November 23, Mr. Shawn Liddle District Clerk Albion Central School District 324 East Avenue Albion, NY 14411

Transcription

1 November 23, 2016 Mr. Shawn Liddle District Clerk Albion Central School District 324 East Avenue Albion, NY Re: Lead in Sampling Report Albion Central School District Sodoma Elementary School Dear Mr. Liddle: At your request, Sienna Environmental Technologies conducted water sampling, screening for lead contaminants at the above referenced properties in accordance with 1370-a and 1110, Subpart 67-4 of Title 10 (Health) of the Official Compilation of Codes, Rules and Regulations of the State of New York, and US EPA guidelines. If you have any questions, or if we can be of assistance in any other way, please do not hesitate to call. Thank you for the opportunity to be of service to Albion Central School District. Sincerely, Sienna Environmental Technologies, LLC Raymond Cich Operations Manager

2 Lead in Sampling In Accordance with NYCRR Title 10, Subpart 67-4 OF THE: Albion Central School District Sodoma Elementary School PREPARED BY: PREPARED FOR: Albion Central School District 324 East Avenue Albion, NY CONDITIONS AS OF: September 29, 2016

3 Summary Tabulation 1. Lead in Sampling 1.1 Introduction 1.2 Summary Table of Analysis that exceeds the action Level 1.3 Discussion and Recommendations Appendices A General Conditions of Inspection B Chains of Custody and oratory Reports C Sample Location Maps and Client Supplied Sample List D NYCRR Title 10, Subpart 67-4

4 1. Lead in Sampling 1.1 Introduction Sienna Environmental Technologies performed client directed sampling of potable water outlets. The sampling event was conducted on September 13 and September 29, 2016 prior to the facilities opening in the morning and before any water was used; known as a first-draw sample. The outlets tested were reported to be out of service for a minimum of 8 hours, but not more than 18 hours, prior to sample collection. Sampling was conducted at outlets specified by the client at the following school: Sodoma Elementary School Sienna Environmental Technologies was charged with: 1. Collecting a first-draw sample volume of 250 milliliters (ml), collected from cold water outlets after not being used for 8-18 hours. Sample locations were client directed. 2. Sending samples to an independent laboratory for lead analysis by ICP in conformance with NYS and US EPA guidelines. 3. Providing a report of the sampling and analysis of the potable water for lead contamination to the School District.

5 1.2 Summary of Non-Compliant Analysis NYCRR Title 10, Subpart 67-4 recommends that any water fountains and/or outlets be taken out of service if analysis indicates lead levels which exceed 15 parts per billion (ppb) based on a 250 ml firstdraw sample. 15 ppb is equivalent to 15 micrograms per liter (µg/l). The following is a list of outlets in excess of 15 ppb. For a comprehensive list of outlets sampled, see appendix B. Sample Date Client ID Sample No. Sample Description Location of Outlet of Outlet Result (µg/l) Sodoma Elementary School ES-B8-DW-01 Room B8 Drinking Fountain Without Chiller ES-KITCHEN KETTLE WEST-KCC-01 Kitchen Kitchen Kettle Filler ES-C8-CFC-01 Room C8 Classroom Faucet Cold ES-E7-RR-BFC-01 Room E7 Rest Room Bathroom Faucet Cold ES-E4-CFC-01 Room E4 Classroom Faucet Cold ES-NMO-CSC-01 Near Main Office Custodial Slop Sink Cold ES-B8-BFC-01 Bathroom B8 Bathroom Faucet Cold ES-B8-CFC-01 Room B8 Classroom Faucet Cold ES-G7-RR-BFC-01 Room G7 Rest Room Bathroom Faucet Cold ES-WSGW-HBC-01 West Side G Wing Hose Bib Cold ES-WSEW-HBC-01 West Side E Wing Hose Bib Cold ES-WSDW-HBC-01 West Side D Wing Hose Bib Cold ES-NSDW-HBC-01 North Side D Wing Hose Bib Cold ES-NEAW-HBC-01 North End A Wing Hose Bib Cold ES-ESGW-HBC-01 East Side G Wing Hose Bib Cold ES-ESHW-HBC-01 East Side H Wing Hose Bib Cold ES-NSJW-HBC-01 North Side J Wing Hose Bib Cold ES-WSR-HBC-01 West Side Receiving Hose Bib Cold 16

6 1.3 Discussion and Recommendations The testing provided is representative of the water that may be consumed at the beginning of the day or after infrequent use. It consists of water that has been in contact with the fixture and the plumbing connecting the faucet or the lateral pipes. Section Response should be followed as your next steps to comply with NYCRR Title 10, Subpart Once section has been completed, Sienna recommends the following actions for samples that exceed the action limit: Collect an additional first draw sample for analysis. Collect a follow-up flush sample. This sample is collected after the first draw sample is collected and the faucet is allowed to run for 30 seconds and is representative of the water that is in the plumbing upstream from the faucet. This testing protocol will aid in identifying the potential source of the elevated lead level. If the lead level in the first draw sample is higher than that in the follow-up flush sample, the source of lead is the water faucet and/or the plumbing upstream from the faucet. If the lead level in follow-up flush sample is very low, i.e. close to 5 ppb, very little lead is coming from the plumbing upstream from the faucet. The majority or all of the lead in the water is from the faucet and/or the plumbing connecting the faucet to the lateral. If the lead level in the follow-up flush sample significantly exceeds 5 ppb (i.e. close to 10 ppb), lead from the plumbing upstream from the faucet may be contributing to these results. In Addition, NYCRR Title 10, Subpart 67-4 states that you may find the United States Environmental Protection Agency s guidance document helpful, titled 3Ts for Reducing Lead in Drinking in Schools, Revised Technical Guidance. This document includes sample notifications letters, press releases, and provides guidance through the process of reducing lead exposure.

7 Appendix A General Conditions of Sampling 1. Sienna Environmental Technologies, LLC neither accepts nor implies any liability for the implementation of the recommendations found within this report. 2. The results of the laboratory analytical reports that may be contained herein are the product of the knowledge, experience and expertise of the laboratory retained to perform such services. Sienna Environmental Technologies neither accepts nor implies any liability for sample analysis reports compiled by others. 3. This report is based on the condition and contents present at the site on the day of the inspection. Sienna Environmental Technologies, LLC is not liable for materials, chemicals or other substances of concern that may have been removed or introduced to the site, prior to the inspection date or subsequent to that date.

8 Appendix B Chains of Custody and oratory Reports

9 ANALYTICAL REPORT TestAmerica oratories, Inc. TestAmerica Buffalo 10 Hazelwood Drive Amherst, NY Tel: (716) TestAmerica Job ID: TestAmerica Sample Delivery Group: SET2893 Client Project/Site: Albion CSD For: Sienna Environmental Technologies LLC 350 Elmwood Avenue Buffalo, New York Attn: Suzanne Kelley Authorized for release by: 9/22/2016 3:17:19 PM Rebecca Jones, Project Management Assistant I rebecca.jones@testamericainc.com Designee for Melissa Deyo, Project Manager I (716) melissa.deyo@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

10 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Table of Contents TestAmerica Job ID: SDG: SET2893 Cover Page Table of Contents Definitions/Glossary Case Narrative Detection Summary Client Sample Results QC Sample Results QC Association Summary Chronicle Certification Summary Summary Sample Summary Chain of Custody Receipt Checklists Page 2 of 68 TestAmerica Buffalo 9/22/2016

11 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Qualifiers Metals Qualifier J F2 Glossary Abbreviation Definitions/Glossary Qualifier Description Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. MS/MSD RPD exceeds control limits These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac DL, RA, RE, IN Indicates a, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Job ID: SDG: SET TestAmerica Buffalo Page 3 of 68 9/22/2016

12 Case Narrative Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Job ID: oratory: TestAmerica Buffalo Narrative Job Narrative Receipt The samples were received on 9/14/ :45 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 11.0º C and 18.0º C. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page TestAmerica Buffalo Page 4 of 68 9/22/2016

13 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-A1-DW-01 Sample ID: No Detections. Client Sample ID: ES-A2-DW-01 Sample ID: No Detections. Client Sample ID: ES-A3-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.26 J ug/l Client Sample ID: ES-A4-DW-01 Sample ID: No Detections. Client Sample ID: ES-A5-DW-01 Sample ID: No Detections. Client Sample ID: ES-A6-DW-01 Sample ID: No Detections. Client Sample ID: ES-B1-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.52 J ug/l Client Sample ID: ES-B2-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.89 J ug/l Client Sample ID: ES-B4-BFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-B5-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-B6-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.73 J ug/l Client Sample ID: ES-B8-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 5 of 68 9/22/2016

14 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-C1-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.44 J ug/l Client Sample ID: ES-C2-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.91 J ug/l Client Sample ID: ES-C4-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-C5-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-C6-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-C8-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.71 J ug/l Client Sample ID: ES-D1-DW-01 Sample ID: No Detections. Client Sample ID: ES-D2-DW-01 Sample ID: No Detections. Client Sample ID: ES-D3-DW-01 Sample ID: No Detections. Client Sample ID: ES-D4-DW-01 Sample ID: No Detections. Client Sample ID: ES-D5-DW-01 Sample ID: No Detections. Client Sample ID: ES-D6-DW-01 Sample ID: No Detections. This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 6 of 68 9/22/2016

15 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-E1-DW-01 Sample ID: No Detections. Client Sample ID: ES-E2-DW-01 Sample ID: No Detections. Client Sample ID: ES-E3-DW-01 Sample ID: No Detections. Client Sample ID: ES-E4-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.25 J ug/l Client Sample ID: ES-E5-DW-01 Sample ID: No Detections. Client Sample ID: ES-E6-DW-01 Sample ID: No Detections. Client Sample ID: ES-G1-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.20 J ug/l Client Sample ID: ES-G2-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.30 J ug/l Client Sample ID: ES-G3-DW-01 Sample ID: No Detections. Client Sample ID: ES-G4-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.26 J ug/l Client Sample ID: ES-G5-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.35 J ug/l Client Sample ID: ES-G6-DW-01 Sample ID: No Detections. This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 7 of 68 9/22/2016

16 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-H1-DW-01 Sample ID: No Detections. Client Sample ID: ES-H2-DW-01 Sample ID: No Detections. Client Sample ID: ES-H3-DW-01 Sample ID: No Detections. Client Sample ID: ES-H4-DW-01 Sample ID: No Detections. Client Sample ID: ES-H6-DW-01 Sample ID: No Detections. Client Sample ID: ES-H7-DW-01 Sample ID: No Detections. Client Sample ID: ES-J1-DW-01 Sample ID: No Detections Client Sample ID: ES-J2-DW-01 Sample ID: No Detections. Client Sample ID: ES-J3-DW-01 Sample ID: No Detections. Client Sample ID: ES-J4-DW-01 Sample ID: No Detections. Client Sample ID: ES-J5-DW-01 Sample ID: No Detections. Client Sample ID: ES-J6-DW-01 Sample ID: No Detections. Client Sample ID: ES-J7-DW-01 Sample ID: No Detections. Client Sample ID: ES-J8-DW-01 Sample ID: No Detections. This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 8 of 68 9/22/2016

17 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-J9-DW-01 Sample ID: No Detections. Client Sample ID: ES-J11-DW-01 Sample ID: No Detections. Client Sample ID: ES-I1-DW-01 Sample ID: No Detections. Client Sample ID: ES-I2-DW-01 Sample ID: No Detections. Client Sample ID: ES-I3-DW-01 Sample ID: No Detections. Client Sample ID: ES-I4-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.19 J ug/l Client Sample ID: ES-I6-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.29 J ug/l Client Sample ID: ES-I7-DW-01 Sample ID: No Detections. Client Sample ID: ES-K1-DW-01 Sample ID: No Detections. Client Sample ID: ES-K2-DW-01 Sample ID: No Detections. Client Sample ID: ES-K3-DW-01 Sample ID: No Detections. Client Sample ID: ES-K4-DW-01 Sample ID: No Detections. Client Sample ID: ES-K5-DW-01 Sample ID: No Detections. This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 9 of 68 9/22/2016

18 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-K6-DW-01 Sample ID: No Detections. Client Sample ID: ES-K7-DW-01 Sample ID: No Detections. Client Sample ID: ES-K8-DW-01 Sample ID: No Detections. Client Sample ID: ES-SOUTH HALL-WC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-HALL MAIL RM-WC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-HALL BAND RM-WC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-F HALL-WC-01 Sample ID: No Detections. Client Sample ID: ES-COMMUNITY-WC-01 Sample ID: No Detections. Client Sample ID: ES-COMMUNITY NORTH-WC-01 Sample ID: No Detections. Client Sample ID: ES-BOYS LR-WC-01 Sample ID: No Detections. Client Sample ID: ES-GIRLS LR-WC-01 Sample ID: No Detections. Client Sample ID: ES-J HALL-WC-01 Sample ID: No Detections. Client Sample ID: ES-K HALL-WC-01 Sample ID: No Detections. This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 10 of 68 9/22/2016

19 Detection Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-K HALL WEST-WC-01 Sample ID: No Detections. Client Sample ID: ES-K9-DW-01 Sample ID: No Detections. Client Sample ID: ES-K13-DW-01 Sample ID: No Detections. Client Sample ID: ES-J11-CFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-HEALTH OFFICE WEST-CFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.69 J ug/l Client Sample ID: ES-KITCHEN PREP-KFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-KITCHEN KETTLE SOUTH-KFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-KITCHEN-KWS-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-KITCHEN EAST KETTLE-KCC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-KITCHEN KETTLE WEST-KCC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-KITCHEN-IM-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-RECIEVING-IM-01 Sample ID: This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 11 of 68 9/22/2016

20 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Detection Summary TestAmerica Job ID: SDG: SET2893 Client Sample ID: ES-RECIEVING-IM-01 (Continued) Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-PLAYGROUND-DW-01 Sample ID: Lead Result Qualifier RL MDL Unit Dil Fac D ug/l Client Sample ID: ES-CONCESSION STAND SOUTH-DW-01 Sample ID: Lead Result Qualifier RL MDL Unit Dil Fac D Client Sample ID: ES-STACKWICK BLDG SOUTH WEST-DW-01 Lead ug/l Sample ID: Result Qualifier RL MDL Unit Dil Fac D Client Sample ID: ES-STACKWICK BLDG SOUTH EAST-DW-01 Lead ug/l Sample ID: Result Qualifier RL MDL Unit Dil Fac D ug/l Client Sample ID: ES-EAST PRESS BOX-DW-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead 0.95 J ug/l Client Sample ID: ES-CONCESSION STAND NORTH-KFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l Client Sample ID: ES-CONCESSION STAND SOUTH-KFC-01 Sample ID: Result Qualifier RL MDL Unit Dil Fac D Lead ug/l This Detection Summary does not include radiochemical test results. TestAmerica Buffalo Page 12 of 68 9/22/2016

21 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-A1-DW-01 Date Collected: 09/13/16 06:26 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 17:00 09/17/16 05:07 1 Client Sample ID: ES-A2-DW-01 Date Collected: 09/13/16 06:29 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 17:00 09/17/16 05:18 1 Client Sample ID: ES-A3-DW-01 Date Collected: 09/13/16 06:31 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead 0.26 J ug/l 09/16/16 17:00 09/17/16 05:21 1 Client Sample ID: ES-A4-DW-01 Date Collected: 09/13/16 06:32 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:00 09/17/16 05:24 1 Client Sample ID: ES-A5-DW-01 Date Collected: 09/13/16 06:33 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:00 09/17/16 05:33 1 Client Sample ID: ES-A6-DW-01 Date Collected: 09/13/16 06:34 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:00 09/17/16 05:36 1 Client Sample ID: ES-B1-DW-01 Date Collected: 09/13/16 06:40 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.52 J ug/l 09/16/16 17:00 09/17/16 05:39 1 TestAmerica Buffalo Page 13 of 68 9/22/2016

22 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-B2-DW-01 Date Collected: 09/13/16 06:41 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead 0.89 J ug/l 09/16/16 17:00 09/17/16 05:42 1 Client Sample ID: ES-B4-BFC-01 Date Collected: 09/13/16 06:44 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/16/16 17:00 09/18/16 18:53 1 Client Sample ID: ES-B5-DW-01 Date Collected: 09/13/16 06:45 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/16/16 17:00 09/17/16 05:47 1 Client Sample ID: ES-B6-DW-01 Date Collected: 09/13/16 06:47 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.73 J ug/l 09/16/16 17:00 09/17/16 05:50 1 Client Sample ID: ES-B8-DW-01 Date Collected: 09/13/16 06:50 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/16/16 17:00 09/17/16 05:53 1 Client Sample ID: ES-C1-DW-01 Date Collected: 09/13/16 06:55 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.44 J ug/l 09/16/16 17:00 09/17/16 05:55 1 Client Sample ID: ES-C2-DW-01 Date Collected: 09/13/16 06:57 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.91 J ug/l 09/16/16 17:00 09/17/16 05:58 1 TestAmerica Buffalo Page 14 of 68 9/22/2016

23 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-C4-DW-01 Date Collected: 09/13/16 06:58 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ug/l 09/16/16 17:00 09/17/16 06:08 1 Client Sample ID: ES-C5-DW-01 Date Collected: 09/13/16 07:00 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/16/16 17:00 09/17/16 06:11 1 Client Sample ID: ES-C6-DW-01 Date Collected: 09/13/16 07:02 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/16/16 17:30 09/17/16 06:29 1 Client Sample ID: ES-C8-DW-01 Date Collected: 09/13/16 07:04 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.71 J ug/l 09/16/16 17:30 09/17/16 06:46 1 Client Sample ID: ES-D1-DW-01 Date Collected: 09/13/16 07:11 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 06:49 1 Client Sample ID: ES-D2-DW-01 Date Collected: 09/13/16 07:12 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 06:52 1 Client Sample ID: ES-D3-DW-01 Date Collected: 09/13/16 07:13 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 06:55 1 TestAmerica Buffalo Page 15 of 68 9/22/2016

24 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-D4-DW-01 Date Collected: 09/13/16 07:16 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 17:30 09/17/16 06:57 1 Client Sample ID: ES-D5-DW-01 Date Collected: 09/13/16 07:17 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 17:30 09/17/16 07:00 1 Client Sample ID: ES-D6-DW-01 Date Collected: 09/13/16 07:18 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 17:30 09/17/16 07:03 1 Client Sample ID: ES-E1-DW-01 Date Collected: 09/13/16 07:21 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 07:06 1 Client Sample ID: ES-E2-DW-01 Date Collected: 09/13/16 07:22 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 07:08 1 Client Sample ID: ES-E3-DW-01 Date Collected: 09/13/16 07:24 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 07:11 1 Client Sample ID: ES-E4-DW-01 Date Collected: 09/13/16 07:25 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.25 J ug/l 09/16/16 17:30 09/17/16 07:21 1 TestAmerica Buffalo Page 16 of 68 9/22/2016

25 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-E5-DW-01 Date Collected: 09/13/16 07:27 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 17:30 09/17/16 07:23 1 Client Sample ID: ES-E6-DW-01 Date Collected: 09/13/16 07:28 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 17:30 09/17/16 07:26 1 Client Sample ID: ES-G1-DW-01 Date Collected: 09/13/16 07:33 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead 0.20 J ug/l 09/16/16 17:30 09/17/16 07:29 1 Client Sample ID: ES-G2-DW-01 Date Collected: 09/13/16 07:34 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.30 J ug/l 09/16/16 17:30 09/17/16 07:32 1 Client Sample ID: ES-G3-DW-01 Date Collected: 09/13/16 07:35 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 07:49 1 Client Sample ID: ES-G4-DW-01 Date Collected: 09/13/16 07:38 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.26 J ug/l 09/16/16 18:00 09/17/16 08:07 1 Client Sample ID: ES-G5-DW-01 Date Collected: 09/13/16 07:39 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.35 J ug/l 09/16/16 18:00 09/17/16 08:10 1 TestAmerica Buffalo Page 17 of 68 9/22/2016

26 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-G6-DW-01 Date Collected: 09/13/16 07:40 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 18:00 09/17/16 08:13 1 Client Sample ID: ES-H1-DW-01 Date Collected: 09/13/16 07:42 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:00 09/17/16 08:16 1 Client Sample ID: ES-H2-DW-01 Date Collected: 09/13/16 07:45 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:00 09/17/16 08:18 1 Client Sample ID: ES-H3-DW-01 Date Collected: 09/13/16 07:46 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 08:21 1 Client Sample ID: ES-H4-DW-01 Date Collected: 09/13/16 07:48 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 08:24 1 Client Sample ID: ES-H6-DW-01 Date Collected: 09/13/16 07:49 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 08:33 1 Client Sample ID: ES-H7-DW-01 Date Collected: 09/13/16 07:51 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 08:36 1 TestAmerica Buffalo Page 18 of 68 9/22/2016

27 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-J1-DW-01 Date Collected: 09/13/16 07:57 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 18:00 09/17/16 08:39 1 Client Sample ID: ES-J2-DW-01 Date Collected: 09/13/16 07:58 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:00 09/17/16 08:42 1 Client Sample ID: ES-J3-DW-01 Date Collected: 09/13/16 08:00 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:00 09/17/16 08:44 1 Client Sample ID: ES-J4-DW-01 Date Collected: 09/13/16 08:01 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 08:47 1 Client Sample ID: ES-J5-DW-01 Date Collected: 09/13/16 08:02 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 08:50 1 Client Sample ID: ES-J6-DW-01 Date Collected: 09/13/16 08:04 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND F ug/l 09/16/16 18:00 09/17/16 08:53 1 Client Sample ID: ES-J7-DW-01 Date Collected: 09/13/16 08:05 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 09:13 1 TestAmerica Buffalo Page 19 of 68 9/22/2016

28 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-J8-DW-01 Date Collected: 09/13/16 08:06 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 18:30 09/17/16 09:24 1 Client Sample ID: ES-J9-DW-01 Date Collected: 09/13/16 08:08 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:30 09/17/16 09:27 1 Client Sample ID: ES-J11-DW-01 Date Collected: 09/13/16 08:10 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:30 09/17/16 09:30 1 Client Sample ID: ES-I1-DW-01 Date Collected: 09/13/16 06:48 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 09:32 1 Client Sample ID: ES-I2-DW-01 Date Collected: 09/13/16 06:51 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 09:42 1 Client Sample ID: ES-I3-DW-01 Date Collected: 09/13/16 06:55 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 09:45 1 Client Sample ID: ES-I4-DW-01 Date Collected: 09/13/16 06:58 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.19 J ug/l 09/16/16 18:30 09/17/16 09:47 1 TestAmerica Buffalo Page 20 of 68 9/22/2016

29 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-I6-DW-01 Date Collected: 09/13/16 07:00 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead 0.29 J ug/l 09/16/16 18:30 09/17/16 09:50 1 Client Sample ID: ES-I7-DW-01 Date Collected: 09/13/16 07:04 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:30 09/17/16 09:53 1 Client Sample ID: ES-K1-DW-01 Date Collected: 09/13/16 07:07 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/16/16 18:30 09/17/16 09:56 1 Client Sample ID: ES-K2-DW-01 Date Collected: 09/13/16 07:11 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 09:58 1 Client Sample ID: ES-K3-DW-01 Date Collected: 09/13/16 07:15 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 10:01 1 Client Sample ID: ES-K4-DW-01 Date Collected: 09/13/16 07:17 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 10:04 1 Client Sample ID: ES-K5-DW-01 Date Collected: 09/13/16 07:21 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 10:07 1 TestAmerica Buffalo Page 21 of 68 9/22/2016

30 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-K6-DW-01 Date Collected: 09/13/16 07:24 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/16/16 18:30 09/17/16 10:16 1 Client Sample ID: ES-K7-DW-01 Date Collected: 09/13/16 07:26 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 19:03 1 Client Sample ID: ES-K8-DW-01 Date Collected: 09/13/16 07:30 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 19:14 1 Client Sample ID: ES-SOUTH HALL-WC-01 Date Collected: 09/13/16 08:00 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:00 09/18/16 19:17 1 Client Sample ID: ES-HALL MAIL RM-WC-01 Date Collected: 09/13/16 08:06 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:00 09/18/16 19:27 1 Client Sample ID: ES-HALL BAND RM-WC-01 Date Collected: 09/13/16 08:10 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:00 09/18/16 19:30 1 Client Sample ID: ES-F HALL-WC-01 Date Collected: 09/13/16 07:55 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:00 09/18/16 19:32 1 TestAmerica Buffalo Page 22 of 68 9/22/2016

31 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-COMMUNITY-WC-01 Date Collected: 09/13/16 07:52 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 19:35 1 Client Sample ID: ES-COMMUNITY NORTH-WC-01 Date Collected: 09/13/16 07:50 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 19:38 1 Client Sample ID: ES-BOYS LR-WC-01 Date Collected: 09/13/16 07:45 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 19:41 1 Client Sample ID: ES-GIRLS LR-WC-01 Date Collected: 09/13/16 07:47 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:00 09/18/16 19:43 1 Client Sample ID: ES-J HALL-WC-01 Date Collected: 09/13/16 07:43 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:00 09/18/16 19:46 1 Client Sample ID: ES-K HALL-WC-01 Date Collected: 09/13/16 07:37 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:00 09/18/16 19:49 1 Client Sample ID: ES-K HALL WEST-WC-01 Date Collected: 09/13/16 07:35 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:00 09/18/16 19:52 1 TestAmerica Buffalo Page 23 of 68 9/22/2016

32 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-K9-DW-01 Date Collected: 09/13/16 07:33 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 20:01 1 Client Sample ID: ES-K13-DW-01 Date Collected: 09/13/16 07:40 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ND ug/l 09/18/16 14:00 09/18/16 20:04 1 Client Sample ID: ES-J11-CFC-01 Date Collected: 09/13/16 08:18 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/18/16 14:00 09/18/16 20:07 1 Client Sample ID: ES-HEALTH OFFICE WEST-CFC-01 Date Collected: 09/13/16 07:07 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead 0.69 J ug/l 09/18/16 14:30 09/18/16 20:23 1 Client Sample ID: ES-KITCHEN PREP-KFC-01 Date Collected: 09/13/16 06:20 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 20:41 1 Client Sample ID: ES-KITCHEN KETTLE SOUTH-KFC-01 Date Collected: 09/13/16 06:24 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 20:43 1 Client Sample ID: ES-KITCHEN-KWS-01 Date Collected: 09/13/16 06:28 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 20:46 1 TestAmerica Buffalo Page 24 of 68 9/22/2016

33 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-KITCHEN EAST KETTLE-KCC-01 Date Collected: 09/13/16 06:31 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ug/l 09/18/16 14:30 09/18/16 20:49 1 Client Sample ID: ES-KITCHEN KETTLE WEST-KCC-01 Date Collected: 09/13/16 06:33 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/18/16 14:30 09/18/16 20:52 1 Client Sample ID: ES-KITCHEN-IM-01 Date Collected: 09/13/16 06:39 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/18/16 14:30 09/18/16 20:55 1 Client Sample ID: ES-RECIEVING-IM-01 Date Collected: 09/13/16 06:43 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 20:57 1 Client Sample ID: ES-PLAYGROUND-DW-01 Date Collected: 09/13/16 08:04 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 21:00 1 Client Sample ID: ES-CONCESSION STAND SOUTH-DW-01 Date Collected: 09/13/16 08:51 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/20/16 08:45 09/20/16 23:28 1 Client Sample ID: ES-STACKWICK BLDG SOUTH WEST-DW-01 Date Collected: 09/13/16 08:45 Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 21:12 1 TestAmerica Buffalo Page 25 of 68 9/22/2016

34 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Client Sample ID: ES-STACKWICK BLDG SOUTH EAST-DW-01 Date Collected: 09/13/16 08:48 Result Client Sample Results Qualifier RL MDL TestAmerica Job ID: SDG: SET2893 Sample ID: Analyzed Lead ug/l 09/18/16 14:30 09/18/16 21:15 1 Client Sample ID: ES-EAST PRESS BOX-DW-01 Date Collected: 09/13/16 08:49 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead 0.95 J ug/l 09/18/16 14:30 09/18/16 21:18 1 Client Sample ID: ES-CONCESSION STAND NORTH-KFC-01 Date Collected: 09/13/16 08:57 Result Qualifier RL MDL Unit D Dil Fac Sample ID: Analyzed Lead ug/l 09/18/16 14:30 09/18/16 21:21 1 Client Sample ID: ES-CONCESSION STAND SOUTH-KFC-01 Date Collected: 09/13/16 08:58 Unit D Dil Fac Sample ID: Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ug/l 09/18/16 14:30 09/18/16 21:24 1 TestAmerica Buffalo Page 26 of 68 9/22/2016

35 QC Sample Results Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:00 09/17/16 05:01 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MS Client Sample ID: ES-A1-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ND ug/l Sample ID: MSD Client Sample ID: ES-A1-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ND ug/l Sample ID: MS Client Sample ID: ES-C5-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MSD Client Sample ID: ES-C5-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ug/l Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 17:30 09/17/16 06:23 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l TestAmerica Buffalo Page 27 of 68 9/22/2016

36 QC Sample Results Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Sample ID: MS Client Sample ID: ES-C6-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MSD Client Sample ID: ES-C6-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ug/l Sample ID: MS Client Sample ID: ES-G2-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead 0.30 J ug/l Sample ID: MSD Client Sample ID: ES-G2-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead 0.30 J ug/l Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:00 09/17/16 07:44 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MS Client Sample ID: ES-G3-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ND ug/l Sample ID: MSD Client Sample ID: ES-G3-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ND ug/l TestAmerica Buffalo Page 28 of 68 9/22/2016

37 QC Sample Results Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 (Continued) Sample ID: MS Client Sample ID: ES-J6-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ND F ug/l Sample ID: MSD Client Sample ID: ES-J6-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ND F F2 ug/l Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/16/16 18:30 09/17/16 09:08 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MS Client Sample ID: ES-J7-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ND ug/l Sample ID: MSD Client Sample ID: ES-J7-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ND ug/l Sample ID: MS Client Sample ID: ES-K6-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ND ug/l Sample ID: MSD Client Sample ID: ES-K6-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ND ug/l TestAmerica Buffalo Page 29 of 68 9/22/2016

38 QC Sample Results Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:00 09/18/16 18:57 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MS Client Sample ID: ES-K7-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ND ug/l Sample ID: MSD Client Sample ID: ES-K7-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ND ug/l Sample ID: MS Client Sample ID: ES-J11-CFC-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MSD Client Sample ID: ES-J11-CFC-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ug/l Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/18/16 14:30 09/18/16 20:17 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l TestAmerica Buffalo Page 30 of 68 9/22/2016

39 QC Sample Results Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 (Continued) Sample ID: MS Client Sample ID: ES-HEALTH OFFICE WEST-CFC-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead 0.69 J ug/l Sample ID: MSD Client Sample ID: ES-HEALTH OFFICE WEST-CFC-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead 0.69 J ug/l Sample ID: MS Client Sample ID: ES-CONCESSION STAND SOUTH-KFC-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MSD Client Sample ID: ES-CONCESSION STAND SOUTH-KFC-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ug/l Sample ID: MB /1-A Client Sample ID: Blank : Analysis : Prep : MB MB Result Qualifier RL MDL Unit D Analyzed Dil Fac Lead ND ug/l 09/20/16 08:45 09/20/16 21:26 1 Sample ID: LCS /2-A Client Sample ID: Control Sample : Analysis : Prep : Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MS Client Sample ID: ES-CONCESSION STAND SOUTH-DW-01 : Analysis : Prep : Sample Sample Spike MS MS %Rec. Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead ug/l Sample ID: MSD Client Sample ID: ES-CONCESSION STAND SOUTH-DW-01 : Analysis : Prep : Sample Sample Spike MSD MSD %Rec. RPD Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Lead ug/l TestAmerica Buffalo Page 31 of 68 9/22/2016

40 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD QC Sample Results TestAmerica Job ID: SDG: SET TestAmerica Buffalo Page 32 of 68 9/22/2016

41 QC Association Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Metals Prep : Sample ID Client Sample ID Matrix Prep ES-A1-DW ES-A2-DW ES-A3-DW ES-A4-DW ES-A5-DW ES-A6-DW ES-B1-DW ES-B2-DW ES-B4-BFC ES-B5-DW ES-B6-DW ES-B8-DW ES-C1-DW ES-C2-DW ES-C4-DW ES-C5-DW-01 MB /1-A Blank LCS /2-A Control Sample MS ES-A1-DW MSD ES-A1-DW MS ES-C5-DW MSD ES-C5-DW Prep : Sample ID Client Sample ID Matrix Prep ES-C6-DW ES-C8-DW ES-D1-DW ES-D2-DW ES-D3-DW ES-D4-DW ES-D5-DW ES-D6-DW ES-E1-DW ES-E2-DW ES-E3-DW ES-E4-DW ES-E5-DW ES-E6-DW ES-G1-DW ES-G2-DW-01 MB /1-A Blank LCS /2-A Control Sample MS ES-C6-DW MSD ES-C6-DW MS ES-G2-DW MSD ES-G2-DW-01 Prep : Sample ID Client Sample ID Matrix Prep ES-G3-DW-01 TestAmerica Buffalo Page 33 of 68 9/22/2016

42 QC Association Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Metals (Continued) Prep : (Continued) Sample ID Client Sample ID Matrix Prep ES-G4-DW ES-G5-DW ES-G6-DW ES-H1-DW ES-H2-DW ES-H3-DW ES-H4-DW ES-H6-DW ES-H7-DW ES-J1-DW ES-J2-DW ES-J3-DW ES-J4-DW ES-J5-DW ES-J6-DW-01 MB /1-A Blank LCS /2-A Control Sample MS ES-G3-DW MSD ES-G3-DW MS ES-J6-DW MSD ES-J6-DW Prep : Sample ID Client Sample ID Matrix Prep ES-J7-DW ES-J8-DW ES-J9-DW ES-J11-DW ES-I1-DW ES-I2-DW ES-I3-DW ES-I4-DW ES-I6-DW ES-I7-DW ES-K1-DW ES-K2-DW ES-K3-DW ES-K4-DW ES-K5-DW ES-K6-DW-01 MB /1-A Blank LCS /2-A Control Sample MS ES-J7-DW MSD ES-J7-DW MS ES-K6-DW MSD ES-K6-DW-01 Prep : Sample ID Client Sample ID Matrix Prep ES-K7-DW ES-K8-DW-01 TestAmerica Buffalo Page 34 of 68 9/22/2016

43 QC Association Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Metals (Continued) Prep : (Continued) Sample ID Client Sample ID Matrix Prep ES-SOUTH HALL-WC ES-HALL MAIL RM-WC ES-HALL BAND RM-WC ES-F HALL-WC ES-COMMUNITY-WC ES-COMMUNITY NORTH-WC ES-BOYS LR-WC ES-GIRLS LR-WC ES-J HALL-WC ES-K HALL-WC ES-K HALL WEST-WC ES-K9-DW ES-K13-DW ES-J11-CFC-01 MB /1-A Blank LCS /2-A Control Sample MS ES-K7-DW MSD ES-K7-DW MS ES-J11-CFC MSD ES-J11-CFC-01 Prep : Sample ID Client Sample ID Matrix Prep ES-HEALTH OFFICE WEST-CFC ES-KITCHEN PREP-KFC ES-KITCHEN KETTLE SOUTH-KFC ES-KITCHEN-KWS ES-KITCHEN EAST KETTLE-KCC ES-KITCHEN KETTLE WEST-KCC ES-KITCHEN-IM ES-RECIEVING-IM ES-PLAYGROUND-DW ES-STACKWICK BLDG SOUTH WEST-DW ES-STACKWICK BLDG SOUTH EAST-DW ES-EAST PRESS BOX-DW ES-CONCESSION STAND NORTH-KFC ES-CONCESSION STAND SOUTH-KFC-01 MB /1-A Blank LCS /2-A Control Sample MS ES-HEALTH OFFICE WEST-CFC MSD ES-HEALTH OFFICE WEST-CFC MS ES-CONCESSION STAND SOUTH-KFC MSD ES-CONCESSION STAND SOUTH-KFC-01 Analysis : Sample ID Client Sample ID Matrix Prep ES-A1-DW ES-A2-DW ES-A3-DW ES-A4-DW ES-A5-DW TestAmerica Buffalo Page 35 of 68 9/22/2016

44 QC Association Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Metals (Continued) Analysis : (Continued) Sample ID Client Sample ID Matrix Prep ES-A6-DW ES-B1-DW ES-B2-DW ES-B5-DW ES-B6-DW ES-B8-DW ES-C1-DW ES-C2-DW ES-C4-DW ES-C5-DW ES-C6-DW ES-C8-DW ES-D1-DW ES-D2-DW ES-D3-DW ES-D4-DW ES-D5-DW ES-D6-DW ES-E1-DW ES-E2-DW ES-E3-DW ES-E4-DW ES-E5-DW ES-E6-DW ES-G1-DW ES-G2-DW ES-G3-DW ES-G4-DW ES-G5-DW ES-G6-DW ES-H1-DW ES-H2-DW ES-H3-DW ES-H4-DW ES-H6-DW ES-H7-DW ES-J1-DW ES-J2-DW ES-J3-DW ES-J4-DW ES-J5-DW ES-J6-DW ES-J7-DW ES-J8-DW ES-J9-DW ES-J11-DW ES-I1-DW ES-I2-DW ES-I3-DW ES-I4-DW ES-I6-DW TestAmerica Buffalo Page 36 of 68 9/22/2016

45 QC Association Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Metals (Continued) Analysis : (Continued) Sample ID Client Sample ID Matrix Prep ES-I7-DW ES-K1-DW ES-K2-DW ES-K3-DW ES-K4-DW ES-K5-DW ES-K6-DW MB /1-A Blank MB /1-A Blank MB /1-A Blank MB /1-A Blank LCS /2-A Control Sample LCS /2-A Control Sample LCS /2-A Control Sample LCS /2-A Control Sample MS ES-A1-DW MSD ES-A1-DW MS ES-C5-DW MSD ES-C5-DW MS ES-C6-DW MSD ES-C6-DW MS ES-G2-DW MSD ES-G2-DW MS ES-G3-DW MSD ES-G3-DW MS ES-J6-DW MSD ES-J6-DW MS ES-J7-DW MSD ES-J7-DW MS ES-K6-DW MSD ES-K6-DW Analysis : Sample ID Client Sample ID Matrix Prep ES-B4-BFC ES-K7-DW ES-K8-DW ES-SOUTH HALL-WC ES-HALL MAIL RM-WC ES-HALL BAND RM-WC ES-F HALL-WC ES-COMMUNITY-WC ES-COMMUNITY NORTH-WC ES-BOYS LR-WC ES-GIRLS LR-WC ES-J HALL-WC ES-K HALL-WC ES-K HALL WEST-WC ES-K9-DW ES-K13-DW ES-J11-CFC TestAmerica Buffalo Page 37 of 68 9/22/2016

46 QC Association Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Metals (Continued) Analysis : (Continued) Sample ID Client Sample ID Matrix Prep ES-HEALTH OFFICE WEST-CFC ES-KITCHEN PREP-KFC ES-KITCHEN KETTLE SOUTH-KFC ES-KITCHEN-KWS ES-KITCHEN EAST KETTLE-KCC ES-KITCHEN KETTLE WEST-KCC ES-KITCHEN-IM ES-RECIEVING-IM ES-PLAYGROUND-DW ES-STACKWICK BLDG SOUTH WEST-DW ES-STACKWICK BLDG SOUTH EAST-DW ES-EAST PRESS BOX-DW ES-CONCESSION STAND NORTH-KFC ES-CONCESSION STAND SOUTH-KFC MB /1-A Blank MB /1-A Blank LCS /2-A Control Sample LCS /2-A Control Sample MS ES-K7-DW MSD ES-K7-DW MS ES-J11-CFC MSD ES-J11-CFC MS ES-HEALTH OFFICE WEST-CFC MSD ES-HEALTH OFFICE WEST-CFC MS ES-CONCESSION STAND SOUTH-KFC MSD ES-CONCESSION STAND SOUTH-KFC Prep : Sample ID Client Sample ID Matrix Prep ES-CONCESSION STAND SOUTH-DW MB /1-A Blank LCS /2-A Control Sample MS ES-CONCESSION STAND SOUTH-DW MSD ES-CONCESSION STAND SOUTH-DW Analysis : Sample ID Client Sample ID Matrix Prep ES-CONCESSION STAND SOUTH-DW MB /1-A Blank LCS /2-A Control Sample MS ES-CONCESSION STAND SOUTH-DW MSD ES-CONCESSION STAND SOUTH-DW TestAmerica Buffalo Page 38 of 68 9/22/2016

47 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-A1-DW-01 Sample ID: Date Collected: 09/13/16 06:26 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:07 MTM2 TAL BUF Client Sample ID: ES-A2-DW-01 Sample ID: Date Collected: 09/13/16 06:29 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:18 MTM2 TAL BUF Client Sample ID: ES-A3-DW-01 Sample ID: Date Collected: 09/13/16 06:31 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:21 MTM2 TAL BUF Client Sample ID: ES-A4-DW-01 Sample ID: Date Collected: 09/13/16 06:32 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:24 MTM2 TAL BUF Client Sample ID: ES-A5-DW-01 Sample ID: Date Collected: 09/13/16 06:33 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:33 MTM2 TAL BUF Client Sample ID: ES-A6-DW-01 Sample ID: Date Collected: 09/13/16 06:34 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:36 MTM2 TAL BUF TestAmerica Buffalo Page 39 of 68 9/22/2016

48 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-B1-DW-01 Sample ID: Date Collected: 09/13/16 06: Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:39 MTM2 TAL BUF 5 6 Client Sample ID: ES-B2-DW-01 Sample ID: Date Collected: 09/13/16 06:41 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:42 MTM2 TAL BUF Client Sample ID: ES-B4-BFC-01 Sample ID: Date Collected: 09/13/16 06:44 Prep /16/16 17:00 MTM2 TAL BUF Analysis /18/16 18:53 MTM2 TAL BUF Client Sample ID: ES-B5-DW-01 Sample ID: Date Collected: 09/13/16 06:45 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:47 MTM2 TAL BUF Client Sample ID: ES-B6-DW-01 Sample ID: Date Collected: 09/13/16 06:47 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:50 MTM2 TAL BUF Client Sample ID: ES-B8-DW-01 Sample ID: Date Collected: 09/13/16 06:50 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:53 MTM2 TAL BUF TestAmerica Buffalo Page 40 of 68 9/22/2016

49 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-C1-DW-01 Sample ID: Date Collected: 09/13/16 06: Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:55 MTM2 TAL BUF 5 6 Client Sample ID: ES-C2-DW-01 Sample ID: Date Collected: 09/13/16 06:57 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 05:58 MTM2 TAL BUF Client Sample ID: ES-C4-DW-01 Sample ID: Date Collected: 09/13/16 06:58 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 06:08 MTM2 TAL BUF Client Sample ID: ES-C5-DW-01 Sample ID: Date Collected: 09/13/16 07:00 Prep /16/16 17:00 MTM2 TAL BUF Analysis /17/16 06:11 MTM2 TAL BUF Client Sample ID: ES-C6-DW-01 Sample ID: Date Collected: 09/13/16 07:02 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 06:29 MTM2 TAL BUF Client Sample ID: ES-C8-DW-01 Sample ID: Date Collected: 09/13/16 07:04 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 06:46 MTM2 TAL BUF TestAmerica Buffalo Page 41 of 68 9/22/2016

50 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-D1-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 06:49 MTM2 TAL BUF 5 6 Client Sample ID: ES-D2-DW-01 Sample ID: Date Collected: 09/13/16 07:12 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 06:52 MTM2 TAL BUF Client Sample ID: ES-D3-DW-01 Sample ID: Date Collected: 09/13/16 07:13 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 06:55 MTM2 TAL BUF Client Sample ID: ES-D4-DW-01 Sample ID: Date Collected: 09/13/16 07:16 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 06:57 MTM2 TAL BUF Client Sample ID: ES-D5-DW-01 Sample ID: Date Collected: 09/13/16 07:17 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:00 MTM2 TAL BUF Client Sample ID: ES-D6-DW-01 Sample ID: Date Collected: 09/13/16 07:18 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:03 MTM2 TAL BUF TestAmerica Buffalo Page 42 of 68 9/22/2016

51 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-E1-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:06 MTM2 TAL BUF 5 6 Client Sample ID: ES-E2-DW-01 Sample ID: Date Collected: 09/13/16 07:22 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:08 MTM2 TAL BUF Client Sample ID: ES-E3-DW-01 Sample ID: Date Collected: 09/13/16 07:24 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:11 MTM2 TAL BUF Client Sample ID: ES-E4-DW-01 Sample ID: Date Collected: 09/13/16 07:25 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:21 MTM2 TAL BUF Client Sample ID: ES-E5-DW-01 Sample ID: Date Collected: 09/13/16 07:27 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:23 MTM2 TAL BUF Client Sample ID: ES-E6-DW-01 Sample ID: Date Collected: 09/13/16 07:28 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:26 MTM2 TAL BUF TestAmerica Buffalo Page 43 of 68 9/22/2016

52 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-G1-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:29 MTM2 TAL BUF 5 6 Client Sample ID: ES-G2-DW-01 Sample ID: Date Collected: 09/13/16 07:34 Prep /16/16 17:30 MTM2 TAL BUF Analysis /17/16 07:32 MTM2 TAL BUF Client Sample ID: ES-G3-DW-01 Sample ID: Date Collected: 09/13/16 07:35 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 07:49 MTM2 TAL BUF Client Sample ID: ES-G4-DW-01 Sample ID: Date Collected: 09/13/16 07:38 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:07 MTM2 TAL BUF Client Sample ID: ES-G5-DW-01 Sample ID: Date Collected: 09/13/16 07:39 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:10 MTM2 TAL BUF Client Sample ID: ES-G6-DW-01 Sample ID: Date Collected: 09/13/16 07:40 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:13 MTM2 TAL BUF TestAmerica Buffalo Page 44 of 68 9/22/2016

53 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-H1-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:16 MTM2 TAL BUF 5 6 Client Sample ID: ES-H2-DW-01 Sample ID: Date Collected: 09/13/16 07:45 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:18 MTM2 TAL BUF Client Sample ID: ES-H3-DW-01 Sample ID: Date Collected: 09/13/16 07:46 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:21 MTM2 TAL BUF Client Sample ID: ES-H4-DW-01 Sample ID: Date Collected: 09/13/16 07:48 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:24 MTM2 TAL BUF Client Sample ID: ES-H6-DW-01 Sample ID: Date Collected: 09/13/16 07:49 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:33 MTM2 TAL BUF Client Sample ID: ES-H7-DW-01 Sample ID: Date Collected: 09/13/16 07:51 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:36 MTM2 TAL BUF TestAmerica Buffalo Page 45 of 68 9/22/2016

54 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-J1-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:39 MTM2 TAL BUF 5 6 Client Sample ID: ES-J2-DW-01 Sample ID: Date Collected: 09/13/16 07:58 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:42 MTM2 TAL BUF Client Sample ID: ES-J3-DW-01 Sample ID: Date Collected: 09/13/16 08:00 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:44 MTM2 TAL BUF Client Sample ID: ES-J4-DW-01 Sample ID: Date Collected: 09/13/16 08:01 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:47 MTM2 TAL BUF Client Sample ID: ES-J5-DW-01 Sample ID: Date Collected: 09/13/16 08:02 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:50 MTM2 TAL BUF Client Sample ID: ES-J6-DW-01 Sample ID: Date Collected: 09/13/16 08:04 Prep /16/16 18:00 MTM2 TAL BUF Analysis /17/16 08:53 MTM2 TAL BUF TestAmerica Buffalo Page 46 of 68 9/22/2016

55 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-J7-DW-01 Sample ID: Date Collected: 09/13/16 08: Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:13 MTM2 TAL BUF 5 6 Client Sample ID: ES-J8-DW-01 Sample ID: Date Collected: 09/13/16 08:06 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:24 MTM2 TAL BUF Client Sample ID: ES-J9-DW-01 Sample ID: Date Collected: 09/13/16 08:08 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:27 MTM2 TAL BUF Client Sample ID: ES-J11-DW-01 Sample ID: Date Collected: 09/13/16 08:10 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:30 MTM2 TAL BUF Client Sample ID: ES-I1-DW-01 Sample ID: Date Collected: 09/13/16 06:48 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:32 MTM2 TAL BUF Client Sample ID: ES-I2-DW-01 Sample ID: Date Collected: 09/13/16 06:51 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:42 MTM2 TAL BUF TestAmerica Buffalo Page 47 of 68 9/22/2016

56 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-I3-DW-01 Sample ID: Date Collected: 09/13/16 06: Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:45 MTM2 TAL BUF 5 6 Client Sample ID: ES-I4-DW-01 Sample ID: Date Collected: 09/13/16 06:58 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:47 MTM2 TAL BUF Client Sample ID: ES-I6-DW-01 Sample ID: Date Collected: 09/13/16 07:00 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:50 MTM2 TAL BUF Client Sample ID: ES-I7-DW-01 Sample ID: Date Collected: 09/13/16 07:04 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:53 MTM2 TAL BUF Client Sample ID: ES-K1-DW-01 Sample ID: Date Collected: 09/13/16 07:07 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:56 MTM2 TAL BUF Client Sample ID: ES-K2-DW-01 Sample ID: Date Collected: 09/13/16 07:11 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 09:58 MTM2 TAL BUF TestAmerica Buffalo Page 48 of 68 9/22/2016

57 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-K3-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 10:01 MTM2 TAL BUF 5 6 Client Sample ID: ES-K4-DW-01 Sample ID: Date Collected: 09/13/16 07:17 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 10:04 MTM2 TAL BUF Client Sample ID: ES-K5-DW-01 Sample ID: Date Collected: 09/13/16 07:21 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 10:07 MTM2 TAL BUF Client Sample ID: ES-K6-DW-01 Sample ID: Date Collected: 09/13/16 07:24 Prep /16/16 18:30 MTM2 TAL BUF Analysis /17/16 10:16 MTM2 TAL BUF Client Sample ID: ES-K7-DW-01 Sample ID: Date Collected: 09/13/16 07:26 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:03 MTM2 TAL BUF Client Sample ID: ES-K8-DW-01 Sample ID: Date Collected: 09/13/16 07:30 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:14 MTM2 TAL BUF TestAmerica Buffalo Page 49 of 68 9/22/2016

58 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-SOUTH HALL-WC-01 Sample ID: Date Collected: 09/13/16 08: Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:17 MTM2 TAL BUF 5 6 Client Sample ID: ES-HALL MAIL RM-WC-01 Sample ID: Date Collected: 09/13/16 08:06 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:27 MTM2 TAL BUF Client Sample ID: ES-HALL BAND RM-WC-01 Sample ID: Date Collected: 09/13/16 08:10 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:30 MTM2 TAL BUF Client Sample ID: ES-F HALL-WC-01 Sample ID: Date Collected: 09/13/16 07:55 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:32 MTM2 TAL BUF Client Sample ID: ES-COMMUNITY-WC-01 Sample ID: Date Collected: 09/13/16 07:52 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:35 MTM2 TAL BUF Client Sample ID: ES-COMMUNITY NORTH-WC-01 Sample ID: Date Collected: 09/13/16 07:50 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:38 MTM2 TAL BUF TestAmerica Buffalo Page 50 of 68 9/22/2016

59 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-BOYS LR-WC-01 Sample ID: Date Collected: 09/13/16 07: Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:41 MTM2 TAL BUF 5 6 Client Sample ID: ES-GIRLS LR-WC-01 Sample ID: Date Collected: 09/13/16 07:47 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:43 MTM2 TAL BUF Client Sample ID: ES-J HALL-WC-01 Sample ID: Date Collected: 09/13/16 07:43 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:46 MTM2 TAL BUF Client Sample ID: ES-K HALL-WC-01 Sample ID: Date Collected: 09/13/16 07:37 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:49 MTM2 TAL BUF Client Sample ID: ES-K HALL WEST-WC-01 Sample ID: Date Collected: 09/13/16 07:35 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 19:52 MTM2 TAL BUF Client Sample ID: ES-K9-DW-01 Sample ID: Date Collected: 09/13/16 07:33 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 20:01 MTM2 TAL BUF TestAmerica Buffalo Page 51 of 68 9/22/2016

60 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-K13-DW-01 Sample ID: Date Collected: 09/13/16 07: Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 20:04 MTM2 TAL BUF 5 6 Client Sample ID: ES-J11-CFC-01 Sample ID: Date Collected: 09/13/16 08:18 Prep /18/16 14:00 MTM2 TAL BUF Analysis /18/16 20:07 MTM2 TAL BUF Client Sample ID: ES-HEALTH OFFICE WEST-CFC-01 Sample ID: Date Collected: 09/13/16 07:07 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:23 MTM2 TAL BUF Client Sample ID: ES-KITCHEN PREP-KFC-01 Sample ID: Date Collected: 09/13/16 06:20 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:41 MTM2 TAL BUF Client Sample ID: ES-KITCHEN KETTLE SOUTH-KFC-01 Sample ID: Date Collected: 09/13/16 06:24 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:43 MTM2 TAL BUF Client Sample ID: ES-KITCHEN-KWS-01 Sample ID: Date Collected: 09/13/16 06:28 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:46 MTM2 TAL BUF TestAmerica Buffalo Page 52 of 68 9/22/2016

61 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-KITCHEN EAST KETTLE-KCC-01 Sample ID: Date Collected: 09/13/16 06: Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:49 MTM2 TAL BUF 5 6 Client Sample ID: ES-KITCHEN KETTLE WEST-KCC-01 Sample ID: Date Collected: 09/13/16 06:33 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:52 MTM2 TAL BUF Client Sample ID: ES-KITCHEN-IM-01 Sample ID: Date Collected: 09/13/16 06:39 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:55 MTM2 TAL BUF Client Sample ID: ES-RECIEVING-IM-01 Sample ID: Date Collected: 09/13/16 06:43 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 20:57 MTM2 TAL BUF Client Sample ID: ES-PLAYGROUND-DW-01 Sample ID: Date Collected: 09/13/16 08:04 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 21:00 MTM2 TAL BUF Client Sample ID: ES-CONCESSION STAND SOUTH-DW-01 Sample ID: Date Collected: 09/13/16 08:51 Prep /20/16 08:45 RMZ TAL BUF Analysis /20/16 23:28 MTM2 TAL BUF TestAmerica Buffalo Page 53 of 68 9/22/2016

62 Chronicle Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 Client Sample ID: ES-STACKWICK BLDG SOUTH WEST-DW-01 Date Collected: 09/13/16 08:45 Prep /18/16 14:30 MTM2 TAL BUF Sample ID: Analysis /18/16 21:12 MTM2 TAL BUF Client Sample ID: ES-STACKWICK BLDG SOUTH EAST-DW-01 Date Collected: 09/13/16 08:48 Prep /18/16 14:30 MTM2 TAL BUF Sample ID: Analysis /18/16 21:15 MTM2 TAL BUF Client Sample ID: ES-EAST PRESS BOX-DW-01 Sample ID: Date Collected: 09/13/16 08:49 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 21:18 MTM2 TAL BUF Client Sample ID: ES-CONCESSION STAND NORTH-KFC-01 Sample ID: Date Collected: 09/13/16 08:57 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 21:21 MTM2 TAL BUF Client Sample ID: ES-CONCESSION STAND SOUTH-KFC-01 Sample ID: Date Collected: 09/13/16 08:58 Prep /18/16 14:30 MTM2 TAL BUF Analysis /18/16 21:24 MTM2 TAL BUF oratory References: TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY , TEL (716) TestAmerica Buffalo Page 54 of 68 9/22/2016

63 Certification Summary Client: Sienna Environmental Technologies LLC TestAmerica Job ID: Project/Site: Albion CSD SDG: SET2893 oratory: TestAmerica Buffalo Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Program EPA Region Certification ID Expiration Date New York NELAP Analysis Prep Matrix TestAmerica Buffalo Page 55 of 68 9/22/2016

64 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Summary TestAmerica Job ID: SDG: SET2893 Description Protocol oratory Metals (ICP/MS) EPA TAL BUF Protocol References: EPA = US Environmental Protection Agency oratory References: TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY , TEL (716) TestAmerica Buffalo Page 56 of 68 9/22/2016

65 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Sample Summary TestAmerica Job ID: SDG: SET2893 Sample ID Client Sample ID Matrix Collected Received ES-A1-DW-01 09/13/16 06:26 09/14/16 11: ES-A2-DW-01 09/13/16 06:29 09/14/16 11: ES-A3-DW-01 09/13/16 06:31 09/14/16 11: ES-A4-DW-01 09/13/16 06:32 09/14/16 11: ES-A5-DW-01 09/13/16 06:33 09/14/16 11: ES-A6-DW-01 09/13/16 06:34 09/14/16 11: ES-B1-DW-01 09/13/16 06:40 09/14/16 11: ES-B2-DW-01 09/13/16 06:41 09/14/16 11: ES-B4-BFC-01 09/13/16 06:44 09/14/16 11: ES-B5-DW-01 09/13/16 06:45 09/14/16 11: ES-B6-DW-01 09/13/16 06:47 09/14/16 11: ES-B8-DW-01 09/13/16 06:50 09/14/16 11: ES-C1-DW-01 09/13/16 06:55 09/14/16 11: ES-C2-DW-01 09/13/16 06:57 09/14/16 11: ES-C4-DW-01 09/13/16 06:58 09/14/16 11: ES-C5-DW-01 09/13/16 07:00 09/14/16 11: ES-C6-DW-01 09/13/16 07:02 09/14/16 11: ES-C8-DW-01 09/13/16 07:04 09/14/16 11: ES-D1-DW-01 09/13/16 07:11 09/14/16 11: ES-D2-DW-01 09/13/16 07:12 09/14/16 11: ES-D3-DW-01 09/13/16 07:13 09/14/16 11: ES-D4-DW-01 09/13/16 07:16 09/14/16 11: ES-D5-DW-01 09/13/16 07:17 09/14/16 11: ES-D6-DW-01 09/13/16 07:18 09/14/16 11: ES-E1-DW-01 09/13/16 07:21 09/14/16 11: ES-E2-DW-01 09/13/16 07:22 09/14/16 11: ES-E3-DW-01 09/13/16 07:24 09/14/16 11: ES-E4-DW-01 09/13/16 07:25 09/14/16 11: ES-E5-DW-01 09/13/16 07:27 09/14/16 11: ES-E6-DW-01 09/13/16 07:28 09/14/16 11: ES-G1-DW-01 09/13/16 07:33 09/14/16 11: ES-G2-DW-01 09/13/16 07:34 09/14/16 11: ES-G3-DW-01 09/13/16 07:35 09/14/16 11: ES-G4-DW-01 09/13/16 07:38 09/14/16 11: ES-G5-DW-01 09/13/16 07:39 09/14/16 11: ES-G6-DW-01 09/13/16 07:40 09/14/16 11: ES-H1-DW-01 09/13/16 07:42 09/14/16 11: ES-H2-DW-01 09/13/16 07:45 09/14/16 11: ES-H3-DW-01 09/13/16 07:46 09/14/16 11: ES-H4-DW-01 09/13/16 07:48 09/14/16 11: ES-H6-DW-01 09/13/16 07:49 09/14/16 11: ES-H7-DW-01 09/13/16 07:51 09/14/16 11: ES-J1-DW-01 09/13/16 07:57 09/14/16 11: ES-J2-DW-01 09/13/16 07:58 09/14/16 11: ES-J3-DW-01 09/13/16 08:00 09/14/16 11: ES-J4-DW-01 09/13/16 08:01 09/14/16 11: ES-J5-DW-01 09/13/16 08:02 09/14/16 11: ES-J6-DW-01 09/13/16 08:04 09/14/16 11: ES-J7-DW-01 09/13/16 08:05 09/14/16 11: ES-J8-DW-01 09/13/16 08:06 09/14/16 11: ES-J9-DW-01 09/13/16 08:08 09/14/16 11: ES-J11-DW-01 09/13/16 08:10 09/14/16 11: ES-I1-DW-01 09/13/16 06:48 09/14/16 11: TestAmerica Buffalo Page 57 of 68 9/22/2016

66 Client: Sienna Environmental Technologies LLC Project/Site: Albion CSD Sample Summary TestAmerica Job ID: SDG: SET2893 Sample ID Client Sample ID Matrix Collected Received ES-I2-DW-01 09/13/16 06:51 09/14/16 11: ES-I3-DW-01 09/13/16 06:55 09/14/16 11: ES-I4-DW-01 09/13/16 06:58 09/14/16 11: ES-I6-DW-01 09/13/16 07:00 09/14/16 11: ES-I7-DW-01 09/13/16 07:04 09/14/16 11: ES-K1-DW-01 09/13/16 07:07 09/14/16 11: ES-K2-DW-01 09/13/16 07:11 09/14/16 11: ES-K3-DW-01 09/13/16 07:15 09/14/16 11: ES-K4-DW-01 09/13/16 07:17 09/14/16 11: ES-K5-DW-01 09/13/16 07:21 09/14/16 11: ES-K6-DW-01 09/13/16 07:24 09/14/16 11: ES-K7-DW-01 09/13/16 07:26 09/14/16 11: ES-K8-DW-01 09/13/16 07:30 09/14/16 11: ES-SOUTH HALL-WC-01 09/13/16 08:00 09/14/16 11: ES-HALL MAIL RM-WC-01 09/13/16 08:06 09/14/16 11: ES-HALL BAND RM-WC-01 09/13/16 08:10 09/14/16 11: ES-F HALL-WC-01 09/13/16 07:55 09/14/16 11: ES-COMMUNITY-WC-01 09/13/16 07:52 09/14/16 11: ES-COMMUNITY NORTH-WC-01 09/13/16 07:50 09/14/16 11: ES-BOYS LR-WC-01 09/13/16 07:45 09/14/16 11: ES-GIRLS LR-WC-01 09/13/16 07:47 09/14/16 11: ES-J HALL-WC-01 09/13/16 07:43 09/14/16 11: ES-K HALL-WC-01 09/13/16 07:37 09/14/16 11: ES-K HALL WEST-WC-01 09/13/16 07:35 09/14/16 11: ES-K9-DW-01 09/13/16 07:33 09/14/16 11: ES-K13-DW-01 09/13/16 07:40 09/14/16 11: ES-J11-CFC-01 09/13/16 08:18 09/14/16 11: ES-HEALTH OFFICE WEST-CFC-01 09/13/16 07:07 09/14/16 11: ES-KITCHEN PREP-KFC-01 09/13/16 06:20 09/14/16 11: ES-KITCHEN KETTLE SOUTH-KFC-01 09/13/16 06:24 09/14/16 11: ES-KITCHEN-KWS-01 09/13/16 06:28 09/14/16 11: ES-KITCHEN EAST KETTLE-KCC-01 09/13/16 06:31 09/14/16 11: ES-KITCHEN KETTLE WEST-KCC-01 09/13/16 06:33 09/14/16 11: ES-KITCHEN-IM-01 09/13/16 06:39 09/14/16 11: ES-RECIEVING-IM-01 09/13/16 06:43 09/14/16 11: ES-PLAYGROUND-DW-01 09/13/16 08:04 09/14/16 11: ES-CONCESSION STAND SOUTH-DW-01 09/13/16 08:51 09/14/16 11: ES-STACKWICK BLDG SOUTH WEST-DW-01 09/13/16 08:45 09/14/16 11: ES-STACKWICK BLDG SOUTH EAST-DW-01 09/13/16 08:48 09/14/16 11: ES-EAST PRESS BOX-DW-01 09/13/16 08:49 09/14/16 11: ES-CONCESSION STAND NORTH-KFC-01 09/13/16 08:57 09/14/16 11: ES-CONCESSION STAND SOUTH-KFC-01 09/13/16 08:58 09/14/16 11: TestAmerica Buffalo Page 58 of 68 9/22/2016

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76 Login Sample Receipt Checklist Client: Sienna Environmental Technologies LLC Job : Login : List : 1 Creator: Janish, Carl M Question Answer Comment Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. Is the Field Sampler's name present on COC? There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time (Excluding tests with immediate HTs).. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. Sample Preservation Verified There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Sampling Company provided. Samples received within 48 hours of sampling. Samples requiring field filtration have been filtered in the field. Chlorine Residual checked. True True True True True True True True True True True True True True True True True True True True True True True False True N/A N/A SDG : SET2893 List Source: TestAmerica Buffalo TestAmerica Buffalo Page 68 of 68 9/22/2016

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130 Appendix D NYCRR Title 10, Subpart 67-4