ANALYTICAL RESULTS. Project: Mayflower, AR Pipeline Incident
|
|
- Jeremy Caldwell
- 6 years ago
- Views:
Transcription
1 ANALYTICAL RESULTS Prepared by: Eurofins Lancaster Laboratories Environmental 2425 New Holland Pike Lancaster, PA 760 Prepared for: Mobil Pipeline Company PO Box 446 Houston TX July 30, 203 Project: Mayflower, AR Pipeline Incident Submittal Date: 07/27/203 Group Number: SDG: PEJ53 PO Number: Release Number: MAYFLOWER 406 State of Sample Origin: AR Client Sample Description Lancaster Labs (LL) # SH Grab Surface Water SH Filtered Grab Surface Water SH Grab Surface Water SH Filtered Grab Surface Water WS-TB Water The specific methodologies used in obtaining the enclosed analytical results are indicated on the Laboratory Sample Analysis Record. ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ELECTRONIC COPY TO ARCADIS ARCADIS ARCADIS ARCADIS ARCADIS Attn: Stephen Barrick Attn: Lyndi Mott Attn: Michael J. Firth Attn: Emily Leamer Attn: Rhiannon Parmalee Attn: Jamie Pritchard Attn: Michael L Sixsmith Attn: Julie Foster Attn: Carl Wideman Page of 26
2 Respectfully Submitted, (77) Page 2 of 26
3 Case Narrative Project Name: Mayflower, AR Pipeline Incident LLI Group #: General Comments: See the Laboratory Sample Analysis Record section of the Analysis Report for the method references. All QC met criteria unless otherwise noted in an Analysis Specific Comment below. Refer to the QC Summary for specific values and acceptance criteria. Project specific QC samples are not included in this data set Matrix QC may not be reported if site-specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise specified in the method. Surrogate recoveries (if applicable) which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in an Analysis Specific Comment below. The samples were received at the appropriate temperature and in accordance with the chain of custody unless otherwise noted. Analysis Specific Comments: SW B 25mL purge, GC/MS Volatiles Batch #: I320AA (Sample number(s): , , UNSPK: P42305) The recovery(ies) for the following analyte(s) in the MS and/or MSD was outside the acceptance window: Hexachlorobutadiene, Methyl Tertiary Butyl Ether The relative percent difference(s) for the following analyte(s) in the MS/MSD were outside outside acceptance windows: Hexachlorobutadiene SW C SIM, GC/MS Semivolatiles Batch #: 3209WAA026 (Sample number(s): , UNSPK: P42306) The recovery(ies) for the following analyte(s) in the MS and/or MSD was outside the acceptance window: Benzo(a)pyrene The recovery(ies) for one or more surrogates were outside of the QC window for sample(s) , Sample #s: , The recovery for the sample surrogate(s) is outside the QC acceptance limits as noted on the QC Summary. The client was contacted and the data reported. SW B, Metals Batch #: (Sample number(s): UNSPK: P42305 BKG: P42305) The recovery(ies) for the following analyte(s) in the MS and/or MSD was outside the acceptance window: Magnesium, Lead SW B, Metals Dissolved Batch #: (Sample number(s): UNSPK: P42305 BKG: P42305) The recovery(ies) for the following analyte(s) in the MS and/or MSD was outside the acceptance window: Lead v.8.8 7/30/203 :08:07PM Page 3 of 26
4 EPA 664A, Wet Chemistry Batch #: A (Sample number(s): , UNSPK: P42306 BKG: P42306) The recovery(ies) for the following analyte(s) in the MS and/or MSD was outside the acceptance window: HEM (oil & grease) v.8.8 7/30/203 :08:07PM Page 4 of 26
5 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:30 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH0- CAT SDG#: PEJ53-0 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation GC/MS Volatiles SW B 25mL purge Acetone J Allyl Chloride N.D Benzene N.D Bromobenzene N.D Bromochloromethane N.D Bromodichloromethane N.D Bromoform N.D Bromomethane N.D Butanone N.D n-butylbenzene N.D sec-butylbenzene N.D tert-butylbenzene N.D Carbon Tetrachloride N.D Chlorobenzene N.D Chloroethane N.D Chloroform N.D Chloromethane N.D Chlorotoluene N.D Chlorotoluene N.D ,2-Dibromo-3-chloropropane N.D Dibromochloromethane N.D ,2-Dibromoethane N.D Dibromomethane N.D ,2-Dichlorobenzene N.D ,3-Dichlorobenzene N.D ,4-Dichlorobenzene N.D Dichlorodifluoromethane N.D ,-Dichloroethane N.D ,2-Dichloroethane N.D ,-Dichloroethene N.D cis-,2-dichloroethene N.D trans-,2-dichloroethene N.D Dichlorofluoromethane N.D ,2-Dichloropropane N.D ,3-Dichloropropane N.D ,2-Dichloropropane N.D ,-Dichloropropene N.D cis-,3-dichloropropene N.D trans-,3-dichloropropene N.D Ethyl ether N.D Ethylbenzene N.D Freon N.D Hexachlorobutadiene N.D Isopropylbenzene N.D p-isopropyltoluene N.D Methyl Tertiary Butyl Ether N.D Methyl-2-Pentanone N.D Methylene Chloride N.D *=This limit was used in the evaluation of the final result Page 5 of 26
6 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:30 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH0- CAT SDG#: PEJ53-0 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation GC/MS Volatiles SW B 25mL purge n-propylbenzene N.D Styrene N.D ,,,2-Tetrachloroethane N.D ,,2,2-Tetrachloroethane N.D Tetrachloroethene N.D Tetrahydrofuran N.D Toluene ,2,3-Trichlorobenzene N.D ,2,4-Trichlorobenzene N.D ,,-Trichloroethane N.D ,,2-Trichloroethane N.D Trichloroethene N.D Trichlorofluoromethane N.D ,2,3-Trichloropropane N.D ,2,4-Trimethylbenzene N.D ,3,5-Trimethylbenzene N.D Vinyl Chloride N.D Xylene (Total) N.D GC/MS Semivolatiles SW C SIM Acenaphthene N.D Acenaphthylene N.D Anthracene N.D Benzo(a)anthracene N.D Benzo(a)pyrene N.D Benzo(b)fluoranthene N.D Benzo(g,h,i)perylene N.D Benzo(k)fluoranthene N.D Chrysene N.D Dibenz(a,h)anthracene N.D Fluoranthene N.D Fluorene N.D Indeno(,2,3-cd)pyrene N.D Methylnaphthalene J Methylnaphthalene J Naphthalene N.D Phenanthrene N.D Pyrene N.D The recovery for the sample surrogate(s) is outside the QC acceptance limits as noted on the QC Summary. The client was contacted and the data reported. Metals SM 2340 B Total Hardness as CaCO SW B Arsenic J Barium *=This limit was used in the evaluation of the final result Page 6 of 26
7 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:30 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH0- CAT SDG#: PEJ53-0 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation Metals SW B Cadmium N.D Calcium Chromium J Lead Magnesium Nickel Selenium N.D Silver J Vanadium SW A Mercury N.D Wet Chemistry EPA 664A HEM (oil & grease) n.a. N.D General Sample Comments All QC is compliant unless otherwise noted. Please refer to the Quality Control Summary for overall QC performance data and associated samples. CAT Analysis Name Silvertip & Mayflower VOCs GC/MS VOA Water Prep PAHs in waters by SIM 0470 BNA Water Extraction (SIM) Total Hardness as CaCO Arsenic Barium Cadmium 0750 Calcium 0705 Chromium Lead 0757 Magnesium 0706 Nickel Selenium Silver 0707 Vanadium Mercury 0848 WW SW846 ICP Digest (tot rec) 0573 WW SW846 Hg Digest Laboratory Sample Analysis Record Trial# Batch# Analysis Date and Time SW B 25mL I320AA 07/29/203 2:07 purge SW B I320AA 07/29/203 2:07 SW C SIM 3209WAA026 07/30/203 05:8 SW C 3209WAA026 07/29/203 9:45 SM 2340 B-997 SW B SW B SW B SW B SW B SW B SW B SW B SW B SW B SW B SW A SW A SW A /30/203 04: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 06: /29/203 6: /29/203 6:30 *=This limit was used in the evaluation of the final result Analyst Kerri E Legerlotz Kerri E Legerlotz Brian K Graham Nicholas W Shroyer Deborah A Krady Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Damary Valentin Kevin C Piaskowski Nelli S Markaryan Page 7 of 26
8 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:30 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH0- SDG#: PEJ53-0 Laboratory Sample Analysis Record CAT Analysis Name HEM (oil & grease) EPA 664A Trial# Batch# A Analysis Date and Time 07/29/203 08:37 Analyst Yolunder Y Bunch *=This limit was used in the evaluation of the final result Page 8 of 26
9 Sample Description: SH Filtered Grab Surface Water Mayflower, AR Pipeline Incident LL Sample # WW LL Group # Account # 4739 Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:30 by JW Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 Mobil Pipeline Company PO Box 446 Houston TX SH0F CAT SDG#: PEJ53-02 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation Metals Dissolved SW B Arsenic N.D Barium Cadmium N.D Chromium N.D Lead N.D Nickel J Selenium N.D Silver N.D Vanadium N.D SW A Mercury N.D General Sample Comments This sample was filtered in the laboratory for dissolved metals. All QC is compliant unless otherwise noted. Please refer to the Quality Control Summary for overall QC performance data and associated samples. CAT Analysis Name Arsenic Barium Cadmium 0705 Chromium Lead 0706 Nickel Selenium Silver 0707 Vanadium Mercury 0848 WW SW846 ICP Digest (tot rec) 0573 WW SW846 Hg Digest Laboratory Sample Analysis Record Trial# Batch# Analysis Date and Time SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW B /30/203 02:48 SW A /30/203 06:04 SW A /29/203 6:5 SW A /29/203 6:30 Analyst Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Damary Valentin Kevin C Piaskowski Nelli S Markaryan *=This limit was used in the evaluation of the final result Page 9 of 26
10 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:45 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH02- CAT SDG#: PEJ53-03 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation GC/MS Volatiles SW B 25mL purge Acetone J Allyl Chloride N.D Benzene N.D Bromobenzene N.D Bromochloromethane N.D Bromodichloromethane N.D Bromoform N.D Bromomethane N.D Butanone N.D n-butylbenzene N.D sec-butylbenzene N.D tert-butylbenzene N.D Carbon Tetrachloride N.D Chlorobenzene N.D Chloroethane N.D Chloroform N.D Chloromethane N.D Chlorotoluene N.D Chlorotoluene N.D ,2-Dibromo-3-chloropropane N.D Dibromochloromethane N.D ,2-Dibromoethane N.D Dibromomethane N.D ,2-Dichlorobenzene N.D ,3-Dichlorobenzene N.D ,4-Dichlorobenzene N.D Dichlorodifluoromethane N.D ,-Dichloroethane N.D ,2-Dichloroethane N.D ,-Dichloroethene N.D cis-,2-dichloroethene N.D trans-,2-dichloroethene N.D Dichlorofluoromethane N.D ,2-Dichloropropane N.D ,3-Dichloropropane N.D ,2-Dichloropropane N.D ,-Dichloropropene N.D cis-,3-dichloropropene N.D trans-,3-dichloropropene N.D Ethyl ether N.D Ethylbenzene N.D Freon N.D Hexachlorobutadiene N.D Isopropylbenzene N.D p-isopropyltoluene N.D Methyl Tertiary Butyl Ether N.D Methyl-2-Pentanone N.D Methylene Chloride N.D *=This limit was used in the evaluation of the final result Page 0 of 26
11 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:45 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH02- CAT SDG#: PEJ53-03 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation GC/MS Volatiles SW B 25mL purge n-propylbenzene N.D Styrene N.D ,,,2-Tetrachloroethane N.D ,,2,2-Tetrachloroethane N.D Tetrachloroethene N.D Tetrahydrofuran N.D Toluene ,2,3-Trichlorobenzene N.D ,2,4-Trichlorobenzene N.D ,,-Trichloroethane N.D ,,2-Trichloroethane N.D Trichloroethene N.D Trichlorofluoromethane N.D ,2,3-Trichloropropane N.D ,2,4-Trimethylbenzene N.D ,3,5-Trimethylbenzene N.D Vinyl Chloride N.D Xylene (Total) N.D GC/MS Semivolatiles SW C SIM Acenaphthene N.D Acenaphthylene N.D Anthracene N.D Benzo(a)anthracene J Benzo(a)pyrene N.D Benzo(b)fluoranthene N.D Benzo(g,h,i)perylene J Benzo(k)fluoranthene N.D Chrysene J Dibenz(a,h)anthracene N.D Fluoranthene N.D Fluorene J Indeno(,2,3-cd)pyrene N.D Methylnaphthalene J Methylnaphthalene J Naphthalene N.D Phenanthrene J Pyrene J The recovery for the sample surrogate(s) is outside the QC acceptance limits as noted on the QC Summary. The client was contacted and the data reported. Metals SM 2340 B Total Hardness as CaCO SW B Arsenic J Barium *=This limit was used in the evaluation of the final result Page of 26
12 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:45 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH02- CAT SDG#: PEJ53-03 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation Metals SW B Cadmium N.D Calcium Chromium J Lead J Magnesium Nickel J Selenium N.D Silver N.D Vanadium SW A Mercury N.D Wet Chemistry EPA 664A HEM (oil & grease) n.a. N.D General Sample Comments All QC is compliant unless otherwise noted. Please refer to the Quality Control Summary for overall QC performance data and associated samples. CAT Analysis Name Silvertip & Mayflower VOCs GC/MS VOA Water Prep PAHs in waters by SIM 0470 BNA Water Extraction (SIM) Total Hardness as CaCO Arsenic Barium Cadmium 0750 Calcium 0705 Chromium Lead 0757 Magnesium 0706 Nickel Selenium Silver 0707 Vanadium Mercury 0848 WW SW846 ICP Digest (tot rec) 0573 WW SW846 Hg Digest Laboratory Sample Analysis Record Trial# Batch# Analysis Date and Time SW B 25mL I320AA 07/29/203 2:28 purge SW B I320AA 07/29/203 2:28 SW C SIM 3209WAA026 07/30/203 05:48 SW C 3209WAA026 07/29/203 9:45 SM 2340 B-997 SW B SW B SW B SW B SW B SW B SW B SW B SW B SW B SW B SW A SW A SW A /30/203 04: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 02: /30/203 06: /29/203 6: /29/203 6:30 *=This limit was used in the evaluation of the final result Analyst Kerri E Legerlotz Kerri E Legerlotz Brian K Graham Nicholas W Shroyer Deborah A Krady Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Damary Valentin Kevin C Piaskowski Nelli S Markaryan Page 2 of 26
13 Sample Description: SH Grab Surface Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:45 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 by JW Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 SH02- SDG#: PEJ53-03 Laboratory Sample Analysis Record CAT Analysis Name HEM (oil & grease) EPA 664A Trial# Batch# A Analysis Date and Time 07/29/203 08:37 Analyst Yolunder Y Bunch *=This limit was used in the evaluation of the final result Page 3 of 26
14 Sample Description: SH Filtered Grab Surface Water Mayflower, AR Pipeline Incident LL Sample # WW LL Group # Account # 4739 Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 08:45 by JW Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 Mobil Pipeline Company PO Box 446 Houston TX SH02F CAT SDG#: PEJ53-04 Analysis Name CAS Number Result Detection Limit* Limit of Quantitation Metals Dissolved SW B Arsenic N.D Barium Cadmium N.D Chromium N.D Lead N.D Nickel J Selenium N.D Silver N.D Vanadium N.D SW A Mercury N.D General Sample Comments This sample was filtered in the laboratory for dissolved metals. All QC is compliant unless otherwise noted. Please refer to the Quality Control Summary for overall QC performance data and associated samples. CAT Analysis Name Arsenic Barium Cadmium 0705 Chromium Lead 0706 Nickel Selenium Silver 0707 Vanadium Mercury 0848 WW SW846 ICP Digest (tot rec) 0573 WW SW846 Hg Digest Laboratory Sample Analysis Record Trial# Batch# Analysis Date and Time SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW B /30/203 02:56 SW A /30/203 06:4 SW A /29/203 6:5 SW A /29/203 6:30 Analyst Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Tara L Snyder Damary Valentin Kevin C Piaskowski Nelli S Markaryan *=This limit was used in the evaluation of the final result Page 4 of 26
15 Sample Description: WS-TB Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 TB06 CAT SDG#: PEJ53-05TB* Analysis Name CAS Number Result Detection Limit* Limit of Quantitation GC/MS Volatiles SW B 25mL purge Acetone N.D Allyl Chloride N.D Benzene N.D Bromobenzene N.D Bromochloromethane N.D Bromodichloromethane N.D Bromoform N.D Bromomethane N.D Butanone N.D n-butylbenzene N.D sec-butylbenzene N.D tert-butylbenzene N.D Carbon Tetrachloride N.D Chlorobenzene N.D Chloroethane N.D Chloroform N.D Chloromethane N.D Chlorotoluene N.D Chlorotoluene N.D ,2-Dibromo-3-chloropropane N.D Dibromochloromethane N.D ,2-Dibromoethane N.D Dibromomethane N.D ,2-Dichlorobenzene N.D ,3-Dichlorobenzene N.D ,4-Dichlorobenzene N.D Dichlorodifluoromethane N.D ,-Dichloroethane N.D ,2-Dichloroethane N.D ,-Dichloroethene N.D cis-,2-dichloroethene N.D trans-,2-dichloroethene N.D Dichlorofluoromethane N.D ,2-Dichloropropane N.D ,3-Dichloropropane N.D ,2-Dichloropropane N.D ,-Dichloropropene N.D cis-,3-dichloropropene N.D trans-,3-dichloropropene N.D Ethyl ether N.D Ethylbenzene N.D Freon N.D Hexachlorobutadiene N.D Isopropylbenzene N.D p-isopropyltoluene N.D Methyl Tertiary Butyl Ether N.D Methyl-2-Pentanone N.D Methylene Chloride N.D *=This limit was used in the evaluation of the final result Page 5 of 26
16 Sample Description: WS-TB Water Mayflower, AR Pipeline Incident Project Name: Mayflower, AR Pipeline Incident Collected: 07/26/203 Submitted: 07/27/203 09:35 Reported: 07/30/203 3:04 Mobil Pipeline Company PO Box 446 Houston TX LL Sample # WW LL Group # Account # 4739 TB06 CAT SDG#: PEJ53-05TB* Analysis Name CAS Number Result Detection Limit* Limit of Quantitation GC/MS Volatiles SW B 25mL purge n-propylbenzene N.D Styrene N.D ,,,2-Tetrachloroethane N.D ,,2,2-Tetrachloroethane N.D Tetrachloroethene N.D Tetrahydrofuran N.D Toluene N.D ,2,3-Trichlorobenzene N.D ,2,4-Trichlorobenzene N.D ,,-Trichloroethane N.D ,,2-Trichloroethane N.D Trichloroethene N.D Trichlorofluoromethane N.D ,2,3-Trichloropropane N.D ,2,4-Trimethylbenzene N.D ,3,5-Trimethylbenzene N.D Vinyl Chloride N.D Xylene (Total) N.D General Sample Comments All QC is compliant unless otherwise noted. Please refer to the Quality Control Summary for overall QC performance data and associated samples. Laboratory Sample Analysis Record CAT Analysis Name Silvertip & Mayflower VOCs GC/MS VOA Water Prep SW B 25mL purge SW B Trial# Batch# I320AA I320AA Analysis Date and Time 07/29/203 3:0 07/29/203 3:0 Analyst Kerri E Legerlotz Kerri E Legerlotz *=This limit was used in the evaluation of the final result Page 6 of 26
17 Page of 6 Quality Control Summary Client Name: Group Number: Reported: 07/30/3 at 0:04 PM Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise specified in the method. All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless otherwise noted on the Analysis Report. Laboratory Compliance Quality Control Blank Blank Blank Report LCS LCSD LCS/LCSD Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max Batch number: I320AA Sample number(s): ,742342, Acetone N.D Allyl Chloride N.D Benzene N.D Bromobenzene N.D Bromochloromethane N.D Bromodichloromethane N.D Bromoform N.D Bromomethane N.D Butanone N.D n-butylbenzene N.D sec-butylbenzene N.D tert-butylbenzene N.D Carbon Tetrachloride N.D Chlorobenzene N.D Chloroethane N.D Chloroform N.D Chloromethane N.D Chlorotoluene N.D Chlorotoluene N.D ,2-Dibromo-3-chloropropane N.D Dibromochloromethane N.D ,2-Dibromoethane N.D Dibromomethane N.D ,2-Dichlorobenzene N.D ,3-Dichlorobenzene N.D ,4-Dichlorobenzene N.D Dichlorodifluoromethane N.D ,-Dichloroethane N.D ,2-Dichloroethane N.D ,-Dichloroethene N.D cis-,2-dichloroethene N.D trans-,2-dichloroethene N.D Dichlorofluoromethane N.D ,2-Dichloropropane N.D ,3-Dichloropropane N.D ,2-Dichloropropane N.D ,-Dichloropropene N.D cis-,3-dichloropropene N.D trans-,3-dichloropropene N.D Ethyl ether N.D Ethylbenzene N.D Freon 3 N.D Hexachlorobutadiene N.D *- Outside of specification **-This limit was used in the evaluation of the final result for the blank () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added. Page 7 of 26
18 Page 2 of 6 Quality Control Summary Client Name: Group Number: Reported: 07/30/3 at 0:04 PM Blank Blank Blank Report LCS LCSD LCS/LCSD Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max Isopropylbenzene N.D p-isopropyltoluene N.D Methyl Tertiary Butyl Ether N.D Methyl-2-Pentanone N.D Methylene Chloride N.D n-propylbenzene N.D Styrene N.D ,,,2-Tetrachloroethane N.D ,,2,2-Tetrachloroethane N.D Tetrachloroethene N.D Tetrahydrofuran N.D Toluene N.D ,2,3-Trichlorobenzene N.D ,2,4-Trichlorobenzene N.D ,,-Trichloroethane N.D ,,2-Trichloroethane N.D Trichloroethene N.D Trichlorofluoromethane N.D ,2,3-Trichloropropane N.D ,2,4-Trimethylbenzene N.D ,3,5-Trimethylbenzene N.D Vinyl Chloride N.D Xylene (Total) N.D Batch number: 3209WAA026 Sample number(s): , Acenaphthene N.D Acenaphthylene N.D Anthracene N.D Benzo(a)anthracene N.D Benzo(a)pyrene N.D Benzo(b)fluoranthene N.D Benzo(g,h,i)perylene N.D Benzo(k)fluoranthene N.D Chrysene N.D Dibenz(a,h)anthracene N.D Fluoranthene N.D Fluorene N.D Indeno(,2,3-cd)pyrene N.D Methylnaphthalene N.D Methylnaphthalene N.D Naphthalene N.D Phenanthrene N.D Pyrene N.D Batch number: Sample number(s): Arsenic N.D Barium N.D Cadmium N.D Calcium 0.06 J Chromium N.D Lead N.D Magnesium N.D Nickel N.D Selenium N.D Silver N.D Vanadium N.D *- Outside of specification **-This limit was used in the evaluation of the final result for the blank () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added. Page 8 of 26
19 Page 3 of 6 Quality Control Summary Client Name: Group Number: Reported: 07/30/3 at 0:04 PM Blank Blank Blank Report LCS LCSD LCS/LCSD Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max Batch number: Sample number(s): Mercury N.D Batch number: A Sample number(s): , HEM (oil & grease) N.D Sample Matrix Quality Control Unspiked (UNSPK) = the sample used in conjunction with the matrix spike Background (BKG) = the sample used in conjunction with the duplicate MS MSD MS/MSD RPD BKG DUP DUP Dup RPD Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max Batch number: I320AA Sample number(s): ,742342, UNSPK: P42305 Acetone Allyl Chloride Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Butanone n-butylbenzene sec-butylbenzene tert-butylbenzene Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chlorotoluene Chlorotoluene ,2-Dibromo-3-chloropropane Dibromochloromethane ,2-Dibromoethane Dibromomethane ,2-Dichlorobenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Dichlorodifluoromethane ,-Dichloroethane ,2-Dichloroethane ,-Dichloroethene cis-,2-dichloroethene trans-,2-dichloroethene Dichlorofluoromethane ,2-Dichloropropane ,3-Dichloropropane ,2-Dichloropropane ,-Dichloropropene *- Outside of specification **-This limit was used in the evaluation of the final result for the blank () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added. Page 9 of 26
20 Page 4 of 6 Quality Control Summary Client Name: Group Number: Reported: 07/30/3 at 0:04 PM Sample Matrix Quality Control Unspiked (UNSPK) = the sample used in conjunction with the matrix spike Background (BKG) = the sample used in conjunction with the duplicate MS MSD MS/MSD RPD BKG DUP DUP Dup RPD Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max cis-,3-dichloropropene trans-,3-dichloropropene Ethyl ether Ethylbenzene Freon Hexachlorobutadiene 87 63* * 30 Isopropylbenzene p-isopropyltoluene Methyl Tertiary Butyl Ether 79* Methyl-2-Pentanone Methylene Chloride n-propylbenzene Styrene ,,,2-Tetrachloroethane ,,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,,-Trichloroethane ,,2-Trichloroethane Trichloroethene Trichlorofluoromethane ,2,3-Trichloropropane ,2,4-Trimethylbenzene ,3,5-Trimethylbenzene Vinyl Chloride Xylene (Total) Batch number: 3209WAA026 Sample number(s): , UNSPK: P42306 Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene 60* 60* Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a,h)anthracene Fluoranthene Fluorene Indeno(,2,3-cd)pyrene Methylnaphthalene Methylnaphthalene Naphthalene Phenanthrene Pyrene Batch number: Sample number(s): UNSPK: P42305 BKG: P42305 Arsenic *- Outside of specification **-This limit was used in the evaluation of the final result for the blank () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added. Page 20 of 26
21 Page 5 of 6 Quality Control Summary Client Name: Group Number: Reported: 07/30/3 at 0:04 PM Sample Matrix Quality Control Unspiked (UNSPK) = the sample used in conjunction with the matrix spike Background (BKG) = the sample used in conjunction with the duplicate MS MSD MS/MSD RPD BKG DUP DUP Dup RPD Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max Barium Cadmium () 20 Calcium 05 (2) (2) Chromium Lead 9 (2) 53 (2) Magnesium 9 (2) 52 (2) Nickel Selenium J 0.07 J 8 () 20 Silver J J 2 () 20 Vanadium Batch number: Sample number(s): UNSPK: BKG: Mercury N.D. N.D. 0 () 20 Batch number: A Sample number(s): , UNSPK: P42306 BKG: P42306 HEM (oil & grease) 66* 64* N.D. N.D. 0 () 8 Surrogate Quality Control Surrogate recoveries which are outside of the QC window are confirmed unless attributed to dilution or otherwise noted on the Analysis Report. Analysis Name: BTEX 25-ml purge Batch number: I320AA Dibromofluoromethane,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Blank LCS MS MSD Limits: Analysis Name: PAHs in waters by SIM Batch number: 3209WAA026 Fluoranthene-d0 Benzo(a)pyrene-d2 -Methylnaphthalened * * 89 Blank LCS MS MSD Limits: *- Outside of specification **-This limit was used in the evaluation of the final result for the blank () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added. Page 2 of 26
22 Page 6 of 6 Quality Control Summary Client Name: Group Number: Reported: 07/30/3 at 0:04 PM Surrogate Quality Control *- Outside of specification **-This limit was used in the evaluation of the final result for the blank () The result for one or both determinations was less than five times the LOQ. (2) The unspiked result was more than four times the spike added. Page 22 of 26
23 Page 23 of 26
24 Page 24 of 26
25 Page 25 of 26
26 Explanation of Symbols and Abbreviations The following defines common symbols and abbreviations used in reporting technical data: RL Reporting Limit BMQL Below Minimum Quantitation Level N.D. none detected MPN Most Probable Number TNTC Too Numerous To Count CP Units cobalt-chloroplatinate units IU International Units NTU nephelometric turbidity units umhos/cm micromhos/cm ng nanogram(s) C degrees Celsius F degrees Fahrenheit meq milliequivalents lb. pound(s) g gram(s) kg kilogram(s) µg microgram(s) mg milligram(s) ml milliliter(s) L liter(s) m3 cubic meter(s) µl microliter(s) pg/l picogram/liter ppm ppb < less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can be reliably determined using this specific test. > greater than parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (), because one liter of water has a weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas. parts per billion Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight basis concentration to approximate the value present in a similar sample without moisture. All other results are reported on an as-received basis. Data Qualifiers: C result confirmed by reanalysis. J - estimated value The result is the Detection Limit (MDL) and < the Limit of Quantitation (LOQ). U.S. EPA CLP Data Qualifiers: Organic Qualifiers Inorganic Qualifiers A TIC is a possible aldol-condensation product B Value is <CRDL, but IDL B Analyte was also detected in the blank E Estimated due to interference C Pesticide result confirmed by GC/MS M Duplicate injection precision not met D Compound quantitated on a diluted sample N Spike sample not within control limits E Concentration exceeds the calibration range of S of standard additions (MSA) used the instrument for calculation N Presumptive evidence of a compound (TICs only) U Compound was not detected P Concentration difference between primary and W Post digestion spike out of control limits confirmation columns >25% * Duplicate analysis not within control limits U Compound was not detected + Correlation coefficient for MSA <0.995 X,Y,Z Defined in case narrative Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis. Measurement uncertainty values, as applicable, are available upon request. Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. This report shall not be reproduced except in full, without the written approval of the laboratory. Times are local to the area of activity. Parameters listed in the 40 CFR part 36 Table II as analyze immediately are not performed within 5 minutes. WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL, CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND (B) WHETHER EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client Page 26 of 26
ANALYTICAL RESULTS. Project: Mayflower, AR Pipeline Incident
ANALYTICAL RESULTS Prepared by: Eurofins Lancaster Laboratories Environmental 2425 New Holland Pike Lancaster, PA 760 Prepared for: Houston TX 7720-4592 August 9, 204 Project: Mayflower, AR Pipeline Incident
More informationANALYTICAL RESULTS. Project: Mayflower, AR Pipeline Incident
ANALYTICAL RESULTS Prepared by: Eurofins Lancaster Laboratories Environmental 2425 New Holland Pike Lancaster, PA 760 Prepared for: PO Box 4592 Houston TX 7720-4592 June 8, 204 Project: Mayflower, AR Pipeline
More informationANALYTICAL RESULTS. Project: Mayflower, AR Pipeline Incident
ANALYTICAL RESULTS Prepared by: Eurofins Lancaster Laboratories Environmental 2425 New Holland Pike Lancaster, PA 760 Prepared for: PO Box 4592 Houston TX 7720-4592 April 3, 205 Project: Mayflower, AR
More informationBIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: CTRA Project: 6454 T Lab Order: A 6454 Aqueous 3/1/2013.
Date: 08-Mar-13 Work Order Sample Summary Lab Sample ID Client Sample ID Matrix Collection Date Date Received 1303004-01A 6454 Aqueous 3/1/2013 3/1/2013 Page 1 of 1 Date: 08-Mar-13 CASE NARRATIVE Samples
More informationBIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: Cascade Thornapple River Assoc. Project: Water Analysis Lab Order:
Date: 31-Jul-18 Work Order Sample Summary Lab Sample ID Client Sample ID Matrix Collection Date Date Received 1807123-01A Dam & Burger Water 7/25/2018 7/25/2018 1807123-02A 48th & RR Water 7/25/2018 7/25/2018
More informationANALYTICAL REPORT. Job Number: Job Description: Transform Complete
ANALYTICAL REPORT Job Number: 640-4848-1 Job Description: Transform Complete For: American Master*Tech Scientific, Inc. 1330 Thurman Street PO BOX 2539 Lodi, CA 95240 Attention: Mr. Adam Kowalczyk Chad
More informationEPA TO-17 Volatile Organic Compounds
EPA TO-17 Volatile Organic Compounds Method TO-17 is used to analyze samples for volatile organic compounds collected on multi-bed sorbent tubes, which are thermally desorbed and cryo-focused on the capillary
More informationValidation of Environmental Water Methods on One System: Considerations for Sample Volume, Purge Parameters and Quality Control Parameters
Validation of Environmental Water Methods on One System: Considerations for Sample Volume, Purge Parameters and Quality Control Parameters Application Note Abstract Water quality laboratories across the
More informationUS EPA Method with the Tekmar Lumin P&T Concentrator, AQUATek LVA and Agilent 7890B GC/5977A MS
APPLICATION NOTE: TECHNOLOGY: INDUSTRY: AN1806 P+T VOC ENV US EPA Method 524.2 with the Tekmar Lumin P&T Concentrator, AQUATek LVA and Agilent 7890B GC/5977A MS Amy Nutter, Applications Chemist; Teledyne
More informationUS EPA Method 8260 with the Tekmar Atomx XYZ P&T System and Agilent 7890B GC/5977A MS
Application Note US EPA Method 8260 with the Tekmar Atomx XYZ P&T System and Agilent 7890B GC/5977A MS Author Amy Nutter Applications Chemist, Teledyne Tekmar Abstract US EPA Method 8260 in conjunction
More informationSolid Phase Micro Extraction of Flavor Compounds in Beer
Solid Phase Micro Extraction of Flavor s in Beer ANNE JUREK USEPA 524.2 Method Validation Using the Evolution Purge and Trap Concentrator and the Centurion WS Autosampler Application Note Environmental
More informationValidation of USEPA Method Using a Stratum PTC, AQUATek 100 Autosampler, and Perkin-Elmer Clarus 600 GC/MS
Validation of USEPA Method 524.2 Using a Stratum PTC, AQUATek 100 Autosampler, and Perkin-Elmer Clarus 600 GC/MS Application Note By: Nathan Valentine Abstract The US EPA developed Method 524.2¹, Measurement
More informationTable 1 Soil and Groundwater Sampling Summary Table
Table Soil and Groundwater Sampling Summary Table Phase II Investigation Consolidated Edison - Former kent Avenue Generating Station 0 Kent Avenue Brooklyn, NY Sample ID Date Installed Date Sample Collected
More informationBuilding 280A and Building 450 Soil Sampling Results Richmond Field Station Site Berkeley Global Campus at Richmond Bay, Richmond, California
TETRA TECH, INC. February 5, 2016 Lynn Nakashima Berkeley Regional Office 700 Heinz Avenue, Suite 200C Berkeley, California 94710 Subject: Building 280A and Building 450 Soil Sampling Results Richmond
More informationAnalysis of Volatile Organic Compounds Using USEPA Method 8260 and the 4760 Purge and Trap and the 4100 Autosampler
Analysis of Volatile Organic Compounds Using USEPA Method 8260 and the 4760 Purge and Trap and the Introduction Although analysis of VOCs by purge and trap is considered a mature technique, advances in
More informationRoger Bardsley, Applications Chemist; Teledyne Tekmar Page 1
Application Note US EPA Method 524.2 with the Teledyne Tekmar Lumin P&T Concentrator and Agilent 7890B GC / 5977A MS Roger Bardsley, Applications Chemist; Teledyne Tekmar Page 1 Abstract US EPA Method
More informationUsing Hydrogen as An Alternative Carrier Gas for US EPA 8260
Using Hydrogen as An Alternative Carrier Gas for US EPA 8260 Application Note Abstract Due to regional shortages and increasing costs of helium, the preferred carrier gas in gas chromatography, alternative
More informationThe following report includes the data for the above referenced project for sample(s) received on 5/15/2017 at Air Toxics Ltd.
5/26/2017 Ms. Anna Kelley Hamilton Co. Environmental Services 250 Wm. Howard Taft Cincinnati OH 45219 Project Name: Sun Coke Project #: Workorder #: 1705303 Dear Ms. Anna Kelley The following report includes
More informationLaboratory Report Number(s) Lone Tree Road (Deep) 10/5/15, 10/19/15, 6/13/16. Address Sample Date(s) Analyses Requested
July 14, 216 Mr. Shaun Lehman MDEQ-OOGM Lansing District Office Constitution Hall 2 South 525 West Allegan Street Lansing, MI 48913 Re: Residential Well Sampling Hartland 36 Gas Plant SE/NE/NW Section
More informationOptimal VOC Method Parameters for the StratUm PTC Purge & Trap Concentrator
Optimal VOC Method Parameters for the StratUm PTC Purge & Trap Concentrator Application Note Introduction Environmental laboratories have utilized the Purge & Trap sample concentration technique for over
More informationMethanol Extraction of high level soil samples by USEPA Method 8260C
Methanol Extraction of high level soil samples by USEPA Method 8260C Abstract In order to determine the concentration of Volatile Organic Compounds (VOCs) in soil and waste samples the USEPA developed
More informationPerformance of a Next Generation Vial Autosampler for the Analysis of VOCs in Water Matrices
Application Note Performance of a Next Generation Vial Autosampler for the Analysis of VOCs in Water Matrices Abstract By: Ed Price In today s laboratories, increased efficiency and productivity are of
More informationValidation of USEPA Method 8260C Using Teledyne Tekmar Atomx, and Perkin-Elmer Clarus 600 GC/MS
Validation of USEPA Method 8260C Using Teledyne Tekmar Atomx, and Perkin-Elmer Clarus 600 GC/MS Application Note By Tyler Trent Abstract In order to determine the concentration of volatile organic compounds
More informationValidation of Volatile Organic Compound by USEPA. Method 8260C. Application Note. Abstract. Introduction. Experimental-Instrument Conditions
Validation of Volatile Organic Compound by USEPA Method 8260C Application Note Abstract In order to determine the concentration of volatile organic compounds (VOCs) in water and soil matrices the USEPA
More informationANALYTICAL REPORT. Results relate only to the items tested and the sample(s) as received by the laboratory. Page 1 of 5
ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Client For: Imperial Paints LLC PO BOX 489 Fairforest, South Carolina 29336
More informationKSA Environmental Laboratory Inc.
February 26, 07 KSA Environmental Laboratory Inc. Hydrologic Associates - Miami Attn: Brad Waller 8925 S.W. 148th Street Suite 212 Miami, FL 33176 RE: Parkland KSA Workorder: Q0012 Dear Brad Waller, Enclosed
More informationRoger Bardsley, Applications Chemist; Teledyne Tekmar P a g e 1
Application Note US EPA Method 524.4 with the Tekmar Lumin P & T Concentrator and Thermo Scientific TRACE 1310 GC and ISQ LT MS System Roger Bardsley, Applications Chemist; Teledyne Tekmar P a g e 1 Abstract
More informationMaximizing Sample Throughput In Purge And Trap Analysis
Maximizing Sample Throughput In Purge And Trap Analysis LINDSEY PYRON ANNE JUREK INTRODUCTION There are several demands and requirements imposed on chemists performing volatile organic analysis (VOC) in
More informationA Comparison of Volatile Organic Compound Response When Using Nitrogen as a Purge Gas
A Comparison of Volatile Organic Compound When Using Nitrogen as a Gas Application Note By: Anne Jurek Abstract For many years Helium has been the gas of choice for purging Volatile Organic Compounds (VOCs).
More information2017 EPA Method Update Rule and EPA Method 624.1
Introduction Method 624 is for the determination of volatile organic compounds in industrial discharges and other liquid environmental samples by gas chromatography combined with mass spectrometry (GC/MS).
More informationAnalysis of Volatile Organic Compounds in Water and Soil by EPA Method 8260 with the Atomx Concentrator/Multimatrix Autosampler
Analysis of Volatile Organic Compounds in Water and Soil by EPA Method 8260 with the Atomx Concentrator/Multimatrix Autosampler Application Note By: Anne Jurek Abstract In order to determine the amount
More informationAnalysis of Volatile Organic Compounds in Soil Samples by EPA Method 8260 with The Stratum PTC and SOLATek 72 Multi-Matrix Autosampler
Analysis of Volatile Organic Compounds in Soil Samples by EPA Method 8260 with The Stratum PTC and SOLATek 72 Multi-Matrix Autosampler Application Note By: Teri Dattilio Introduction Purge and Trap concentration
More informationOptimizing. Abstract: is standardd. procedures. altered to
Optimizing Standard Preparation ANNE JUREK Abstract: Standardd preparation can often be a time consuming, tedious process. The opportunity for human error or inconsistencies between individual preparation
More informationTarget Compound Results Summary
Phone/ (86)88-4800 / (86)88-471 http://www.emsl.com to1lab@emsl.com Customer ID: EMSL0A K12312.D 28 cc 0 0/01/2017 K12327.D 21 cc 600 Target Compound Results Summary Propylene 11-07-1 42.08 ND.0 ND 8.6
More informationImproved Volatiles Analysis Using Static Headspace, the Agilent 5977B GC/MSD, and a High-efficiency Source
Improved Volatiles Analysis Using Static Headspace, the Agilent 5977B GC/MSD, and a High-efficiency Source Application Note Environmental Authors Peter Gautschi and Harry Prest Senior Application Scientist
More informationValidation of USEPA Method Using a Stratum PTC and the New AQUATek 100 Autosampler
Validation of USEPA Method 524.2 Using a Stratum PTC and the New AQUATek 100 Autosampler Application Note Abstract Automation is the key to increasing laboratory productivity and minimizing costs. It is
More informationExploring US EPA Method 524 Purge and Trap Variables: Water Vapor Reduction and Minimizing Cycle Time
Exploring US EPA Method 524 Purge and Trap Variables: Water Vapor Reduction and Minimizing Cycle Time Roger Bardsley, Applications Chemist; Teledyne Tekmar Page 1 Introduction Purge and Trap (P&T) concentrators
More informationNon-Potable Water A2LA Certificate
COLOR Color Biochemical Oxygen Demand (BOD); Carbonaceous DEMAND BOD; Chemical Oxygen Demand (COD); Total Organic Carbon (TOC) HEXAVALENT CHROMIUM INORGANIC NUTRIENTS LOW-LEVEL MERCURY METALS I & II METALS
More informationAnalysis. Introduction: necessary. presented. Discussion: As part of be carried. consistent and reliable data. (MoRT) to.
Optimal Conditions for USEPA Method 8260 Analysis Anne Jurek Introduction: Over the past decade, the need for environmental laboratoriess using purge and trap systems to report at or below the Method Detection
More informationSystem and JUREK ANNE. Introduction: in an in purge and. trap sampling. Discussion: As part of. consistent and reliable data. (MoRT) to.
ANNE JUREK Optimal Conditions for USEPA Method 8260B Analysis Using the EST Analyticall Sampling System and the Shimadzu GCMS-QP2010s Introduction: The USEPA developedd Method 8260B for the determination
More informationAppendix 2 Data Distributions for Contaminants in Water and Sediment Samples in Response to the Deepwater Horizon Oil Spill, 2010
University of Nebraska - Lincoln DigitalCommons@University of Nebraska - Lincoln Publications of the US Geological Survey US Geological Survey 2013 Appendix 2 Data Distributions for Contaminants in Water
More informationAmec Foster Wheeler Environment & Infrastructure, Inc BIG SHANTY ROAD, NW, SUITE 100 KENNESAW, GEORGIA (770)
Dutch Valley Rd NE Worchester Dr NE Hillpine Dr NE Maddox Dr NE Lee St SW Maddox Dr NE Avery Dr NE E Park Ln NE Piedmont Ave NE Yorkshire Rd NE ³ Park Ln NE Westminster Dr NE Piedmont Way NE Westminster
More informationCertificate of Accreditation
PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: (Hereinafter called the Organization) and hereby declares
More information2. September 2015 Sub-Concrete Slab Soil Investigation
To: Pam Barnett, RACER Ref. No.: 11109615 From: John-eric Pardys/kf/1 Date: October 30, 2015 Re: Summary of Sub-Concrete Slab Soil Investigation RACER Fredericksburg Facility Spotsylvania County, Virginia
More informationCALA Directory of Laboratories
CALA Directory of Laboratories Membership Number: 2628 Laboratory Name: Caduceon Environmental Laboratories (Richmond Hill) Parent Institution: Caduceon Enterprises Inc. Address: 110 West Beavercreek Rd.
More informationAUTONOMOUS, REAL TIME DETECTION OF 58 VOCS IN THE PANAMA CANAL
AUTONOMOUS, REAL TIME DETECTION OF 58 VOCS IN THE PANAMA CANAL Challenges of Water Monitoring Volatile Organic Compounds (VOCs) can have negative health impacts even at ppb levels VOC concentrations can
More informationEd George and Anaïs Viven Varian, Inc.
Application Note SI-02408 Evaluation of EPA Method 524.3: a New Draft Method for the Analysis of VOCs in Drinking Water using GC/MS and V:Results GC/MS Software Ed George and Anaïs Viven Varian, Inc. Introduction
More informationSolid Phase Micro Extraction of Flavor Compounds in Beer
Solid Phase Micro Extraction of Flavor Compounds in Beer ANNE JUREK Automed Sampling of Methanol Extractions Applicion Note Environmental Author Anne Jurek Applicions Chemist EST Analytical Cincinni, OH
More informationU.S. EPA VOLATILE ORGANICS METHOD USING PURGE AND TRAP GC/MS
ENVIRONMENTAL application note U.S. EPA VOLATILE ORGANICS METHOD 524.2 USING PURGE AND TRAP GC/MS Cheri Coody, Public Health Laboratory, Mississippi State Health Department, Jackson, MS USA Michael J.
More informationANALYTICAL REPORT. Attn: Dan Spector
ANALYTICAL REPORT TestAmerica Laboratories, Inc. Benjamin Road Suite 0 Tampa, FL Tel: ()- TestAmerica Job I: 0-- Client Revision: For: Langan Engineering & Environmental Srvcs 0 NW th Court Suite 00 Miami
More informationJanuary 19, Dear Mr. Nightingale:
January 19, 2011 Mr. Steven F. Nightingale, P.E. Manager, Permit Section Illinois Environmental Protection Agency Bureau of Land 1021 North Grand Avenue East Springfield, Illinois 62794 Subject: Supplemental
More informationMaximizing Production While Minimizing Costs
JSB is an authorised partner of Maximizing Production While Minimizing Costs Anne Jurek #123 Abstract: The need to increase productivity and reduce cost is becoming of greater concern to environmental
More informationNational Pollutant Discharge Elimination System (NPDES); BADCT Limits for Volatile Organic Compounds
Permit Guidance 12 Final National Pollutant Discharge Elimination System (NPDES); BADCT Limits for Volatile Organic Compounds Statutory references: ORC 6111.01, 6111.03, 6111.04 Rule references: OAC 3745-1-05,
More informationCERTIFICATE OF ANALYSIS
Your Project #: VILLAGE OF TAHSIS Your C.O.C. #: 084437 Attention:Mark DeGagne -35 Estevan Rd Nanaimo, BC CANADA V9S 3Y3 Report #: R24287 Version: - Final MAXXAM JOB #: B5B343 Received: 205/2/22, 5:45
More informationANALYTICAL REPORT. Job Number: SDG Number: Job Description: Joint Base Cape Cod
ANALYTICAL REPORT Job Number: 200-33700-1 SDG Number: 33700 Job Description: Joint Base Cape Cod For: Dawson Technical, LLC 900 Fort Street Mall Suite 1700 Honolulu, HI 96813 Attention: Troy Hile James
More informationA Single Calibration Method for Water AND Soil Samples Performing EPA Method 8260
JSB is an authorised partner of A Single Calibration Method for Water AND Soil Samples Performing EPA Method 8260 Anne Jurek #101 Introduction: The United States Environmental Protection Agency (USEPA)
More informationMethod 8260C by Purge and Trap Gas Chromatography Mass Spectrometry using the Clarus SQ 8
application Note Gas Chromatography/ Mass Spectrometry Authors Ruben Garnica Dawn May PerkinElmer, Inc. Shelton, CT USA Method by Purge and Trap Gas Chromatography Mass Spectrometry using the Clarus SQ
More informationA Site Location Map and Site and Surrounding Properties Map are attached as Figure 1 and Figure 2, respectively.
February 23, 216 Mr. Shaun Lehman MDEQ-OOGM Lansing District Office Constitution Hall 2 South 525 West Allegan Street Lansing, MI 48913 Re: Groundwater Characterization Work Plan Hartland 36 Gas Plant
More informationSUMMARY REPORT OF AIR MONITORING FOR LEED CERTIFICATION PHASE 2 SWANSFIELD ELEMENTARY SCHOOL 5610 CEDAR LANE COLUMBIA, MD PREPARED FOR:
SUMMARY REPORT OF AIR MONITORING FOR LEED CERTIFICATION PHASE 2 SWANSFIELD ELEMENTARY SCHOOL 5610 CEDAR LANE COLUMBIA, MD 21044 PREPARED FOR: HOWARD COUNTY PUBLIC SCHOOL SYSTEM 10910 ROUTE 108 ELLICOTT
More information317 Elm Street Milford, NH (603) Fax (603)
317 Elm Street Milford, NH 03055 (603) 673-5440 Fax (603) 673-0366 Sales@chemservelab.com Friday, October 06, 2017 Domenic Carapella Greenplay Organics, LLC 6 Hawthorne Ave Merrick NY 11566 Project Name:
More informationOctober 26, Dear Mr. White:
ExxonMobil Environmental Services Company 38 Varick Street Brooklyn, New York 11222 October 26, 2011 New York State Department of Environmental Conservation Division of Environmental Remediation Remedial
More informationOptimal Conditions for USEPA Method 8260B Analysis using the EST Analytical Sampling system and the Shimadzu GCMS-QP2010s
JSB is an authorised partner of Optimal Conditions for USEPA Method 8260B Analysis using the EST Analytical Sampling system and the Shimadzu GCMS-QP2010s Anne Jurek #120 Introduction: The USEPA developed
More informationCopies: Dave Favero, RACER File
MEMO To: Nate Nemani USEPA Region 5 77 West Jackson Boulevard Mail Code: LU-9J Chicago, Illinois 60604-3507 Copies: Dave Favero, RACER File Arcadis of Michigan, LLC 300 S. Washington Square Suite 315 Lansing
More informationOptimizing of Volatile Organic Compound Determination by Static Headspace Sampling
JSB is an authorised partner of Optimizing of Volatile Organic Compound Determination by Static Headspace Sampling Anne Jurek Introduction: #134 Static headspace sampling has always been a viable option
More informationDetection of Volatile Organic Compounds in polluted air by an Agilent mini Thermal Desorber and an Agilent 5975T LTM GC/MS
Detection of Volatile Organic Compounds in polluted air by an Agilent mini Thermal Desorber and an Agilent 5975T LTM GC/MS Application Note Environmental Author Xiaohua Li Agilent Technologies (Shanghai)
More informationCertificate of Accreditation
PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: (Hereinafter called the Organization) and hereby declares
More information/J~ GOLDER. Golder Associates Inc. golder.com. Project No April 25, 2018
GOLDER April 25, 2018 Project No. 0236105018 Canadian Pacific Plaza Attn: Aimee Zack 120 South 6th Street Suite 700 Minneapolis, MN 55402 RE: SHOREHAM YARD - SOUTHEAST PUMP & TREAT SYSTEM MCES SPECIAL
More informationCertificate of Accreditation
PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: (Hereinafter called the Organization) and hereby declares
More informationOptimizing Standard Preparation
JSB is an authorised partner of Optimizing Standard Preparation Anne Jurek #106 Abstract: Standard preparation can often be a time consuming, tedious process. The opportunity for human error or inconsistencies
More informationOREGON Environmental Laboratory Accreditation Program ORELAP Fields of Accreditation ALS Environmental - Simi Valley
MATRIX Reference Code Analyte Code Description ASTM C471M- 14 2014 ASTM D5504-12 2012 3964 Orthorhombic Cyclooctasulfur 4842 1-Propanethiol 6113 2,5-Dimethylthiophene 4544 2-Ethylthiophene 4843 2-Propanethiol
More informationAPPENDIX D Laboratory Analytical Reports
Allied Aviation Initial Abatement Report, Arlington, VA December 4, 2015 Amec Foster Wheeler Project 37650016 APPENDIX D Laboratory Analytical Reports #=CL# LIMS USE: FR - JOHN MITTAUER LIMS OBJECT ID:
More informationHelium conservation in volatile organic compound analysis using U.S. EPA Method 8260C
APPLICATION NOTE 10441 Helium conservation in volatile organic compound analysis using U.S. EPA Method 8260C Authors Andrea Caruso, 1 Tommaso Albertini, 1 Jacob A. Rebholz 2 ; 1 Thermo Fisher Scientific,
More informationApplication News AD Quantitative Determination of Volatile Organic Compounds in Drinking Water by EPA Method with Headspace Trap GC-MS
HS-20 & GCMS-QP2010Ultra Quantitative Determination of Volatile Organic Compounds in Drinking Water by EPA Method with Headspace Trap GC-MS Introduction Volatile Organic Compounds (VOCs) refer to a group
More informationINNOVATIVE PRODUCTS, SUPERIOR SUPPORT. Presenter: Anne Jurek, Senior Applications Chemist, EST Analytical
INNOVATIVE PRODUCTS, SUPERIOR SUPPORT Presenter: Anne Jurek, Senior Applications Chemist,, pp, EST Analytical Air pollution is a growing problem due to the global economy and industrial development in
More informationDate Issued: April 01, 2013 Expiration Date: June 30, 2013
State of Florida Department of Health~Bureau of Public Health Laboratories I his is to certify that ALS ENVIRONMENTAL - SIMI VALLEY 2655 PARK CENTER DRIVE, SUITE A SIMI VALLEY, CA 93065 has complied with
More informationChemical Solvents 1010 Dennison Road Cleveland, OH 44109 Chris Rander Client Project: S12054050614/2106050914 EA Group Workorder Number: 140500165 Received on May 9, 2014 The following analytical report
More informationCertificate of Accreditation
PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: (Hereinafter called the Organization) and hereby declares
More informationDetection of Environmental Contaminants Caused by the Oil Spill in the Gulf of Mexico by GC and Hplc
Detection of Environmental Contaminants Caused by the Oil Spill in the Gulf of Mexico by GC and Hplc Sky Countryman, Ngoc Nguyen, Jeff Layne, Kory Kelly, and Zeshan Aqeel Phenomenex, Inc., 411 Madrid Ave.,
More informationMethods and Analytes Requiring Laboratory Certification Attachment 3
s and s Requiring Laboratory Certification Attachment 3 Current as of July 1, 2011 Laboratory Certificates need to accurately reflect the methods performed and reported by the laboratory, including the
More informationSolid Phase Microextraction of Cyanogen Chloride and Other Volatile Organic Compounds in Drinking Water with Fast Analysis by GC-TOFMS
Solid Phase Microextraction of Cyanogen Chloride and Other Volatile Organic Compounds in Drinking Water with Fast Analysis by GC-TOFMS LECO Corporation; Saint Joseph, Michigan USA Key Words: GC-TOFMS,
More informationBarbara Johnson, PE Associate
Q'/jt Golder Associates September 29, 2017 Project No.:023-6105.017 Metropolitan Council Environmental Services Industrial Waste Division 390 Robert St. N. St. Paul, MN 55101 Attention: Ms. Ashley Corbeille
More informationGOLDER. Golder Associates Inc. Al-1!1f;s. golder.com. June 22, Project No
GOLDER June 22, 2018 Project No. 0236105018 Canadian Pacific Plaza Attn: Aimee Zack 120 South 6th Street Suite 700 Minneapolis, MN 55402 RE: SHOREHAM YARD-SOUTHEAST PUMP & TREAT SYSTEM MCES SPECIAL DISCHARGE
More informationMeasuring Environmental Volatile Organic Compounds by U.S. EPA Method 8260B with Headspace Trap GC/MS
application Note Gas Chromatography Author Heidi Grecsek PerkinElmer, Inc. Shelton, CT 06484 USA Measuring Environmental Volatile Organic Compounds by U.S. EPA Method 8260B with Headspace Trap GC/MS Introduction
More informationAnalysis of Low Level Volatile Organic Compounds in Air Anne Jurek
JSB is an authorised partner of Analysis of Low Level Volatile Organic s in Air Anne Jurek #111 Introduction The New Jersey Department of Environmental Protection (NJDEP) developed a new low level TO-15
More informationMethod 8270C PAH. FD- Field Duplicate Samples
Mr. John Rendall Maine Yankee 321 Old Ferry Road Wiscasset, Maine 04578 RE: Project No.: Maine Yankee Sediment Samples Lab Name: Katahdin Analytical Services, Westbrook, Maine Site Name: Maine Yankee Nuclear
More information1. Introduction. 2. Sampling Activities
CH2M HILL Canada Limited 72 Victoria Street Suite 0 Kitchener, ON N2G 4Y9 O +519 579 3500 F +519 579 8986 www.ch2m.com Tara Tran, MCIP, RPP Policy Planner The Corporation of the City of Brantford 100 Wellington
More informationNELAC PT for Accreditation Fields of Proficiency Testing with PTRLs Drinking Water Effective: November 03, 2017
Microbiology CFU/100 ml CFU/100 ml 054 500 Total Coliform 8,9,10 Nine out of ten correct with no false negatives Not Applicable 055 530 Fecal Coliform 8,9,10 Nine out of ten correct with no false negatives
More informationIf you have any questions or concerns, please do not hesitate to contact our office at
May 22, 2015 Jeannette DeBartolomeo Environmental Compliance Specialist MDE-OCP 1800 Washington Blvd. Suite 620 Baltimore, MD 21230 RE: Groundwater and Drinking Water Results Calvert Citgo (Former Alger
More informationMETHOD 5021 VOLATILE ORGANIC COMPOUNDS IN SOILS AND OTHER SOLID MATRICES USING EQUILIBRIUM HEADSPACE ANALYSIS
METHOD 5021 VOLATILE ORGANIC COMPOUNDS IN SOILS AND OTHER SOLID MATRICES USING EQUILIBRIUM HEADSPACE ANALYSIS 1.0 SCOPE AND APPLICATION 1.1 Method 5021 is a general purpose method for the preparation of
More informationTETRA TECH, INC. December 8, Lynn Nakashima Berkeley Regional Office 700 Heinz Avenue, Suite 200C Berkeley, California 94710
TETRA TECH, INC. December 8, 2014 Lynn Nakashima Berkeley Regional Office 700 Heinz Avenue, Suite 200C Berkeley, California 94710 Subject: LBNL Fiber Optic Distributed Acoustic Sensor (DAS) Survey Sampling
More informationR.E.A.C.T. Roxbury Environmental Action CoaliTion P.O. Box 244 Ledgewood, N.J Website:
R.E.A.C.T. Roxbury Environmental Action CoaliTion P.O. Box 244 Ledgewood, N.J. 07852 Website: www.reactnj.org Email: info@reactnj.org RE: Air Test Results R.E.A.C.T. has facilitated an ambient air test
More informationA Single Calibration for Waters and Soil Samples Performing EPA Method Anne Jurek Applications Chemist
A Single Calibration for Waters and Soil Samples Performing EPA Method 8260 Anne Jurek Applications Chemist Abstract A Single Calibration Method for Water AND Soil Samples The United States Environmental
More informationReduced VOC Sample Analysis Times Using a New Dual Purge-and-Trap System
Reduced VOC Sample Analysis Times Using a New Dual Purge-and-Trap System Application Note 19080203 Keywords Dual Purge-and-Trap Eclipse Sample Concentrator Gas Chromatography GC GC/MS Model 4560 Sample
More informationCALA Directory of Laboratories
CALA Directory of Laboratories Membership Number: 2460 Laboratory Name: ROPEC Laboratory Parent Institution: City of Ottawa, Laboratory Services Address: 800 Greens Creek Dr, Ottawa ON K1J 1A6 Contact:
More informationMcCAMPBELL ANALYTICAL INC Willow Pass Road Pittsburg CA
Comparison of VOC : s, Target Lists, MAI Acenaphthene 83-32-9 Acetalaldehyde (Ethanal) 75-07-0 Acetone 67-64-1 Acetonitrile 75-05-8 Acetophenone 96-86-2 Acrolein (Propenal) 107-02-8 Acrylamide 79-06-1
More informationCertificate of Accreditation
PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: 6701 Aberdeen Avenue, Suite #9, Lubbock, TX 79424
More informationSUBSURFACE (PHASE II) INVESTIGATION REPORT
SUBSURFACE (PHASE II) INVESTIGATION REPORT AKRF, Inc. 440 Park Avenue South New York, NY 10016 212-696-0670 Submitted to: Cayuga Indian Nation P.O. Box 11 Versailles, New York 14168 299 Cayuga Street Village
More informationDetermination of Volatile Organic Compounds in Air
JSB is an authorised partner of Determination of Volatile Organic s in Air Anne Jurek #126 Introduction Air pollution is a growing problem due to the global economy and industrial development in many countries.
More information