GENERAL. Bottle Type (Mimimum required) Water/ WW Methods. Label Color SW84 6. Parameter. Holding Time. Preservative

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1 Bottle Chart Parameter Water/ WW Methods SW84 6 Label Color Bottle Type (Mimimum requi) Preservative Holding Time GENERAL Acidity SM 19 th 2310B Alkalinity (200ml) Ammonia yellow 250 Plastic Biochemical Oxygen Demand Biochemical Oxygen Demand (carbonaceous) (500ml) SM 18 th 5210B (500ml) Bromide None requi Chemical Oxygen Demand yellow Chloride None requi Chlorine Residual None requi Coliform, Coliform, Fecal SM 19 th Ed 9223 B SM 19 th Ed D beige beige ml sterile Plastic 100 ml sterile Plastic.008% Cool 4C.008% 30 hours 6 hours Color (200ml) Conductivity A Cyanide purple NaOH to >12 w/ascorbic acid Fluoride None requi Hardness, <2 w/hno days

2 Chromium VIaqueous SM 19 th 3500-Cr D Method 7196A 24 hours Chromium VIsoil Mercury Aqueous Mercury Solid Metals (Except Cr+6) Metals (Solid) / / A *MOD 7470A 7471A 6010A / 6020A 6010A / 6020A 9 Oz Soil Jar (4oz) 24 Hours HNO 3 < 2 9 oz Glass (4oz) 28days HNO 3 < 2 6 months 9 oz Glass (4oz) 6 months Nitrate Nitrite hrs Nitrate-Nitrite yellow 250 ml H 2 SO 4 Nitrogen yellow (150ml) Oil and Grease 1664A 2-1L Glass Orthophosphate Oxygen Dissolved Probe Oxygen Dissolved Winkler ph H 2 SO < 2 4 H 2 SO < 2 4 Cool 4C Filter ** No Plastic None Requi SM 19th H+ B Method 9040 B Phenols SS% (Residue settable) Silicon Recoverable Specific Conductance Sulfate Sulfide A 9050A A **300 ml BOD Bottle Fix on Site Store in Dark None requi pink Sulfite Surfactants ml Amber glass (200ml) HNO3 <2 ZnAc Plus NaOH 9 None Requi 8 hours VA SM 5910 blue Amber Liter

3 Silica-Gel Treated Oil and Grease (TPH) ea/1L Glass Temperature None requi Carbon/Water TDS Residue(Filterable) TSS Residue(Non- Filterable) TR Residue total SM 19 th Ed. 5310C Turbidity VSS (Residue-Volatile) (200ml) DRINKING WATER Bromate orange Chlorate orange Chlorite orange Haloacetic Acid L amber glass IC Parameters (NO 3, NO 2, F-, SO 4, Ortho-P,Bromide) NH 4 Cl Perchlorate SUVA (DOC, UV254) SM 5910B SM 5310C Trihalomethanes TOC TCLP + RCI SM 10 th Ed. 5310C 8260B ml plastic blue 1L amber glass 48 Hrs 3 40 ml vials Cool 4C w/.008% HAZARDOUS WASTE CHARACTERIZATION Ch 7 & A 9030A grey 7-Glass wide mouth liquid 2-Glass wide mouth solid Cool 4C

4 BTEX GC BTEX GC/MS B ORGANICS dark blue dark blue Herbicides A blue PCB blue 2ea/ 40 ml Glass Vial 2ea/ 40 ml Glass Viall HCl <2 HCl <2 PCB Oil ml Vial Pesticides A blue Organophosph oros Pesticides Semi-Volatiles s TOX Halogens Liq Aquous TOX Halogins-Oil (SGT) Hydrocarbon (DRO) (GRO) A blue C blue 9020B 1 L Amber Glass Oz Soil Jar L Glass TX1005 TX MOD blue 3-40 ml glass vial (2/3 full) 1 L Amber glass NaHSO4 to <2 28 Days 7 Days 7 Days 8015 MOD 2/40 ml VOA Vial 7 Days Volatile s B blue 2/40 ml Glass Vial w/hcl <2

5 Radiological Gross Alpha Radiological Gross Beta Radium 226 & 228 RADIOLOGICAL Subcontract grey 1L Glass HNO 3 to <2 6 months Subcontract grey 1L Glass HNO 3 < 2 6 months Subcontract grey 1L Glass HNO 3 < 2 6 months HCl = Hydrochloric Acid HNO 3 = Nitric Acid H 2 SO 4 = Sulfuric Acid = Sodium Thiosulfate NaOH = Sodium Hydroxide NaHSO 4 = Sodium Bisulfate ZnAc = Zinc Acetate August 12, 2003

6-24 hours e. Coliform, Fecal and Total W, DW P,G Cool, 4 C, 0.008% Na 2 S 2 O 3. Fecal Streptococci W P,G Cool, 4 C, 0.

6-24 hours e. Coliform, Fecal and Total W, DW P,G Cool, 4 C, 0.008% Na 2 S 2 O 3. Fecal Streptococci W P,G Cool, 4 C, 0. Coliform, Colilert, P, Bottle or Bag Cool, 4 C, 0.008% Na 2 S 2 O 3 d Coliform, Fecal and Total, P,G Cool, 4 C, 0.008% Na 2 S 2 O 3 d Fecal Streptococci P,G Cool, 4 C, 0.008% Na 2 S 2 O 3 d INORGANIC TESTS

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