DHL Analytical received 2 sample(s) on 6/18/2009 for the analyses presented in the following report.
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1 June 26, 2009 Charles E. Martin Breininger Road Hicksvile, OH TEL: (419) FAX: (419) Order No: RE: Dear Charles E. Martin: DHL Analytical received 2 sample(s) on 6/18/2009 for the analyses presented in the following report. There were no problems with the analyses and all data met requirements of NELAC except where noted in the Case Narrative. All non-nelac methods will be identified accordingly in the case narrative and all estimated uncertainties of test results are within method or EPA specifications. If you have any questions regarding these tests results, please feel free to call. Thank you for using DHL Analytical. Sincerely, John DuPont Lab Manager This report was performed under the accreditation of the State of Texas Laboratory Certification Number: T TX 2300 Double Creek Dr. Round Rock, TX Phone: (512) Fax: (512) Page 1 of 14
2 Table of Contents Miscellaneous Documents... 3 Case Narrative... 6 Sample Summary... 7 Prep Dates Report... 8 TCLP Dates Report... 9 Analytical Dates Report Sample Results Analytical QC Summary Report Page 2 of 14
3 Page 3 of 14
4 Page 5 of 14
5 Lab Order: CASE NARRATIVE The samples were analyzed using the method outlined in the following reference: Method SW1311/ TCLP Metals LOG IN A total of 2 samples were received and logged-in on 6/18/2009. The samples arrived in good condition and were properly packaged. TCLP METALS ANALYSIS For TCLP Metals analysis, Copper was detected below the reporting limit for the TCLP Method Blank (MB TCLP). All associated samples showed Copper at greater than ten times the concentration detected in the TCPL MB. This analyte was not detected in the Method Blank for this batch (MB-35630). No further corrective actions were taken. All sample results were below TCLP or RCRA characterization limits. The samples are therefore nonhazardous for the parameters that were analyzed. Page 6 of 14
6 Lab Order: Work Order Sample Summary Lab Smp ID Client Sample ID Tag Number Date Collected Date Recv'd /15/09 01:00 PM 06/18/ /15/09 01:00 PM 06/18/09 Page 7 of 14
7 Lab Order: PREP DATES REPORT Sample ID Client Sample ID Collection Date Matrix Test Number Test Name Prep Date Batch ID A /15/09 01:00 PM Solid SW3005A Aq Prep Metals : ICP-MS 06/24/09 09:00 AM /15/09 01:00 PM Solid SW3005A Aq Prep Metals : ICP-MS 06/24/09 09:00 AM A /15/09 01:00 PM Solid SW3005A Aq Prep Metals : ICP-MS 06/24/09 09:00 AM /15/09 01:00 PM Solid SW3005A Aq Prep Metals : ICP-MS 06/24/09 09:00 AM Page 8 of 14
8 Lab Order: TCLP DATES REPORT Sample ID Client Sample ID Collection Date Matrix Test Number Test Name Prep Date Batch ID A /15/09 01:00 PM Solid SW1311 TCLP Sample Prep (Metals) 06/23/09 04:30 PM A /15/09 01:00 PM Solid SW1311 TCLP Sample Prep (Metals) 06/23/09 04:30 PM Page 9 of 14
9 Lab Order: ANALYTICAL DATES REPORT Sample ID Client Sample ID Matrix Test Number Test Name Batch ID Dilution Analysis Date Run ID A Solid SW1311/6020 TCLP Metals /24/09 03:18 PM ICP-MS2_090624A Solid SW1311/6020 TCLP Metals /24/09 04:40 PM ICP-MS2_090624A A Solid SW1311/6020 TCLP Metals /24/09 03:23 PM ICP-MS2_090624A Solid SW1311/6020 TCLP Metals /24/09 04:45 PM ICP-MS2_090624A Page 10 of 14
10 Client Sample ID: Lab ID: Project No: Collection Date: 06/15/09 01:00 PM Lab Order: Matrix: Solid Analyses Result MDL RL Qual Units DF Date Analyzed TCLP Metals SW1311/6020 Analyst: KW Copper mg/l 50 06/24/09 04:40 PM Nickel mg/l 1 06/24/09 03:18 PM Qualifiers: * Value exceeds TCLP Maximum Concentration Level B Analyte detected in the associated Method Blank C Sample Result or QC discussed in the Case Narrative DF Dilution Factor E TPH pattern not Gas or Diesel Range Pattern J MDL N ND RL S Analyte detected between MDL and RL Method Detection Limit Parameter not NELAC certified Not Detected at the Method Detection Limit Reporting Limit Spike Recovery outside control limits Page 11 of 14
11 Client Sample ID: Lab ID: Project No: Collection Date: 06/15/09 01:00 PM Lab Order: Matrix: Solid Analyses Result MDL RL Qual Units DF Date Analyzed TCLP Metals SW1311/6020 Analyst: KW Copper mg/l /24/09 04:45 PM Nickel mg/l 1 06/24/09 03:23 PM Qualifiers: * Value exceeds TCLP Maximum Concentration Level B Analyte detected in the associated Method Blank C Sample Result or QC discussed in the Case Narrative DF Dilution Factor E TPH pattern not Gas or Diesel Range Pattern J MDL N ND RL S Analyte detected between MDL and RL Method Detection Limit Parameter not NELAC certified Not Detected at the Method Detection Limit Reporting Limit Spike Recovery outside control limits Page 12 of 14
12 Work Order: ANALYTICAL QC SUMMARY REPORT RunID: ICP-MS2_090624A Sample ID: MB Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: MBLK Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 02:51 PM Prep Date: 06/24/09 Copper ND Nickel ND Sample ID: MB TCLP Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: MBLK Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 02:56 PM Prep Date: 06/24/09 Copper Nickel ND Sample ID: LCS Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: LCS Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 03:02 PM Prep Date: 06/24/09 Copper Nickel Sample ID: LCSD Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: LCSD Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 03:07 PM Prep Date: 06/24/09 Copper Nickel Sample ID: A SD Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: SD Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 04:18 PM Prep Date: 06/24/09 Copper Nickel Sample ID: A PDS Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: PDS Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 04:24 PM Prep Date: 06/24/09 Copper Nickel Sample ID: A MS Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: MS Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 04:29 PM Prep Date: 06/24/09 Copper Nickel Sample ID: A MSD Batch ID: TestNo: SW1311/6020 Units: mg/l SampType: MSD Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 04:34 PM Prep Date: 06/24/09 Copper Nickel Qualifiers: B Analyte detected in the associated Method Blank DF Dilution Factor J Analyte detected between MDL and RL MDL Method Detection Limit ND Not Detected at the Method Detection Limit R RL S J N RPD outside accepted control limits Reporting Limit Spike Recovery outside control limits Analyte detected between SDL and RL Parameter not NELAC certified Page 13 of 14
13 Work Order: ANALYTICAL QC SUMMARY REPORT RunID: ICP-MS2_090624A Sample ID: ICV Batch ID: R43965 TestNo: SW1311/6020 Units: mg/l SampType: ICV Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 02:23 PM Prep Date: Copper Nickel Sample ID: CCV Batch ID: R43965 TestNo: SW1311/6020 Units: mg/l SampType: CCV Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 03:51 PM Prep Date: Copper Nickel Sample ID: CCV Batch ID: R43965 TestNo: SW1311/6020 Units: mg/l SampType: CCV Run ID: ICP-MS2_090624A Analysis Date: 06/24/09 04:50 PM Prep Date: Copper Nickel Qualifiers: B Analyte detected in the associated Method Blank DF Dilution Factor J Analyte detected between MDL and RL MDL Method Detection Limit ND Not Detected at the Method Detection Limit R RL S J N RPD outside accepted control limits Reporting Limit Spike Recovery outside control limits Analyte detected between SDL and RL Parameter not NELAC certified Page 14 of 14
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