ANALYTICAL REPORT. Job Number: Job Description: Transform Complete

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1 ANALYTICAL REPORT Job Number: Job Description: Transform Complete For: American Master*Tech Scientific, Inc Thurman Street PO BOX 2539 Lodi, CA Attention: Mr. Adam Kowalczyk Chad Bechtold Project Manager I cbechtold@stl-inc.com 01/26/2006 These test results meet all the requirements of NELAC. All questions regarding this test report should be directed to the STL Project Manager who signed this test report. Measurement uncertainty data, as referenced in Section 8.6 of the STL Tallahassee LQM, are available upon request. Severn Trent Laboratories, Inc. STL Tallahassee 2846 Industrial Plaza Drive, Tallahassee, FL Tel Fax Page 1 of 17

2 CASE NARRATIVE STL Log No(s): Client Project ID: Transform Complete I. RECEIPT The samples were received at 15.6 degrees Celsius with no ice or water present in the cooler. Per the client, the laboratory proceeded with the analysis. II. HOLDING TIMES The Transform Complete sample vials for method 8260B were determined to have a ph of 7 even though the vials were HCl preserved. The sample was analyzed for method 8260B two days outside a shortened 7 day holding time imposed for samples with a ph greater than 2. III. PREPARATION Sample preparation proceeded normally. IV. ANALYSIS A. Calibration: All acceptance criteria were met. B. Blanks: The method blank for formaldehyde had a hit at 62 ug/l. This is due to the extremely high concentration of formaldehyde in the 10 % Formalin Solution sample. All other acceptance criteria were met. C. Spikes: The Laboratory Control Standard (LCS) for formaldehyde was biased high. The formaldehyde LCSD met acceptance criteria. Several compounds were biased high for the method 8260B LCS/LCSD. These compounds have been qualified with an *. No hits were detected in the sample for the compounds with high bias. D. Surrogates: All acceptance criteria were met. E. Samples: No analytical problems were encountered. Page 2 of 17

3 METHOD SUMMARY Description Lab Location Method Preparation Method Matrix: Water Volatile Organic Compounds by GC/MS STL-TAL SW B Purge-and-Trap STL-TAL SW B Carbonyl Compounds by HPLC STL-TAL 8315 Solid Phase Extraction STL-TAL SW A SW _W_Prep ph, Electrometric STL-TAL MCAWW LAB REFERENCES: STL-TAL = STL-Tallahassee METHOD REFERENCES: MCAWW - "Methods For Chemical Analysis Of Water And Wastes", EPA-600/ , March 1983 And Subsequent Revisions. SW846 - "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. STL Tallahassee Page 3 of 17

4 SAMPLE SUMMARY Lab Sample ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received % Formalin Transform Complete Water 01/09/ /10/ Water 01/09/ /10/ STL Tallahassee Page 4 of 17

5 Analytical Data Client Sample ID: Transform Complete Lab Sample ID: Client Matrix: Water Date Sampled: Date Received: 01/09/ /10/ B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B Analysis Batch: B /18/ /18/ Instrument ID: VME 5973N Lab File ID: 1E D Analyte Result (ug/l) Qualifier RL 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethylbenzene STL Tallahassee Page 5 of 17 <10 * 10 <25 *

6 Analytical Data Client Sample ID: Transform Complete Lab Sample ID: Client Matrix: Water Date Sampled: Date Received: 01/09/ /10/ B Volatile Organic Compounds by GC/MS Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B Analysis Batch: B /18/ /18/ Instrument ID: VME 5973N Lab File ID: 1E D Analyte Result (ug/l) Qualifier RL Ethylene Dibromide Hexachlorobutadiene Isopropylbenzene Methyl Ethyl Ketone methyl isobutyl ketone Methylene Chloride m-xylene & p-xylene Naphthalene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total <10 * 10 <10 10 < < < Surrogate %Rec Acceptance Limits 1,2-Dichlorobenzene-d4 4-Bromofluorobenzene Dibromofluoromethane Toluene-d STL Tallahassee Page 6 of 17

7 Analytical Data Client Sample ID: 10% Formalin Lab Sample ID: Client Matrix: Water Date Sampled: Date Received: 01/09/ /10/ Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8315A Carbonyl Compounds by HPLC 8315A Analysis Batch: _W_Prep Prep Batch: /12/ /10/ Instrument ID: LCL Waters 486 Lab File ID: 1A12L3.d Injection Volume: 10 ul 4 ml Analyte Result (ug/l) Qualifier RL Formaldehyde B * STL Tallahassee Page 7 of 17

8 Analytical Data Client Sample ID: Transform Complete Lab Sample ID: Client Matrix: Water Date Sampled: Date Received: 01/09/ /10/ A Carbonyl Compounds by HPLC Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8315A Analysis Batch: _W_Prep Prep Batch: /11/ /10/ Instrument ID: LCL Waters 486 Lab File ID: 2A11L22.d Injection Volume: 100 ml 4 ml Analyte Result (ug/l) Qualifier RL Formaldehyde <50 * 50 STL Tallahassee Page 8 of 17

9 Analytical Data General Chemistry Client Sample ID: Transform Complete Lab Sample ID: Client Matrix: Water Date Sampled: Date Received: 01/09/ /10/ Analyte ph Result Qual Units RL Dil Method 6.17 SU Anly Batch: Date Analyzed 01/10/ STL Tallahassee Page 9 of 17

10 DATA REPORTING QUALIFIERS Lab Section Qualifier Description GC/MS VOA * LCS, LCSD, MS, MSD, MD, or Surrogate exceeds the control limits HPLC B * Compound was found in the blank and sample. LCS, LCSD, MS, MSD, MD, or Surrogate exceeds the control limits STL Tallahassee Page 10 of 17

11 Quality Control Results Surrogate Recovery Report 8260B Volatile Organic Compounds by GC/MS Lab Sample ID Client Sample (12DCB) (%Rec) (BFB) (%Rec) (DBFM) (%Rec) (TOL) (%Rec) Transform Complete LCS /3 LCS LCSD /4 LCSD MB /5 MB Surrogate Acceptance Limits (12DCB) 1,2-Dichlorobenzene-d (BFB) 4-Bromofluorobenzene (DBFM) Dibromofluoromethane (TOL) Toluene-d STL Tallahassee Page 11 of 17

12 Quality Control Results Client: American Master*Tech Scientific, Inc. Job Number: Method Blank - Batch: Method: 8260B Preparation: 5030B Lab Sample ID: MB /5 Dilution: 1.0 Date Analyzed: 01/18/ Date Prepared: 01/18/ Analysis Batch: Prep Batch: N/A Units: ug/l Instrument ID: Lab File ID: VME 5973N 1E D Analyte Result Qual RL 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Dibromomethane Dichlorobromomethane <10 10 <25 25 Calculations are performed before rounding to avoid round-off errors in calculated results. STL Tallahassee Page 12 of 17

13 Quality Control Results Client: American Master*Tech Scientific, Inc. Job Number: Method Blank - Batch: Method: 8260B Preparation: 5030B Lab Sample ID: MB /5 Dilution: 1.0 Date Analyzed: 01/18/ Date Prepared: 01/18/ Analysis Batch: Prep Batch: N/A Units: ug/l Instrument ID: Lab File ID: VME 5973N 1E D Analyte Result Qual RL Dichlorodifluoromethane Ethylbenzene Ethylene Dibromide Hexachlorobutadiene Isopropylbenzene Methyl Ethyl Ketone methyl isobutyl ketone Methylene Chloride m-xylene & p-xylene Naphthalene n-butylbenzene N-Propylbenzene o-xylene sec-butylbenzene Styrene tert-butylbenzene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes, Total <10 10 <10 10 < < < Surrogate % Rec Acceptance Limits 1,2-Dichlorobenzene-d Bromofluorobenzene Dibromofluoromethane Toluene-d Calculations are performed before rounding to avoid round-off errors in calculated results. STL Tallahassee Page 13 of 17

14 Quality Control Results Client: American Master*Tech Scientific, Inc. Job Number: Laboratory Control/ Laboratory Control Duplicate Recovery Report - Batch: Method: 8260B Preparation: 5030B LCS Lab Sample ID: LCS /3 Dilution: 1.0 Date Analyzed: 01/18/ Date Prepared: 01/18/ Analysis Batch: Prep Batch: N/A Units: ug/l Instrument ID: Lab File ID: VME 5973N 1E D LCSD Lab Sample ID: LCSD /4 Dilution: 1.0 Date Analyzed: 01/18/ Date Prepared: 01/18/ Analysis Batch: Prep Batch: N/A Units: ug/l Instrument ID: VME 5973N Lab File ID: 1E D Analyte LCS % Rec. LCSD Limit RPD RPD Limit LCS Qual LCSD Qual 1,1-Dichloroethene Benzene Chlorobenzene Toluene Trichloroethene Calculations are performed before rounding to avoid round-off errors in calculated results. STL Tallahassee Page 14 of 17

15 Quality Control Results Client: American Master*Tech Scientific, Inc. Job Number: Method Blank - Batch: Method: 8315A Preparation: 8315_W_Prep Lab Sample ID: MB /1-A Dilution: 50 Date Analyzed: 01/11/ Date Prepared: 01/10/ Analysis Batch: Prep Batch: Units: ug/l Instrument ID: Lab File ID: Injection Volume: LCL Waters 486 2A11L7.d 100 ml 4 ml Analyte Result Qual RL Formaldehyde Laboratory Control/ Laboratory Control Duplicate Recovery Report - Batch: Method: 8315A Preparation: 8315_W_Prep LCS Lab Sample ID: LCS /2-A Dilution: 50 Date Analyzed: 01/11/ Date Prepared: 01/10/ Analysis Batch: Prep Batch: Units: ug/l Instrument ID: LCL Waters 486 Lab File ID: 2A11L8.d 100 ml 4 ml Injection Volume: LCSD Lab Sample ID: LCSD /3-A Dilution: 50 Date Analyzed: 01/11/ Date Prepared: 01/10/ Analysis Batch: Prep Batch: Units: ug/l Instrument ID: LCL Waters 486 Lab File ID: 2A11L9.d 100 ml 4 ml Injection Volume: Analyte LCS % Rec. LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Formaldehyde * Calculations are performed before rounding to avoid round-off errors in calculated results. STL Tallahassee Page 15 of 17

16 Quality Control Results Client: American Master*Tech Scientific, Inc. Job Number: Laboratory Control Sample - Batch: Method: Preparation: N/A Lab Sample ID: LCS /1 Dilution: 1.0 Date Analyzed: 01/10/ Date Prepared: N/A Analysis Batch: Prep Batch: N/A Units: SU Instrument ID: Lab File ID: No Equipment Assigned N/A 50 ml Analyte Spike Amount Result % Rec. Limit Qual ph Matrix Duplicate - Batch: Method: Preparation: N/A Lab Sample ID: Dilution: 1.0 Date Analyzed: 01/10/ Date Prepared: N/A Analysis Batch: Prep Batch: N/A Units: SU Instrument ID: Lab File ID: No Equipment Assigned N/A 50 ml Analyte Sample Result/Qual Result RPD Limit Qual ph Calculations are performed before rounding to avoid round-off errors in calculated results. STL Tallahassee Page 16 of 17

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BIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: CTRA Project: 6454 T Lab Order: A 6454 Aqueous 3/1/2013.

BIO-CHEM Laboratories, Inc. Work Order Sample Summary. CLIENT: CTRA Project: 6454 T Lab Order: A 6454 Aqueous 3/1/2013. Date: 08-Mar-13 Work Order Sample Summary Lab Sample ID Client Sample ID Matrix Collection Date Date Received 1303004-01A 6454 Aqueous 3/1/2013 3/1/2013 Page 1 of 1 Date: 08-Mar-13 CASE NARRATIVE Samples