine, Total Residual.0 U Biochemical Oxygen emand.0 U General Chemistry - issolved il Fac.0.0 mg/l 0// :0.0. mg/l 0// : mg/l 0// : 0// : mg/l 0/0/ 0: mg/l 0/0/ 0: mg/l 0/0/ 0: mg/l 0// : 0// : mg/l 0// :0.0.0 PCU 0/0/ 0:0.0.0 SU 0/0/ 0:0.0.0 mg/l 0/0/ 0: 0 0 mg/l 0// :.0.0 mg/l 0// 0:.0.0 mg/l 0/0/ 0: mg/l 0/0/ 0: Orthophosphate 0.0 J J U mg/l 0/0/ :0 ML il Fac 0 Method: SM B - Coliforms, Total (Membrane Filter) ML il Fac Coliform, Total CFU/00mL 0/0/ : 0 Method: SM - Coliforms, Fecal (Membrane Filter) ML il Fac Coliform, Fecal.0 U.0.0 CFU/00mL 0/0/ : Client Sample I: SW-OUT ate Collected: 0/0/ : ate Received: 0/0/ : Lab Sample I: 0-- Method: 0B - Volatile Organic Compounds (GC/MS) ML il Fac Benzene 0.0 U ug/l 0// : Bromobenzene 0. U.0 0. ug/l 0// : Chlorobromomethane 0. U.0 0. ug/l 0// : ichlorobromomethane 0. U.0 0. ug/l 0// : Bromoform 0. U.0 0. ug/l 0// : Bromomethane. U.0. ug/l 0// : n-butylbenzene 0. U.0 0. ug/l 0// : sec-butylbenzene 0. U.0 0. ug/l 0// : tert-butylbenzene 0. U.0 0. ug/l 0// : Carbon tetrachloride 0. U.0 0. ug/l 0// : Chlorobenzene 0. U.0 0. ug/l 0// : Chloroethane. U.0. ug/l 0// : Chloroform 0.0 U ug/l 0// : Chloromethane.0 U.0.0 ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : Page of //0

90 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-OUT ate Collected: 0/0/ : ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- -Chlorotoluene 0. U.0 0. ug/l 0// : Chlorodibromomethane 0. U,-ibromo--Chloropropane. U Ethylene ibromide 0.0 U ibromomethane 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U ichlorodifluoromethane. U,-ichloroethane 0. U,-ichloroethane 0. U,-ichloroethene 0. U cis-,-ichloroethene 0. U trans-,-ichloroethene 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropene 0. U cis-,-ichloropropene 0. U trans-,-ichloropropene 0. U Ethylbenzene 0. U Hexachlorobutadiene 0.0 U Isopropylbenzene 0. U -Isopropyltoluene 0. U Methylene Chloride.0 U Naphthalene. U N-Propylbenzene 0. U Styrene 0. U,,,-Tetrachloroethane 0. U,,,-Tetrachloroethane 0. U Tetrachloroethene 0.0 U Toluene 0. U,,-Trichlorobenzene 0. U,,-Trichlorobenzene 0. U,,-Trichloroethane 0. U,,-Trichloroethane 0. U Trichloroethene 0.0 U Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U il Fac.0 0. ug/l 0// :.0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : 0. ug/l 0// : 0. ug/l 0// : 0. ug/l 0// :.0.0 ug/l 0// : 0. ug/l 0// :.0 0. ug/l 0// : 0 Page of //0

91 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-OUT ate Collected: 0/0/ : ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- m-xylene & p-xylene 0.0 U ug/l 0// : Surrogate %Recovery Toluene-d (Surr) // : -Bromofluorobenzene // : ibromofluoromethane 0-0 0// : Method: 0C - Semivolatile Organic Compounds (GC/MS),,-Trichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,'-oxybis[-chloropropane] 0. U,,-Trichlorophenol. U,,-Trichlorophenol 0. U,-ichlorophenol 0. U,-imethylphenol 0. U,-initrophenol. U,-initrotoluene. U,-initrotoluene 0. U -Chloronaphthalene 0.0 U -Chlorophenol 0. U -Methylnaphthalene 0. U -Methylphenol 0. U -Nitroaniline 0. U -Nitrophenol 0. U & Methylphenol 0. U,'-ichlorobenzidine 0. U -Nitroaniline. U,-initro--methylphenol 0. U -Bromophenyl phenyl ether. U -Chloro--methylphenol. U -Chloroaniline 0. U -Chlorophenyl phenyl ether 0. U -Nitroaniline. U -Nitrophenol. U Acenaphthene 0.0 U Acenaphthylene 0. U Anthracene. U Benzidine. U Benzo[a]anthracene 0. U Benzo[a]pyrene.0 U Benzo[b]fluoranthene 0. U Benzo[g,h,i]perylene. U Benzo[k]fluoranthene. U Benzoic acid. U Benzyl alcohol 0. U Bis(-chloroethoxy)methane 0. U Bis(-chloroethyl)ether 0. U ML il Fac il Fac il Fac 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0.0 ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 Page of //0

92 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-OUT ate Collected: 0/0/ : ate Received: 0/0/ : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- Bis(-ethylhexyl) phthalate 0. I V 0 0. ug/l 0/0/ :0 0// : Butyl benzyl phthalate 0. U Chrysene 0. U ibenz(a,h)anthracene. U ibenzofuran 0.0 U iethyl phthalate. U imethyl phthalate. U i-n-butyl phthalate. U i-n-octyl phthalate 0. U Fluoranthene. U Fluorene. U Hexachlorobenzene. U Hexachlorobutadiene 0. U Hexachlorocyclopentadiene 0. U Hexachloroethane 0. U Indeno[,,-cd]pyrene. U Isophorone 0. U Naphthalene 0. U Nitrobenzene 0. U N-Nitrosodimethylamine. U N-Nitrosodi-n-propylamine 0. U N-Nitrosodiphenylamine. U Pentachlorophenol. U Phenanthrene. U Phenol 0. U Pyrene.0 U il Fac 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// : 0 0. ug/l 0/0/ :0 0// : 0.0 ug/l 0/0/ :0 0// : 0 Surrogate %Recovery,,-Tribromophenol - 0/0/ :0 0// : -Fluorobiphenyl - 0/0/ :0 0// : -Fluorophenol - 0 0/0/ :0 0// : Nitrobenzene-d - 0/0/ :0 0// : Phenol-d - 0 0/0/ :0 0// : Terphenyl-d 0-0 0/0/ :0 0// : il Fac Method: 00. Rev. - Metals (ICP) - Total Recoverable ML il Fac Chromium 0.00 I mg/l 0/0/ 0: 0// : Copper 0.00 U mg/l 0/0/ 0: 0// : Iron mg/l 0/0/ 0: 0// : Lead U mg/l 0/0/ 0: 0// : General Chemistry ML il Fac HEM (Oil & Grease). I.0 0. mg/l 0// : Chloride mg/l 0// : Sulfate 0.0. mg/l 0// : Nitrogen, Kjeldahl mg/l 0// : 0// : Nitrate Nitrite as N 0.0 U mg/l 0/0/ 0:0 Nitrite as N 0.0 U mg/l 0/0/ 0:0 Page of //0

93 Client Sample s TestAmerica Job I: 0-- Client Sample I: SW-OUT ate Collected: 0/0/ : ate Received: 0/0/ : General Chemistry (Continued) ML Lab Sample I: 0-- Nitrate as N 0.0 U mg/l 0/0/ 0:0 Phosphorus 0.0 I Total Organic Carbon. Color 0 ph at time of analysis. Alkalinity Total issolved Solids 00 Total Suspended Solids. Chlorine, Total Residual.0 U Biochemical Oxygen emand.0 U General Chemistry - issolved il Fac mg/l 0// : 0// : mg/l 0// : 0 0 PCU 0/0/ 0: SU 0/0/ 0: mg/l 0/0/ 0:.0.0 mg/l 0// :.0.0 mg/l 0// 0:.0.0 mg/l 0/0/ 0: mg/l 0/0/ 0: Orthophosphate 0.0 U mg/l 0/0/ :0 Method: SM B - Coliforms, Total (Membrane Filter) ML ML Coliform, Total CFU/00mL 0/0/ : 0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal.0 U.0.0 CFU/00mL 0/0/ : ML il Fac il Fac il Fac 0 Client Sample I: W-OUT ate Collected: 0/0/ :0 ate Received: 0/0/ : Lab Sample I: 0-- Method: 0B - Volatile Organic Compounds (GC/MS) ML il Fac Benzene 0.0 U ug/l 0// : Bromobenzene 0. U.0 0. ug/l 0// : Chlorobromomethane 0. U.0 0. ug/l 0// : ichlorobromomethane 0. U.0 0. ug/l 0// : Bromoform 0. U.0 0. ug/l 0// : Bromomethane. U.0. ug/l 0// : n-butylbenzene 0. U.0 0. ug/l 0// : sec-butylbenzene 0. U.0 0. ug/l 0// : tert-butylbenzene 0. U.0 0. ug/l 0// : Carbon tetrachloride 0. U.0 0. ug/l 0// : Chlorobenzene 0. U.0 0. ug/l 0// : Chloroethane. U.0. ug/l 0// : Chloroform 0.0 U ug/l 0// : Chloromethane.0 U.0.0 ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : -Chlorotoluene 0. U.0 0. ug/l 0// : Chlorodibromomethane 0. U.0 0. ug/l 0// :,-ibromo--chloropropane. U.0. ug/l 0// : Ethylene ibromide 0.0 U ug/l 0// : ibromomethane 0. U.0 0. ug/l 0// :,-ichlorobenzene 0. U.0 0. ug/l 0// : Page of //0

94 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-OUT ate Collected: 0/0/ :0 ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0--,-ichlorobenzene 0. U.0 0. ug/l 0// :,-ichlorobenzene 0. U ichlorodifluoromethane. U,-ichloroethane 0. U,-ichloroethane 0. U,-ichloroethene 0. U cis-,-ichloroethene 0. U trans-,-ichloroethene 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropene 0. U cis-,-ichloropropene 0. U trans-,-ichloropropene 0. U Ethylbenzene 0. U Hexachlorobutadiene 0.0 U Isopropylbenzene 0. U -Isopropyltoluene 0. U Methylene Chloride.0 U Naphthalene. U N-Propylbenzene 0. U Styrene 0. U,,,-Tetrachloroethane 0. U,,,-Tetrachloroethane 0. U Tetrachloroethene 0.0 U Toluene 0. U,,-Trichlorobenzene 0. U,,-Trichlorobenzene 0. U,,-Trichloroethane 0. U,,-Trichloroethane 0. U Trichloroethene 0.0 U Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U il Fac.0 0. ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0.0 ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// :.0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : ug/l 0// : 0. ug/l 0// : 0. ug/l 0// : 0. ug/l 0// :.0.0 ug/l 0// : 0. ug/l 0// :.0 0. ug/l 0// : ug/l 0// : 0 Surrogate %Recovery Toluene-d (Surr) // : -Bromofluorobenzene // : ibromofluoromethane // : il Fac Page 0 of //0

95 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-OUT ate Collected: 0/0/ :0 ate Received: 0/0/ : Method: 0C - Semivolatile Organic Compounds (GC/MS) ML Lab Sample I: 0--,,-Trichlorobenzene 0. U. 0. ug/l 0/0/ :0 0// :,-ichlorobenzene 0. U,-ichlorobenzene 0.0 U,-ichlorobenzene 0. U,'-oxybis[-chloropropane] 0. U,,-Trichlorophenol. U,,-Trichlorophenol 0. U,-ichlorophenol 0. U,-imethylphenol 0. U,-initrophenol. U,-initrotoluene. U,-initrotoluene 0. U -Chloronaphthalene 0. U -Chlorophenol 0.0 U -Methylnaphthalene 0. U -Methylphenol 0. U -Nitroaniline 0. U -Nitrophenol 0. U & Methylphenol 0. U,'-ichlorobenzidine 0. U -Nitroaniline. U,-initro--methylphenol 0. U -Bromophenyl phenyl ether. U -Chloro--methylphenol. U -Chloroaniline 0. U -Chlorophenyl phenyl ether 0. U -Nitroaniline. U -Nitrophenol. U Acenaphthene 0. U Acenaphthylene 0. U Anthracene. U Benzidine. U Benzo[a]anthracene 0. U Benzo[a]pyrene 0. U Benzo[b]fluoranthene 0. U Benzo[g,h,i]perylene. U Benzo[k]fluoranthene. U Benzoic acid. U Benzyl alcohol 0. U Bis(-chloroethoxy)methane 0. U Bis(-chloroethyl)ether 0. U Bis(-ethylhexyl) phthalate. I V Butyl benzyl phthalate 0. U Chrysene 0. U ibenz(a,h)anthracene. U ibenzofuran 0. U iethyl phthalate. U imethyl phthalate. U i-n-butyl phthalate. U il Fac. 0. ug/l 0/0/ :0 0// :. 0.0 ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0.0 ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// : 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// : 0 Page of //0

96 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-OUT ate Collected: 0/0/ :0 ate Received: 0/0/ : Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0-- i-n-octyl phthalate 0. U. 0. ug/l 0/0/ :0 0// : Fluoranthene. U Fluorene. U Hexachlorobenzene. U Hexachlorobutadiene 0.0 U Hexachlorocyclopentadiene 0.0 U Hexachloroethane 0. U Indeno[,,-cd]pyrene. U Isophorone 0. U Naphthalene 0. U Nitrobenzene 0. U N-Nitrosodimethylamine.0 U N-Nitrosodi-n-propylamine 0. U N-Nitrosodiphenylamine. U Pentachlorophenol. U Phenanthrene. U Phenol 0. U Pyrene 0. U Surrogate %Recovery il Fac.. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. 0.0 ug/l 0/0/ :0 0// :. 0.0 ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :..0 ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. ug/l 0/0/ :0 0// :.. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :. 0. ug/l 0/0/ :0 0// :,,-Tribromophenol - 0/0/ :0 0// : -Fluorobiphenyl - 0/0/ :0 0// : -Fluorophenol - 0 0/0/ :0 0// : Nitrobenzene-d - 0/0/ :0 0// : Phenol-d - 0 0/0/ :0 0// : Terphenyl-d 0-0 0/0/ :0 0// : il Fac 0 Method: 00. Rev. - Metals (ICP) - Total Recoverable ML il Fac Chromium I mg/l 0/0/ 0: 0// : Copper 0.00 I mg/l 0/0/ 0: 0// : Iron mg/l 0/0/ 0: 0// : Lead U mg/l 0/0/ 0: 0// : General Chemistry ML il Fac HEM (Oil & Grease) 0. I. 0. mg/l 0// : Chloride.0.0 mg/l 0// : Sulfate. U.0. mg/l 0// : Nitrogen, Kjeldahl mg/l 0// : 0// : Nitrate Nitrite as N 0.0 U mg/l 0/0/ 0:0 Nitrite as N 0.0 U mg/l 0/0/ 0:0 Nitrate as N 0.0 U mg/l 0/0/ 0:0 Phosphorus mg/l 0// : 0// : Total Organic Carbon mg/l 0// : Color.0.0 PCU 0/0/ 0:0 ph at time of analysis..0.0 SU 0/0/ 0:0 Alkalinity mg/l 0/0/ 0: Total issolved Solids mg/l 0// : Total Suspended Solids..0.0 mg/l 0// 0: Page of //0

97 Client Sample s TestAmerica Job I: 0-- Client Sample I: W-OUT ate Collected: 0/0/ :0 ate Received: 0/0/ : General Chemistry (Continued) ML Lab Sample I: 0-- Chlorine, Total Residual.0 U.0.0 mg/l 0/0/ 0:00 Biochemical Oxygen emand.0 U General Chemistry - issolved il Fac.0.0 mg/l 0/0/ 0: Orthophosphate 0.0 U mg/l 0/0/ :0 Method: SM B - Coliforms, Total (Membrane Filter) ML ML Coliform, Total CFU/00mL 0/0/ : 0 Method: SM - Coliforms, Fecal (Membrane Filter) Coliform, Fecal CFU/00mL 0/0/ : Client Sample I: Trip Blank ate Collected: 0/0/ 00:00 ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) ML ML il Fac il Fac il Fac Lab Sample I: 0-- Benzene 0.0 U ug/l 0// 0: Bromobenzene 0. U Chlorobromomethane 0. U ichlorobromomethane 0. U Bromoform 0. U Bromomethane. U n-butylbenzene 0. U sec-butylbenzene 0. U tert-butylbenzene 0. U Carbon tetrachloride 0. U Chlorobenzene 0. U Chloroethane. U Chloroform 0.0 U Chloromethane.0 U -Chlorotoluene 0. U -Chlorotoluene 0. U Chlorodibromomethane 0. U,-ibromo--Chloropropane. U Ethylene ibromide 0.0 U ibromomethane 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U,-ichlorobenzene 0. U ichlorodifluoromethane. U,-ichloroethane 0. U,-ichloroethane 0. U,-ichloroethene 0. U cis-,-ichloroethene 0. U trans-,-ichloroethene 0. U il Fac.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0. ug/l 0// 0: ug/l 0// 0:.0.0 ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0. ug/l 0// 0: ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: 0 Page of //0

98 Client Sample s TestAmerica Job I: 0-- Client Sample I: Trip Blank ate Collected: 0/0/ 00:00 ate Received: 0/0/ : Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) ML Lab Sample I: 0--,-ichloropropane 0. U.0 0. ug/l 0// 0:,-ichloropropane 0. U,-ichloropropane 0. U,-ichloropropene 0. U cis-,-ichloropropene 0. U trans-,-ichloropropene 0. U Ethylbenzene 0. U Hexachlorobutadiene 0.0 U Isopropylbenzene 0. U -Isopropyltoluene 0. U Methylene Chloride.0 U Naphthalene. U N-Propylbenzene 0. U Styrene 0. U,,,-Tetrachloroethane 0. U,,,-Tetrachloroethane 0. U Tetrachloroethene 0.0 U Toluene 0. U,,-Trichlorobenzene 0. U,,-Trichlorobenzene 0. U,,-Trichloroethane 0. U,,-Trichloroethane 0. U Trichloroethene 0.0 U Trichlorofluoromethane. U,,-Trichloropropane 0. U,,-Trimethylbenzene 0. U,,-Trimethylbenzene 0. U Vinyl chloride 0.0 U o-xylene 0.0 U Acetone. U -Butanone (MEK). U -Methyl--pentanone (MIBK). U Carbon disulfide.0 U -Hexanone. U Methyl tert-butyl ether 0. U m-xylene & p-xylene 0.0 U il Fac.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0.0 ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0:.0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0: ug/l 0// 0: 0. ug/l 0// 0: 0. ug/l 0// 0: 0. ug/l 0// 0:.0.0 ug/l 0// 0: 0. ug/l 0// 0:.0 0. ug/l 0// 0: ug/l 0// 0: 0 Surrogate %Recovery Toluene-d (Surr) // 0: -Bromofluorobenzene // 0: ibromofluoromethane // 0: il Fac Page of //0

99 Method: 0B - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 0-/ Analysis Batch: MB MB QC Sample s ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type: Benzene 0.0 U ug/l 0// 0: Bromobenzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane n-butylbenzene sec-butylbenzene tert-butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane -Chlorotoluene -Chlorotoluene Chlorodibromomethane,-ibromo--Chloropropane Ethylene ibromide ibromomethane,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene ichlorodifluoromethane,-ichloroethane,-ichloroethane,-ichloroethene cis-,-ichloroethene trans-,-ichloroethene,-ichloropropane,-ichloropropane,-ichloropropane,-ichloropropene cis-,-ichloropropene trans-,-ichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene -Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene,,,-Tetrachloroethane,,,-Tetrachloroethane Tetrachloroethene Toluene,,-Trichlorobenzene il Fac 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0.0 U ug/l 0// 0:.0 U.0.0 ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0:.0 U.0.0 ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0 Page of //0

100 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MB 0-/ Analysis Batch: MB MB ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type:,,-Trichlorobenzene 0. U.0 0. ug/l 0// 0:,,-Trichloroethane,,-Trichloroethane Trichloroethene Trichlorofluoromethane,,-Trichloropropane,,-Trimethylbenzene,,-Trimethylbenzene Vinyl chloride o-xylene Acetone -Butanone (MEK) -Methyl--pentanone (MIBK) Carbon disulfide -Hexanone Methyl tert-butyl ether m-xylene & p-xylene Surrogate il Fac 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0:. U.0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: 0.0 U ug/l 0// 0:. U 0. ug/l 0// 0:. U 0. ug/l 0// 0:. U 0. ug/l 0// 0:.0 U.0.0 ug/l 0// 0:. U 0. ug/l 0// 0: 0. U.0 0. ug/l 0// 0: 0.0 U ug/l 0// 0: MB %Recovery MB Toluene-d (Surr) // 0: -Bromofluorobenzene // 0: ibromofluoromethane // 0: il Fac 0 Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Spike LCS LCS Added %Rec Benzene 0.0. ug/l 0 - Bromobenzene ug/l Chlorobromomethane 0.0. ug/l 0-0 ichlorobromomethane ug/l Bromoform 0.0. ug/l - 0 Bromomethane 0.0. ug/l - 0 n-butylbenzene ug/l 0 - sec-butylbenzene ug/l 0 - tert-butylbenzene ug/l 0-0 Carbon tetrachloride 0.0. ug/l 0 - Chlorobenzene ug/l Chloroethane 0.0. ug/l - 0 Chloroform ug/l 0-0 Chloromethane ug/l 0-0 -Chlorotoluene ug/l Chlorotoluene ug/l Chlorodibromomethane ug/l 0 0-0,-ibromo--Chloropropane 0.0. ug/l - 0 Ethylene ibromide ug/l 0-0 ibromomethane 0.0. ug/l Page of //0

101 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 0-/ Analysis Batch: Spike Added TestAmerica Job I: 0-- Client Sample I: Lab Control Sample Prep Type:,-ichlorobenzene ug/l LCS LCS %Rec,-ichlorobenzene ug/l 0 0-0,-ichlorobenzene 0.0. ug/l 0-0 ichlorodifluoromethane ug/l 00 -,-ichloroethane ug/l 0-0,-ichloroethane 0.0. ug/l 0 0-0,-ichloroethene 0.0. ug/l 0-0 cis-,-ichloroethene 0.0. ug/l 0-0 trans-,-ichloroethene ug/l 0 -,-ichloropropane 0.0. ug/l 0 0-0,-ichloropropane ug/l 0 0-0,-ichloropropane 0.0. ug/l -,-ichloropropene 0.0. ug/l 0 - cis-,-ichloropropene 0.0. ug/l trans-,-ichloropropene 0.0. ug/l - 0 Ethylbenzene ug/l Hexachlorobutadiene 0.0. ug/l - Isopropylbenzene ug/l 0-0 -Isopropyltoluene 0.0. ug/l 0 - Methylene Chloride 0.0. ug/l - 0 Naphthalene ug/l N-Propylbenzene 0.0. ug/l 0-0 Styrene ug/l 0 -,,,-Tetrachloroethane ug/l 0 0-0,,,-Tetrachloroethane 0.0. ug/l 0-0 Tetrachloroethene ug/l Toluene ug/l 0 0 -,,-Trichlorobenzene ug/l 0 -,,-Trichlorobenzene ug/l 0-0,,-Trichloroethane 0.0. ug/l 0 -,,-Trichloroethane ug/l Trichloroethene ug/l 0 - Trichlorofluoromethane 0.0. ug/l -,,-Trichloropropane ug/l 0-0,,-Trimethylbenzene ug/l 0 0 -,,-Trimethylbenzene ug/l 0 - Vinyl chloride ug/l 0 - o-xylene ug/l 0-0 Acetone 0.0. ug/l - -Butanone (MEK) 0.0. ug/l 0-0 -Methyl--pentanone (MIBK) 0.0. ug/l 0 - Carbon disulfide 0.0. ug/l 0-0 -Hexanone 0.0. ug/l 0 - Methyl tert-butyl ether 0.0. ug/l Surrogate LCS %Recovery LCS Toluene-d (Surr) Bromofluorobenzene Page of //0

102 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 0-/ Analysis Batch: Surrogate LCS %Recovery LCS ibromofluoromethane Lab Sample I: 0--H- MS Analysis Batch: Sample Sample Spike Added TestAmerica Job I: 0-- Client Sample I: Lab Control Sample Prep Type: Benzene 0.0 U ug/l 0 - MS MS %Rec Bromobenzene 0. U ug/l Chlorobromomethane 0. U ug/l ichlorobromomethane 0. U 0.0. ug/l Bromoform 0. U ug/l 0-0 Bromomethane. U 0.0. ug/l - 0 n-butylbenzene 0. U 0.0. ug/l 0 - sec-butylbenzene 0. U ug/l 0 - tert-butylbenzene 0. U 0.0. ug/l 0-0 Carbon tetrachloride 0. U ug/l 0 - Chlorobenzene 0. U ug/l Chloroethane. U 0.0. ug/l - 0 Chloroform 0.0 U ug/l 0-0 Chloromethane.0 U 0.0. ug/l - 0 -Chlorotoluene 0. U ug/l Chlorotoluene 0. U 0.0. ug/l Chlorodibromomethane 0. U 0.0. ug/l 0 0-0,-ibromo--Chloropropane. U 0.0. ug/l 0-0 Ethylene ibromide 0.0 U 0.0. ug/l 0-0 ibromomethane 0. U 0.0. ug/l 0-0,-ichlorobenzene 0. U ug/l 0 0-0,-ichlorobenzene 0. U ug/l 0 0-0,-ichlorobenzene 0. U ug/l ichlorodifluoromethane. U 0.0. ug/l -,-ichloroethane 0. U ug/l 0-0,-ichloroethane 0. U 0.0. ug/l 0 0-0,-ichloroethene 0. U ug/l 0-0 cis-,-ichloroethene 0. U ug/l 0-0 trans-,-ichloroethene 0. U ug/l 00 -,-ichloropropane 0. U 0.0. ug/l 0-0,-ichloropropane 0. U ug/l 0-0,-ichloropropane 0. U 0.0. ug/l 0 -,-ichloropropene 0. U ug/l 0 - cis-,-ichloropropene 0. U 0.0. ug/l 0-0 trans-,-ichloropropene 0. U 0.0. ug/l - 0 Ethylbenzene 0. U ug/l Hexachlorobutadiene 0.0 U ug/l 0 - Isopropylbenzene 0. U 0.0. ug/l 0-0 -Isopropyltoluene 0. U 0.0. ug/l 0 - Methylene Chloride.0 U 0.0. ug/l - 0 Naphthalene. U 0.0. ug/l 0 - Client Sample I: Matrix Spike Prep Type: 0 Page of //0

103 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: 0--H- MS Analysis Batch: Sample Sample Spike Added TestAmerica Job I: 0-- N-Propylbenzene 0. U 0.0. ug/l 0-0 MS MS %Rec Styrene 0. U ug/l 0 -,,,-Tetrachloroethane 0. U ug/l 0 0-0,,,-Tetrachloroethane 0. U ug/l Tetrachloroethene 0.0 U 0.0. ug/l Toluene 0. U 0.0. ug/l 0 0 -,,-Trichlorobenzene 0. U 0.0. ug/l 0 -,,-Trichlorobenzene 0. U 0.0. ug/l 0-0,,-Trichloroethane 0. U ug/l 0 -,,-Trichloroethane 0. U 0.0. ug/l 0-0 Trichloroethene 0.0 U ug/l 0 - Trichlorofluoromethane. U 0.0. ug/l -,,-Trichloropropane 0. U 0.0. ug/l 0-0,,-Trimethylbenzene 0. U ug/l 0 0 -,,-Trimethylbenzene 0. U ug/l 0 - Vinyl chloride 0.0 U ug/l - o-xylene 0.0 U ug/l 0-0 Acetone. U 0.0. ug/l - -Butanone (MEK). U 0.0. ug/l - 0 -Methyl--pentanone (MIBK). J U J ug/l - Carbon disulfide.0 U 0.0. ug/l Hexanone. U 0.0. ug/l 0 - Methyl tert-butyl ether 0. U 0.0. ug/l - 0 Client Sample I: Matrix Spike Prep Type: 0 Surrogate Toluene-d (Surr) MS %Recovery MS -Bromofluorobenzene ibromofluoromethane 0-0 Lab Sample I: 0--- U Analysis Batch: Sample Sample Client Sample I: uplicate Prep Type: Benzene 0.0 U 0.0 U ug/l NC 0 U U Bromobenzene 0. U 0. U ug/l NC 0 Chlorobromomethane 0. U 0. U ug/l NC 0 ichlorobromomethane 0. U 0. U ug/l NC 0 Bromoform 0. U 0. U ug/l NC 0 Bromomethane. U. U ug/l NC 0 n-butylbenzene 0. U 0. U ug/l NC 0 sec-butylbenzene 0. U 0. U ug/l NC 0 tert-butylbenzene 0. U 0. U ug/l NC 0 Carbon tetrachloride 0. U 0. U ug/l NC 0 Chlorobenzene 0. U 0. U ug/l NC 0 Chloroethane. U. U ug/l NC 0 Chloroform 0.0 U 0.0 U ug/l NC 0 Chloromethane.0 U.0 U ug/l NC 0 RP RP Limit Page of //0

104 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: 0--- U Analysis Batch: Sample Sample TestAmerica Job I: 0-- Client Sample I: uplicate Prep Type: -Chlorotoluene 0. U 0. U ug/l NC 0 U U -Chlorotoluene 0. U 0. U ug/l NC 0 Chlorodibromomethane 0. U 0. U ug/l NC 0,-ibromo--Chloropropane. U. U ug/l NC 0 Ethylene ibromide 0.0 U 0.0 U ug/l NC 0 ibromomethane 0. U 0. U ug/l NC 0,-ichlorobenzene 0. U 0. U ug/l NC 0,-ichlorobenzene 0. U 0. U ug/l NC 0,-ichlorobenzene 0. U 0. U ug/l NC 0 ichlorodifluoromethane. U. U ug/l NC 0,-ichloroethane 0. U 0. U ug/l NC 0,-ichloroethane 0. U 0. U ug/l NC 0,-ichloroethene 0. U 0. U ug/l NC 0 cis-,-ichloroethene 0. U 0. U ug/l NC 0 trans-,-ichloroethene 0. U 0. U ug/l NC 0,-ichloropropane 0. U 0. U ug/l NC 0,-ichloropropane 0. U 0. U ug/l NC 0,-ichloropropane 0. U 0. U ug/l NC 0,-ichloropropene 0. U 0. U ug/l NC 0 cis-,-ichloropropene 0. U 0. U ug/l NC 0 trans-,-ichloropropene 0. U 0. U ug/l NC 0 Ethylbenzene 0. U 0. U ug/l NC 0 Hexachlorobutadiene 0.0 U 0.0 U ug/l NC 0 Isopropylbenzene 0. U 0. U ug/l NC 0 -Isopropyltoluene 0. U 0. U ug/l NC 0 Methylene Chloride.0 U.0 U ug/l NC 0 Naphthalene. U. U ug/l NC 0 N-Propylbenzene 0. U 0. U ug/l NC 0 Styrene 0. U 0. U ug/l NC 0,,,-Tetrachloroethane 0. U 0. U ug/l NC 0,,,-Tetrachloroethane 0. U 0. U ug/l NC 0 Tetrachloroethene 0.0 U 0.0 U ug/l NC 0 Toluene 0. U 0. U ug/l NC 0,,-Trichlorobenzene 0. U 0. U ug/l NC 0,,-Trichlorobenzene 0. U 0. U ug/l NC 0,,-Trichloroethane 0. U 0. U ug/l NC 0,,-Trichloroethane 0. U 0. U ug/l NC 0 Trichloroethene 0.0 U 0.0 U ug/l NC 0 Trichlorofluoromethane. U. U ug/l NC 0,,-Trichloropropane 0. U 0. U ug/l NC 0,,-Trimethylbenzene 0. U 0. U ug/l NC 0,,-Trimethylbenzene 0. U 0. U ug/l NC 0 Vinyl chloride 0.0 U 0.0 U ug/l NC 0 o-xylene 0.0 U 0.0 U ug/l NC 0 Acetone. U 0. I ug/l NC 0 -Butanone (MEK). U. U ug/l NC 0 -Methyl--pentanone (MIBK). J U. U ug/l NC 0 Carbon disulfide.0 U.0 U ug/l NC 0 RP RP Limit 0 Page 0 of //0

105 QC Sample s Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: 0--- U Analysis Batch: Sample Sample TestAmerica Job I: 0-- Client Sample I: uplicate Prep Type: -Hexanone. U. U ug/l NC 0 U U Methyl tert-butyl ether 0. U 0. U ug/l NC 0 m-xylene & p-xylene 0.0 U 0.0 U ug/l NC 0 Surrogate Toluene-d (Surr) U %Recovery U -Bromofluorobenzene ibromofluoromethane Method: 0C - Semivolatile Organic Compounds (GC/MS) Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB,,-Trichlorobenzene 0. U 0 0. ug/l 0/0/ :0 0// :,-ichlorobenzene,-ichlorobenzene,-ichlorobenzene,'-oxybis[-chloropropane],,-trichlorophenol,,-trichlorophenol,-ichlorophenol,-imethylphenol,-initrophenol,-initrotoluene,-initrotoluene -Chloronaphthalene -Chlorophenol -Methylnaphthalene -Methylphenol -Nitroaniline -Nitrophenol & Methylphenol,'-ichlorobenzidine -Nitroaniline,-initro--methylphenol -Bromophenyl phenyl ether -Chloro--methylphenol -Chloroaniline -Chlorophenyl phenyl ether -Nitroaniline -Nitrophenol Acenaphthene Acenaphthylene Anthracene Benzidine ML RP RP Limit il Fac 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0.0 U ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0.0 U ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0 Page of //0

106 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-- Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: Prep Batch: MB MB Benzo[a]anthracene 0. U 0 0. ug/l 0/0/ :0 0// : Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Benzoic acid Benzyl alcohol Bis(-chloroethoxy)methane Bis(-chloroethyl)ether Bis(-ethylhexyl) phthalate Butyl benzyl phthalate Chrysene ibenz(a,h)anthracene ibenzofuran iethyl phthalate imethyl phthalate i-n-butyl phthalate i-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[,,-cd]pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene ML il Fac.0 U 0.0 ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. I 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0.0 U ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// :. U 0. ug/l 0/0/ :0 0// : 0. U 0 0. ug/l 0/0/ :0 0// :.0 U 0.0 ug/l 0/0/ :0 0// : 0 Surrogate MB %Recovery MB,,-Tribromophenol 0-0/0/ :0 0// : -Fluorobiphenyl - 0/0/ :0 0// : -Fluorophenol - 0 0/0/ :0 0// : Nitrobenzene-d - 0/0/ :0 0// : Phenol-d 0-0 0/0/ :0 0// : Terphenyl-d 0-0 0/0/ :0 0// : il Fac Page of //0

107 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS Added %Rec,,-Trichlorobenzene ug/l - 00,-ichlorobenzene ug/l - 00,-ichlorobenzene 0.0. ug/l - 00,-ichlorobenzene 0.0. ug/l - 00,'-oxybis[-chloropropane] 0.0. ug/l - 0,,-Trichlorophenol 0.0. ug/l 0 -,,-Trichlorophenol 0.0. ug/l -,-ichlorophenol 0.0. ug/l -,-imethylphenol 0.0. ug/l - 00,-initrophenol I ug/l 0 -,-initrotoluene 0.0. ug/l -,-initrotoluene 0.0. ug/l 0-0 -Chloronaphthalene 0.0. ug/l - -Chlorophenol ug/l Methylnaphthalene ug/l - 0 -Methylphenol 0.0. ug/l - 0 -Nitroaniline 0.0. I ug/l - -Nitrophenol 0.0. ug/l - & Methylphenol 00. ug/l -,'-ichlorobenzidine 0.0. I ug/l 0-0 -Nitroaniline 0.0. I ug/l 0 -,-initro--methylphenol I ug/l 0-0 -Bromophenyl phenyl ether ug/l 0 - -Chloro--methylphenol 0.0. ug/l - -Chloroaniline 0.0. ug/l Chlorophenyl phenyl ether ug/l - -Nitroaniline 0.0. I ug/l - -Nitrophenol 0.0. ug/l 0-0 Acenaphthene 0.0. ug/l - Acenaphthylene 0.0. ug/l 0 - Anthracene ug/l - 0 Benzo[a]anthracene 0.0. ug/l - Benzo[a]pyrene 0.0. ug/l - Benzo[b]fluoranthene 0.0. ug/l - Benzo[g,h,i]perylene 0.0. ug/l - 0 Benzo[k]fluoranthene ug/l 0 - Benzoic acid 0.0. I ug/l - Benzyl alcohol 0.0. ug/l - 0 Bis(-chloroethoxy)methane 0.0. ug/l - Bis(-chloroethyl)ether 0.0. ug/l - 0 Bis(-ethylhexyl) phthalate 0.0. ug/l - Butyl benzyl phthalate 0.0. ug/l - Chrysene 0.0. ug/l - ibenz(a,h)anthracene 0.0. ug/l - ibenzofuran ug/l - 0 iethyl phthalate 0.0. ug/l - imethyl phthalate ug/l 0 - i-n-butyl phthalate ug/l - 0 Page of //0

108 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS Added %Rec i-n-octyl phthalate 0.0. ug/l 0 - Fluoranthene ug/l - Fluorene 0.0. ug/l - Hexachlorobenzene 0.0. ug/l - 0 Hexachlorobutadiene 0.0. ug/l 0-00 Hexachlorocyclopentadiene 0.0. I ug/l 0-00 Hexachloroethane 0.0. ug/l 0-00 Indeno[,,-cd]pyrene 0.0. ug/l - Isophorone ug/l - Naphthalene ug/l - 00 Nitrobenzene 0.0. ug/l - N-Nitrosodimethylamine ug/l 0 - N-Nitrosodi-n-propylamine 0.0. ug/l - 0 N-Nitrosodiphenylamine 0.0. ug/l - Pentachlorophenol 0.0. I ug/l - Phenanthrene 0.0. ug/l - 0 Phenol ug/l 0-0 Pyrene 0.0. ug/l - 0 Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - 0 Nitrobenzene-d - Phenol-d - 0 Terphenyl-d Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS RP Added %Rec,,-Trichlorobenzene ug/l - 00,-ichlorobenzene ug/l - 00,-ichlorobenzene 0.0. ug/l - 00,-ichlorobenzene 0.0. ug/l - 00,'-oxybis[-chloropropane] 0.0. ug/l - 0 0,,-Trichlorophenol ug/l 0-0,,-Trichlorophenol 0.0. ug/l -,-ichlorophenol 0.0. ug/l - 0,-imethylphenol 0.0. ug/l - 00,-initrophenol 0.0. I ug/l 0-0,-initrotoluene 0.0. ug/l - 0,-initrotoluene 0.0. ug/l - 0 -Chloronaphthalene 0.0. ug/l - -Chlorophenol 0.0. ug/l Methylnaphthalene 0.0. ug/l - 0 -Methylphenol ug/l RP Limit Page of //0

109 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS RP Added %Rec -Nitroaniline 0.0. I ug/l - -Nitrophenol 0.0. ug/l - 0 & Methylphenol 00. ug/l -,'-ichlorobenzidine 0.0. ug/l 0-0 -Nitroaniline 0.0. I ug/l 0 -,-initro--methylphenol ug/l Bromophenyl phenyl ether 0.0. ug/l 0-0 -Chloro--methylphenol ug/l - -Chloroaniline 0.0. ug/l Chlorophenyl phenyl ether 0.0. ug/l - 0 -Nitroaniline 0.0. I ug/l - -Nitrophenol ug/l Acenaphthene 0.0. ug/l - Acenaphthylene ug/l 0 - Anthracene 0.0. ug/l Benzo[a]anthracene 0.0. ug/l - Benzo[a]pyrene 0.0. ug/l 0-0 Benzo[b]fluoranthene 0.0. ug/l - 0 Benzo[g,h,i]perylene 0.0. ug/l Benzo[k]fluoranthene ug/l - 0 Benzoic acid 0.0. ug/l 0-0 Benzyl alcohol ug/l Bis(-chloroethoxy)methane 0.0. ug/l - 0 Bis(-chloroethyl)ether 0.0. ug/l Bis(-ethylhexyl) phthalate 0.0. ug/l - 0 Butyl benzyl phthalate 0.0. ug/l - Chrysene 0.0. ug/l - 0 ibenz(a,h)anthracene 0.0. ug/l 0-0 ibenzofuran 0.0. ug/l - 0 iethyl phthalate 0.0. ug/l - imethyl phthalate 0.0. ug/l - i-n-butyl phthalate 0.0. ug/l - i-n-octyl phthalate 0.0. ug/l Fluoranthene 0.0. ug/l - 0 Fluorene 0.0. ug/l - Hexachlorobenzene 0.0. ug/l Hexachlorobutadiene ug/l Hexachlorocyclopentadiene 0.0. I ug/l Hexachloroethane 0.0. ug/l Indeno[,,-cd]pyrene 0.0. ug/l - 0 Isophorone 0.0. ug/l - Naphthalene ug/l - 00 Nitrobenzene 0.0. ug/l - N-Nitrosodimethylamine ug/l - N-Nitrosodi-n-propylamine 0.0. ug/l - 0 N-Nitrosodiphenylamine 0.0. ug/l - Pentachlorophenol 0.0. I ug/l - 0 Phenanthrene 0.0. ug/l RP Limit 0 Page of //0

110 QC Sample s Method: 0C - Semivolatile Organic Compounds (GC/MS) (Continued) TestAmerica Job I: 0-- Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: Prep Batch: Spike LCS LCS RP Added %Rec Phenol 0.0. ug/l Pyrene 0.0. ug/l Surrogate LCS %Recovery LCS,,-Tribromophenol - -Fluorobiphenyl - -Fluorophenol - 0 Nitrobenzene-d 0 - Phenol-d 0-0 Terphenyl-d 0-0 Method: 00. Rev. - Metals (ICP) Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis Batch: Prep Batch: MB MB Chromium U mg/l 0/0/ 0: 0// : Copper Iron Lead ML RP Limit il Fac 0.00 U mg/l 0/0/ 0: 0// : 0.00 U mg/l 0/0/ 0: 0// : U mg/l 0/0/ 0: 0// : 0 Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis Batch: Prep Batch: Spike LCS LCS Added %Rec Chromium mg/l 00 - Copper mg/l - Iron mg/l - Lead mg/l - Lab Sample I: 0--B--B MS Client Sample I: Matrix Spike Prep Type: Total Recoverable Analysis Batch: Prep Batch: Sample Sample Spike MS MS Added %Rec Chromium U.00.0 mg/l 0 - Copper 0.00 U mg/l - Iron 0.00 U mg/l - Lead U mg/l - Page of //0

111 Method: 00. Rev. - Metals (ICP) (Continued) QC Sample s TestAmerica Job I: 0-- Lab Sample I: 0--B--C MS Client Sample I: Matrix Spike uplicate Prep Type: Total Recoverable Analysis Batch: Prep Batch: Sample Sample Spike MS MS RP Added %Rec Chromium U mg/l - 0 Copper 0.00 U mg/l - 0 Iron 0.00 U mg/l - 0 Lead U mg/l - 0 Method: A - HEM and SGT-HEM Lab Sample I: MB 0-/ Analysis Batch: MB MB ML RP Limit Client Sample I: Method Blank Prep Type: HEM (Oil & Grease). U.0. mg/l 0// : Lab Sample I: LCS 0-/ Analysis Batch: Spike Added il Fac Client Sample I: Lab Control Sample Prep Type: HEM (Oil & Grease) 0.0. mg/l 0 - LCS LCS %Rec 0 Lab Sample I: 0--A- MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: Sample Sample Spike MS MS Added %Rec HEM (Oil & Grease) J J. J mg/l - Lab Sample I: 0--A- MS Client Sample I: Matrix Spike uplicate Prep Type: Analysis Batch: Sample Sample Spike MS MS RP Added %Rec RP Limit HEM (Oil & Grease) J J. J mg/l - Method: Anions, Ion Chromatography Lab Sample I: MB 0-/ Analysis Batch: MB MB ML Client Sample I: Method Blank Prep Type: Chloride.0 U.0.0 mg/l 0// :0 Sulfate il Fac. U.0. mg/l 0// :0 Page of //0

112 QC Sample s Method: Anions, Ion Chromatography (Continued) Lab Sample I: LCS 0-/ Analysis Batch: Spike Added TestAmerica Job I: 0-- Client Sample I: Lab Control Sample Prep Type: Chloride mg/l LCS LCS %Rec Sulfate 0.0. mg/l Lab Sample I: LCS 0-/ Analysis Batch: Spike Added Client Sample I: Lab Control Sample up Prep Type: Chloride mg/l LCS LCS %Rec Sulfate 0.0. mg/l Lab Sample I: 0--- MS Analysis Batch: Sample Sample Spike Added Sulfate. U 0.0. mg/l Lab Sample I: 0--- MS Analysis Batch: Sample Sample Spike Added MS MS %Rec RP RP Limit Client Sample I: Matrix Spike Prep Type: Client Sample I: Matrix Spike uplicate Prep Type: Sulfate. U mg/l MS MS %Rec RP RP Limit 0 Method:. - Nitrogen, Total Kjeldahl Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 00 Prep Batch: MB MB ML il Fac Nitrogen, Kjeldahl 0. U mg/l 0// : 0// : Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 00 Prep Batch: Spike LCS LCS Added %Rec Nitrogen, Kjeldahl.00. mg/l 0 - Lab Sample I: 0-- MS Client Sample I: SW-IN Prep Type: Analysis Batch: 00 Prep Batch: Sample Sample Spike MS MS Added %Rec Nitrogen, Kjeldahl..00. mg/l - Page of //0

113 Method:. - Nitrogen, Total Kjeldahl (Continued) QC Sample s TestAmerica Job I: 0-- Lab Sample I: 0-- MS Client Sample I: SW-IN Prep Type: Analysis Batch: 00 Prep Batch: Sample Sample Spike MS MS RP Added %Rec Nitrogen, Kjeldahl..00. mg/l Lab Sample I: 0-- U Client Sample I: W-IN Prep Type: Analysis Batch: 00 Prep Batch: Sample Sample U U RP Nitrogen, Kjeldahl 0. I 0.0 mg/l 0 0 Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 0-/ Analysis Batch: MB MB ML RP RP Limit Limit Client Sample I: Method Blank Prep Type: Nitrate Nitrite as N 0.0 U mg/l 0/0/ 0:0 Nitrite as N Nitrate as N il Fac 0.0 U mg/l 0/0/ 0:0 0.0 U mg/l 0/0/ 0:0 0 Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Spike LCS LCS Added %Rec Nitrate Nitrite as N mg/l 0-0 Nitrite as N I mg/l Lab Sample I: 0-- MS Client Sample I: W-IN Prep Type: Analysis Batch: Sample Sample Spike MS MS Added %Rec Nitrate Nitrite as N 0.0 U.00.0 mg/l Nitrite as N 0.0 U mg/l Lab Sample I: 0-- MS Client Sample I: W-IN Prep Type: Analysis Batch: Sample Sample Spike MS MS RP Added %Rec RP Limit Nitrate Nitrite as N 0.0 U.00.0 mg/l Nitrite as N 0.0 U I mg/l Page of //0

114 Method:. - Phosphorus, Orthophosphate Lab Sample I: MB 0-/ Analysis Batch: MB MB QC Sample s ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type: Orthophosphate 0.0 U mg/l 0/0/ :0 Lab Sample I: LCS 0-/ Analysis Batch: Spike Added il Fac Client Sample I: Lab Control Sample Prep Type: Orthophosphate mg/l Lab Sample I: 0-- MS Analysis Batch: Sample Sample Spike Added LCS LCS %Rec Orthophosphate 0.0 J J U J mg/l 0-0 Lab Sample I: 0-- MS Analysis Batch: Sample Sample Spike Added MS MS %Rec Client Sample I: W-IN Prep Type: issolved Client Sample I: W-IN Prep Type: issolved Orthophosphate 0.0 J J U J mg/l MS MS %Rec RP RP Limit 0 Method:. - Phosphorus, Total Lab Sample I: MB 0-/-A Client Sample I: Method Blank Prep Type: Analysis Batch: 00 Prep Batch: MB MB ML il Fac Phosphorus 0.0 U mg/l 0// : 0// : Lab Sample I: LCS 0-/-A Client Sample I: Lab Control Sample Prep Type: Analysis Batch: 00 Prep Batch: Spike LCS LCS Added %Rec Phosphorus.00.0 mg/l Lab Sample I: 0-- MS Client Sample I: SW-IN Prep Type: Analysis Batch: 00 Prep Batch: Sample Sample Spike MS MS Added %Rec Phosphorus mg/l 0-0 Page 0 of //0

115 Method:. - Phosphorus, Total (Continued) QC Sample s TestAmerica Job I: 0-- Lab Sample I: 0-- MS Client Sample I: SW-IN Prep Type: Analysis Batch: 00 Prep Batch: Sample Sample Spike MS MS RP Added %Rec Phosphorus mg/l Lab Sample I: 0-- U Client Sample I: W-IN Prep Type: Analysis Batch: 00 Prep Batch: Sample Sample U U RP Phosphorus 0.0 I 0.0 I mg/l 0 Method: 00 - Organic Carbon, Total (TOC) Lab Sample I: MB 0-00/ Analysis Batch: 00 MB MB ML RP RP Limit Limit Client Sample I: Method Blank Prep Type: Total Organic Carbon 0.0 U mg/l 0// 0:0 Lab Sample I: LCS 0-00/ Analysis Batch: 00 Spike Added il Fac Client Sample I: Lab Control Sample Prep Type: Total Organic Carbon mg/l LCS LCS %Rec 0 Lab Sample I: LCS 0-00/ Client Sample I: Lab Control Sample up Prep Type: Analysis Batch: 00 Spike LCS LCS RP Added %Rec RP Limit Total Organic Carbon 0.0. mg/l 0-0 Lab Sample I: 0--O- MS Client Sample I: Matrix Spike Prep Type: Analysis Batch: 00 Sample Sample Spike MS MS Added %Rec Total Organic Carbon 0.0 I mg/l 0-0 Lab Sample I: 0--O- MS Client Sample I: Matrix Spike uplicate Prep Type: Analysis Batch: 00 Sample Sample Spike MS MS RP Added %Rec RP Limit Total Organic Carbon 0.0 I mg/l 0-0 Page of //0

116 Method: SM 0B - Color, Colorimetric Lab Sample I: MB 0-/ Analysis Batch: MB MB QC Sample s ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type: Color.0 U.0.0 PCU 0/0/ 0:0 ph at time of analysis Lab Sample I: LCS 0-/ Analysis Batch: il Fac..0.0 SU 0/0/ 0:0 Spike Added Client Sample I: Lab Control Sample Prep Type: Color PCU Lab Sample I: 0-- U Analysis Batch: Sample Sample LCS LCS %Rec Client Sample I: W-OUT Prep Type: Color.0 PCU 0 0 U U ph at time of analysis.. SU 0. Method: SM 0B - Alkalinity RP RP Limit 0 Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Spike LCS LCS Added %Rec Alkalinity mg/l Lab Sample I: 0--C- U Client Sample I: uplicate Prep Type: Analysis Batch: Sample Sample U U RP RP Limit Alkalinity 0 mg/l 0. 0 Method: SM 0C - Solids, Total issolved (TS) Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis Batch: MB MB ML il Fac Total issolved Solids.0 U.0.0 mg/l 0/0/ 0: Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Spike LCS LCS Added %Rec Total issolved Solids mg/l 0-0 Page of //0

117 QC Sample s Method: SM 0C - Solids, Total issolved (TS) (Continued) Lab Sample I: 0--C- U Analysis Batch: Sample Sample TestAmerica Job I: 0-- Client Sample I: uplicate Prep Type: Total issolved Solids 0 mg/l 0 Lab Sample I: MB 0-/ Analysis Batch: MB MB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Total issolved Solids.0 U.0.0 mg/l 0// : Lab Sample I: LCS 0-/ Analysis Batch: Spike Added il Fac Client Sample I: Lab Control Sample Prep Type: Total issolved Solids mg/l 0-0 Lab Sample I: 0--A- U Analysis Batch: Sample Sample LCS LCS %Rec Client Sample I: uplicate Prep Type: Total issolved Solids 00 0 mg/l 0 U U RP RP Limit 0 Method: SM 0 - Solids, Total Suspended (TSS) Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis Batch: MB MB ML il Fac Total Suspended Solids.0 U.0.0 mg/l 0/0/ 0: Lab Sample I: LCS 0-/ Client Sample I: Lab Control Sample Prep Type: Analysis Batch: Spike LCS LCS Added %Rec Total Suspended Solids 00. mg/l 0-0 Lab Sample I: 0-0-B- U Client Sample I: uplicate Prep Type: Analysis Batch: Sample Sample U U RP RP Limit Total Suspended Solids 0 mg/l 0 0 Page of //0

118 QC Sample s Method: SM 0 - Solids, Total Suspended (TSS) (Continued) Lab Sample I: MB 0-/ Analysis Batch: MB MB ML TestAmerica Job I: 0-- Client Sample I: Method Blank Prep Type: Total Suspended Solids.0 U.0.0 mg/l 0// 0: Lab Sample I: LCS 0-/ Analysis Batch: Spike Added il Fac Client Sample I: Lab Control Sample Prep Type: Total Suspended Solids 00. mg/l 0-0 Lab Sample I: 0--H- U Analysis Batch: Sample Sample LCS LCS %Rec Client Sample I: uplicate Prep Type: Total Suspended Solids..0 mg/l 0 0 Method: SM 00 Cl B - Chlorine, Total Residual Lab Sample I: MB 0-0/ Analysis Batch: 0 MB MB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Chlorine, Total Residual.0 U.0.0 mg/l 0/0/ 0:00 il Fac 0 Lab Sample I: 0-- U Client Sample I: SW-IN Prep Type: Analysis Batch: 0 Sample Sample U U RP RP Limit Chlorine, Total Residual.0 U.0 U mg/l NC 0 Method: SM 0B - BO, -ay Lab Sample I: SCB 0-00/ SCB Client Sample I: Method Blank Prep Type: Analysis Batch: 00 SCB SCB ML il Fac Biochemical Oxygen emand.0 U.0.0 mg/l 0/0/ 0: Lab Sample I: USB 0-00/ USB Client Sample I: Method Blank Prep Type: Analysis Batch: 00 USB USB ML il Fac Biochemical Oxygen emand.0 U.0.0 mg/l 0/0/ 0: Page of //0

119 Method: SM 0B - BO, -ay (Continued) Lab Sample I: LCS 0-00/ Analysis Batch: 00 QC Sample s Spike Added TestAmerica Job I: 0-- Client Sample I: Lab Control Sample Prep Type: Biochemical Oxygen emand mg/l - Lab Sample I: 0-- U Analysis Batch: 00 Sample Sample LCS LCS %Rec Client Sample I: W-OUT Prep Type: Biochemical Oxygen emand.0 U.0 U mg/l NC 0 Method: SM B - Coliforms, Total (Membrane Filter) Lab Sample I: MB 0-/ Analysis Batch: MB MB U U ML RP RP Limit Client Sample I: Method Blank Prep Type: Coliform, Total.0 U.0.0 CFU/00mL 0/0/ : Lab Sample I: 0-- U Analysis Batch: Sample Sample il Fac Client Sample I: W-IN Prep Type: Coliform, Total 0 00 CFU/00mL 0 U U RP RP Limit 0 Method: SM - Coliforms, Fecal (Membrane Filter) Lab Sample I: MB 0-/ Client Sample I: Method Blank Prep Type: Analysis Batch: MB MB ML il Fac Coliform, Fecal.0 U.0.0 CFU/00mL 0/0/ : Lab Sample I: 0-- U Client Sample I: SW-IN Prep Type: Analysis Batch: Sample Sample U U RP RP Limit Coliform, Fecal.0 U.0 U CFU/00mL NC 0 Page of //0

120 QC Association Summary TestAmerica Job I: 0-- GC/MS VOA Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN 0B 0-- W-IN 0B 0-- SW-OUT 0B 0-- W-OUT 0B 0-- Trip Blank 0B 0--- U uplicate 0B 0--H- MS Matrix Spike 0B LCS 0-/ Lab Control Sample 0B MB 0-/ Method Blank 0B GC/MS Semi VOA Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN 0C 0-- W-IN 0C 0-- SW-OUT 0C 0-- W-OUT 0C LCS 0-/-A Lab Control Sample 0C LCS 0-/-A Lab Control Sample up 0C MB 0-/-A Method Blank 0C 0 Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN 0C 0-- W-IN 0C 0-- SW-OUT 0C 0-- W-OUT 0C LCS 0-/-A Lab Control Sample 0C LCS 0-/-A Lab Control Sample up 0C MB 0-/-A Method Blank 0C Metals Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--B--B MS Matrix Spike Total Recoverable B--C MS Matrix Spike uplicate Total Recoverable SW-IN Total Recoverable W-IN Total Recoverable SW-OUT Total Recoverable W-OUT Total Recoverable 00. LCS 0-/-A Lab Control Sample Total Recoverable 00. MB 0-/-A Method Blank Total Recoverable 00. Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--B--B MS Matrix Spike Total Recoverable 00. Rev. 0--B--C MS Matrix Spike uplicate Total Recoverable 00. Rev. 0-- SW-IN Total Recoverable 00. Rev. Page of //0

121 QC Association Summary TestAmerica Job I: 0-- Metals (Continued) Analysis Batch: (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- W-IN Total Recoverable 00. Rev. 0-- SW-OUT Total Recoverable 00. Rev. 0-- W-OUT Total Recoverable 00. Rev. LCS 0-/-A Lab Control Sample Total Recoverable 00. Rev. MB 0-/-A Method Blank Total Recoverable 00. Rev. General Chemistry Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-0-B- U uplicate SM SW-IN SM 0 LCS 0-/ Lab Control Sample SM 0 MB 0-/ Method Blank SM 0 Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN SM 0B 0-- W-IN SM 0B 0-- SW-OUT SM 0B 0-- W-OUT SM 0B 0-- U W-OUT SM 0B LCS 0-00/ Lab Control Sample SM 0B SCB 0-00/ SCB Method Blank SM 0B USB 0-00/ USB Method Blank SM 0B 0 Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN SM 00 Cl B 0-- U SW-IN SM 00 Cl B 0-- W-IN SM 00 Cl B 0-- SW-OUT SM 00 Cl B 0-- W-OUT SM 00 Cl B MB 0-0/ Method Blank SM 00 Cl B Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--C- U uplicate SM 0C 0-- SW-IN SM 0C LCS 0-/ Lab Control Sample SM 0C MB 0-/ Method Blank SM 0C Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN issolved. 0-- W-IN issolved. 0-- MS W-IN issolved. 0-- MS W-IN issolved. 0-- SW-OUT issolved. 0-- W-OUT issolved. Page of //0

122 QC Association Summary TestAmerica Job I: 0-- General Chemistry (Continued) Analysis Batch: (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch LCS 0-/ Lab Control Sample. MB 0-/ Method Blank. Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN SM 0B 0-- W-IN SM 0B 0-- SW-OUT SM 0B 0-- W-OUT SM 0B 0-- U W-OUT SM 0B LCS 0-/ Lab Control Sample SM 0B MB 0-/ Method Blank SM 0B Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN. 0-- W-IN. 0-- MS W-IN. 0-- MS W-IN. 0-- SW-OUT. 0-- W-OUT. LCS 0-/ Lab Control Sample. MB 0-/ Method Blank. 0 Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--C- U uplicate SM 0B 0-- SW-IN SM 0B 0-- W-IN SM 0B 0-- SW-OUT SM 0B 0-- W-OUT SM 0B LCS 0-/ Lab Control Sample SM 0B Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--A- U uplicate SM 0C 0-- W-IN SM 0C 0-- SW-OUT SM 0C 0-- W-OUT SM 0C LCS 0-/ Lab Control Sample SM 0C MB 0-/ Method Blank SM 0C Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--H- U uplicate SM W-IN SM SW-OUT SM W-OUT SM 0 LCS 0-/ Lab Control Sample SM 0 MB 0-/ Method Blank SM 0 Page of //0

123 QC Association Summary TestAmerica Job I: 0-- General Chemistry (Continued) Prep Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN igestion 0-- MS SW-IN igestion 0-- MS SW-IN igestion 0-- W-IN igestion 0-- U W-IN igestion 0-- SW-OUT igestion 0-- W-OUT igestion LCS 0-/-A Lab Control Sample igestion MB 0-/-A Method Blank igestion Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--- MS Matrix Spike MS Matrix Spike uplicate SW-IN W-IN SW-OUT W-OUT 00.0 LCS 0-/ Lab Control Sample 00.0 LCS 0-/ Lab Control Sample up 00.0 MB 0-/ Method Blank Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--O- MS Matrix Spike O- MS Matrix Spike uplicate SW-IN W-IN SW-OUT W-OUT 00 LCS 0-00/ Lab Control Sample 00 LCS 0-00/ Lab Control Sample up 00 MB 0-00/ Method Blank 00 Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN. 0-- MS SW-IN. 0-- MS SW-IN. 0-- W-IN. 0-- U W-IN. 0-- SW-OUT. 0-- W-OUT. LCS 0-/-A Lab Control Sample. MB 0-/-A Method Blank. Analysis Batch: 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN. 0-- MS SW-IN. 0-- MS SW-IN. Page of //0

124 QC Association Summary TestAmerica Job I: 0-- General Chemistry (Continued) Analysis Batch: 00 (Continued) Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- W-IN. 0-- U W-IN. 0-- SW-OUT. 0-- W-OUT. LCS 0-/-A Lab Control Sample. MB 0-/-A Method Blank. Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0--A- MS Matrix Spike A 0--A- MS Matrix Spike uplicate A 0-- SW-IN A 0-- W-IN A 0-- SW-OUT A 0-- W-OUT A LCS 0-/ Lab Control Sample A MB 0-/ Method Blank A Biology Analysis Batch: 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN SM 0-- U SW-IN SM 0-- W-IN SM 0-- SW-OUT SM 0-- W-OUT SM MB 0-/ Method Blank SM Analysis Batch: Lab Sample I Client Sample I Prep Type Matrix Method Prep Batch 0-- SW-IN SM B 0-- W-IN SM B 0-- U W-IN SM B 0-- SW-OUT SM B 0-- W-OUT SM B MB 0-/ Method Blank SM B Page 0 of //0

125 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-- Client Sample I: SW-IN Lab Sample I: 0-- ate Collected: 0/0/ 0: ate Received: 0/0/ : Prep Type Total Recoverable Total Recoverable issolved Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// 0: EC TAL TAM Prep 0C 0/0/ :0 QC TAL TAL Analysis 0C 0// : VW TAL TAL Prep 00. 0/0/ 0: GF TAL TAM Analysis 00. Rev. 0// : GF TAL TAM Analysis SM 0 0/0/ 0: TO TAL TAM Analysis SM 0B 00 0/0/ 0: AG TAL TAM Analysis SM 00 Cl B 0 0/0/ 0:00 RWF TAL TAM Analysis SM 0C 0/0/ 0: TO TAL TAM Analysis. 0/0/ :0 RWF TAL TAM Analysis SM 0B 0/0/ 0:0 AG TAL TAM Analysis. 0/0/ 0:0 RWF TAL TAM Analysis SM 0B 0/0/ 0: RWF TAL TAM Analysis // : PAT TAL SAV Analysis // :0 JR TAL SAV Prep igestion 0// : AJO TAL SAV Analysis. 00 0// : JR TAL SAV Analysis. 00 0// : JR TAL SAV Analysis A 0// : JS TAL SAV Analysis SM RWF TAL TAM (Start) (End) 0/0/ : 0/0/ :0 Analysis SM B 0 RWF TAL TAM (Start) (End) 0/0/ : 0/0/ : Lab 0 Client Sample I: W-IN Lab Sample I: 0-- ate Collected: 0/0/ 0:0 ate Received: 0/0/ : Prep Type Total Recoverable Total Recoverable issolved Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// 0: EC TAL TAM Prep 0C 0/0/ :0 QC TAL TAL Analysis 0C 0// :0 VW TAL TAL Prep 00. 0/0/ 0: GF TAL TAM Analysis 00. Rev. 0// : GF TAL TAM Analysis SM 0B 00 0/0/ 0: AG TAL TAM Analysis SM 00 Cl B 0 0/0/ 0:00 RWF TAL TAM Analysis. 0/0/ :0 RWF TAL TAM Analysis SM 0B 0/0/ 0:0 AG TAL TAM Analysis. 0/0/ 0:0 RWF TAL TAM Lab Page of //0

126 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-- Client Sample I: W-IN Lab Sample I: 0-- ate Collected: 0/0/ 0:0 ate Received: 0/0/ : Prep Type Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis SM 0B 0/0/ 0: RWF TAL TAM Analysis SM 0C 0// : TO TAL TAM Analysis SM 0 0// 0: TO TAL TAM Analysis // :0 PAT TAL SAV Analysis // :0 JR TAL SAV Prep igestion 0// : AJO TAL SAV Analysis. 00 0// : JR TAL SAV Lab Analysis. 00 0// : JR TAL SAV Analysis A 0// : JS TAL SAV Analysis SM RWF TAL TAM (Start) (End) 0/0/ : 0/0/ :0 Analysis SM B 0 RWF TAL TAM (Start) (End) 0/0/ : 0/0/ : Client Sample I: SW-OUT Lab Sample I: 0-- ate Collected: 0/0/ : ate Received: 0/0/ : 0 Prep Type Total Recoverable Total Recoverable issolved Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// : EC TAL TAM Prep 0C 0/0/ :0 QC TAL TAL Analysis 0C 0// : VW TAL TAL Prep 00. 0/0/ 0: GF TAL TAM Analysis 00. Rev. 0// : GF TAL TAM Analysis SM 0B 00 0/0/ 0: AG TAL TAM Analysis SM 00 Cl B 0 0/0/ 0:00 RWF TAL TAM Analysis. 0/0/ :0 RWF TAL TAM Analysis SM 0B 0 0/0/ 0:0 AG TAL TAM Analysis. 0/0/ 0:0 RWF TAL TAM Analysis SM 0B 0/0/ 0: RWF TAL TAM Analysis SM 0C 0// : TO TAL TAM Analysis SM 0 0// 0: TO TAL TAM Analysis // : PAT TAL SAV Analysis // : JR TAL SAV Prep igestion 0// : AJO TAL SAV Analysis. 00 0// : JR TAL SAV Analysis. 00 0// : JR TAL SAV Analysis A 0// : JS TAL SAV Lab Page of //0

127 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-- Client Sample I: SW-OUT Lab Sample I: 0-- ate Collected: 0/0/ : ate Received: 0/0/ : Prep Type Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis SM RWF TAL TAM (Start) (End) 0/0/ : 0/0/ :0 Analysis SM B 0 RWF TAL TAM (Start) (End) 0/0/ : 0/0/ : Lab Client Sample I: W-OUT Lab Sample I: 0-- ate Collected: 0/0/ :0 ate Received: 0/0/ : Prep Type Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// : EC TAL TAM Prep 0C 0/0/ :0 QC TAL TAL Analysis 0C 0// : VW TAL TAL Lab 0 Total Recoverable Total Recoverable issolved Prep 00. 0/0/ 0: GF TAL TAM Analysis 00. Rev. 0// : GF TAL TAM Analysis SM 0B 00 0/0/ 0: AG TAL TAM Analysis SM 00 Cl B 0 0/0/ 0:00 RWF TAL TAM Analysis. 0/0/ :0 RWF TAL TAM Analysis SM 0B 0/0/ 0:0 AG TAL TAM Analysis. 0/0/ 0:0 RWF TAL TAM Analysis SM 0B 0/0/ 0: RWF TAL TAM Analysis SM 0C 0// : TO TAL TAM Analysis SM 0 0// 0: TO TAL TAM Analysis // : PAT TAL SAV Analysis // : JR TAL SAV Prep igestion 0// : AJO TAL SAV Analysis. 00 0// : JR TAL SAV Analysis. 00 0// : JR TAL SAV Analysis A 0// : JS TAL SAV Analysis SM RWF TAL TAM (Start) 0/0/ : (End) 0/0/ :0 Analysis SM B 0 RWF TAL TAM (Start) 0/0/ : (End) 0/0/ : Page of //0

128 Lab Chronicle Client: Cardno ENTRIX. TestAmerica Job I: 0-- Client Sample I: Trip Blank Lab Sample I: 0-- ate Collected: 0/0/ 00:00 ate Received: 0/0/ : Prep Type Batch Type Batch Method Run ilution Factor Batch Number or Analyst Analysis 0B 0// 0: EC TAL TAM Lab Laboratory References: TAL SAV = TestAmerica Savannah, 0 LaRoche Avenue, Savannah, GA 0, TEL ()- TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- TAL TAM =, Benjamin Road, Suite 00, Tampa, FL, TEL ()- 0 Page of //0

129 Method Summary TestAmerica Job I: 0-- Method Method escription Protocol Laboratory 0B Volatile Organic Compounds (GC/MS) SW TAL TAM 0C Semivolatile Organic Compounds (GC/MS) SW TAL TAL 00. Rev. Metals (ICP) EPA TAL TAM A HEM and SGT-HEM A TAL SAV 00.0 Anions, Ion Chromatography MCAWW TAL SAV. Nitrogen, Total Kjeldahl MCAWW TAL SAV. Nitrogen, Nitrate-Nitrite MCAWW TAL TAM. Phosphorus, Orthophosphate MCAWW TAL TAM. Phosphorus, Total EPA TAL SAV 00 Organic Carbon, Total (TOC) SW TAL SAV SM 0B Color, Colorimetric SM TAL TAM SM 0B Alkalinity SM TAL TAM SM 0C Solids, Total issolved (TS) SM TAL TAM SM 0 Solids, Total Suspended (TSS) SM TAL TAM SM 00 Cl B Chlorine, Total Residual SM TAL TAM SM 0B BO, -ay SM TAL TAM SM B Coliforms, Total (Membrane Filter) SM TAL TAM SM Coliforms, Fecal (Membrane Filter) SM TAL TAM Protocol References: A = EPA---00 EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of And Wastes", EPA-00/--00, March And Subsequent Revisions. SM = "Standard Methods For The Examination Of And Wastewater", SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its Updates. 0 Laboratory References: TAL SAV = TestAmerica Savannah, 0 LaRoche Avenue, Savannah, GA 0, TEL ()- TAL TAL = TestAmerica Tallahassee, Industrial Plaza rive, Tallahassee, FL 0, TEL (0)- TAL TAM =, Benjamin Road, Suite 00, Tampa, FL, TEL ()- Page of //0

130 Certification Summary Client: Cardno ENTRIX. TestAmerica Job I: 0-- Laboratory: All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Alabama State Program Florida NELAP E 0-0- Georgia State Program USA Federal P Laboratory: TestAmerica Savannah All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate ALA o ELAP ALA ISO/IEC Alabama State Program Alaska (UST) State Program 0 UST California NELAP CA 0-- Colorado State Program N/A -- Connecticut State Program PH Florida NELAP E GA ept. of Agriculture State Program N/A -- Georgia State Program N/A 0-0- Georgia State Program Guam State Program 0-00r 0-- Hawaii State Program N/A 0-0- Illinois NELAP Indiana State Program N/A 0-0- Iowa State Program 0-0- Kentucky State Program Kentucky (UST) State Program 0-- Louisiana NELAP Louisiana NELAP LA Maine State Program GA Maryland State Program 0 -- Massachusetts State Program M-GA Michigan State Program 0-0- Mississippi State Program N/A 0-0- Montana State Program CERT00 -- Nebraska State Program TestAmerica-Savannah 0-0- New Jersey NELAP GA 0-0- New Mexico State Program N/A 0-0- New York NELAP North Carolina ENR State Program -- North Carolina HHS State Program Oklahoma State Program 0-- Pennsylvania NELAP Puerto Rico State Program GA South Carolina State Program Tennessee State Program TN Texas NELAP T00-0-TX -0- USA Federal SAV Virginia NELAP Washington State Program 0 C 0-0- West Virginia State Program 0C -- West Virginia EP State Program Page of //0

131 Certification Summary Client: Cardno ENTRIX. TestAmerica Job I: 0-- Laboratory: TestAmerica Savannah (Continued) All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Wisconsin State Program Wyoming State Program TMS-Q 0-0- Laboratory: TestAmerica Tallahassee All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification I Expiration ate Florida NELAP E Louisiana NELAP New Jersey NELAP FL Texas NELAP T USA Federal P Page of //0

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