Summer 2018 Semi-Annual Water Quality Monitoring Report

Transcription

1 Summer 01 Semi-Annual Water Quality Monitoring Report Persimmon Hollow C& ebris isposal Facility Santa Rosa County, Florida January, 01 Terracon Project No. EA0001 for: Anderson Columbia Company, Inc. Marianna, Florida by: Terracon Consultants, Inc. Pensacola, Florida

2 January, 01 Ms. awn Templin, P.E. Solid Waste Section Supervisor Northwest istrict FEP 0 Governmental Center Pensacola, Florida 01 Re: Summer 01 Semi-Annual Water Quality Monitoring Report Persimmon Hollow C& ebris isposal Facility Santa Rosa County, Florida FEP File #: SO WACS I #: NW//0001 Terracon Project No.: EA0001 ear Ms. Templin: The Automated ata Processing Tool (AaPT) Electronic ata eliverables (Es) have been uploaded to the Florida epartment of Environmental Protection (FEP) Business portal. If you have any additional questions, please feel free to contact me at (0) -01. Sincerely, Terracon Consultants, Inc. Tom Lewis, P.G. Senior Geologist cc: Scott Jordan, Anderson Columbia Company, Inc. (w. enclosure) Scott Cleveland, Anderson Columbia Company, Inc. (w/o enclosure) Terracon Consultants, Inc. 00 N avis Hwy Pensacola, Florida 1 P [0] 0 F [0] 0 terracon.com

3 Table of Contents INTROUCTION... 1 ANALYTICAL RESULTS....1 Field Parameters.... Volatile Organic Compounds.... Metals... Routine Semi-Annual Metals... Non-Routine Appendix I Metals.... General & Mineral Constituents.... Quality Assurance/Quality Control... CONCLUSIONS & RECOMMENATIONS... CERTIFICATION... Figures Figure 1 Site Location Map Figure Groundwater Contour Map August 1, 01 Figure Groundwater Elevations Tables Table 1 Table Table Table Table Table Table Table Monitor Well Locations Current Monitor Well Status Groundwater Elevations Summary of etected Groundwater Constituents: Background Well MW-1 Summary of etected Groundwater Constituents: Compliance Well MW- Summary of etected Groundwater Constituents: Compliance Well MW- Summary of etected Groundwater Constituents: Compliance Well MW- Summary of etected Groundwater Constituents: etection Well MW- Attachments Attachment 1 Summer 01 Laboratory Analytical Report and Field Sampling Logs Attachment Rainfall ata: January 01 August 01 Responsive Resourceful Reliable

4 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 SUMMER 01 SEMI-ANNUAL WATER QUALITY MONITORING REPORT Persimmon Hollow C& ebris isposal Facility Santa Rosa County, Florida FEP File #: SO; WACS I #: NW//0001 Terracon Project No.: EA0001 January, 01 INTROUCTION Terracon Consultants, Inc. (Terracon) is pleased to provide this Summer 01 Semi-Annual Groundwater Monitoring Report and commentary for the Anderson Columbia Persimmon Hollow Construction and emolition (C&) ebris isposal Facility, located in Santa Rosa County, Florida (Figure 1). The Summer 01 semi-annual water quality monitoring was completed in accordance with the Operations Permit of August 1, 01. The groundwater samples for monitoring wells MW-1, MW-, MW-, and MW- were collected on August 1, 01. Unable to access monitoring well MW- during the August 1, 01 sampling event due to a new fence construction, TestAmerica remobilized on September, collected the groundwater sample from monitoring well MW-.. Each groundwater sample was analyzed for the routine parameters listed in the Operations Permit. Confirmation re-sampling was not conducted during this Summer 01 semi-annual period. Field sampling and laboratory analysis was conducted by TestAmerica, a Florida-licensed water quality laboratory located in Tallahassee, Florida. In order to meet all constituent reporting requirements, TestAmerica contracted BENCHMARK EnviroAnalytical Inc. (BENCHMARK), a Florida-licensed water quality laboratory located in Palmetto, Florida to analyze and report sulfide and hydrogen sulfide sample data. The work was completed under the provisions of CompQAP/HRS Certification Numbers 0G and E0. The laboratory analytical results and field sampling data were evaluated using the Florida epartment of Environmental Protection (FEP) Automated ata Processing Tool (AaPT); the laboratory electronic data deliverable (E), the error log, and the field E were uploaded to the FEP Business portal as 1_01_SWzdd.zip and 1_0_SWzdd.zip folders. The laboratory analytical reports, COCs, field sampling logs, calibration logs, and the groundwater monitoring certification form are provided in Attachment 1 of this report. This summary review report was prepared by Terracon, under contract from Anderson Columbia Company, Inc. Terracon s services were performed in a manner consistent with generally accepted practices of the profession undertaken in similar studies in the same geographic area during the same period. Terracon makes no warranties, expressed or implied, regarding its services, findings, conclusions, or recommendations. Please note that Terracon does not warrant the work of laboratories, regulatory agencies, or other third parties supplying information used in the preparation of the report. Responsive Resourceful Reliable 1

5 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 ANALYTICAL RESULTS The Operating Permit for the Persimmon Hollow C& facility requires monitoring of groundwater in five monitoring wells. The five permit-listed monitoring wells that were sampled during the reporting period are currently designated MW-1 (Background), MW- (Compliance), MW- (Compliance), MW- (Compliance), and MW- (etection). Monitoring well MW-R is classified as a piezometer and is only used for water level measurements and assessing groundwater flow direction. Monitoring well locations are shown on Figure. Latitudinal and longitudinal coordinates for each monitoring well are presented in Table 1, and the current status of each monitoring well is presented on Table. Well construction details, development logs, and the surveyor s data for monitoring well MW- were submitted to the FEP on August, 00; the surveyor s data for the remaining monitoring wells was submitted on July, 00. Water level measurements were collected from each accessible on-site well prior to purging and sampling on August 1, 01. A water level was collected from monitoring well MW- on September, 01. The groundwater elevation data is summarized in Table. A groundwater contour map for the August 1, 01 groundwater elevations is depicted in Figure and a hydrograph of the monitoring wells depicting the historical range in groundwater elevations is illustrated in Figure. Compared to the February 01 sampling event, the depth to water measured in the site monitoring wells decreased an average of approximately 0. feet (ft). In the area of the facility, the groundwater flow direction was predominantly toward the west and is consistent with historical observations. The hydraulic gradient as measured between wells MW-1 and MW- was approximately 0.00 feet/foot (ft/ft) [(.1ft -.ft)/0ft] across the site. Rainfall data for the period is provided in Attachment. Groundwater samples collected from each of the five monitoring wells were analyzed for field parameters, volatile organic compounds (VOCs), metals, and general & mineral constituents in accordance with the previously-referenced permit. Groundwater samples for the analysis of dissolved aluminum and iron were also collected. A summary of the groundwater analytical results for each of the sampled wells are provided in Table through Table. Separate discussions of each category of routine monitoring constituents are provided in the following sections with additional discussions of Quality Assurance/Quality Control (QA/QC)..1 Field Parameters Groundwater quality field parameters were measured using a YSI Multi-meter and Hach 0q turbidity meter during this groundwater sampling event. The field parameters included ph, turbidity, temperature, specific conductivity, dissolved oxygen, oxidation-reduction potential (ORP), color, and sheen. Each monitoring well was purged and sampled with an electrical submersible pump (ESP) using high-density polyethylene tubing, and the groundwater samples were reported as clear with no sheens. Following adequate well volumes purged and stabilized field parameters, the Responsive Resourceful Reliable

6 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 groundwater samples were collected. The ESP was decontaminated and the tubing was replaced between well sampling station. uring the August 1, 01 and September, 01 sampling event, field parameters at the facility wells varied as follows. Values of ph ranged from. standard units (su) (MW-) to.1 su (MW-). Conductivity values ranged from micromhos per centimeter (μmhos/cm) (MW-) to μmhos/cm (MW-). Temperature readings ranged from 1. C (MW-) to. C (MW-). issolved oxygen values varied from 1. milligrams per liter (mg/l) (MW-) to. mg/l (MW-). ORP values ranged from. millivolts (mv) (MW-) to.1 mv (MW-). Turbidity measurements remained low and ranged from 1. nephelometric turbidity units (NTUs) in MW- to 1. NTUs (MW-1). The field parameters were within historical ranges.. Volatile Organic Compounds VOCs analyzed in groundwater included parameters listed in EPA Methods 01 and 0. Chloroform was measured above laboratory detection limit in the groundwater sample collected from monitoring well MW- at [0.0 micrograms per liter (µg/l)]. The Groundwater Cleanup Target Level (GCTL) for chloroform is 0 µg/l. The detected chloroform concentration was within the historical ranges. All other groundwater samples collected for VOC analysis were below their respective laboratory detection limit.. Metals Routine Semi-Annual Metals Routine metals analyzed in groundwater included aluminum (total and dissolved), arsenic, boron, cadmium, chromium, iron (total and dissolved), lead, mercury, sodium, and strontium. Cadmium, chromium, mercury, and lead were not detected in the groundwater samples collected during this sampling event. The following is a summary of the analytical results. Total aluminum concentrations ranged from 0.0 (MW-) to 0. mg/l (MW-1). issolved aluminum (collected for informational purposes) ranged from BL (MW-1, MW-, MW-) to 0.0 mg/l (MW-). The Secondary rinking Water Standard (SWS) for aluminum is 0. mg/l. The total aluminum concentrations at MW- (0. mg/l) and MW- (0. mg/l) exceeded the SWS of 0. mg/l. The aluminum concentrations in the groundwater samples collected from each of the wells are within the historical ranges. Arsenic was detected in the groundwater samples collected from monitoring well MW- (0.00 mg/l). The Primary rinking Water Standard (PWS) for arsenic is 0.01 mg/l. Boron was detected in the groundwater samples collected from monitoring wells MW- (0.0 mg/l) and MW- (0.0 mg/l). The GCTL for boron is 1. mg/l. The boron concentrations are within historical ranges. Responsive Resourceful Reliable

7 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 Chromium was detected in the groundwater collected from monitoring wells MW-1 (0.00 mg/l), MW- (0.00 mg/l) and MW- (0.00 mg/l). The PWS for chromium is 0.1 mg/l. The chromium concentrations are within historical ranges. Total iron concentrations were detected in the groundwater samples collected from monitoring wells MW- (. mg/l) and MW- (0.0 mg/l); and dissolved iron (collected for informational purposes) was detected in the groundwater samples collected from monitoring wells MW- (1. mg/l) The total and dissolved iron concentrations at MW- exceeded the SWS of 0. mg/l. The total and dissolved iron concentrations are within the historical ranges. Mercury was detected in the groundwater collected from monitoring wells MW-1 ( mg/l), MW- ( mg/l) and MW- ( mg/l). The GCTL for mercury is 0.00 mg/l. The mercury concentrations are within the historical ranges. Strontium concentrations ranged from 0.01 mg/l (MW-) to 0.0 mg/l (MW-). The GCTL for strontium is. mg/l. The strontium concentrations are within the historical ranges. Non-Routine Appendix I Metals Non-routine Appendix I metals were not analyzed during this sampling event.. General & Mineral Constituents General and mineral constituents analyzed during this sampling event included total dissolved solids (TS), sodium, chloride, sulfide, hydrogen sulfide, sulfate, ammonia, and nitrate. The following is a summary of the analytical results. Total dissolved solids ranged from mg/l (MW-) to 0 mg/l (MW-). The SWS for TS is 00 mg/l. The TS concentrations are within historical ranges. Sodium concentrations ranged from.0 mg/l (MW- and MW-) to mg/l (MW-). The PWS for sodium is 0 mg/l. The sodium concentrations are within historical ranges. Chloride concentrations ranged from. mg/l (MW-) to. mg/l (MW-). The SWS for chloride is 0 mg/l. The chloride concentrations are within historical ranges. Sulfide concentrations ranged from BL mg/l (MW-1, MW-, MW- and MW-) to 0.0 mg/l (MW-). Hydrogen sulfide concentrations ranged from BL mg/l (MW-1, MW-, MW- and MW-) to 0.0 mg/l (MW-). The GCTL for hydrogen sulfide is 0.01 mg/l Responsive Resourceful Reliable

8 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 Sulfate concentrations ranged from.0 mg/l (MW-) to 0 mg/l (MW-). The SWS for sulfate is 0 mg/l. The sulfate concentrations are within historical ranges. Ammonia (as N) concentrations ranged from BL (MW-1, MW-, MW- and MW-) to 1. mg/l (MW-). The ammonia (as N) concentrations are within historical ranges. Nitrate (as N) concentrations ranged from 0. mg/l (MW-) to 1. mg/l (MW-). The PWS for nitrate is mg/l. The nitrate (as N) concentrations are within the historical ranges.. Quality Assurance/Quality Control TestAmerica incorporated Level II QA/QC procedures in the completion of their analytical work. The samples for monitoring wells MW-1, MW-, MW- and MW- were collected on August 1, 01 and received by TestAmerica under Chain of Custody on August 1, 01, intact, and properly preserved at. C. TestAmerica subcontracted BENCHMARK to perform analysis of sulfide and hydrogen sulfide. These samples were received under of Chain of Custody on September, 01 by BENCHMARK, intact, and properly preserved at. C. The sample for monitoring well MW- was collected on September, 01 and received by TestAmerica under Chain of Custody on September, 01, intact, and properly preserved at 0. C. TestAmerica subcontracted BENCHMARK to perform analysis of sulfide and hydrogen sulfide. These samples were received under of Chain of Custody on October, 01 by BENCHMARK, intact, and properly preserved at. C. The QA/QC procedures employed appear to be adequate for the scope of this sampling, and the QA/QC results are satisfactory. The following is a summary of the Case Narrative and associated laboratory qualifiers provided in the laboratory analytical reports provided by TestAmerica (and BENCHMARK) for Job Is: and Method 0B analysis - The matrix spike duplicate (MS) recoveries for analytical batch were outside advisory control limits for -Hexanone, Chloromethane and methyl isobutyl ketone. Because the analytes were biased high in the laboratory control sample (LCS) and were not detected in the associated samples, the data was not reported. The matrix spike duplicate (MS) recoveries for analytical batch were outside advisory control limits for Acetone. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits and therefore the result was reported. Metals Analysis No analytical or quality issues were noted. General Chemistry Method(s) Nitrate by calc: This method requires one to analyze the combination of Nitrate plus Nitrite and then analyze Nitrite. The Nitrate is obtained by subtracting the Nitrite from the Nitrate plus Nitrite results. Although the Nitrate plus Nitrite hold time is days the Nitrite Hold time is hours. Since the Nitrite result is critical in determining the Nitrate Responsive Resourceful Reliable

9 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 concentration the hold time for Nitrate result is effectively hours and the Nitrite analysis date/time is therefore reported for the calculated result: MW- (00--1), MW- (00- -), MW- (00--) and MW-1 (00--). U = Indicates that the compound was analyzed for but not detected. J = Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. I = The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. One trip blank was analyzed for VOCs during this sampling event. No VOCs were detected in the trip blank. An evaluation of the field data sheets (Form F 000- and FT 0) prepared by TestAmerica personnel suggests that equipment calibration, groundwater sampling, and equipment decontamination procedures were adequately performed in accordance with FEP Standard Operating Procedures (EP-SOP-001/01). CONCLUSIONS & RECOMMENATIONS The Summer 01 semi-annual sampling event was completed on August 1, 01 and September, 01 for the facility. Constituents analyzed in groundwater included field parameters, VOCs, metals, and general and mineral constituents, as specified in the Operations Permit. The QA/QC measures reported by TestAmerica and BENCHMARK laboratories meet NELAC criteria and the analytical results provided in this laboratory analytical report are considered valid. The depth to water measurements decreased an average of approximately 0. ft when compared to the previous February, 01 sampling event. Based on the August 1, 01 sampling event, the hydraulic gradient as measured between wells MW-1 and MW- was approximately 0.00 ft/ft across the site and the groundwater flow direction was generally towards the west. This groundwater flow direction is consistent with historical sampling events. The ph in the groundwater at each of the five wells was below the regulatory standard (. su); low ph values are common in the surficial aquifers of Northwest Florida. Total aluminum concentrations ranged from 0.0 (MW-) to 0. mg/l (MW-). issolved aluminum (collected for informational purposes) ranged from BL (MW-1, MW-, MW-) to 0.0 mg/l (MW-). SWS for aluminum is 0. mg/l. The total aluminum concentrations at MW- (0. mg/l) and MW- 0. (mg/l) exceeded the SWS of 0. mg/l. However, aluminum concentrations in the groundwater at each well location were within historical ranges, though elevated the highest since 00. Responsive Resourceful Reliable

10 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 Total iron concentrations were detected in the groundwater samples collected from MW- (. mg/l) and MW- (0.0 mg/l); and dissolved iron (collected for informational purposes) was detected in the groundwater samples collected from MW- (1. mg/l). The total and dissolved iron concentrations at MW- exceeded the SWS of 0. mg/l. However, iron concentrations in the groundwater at MW- are within historical ranges. Sulfide was only detected in the groundwater sample collected from monitoring well MW- (0.0 mg/l) during this sampling event. uring the February 01 event, it was detected at all six monitoring wells. The widespread and anomalous hydrogen sulfide concentrations detected exceeding the GCTL of 0.01 mg/l in the groundwater samples collected from wells MW-1, MW-, MW-, MW-, and MW- in February were not duplicated the Summer 01 semi-annual sampling event and were reduced to only one exceedance at MW- (0.0 mg/l). All other wells were below the detection limit for the laboratory. Hydrogen sulfide is typically formed by sulfur and sulfate-reducing bacteria that occur naturally in groundwater in Florida. The fluctuation in the levels of hydrogen sulfide detected may be related to rainfall level fluctuations. No other constituents were reported outside of applicable regulatory standards during this sampling event. The following recommendations are provided: Semi-annual water quality sampling and reporting should continue with the present schedule. Continue using low-flow purging techniques to reduce sample turbidity. Continue to notify the epartment at least 1 days prior to the next scheduled semi-annual sampling event. Responsive Resourceful Reliable

11 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida January, 01 Terracon Project Number: EA0001 CERTIFICATION This Summer 01 semi-annual water quality monitoring summary for the Anderson Columbia Persimmon Hollow C& debris disposal facility was prepared by Tom E. Lewis, P.G. Mr. Lewis is a professional geologist, licensed in Florida, having over years of experience in water quality monitoring and reporting. Respectfully Submitted, Tom E Lewis, P.G. Florida License # 0 January, 01 My license expires /1/00 Responsive Resourceful Reliable

12 FIGURES

13 SITE PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY ANERSON COLUMBIA SANTA ROSA COUNTY, FLORIA PROJECT NO. EA0001 FIGURE 1 SITE LOCATION MAP USGS Ward Basin Quad. Section, T 1 N, R W SCALE: 1 = 000

14 Legend Surficial Monitoring Well/Piezometer (.) Groundwater Elevation (ft).0 Groundwater Contour (ft) Approximate Site Boundary (not professionally surveyed) MW- (.) MW-1 (.1).0 MW- (.).0 MW- (.) 1.0 MW-R (.) 0.0 Map Source: Google Earth MW- (NM).0 This is not a map of survey Persimmon Hollow C& Facility Anderson-Columbia, Inc. WACS I 1 Santa Rosa County, Florida Figure Groundwater Contour Map August 1, 01

15 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 Figure Ground Water Elevations Persimmon Hollow C& ebris isposal Facility Santa Rosa County, Florida 0 Groundwater Elevation (ft NAV) 0 0 MW-1 MW- MW- MW- MW-/R MW- MW- Responsive Resourceful Reliable

16 TABLES

17 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 Well I.. TOC Ground Casing Total Screened Well Test ate Type Elevation Elevation Height epth Interval Location Site Installed (ft NAV) (ft NAV) (ft) (ft BTOC) (ft bgs) (Lat/Long) Number MW-1 MW- //1 //1 B C N 0º '." W º '.11" N 0º '.0" W º '.0" MW- estroyed NA NA NA MW- //1 TABLE 1 MONITOR WELL LOCATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA C.1. MW- //1 Aband N 0º '." W º '.00" MW-R //00 P N 0º '." W º '." MW- /1/00 C N 0º ' 0." W º '." 000 MW- /1/ N 0º '.0" W º ' 0." -0 NA 10 NA Notes: = etection monitor well. B = Background monitor well. C = Compliance monitor well. P = Piezometer. NA = Not applicable/available. Survey data by Southeastern Environmental Eng. on /0/0. ft NAV = feet North American Vertical atum (1). ft BTOC = feet below top-of-casing. ft bls = feet below ground surface. Responsive Resourceful Reliable

18 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE CURRENT MONITOR WELL STATUS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA Total Well I.. Well Type Status epth Lock/Vault Sealed Inner Cap Comments (ft bgs) MW-1 Background E Yes/Steel Yes Last Inspected 0/1/01 MW- Compliance E Yes/Steel Yes Last Inspected 0//01 MW- estroyed NA NA NA NA NA MW- Compliance E Yes/Steel Yes Last Inspected 0/1/01 MW- Abandoned NA NA NA NA NA MW-R Piezometer E 0 Yes/Steel Yes Last Inspected 0/1/01 MW- Compliance E 0 Yes/Steel Yes Last Inspected 0/1/01 MW- etection E. Yes/Steel Yes Last Inspected 0/1/01 Notes: E = existing monitor well. ft bgs = feet below ground surface. NA = Not applicable. Responsive Resourceful Reliable

19 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE GROUN WATER ELEVATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA TOC Screened epth to Ground Water Well I.. Elevation Interval ate Water Elevation (ft NAV) (ft NAV) (ft btoc) (ft NAV) // /0/ //01..0 //01.. //0.. /0/0.. /1/0.. /1/ /1/0. 0. /1/ // //0.. // //0. 1. //0.. /1/0 NM NM //0.. //0.. //0.. MW-1 (Background) // //0.1. //.. /1/.. // /1/.1. //.. //.1.0 //.0.01 //.. //1.1. //1.. // /1/ // 1.. // //.0 0. /0/.0 1. /1/ // // /1/ Responsive Resourceful Reliable

20 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE GROUN WATER ELEVATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA TOC Screened epth to Ground Water Well I.. Elevation Interval ate Water Elevation (ft NAV) (ft NAV) (ft btoc) (ft NAV) MW- (Compliance) //. 0. 1/0/00.. //01..0 // //0.. /0/0.0. /1/0.. /1/0.. /1/0.. /1/0.1.1 //0.. //0.. //0.. //0.0. //0.0. /1/0 NM NM //0.. //0.. // //0 1.. //0.. //.. /1/.0.00 //..0 /1/.. //.. //.. //..0 //.0. //1.1.1 //1.. //1..0 /1/1.. //.1. //.. //..0 /0/..0 /1/1.. //1.0. // /1/1.1.1 Responsive Resourceful Reliable

21 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE GROUN WATER ELEVATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA TOC Screened epth to Ground Water Well I.. Elevation Interval ate Water Elevation (ft NAV) (ft NAV) (ft btoc) (ft NAV) MW- (Abandoned) MW- (Compliance) 1. NA // //.0. 1/0/00 NM NM // //01.. //0.. /0/0.01. /1/0. 1. /1/0.. /1/0.1. /1/ //0..01 // //0.. //0.. //0.. /1/ //0 0.. //0 0.. //0 1.. // // //.. /1/.01. //.0.1 /1/.. // 0.. // // 1.. // 0.1. //1 0.. //1.0. //1.. /1/1. 0. //.1.0 //.1. //..0 /0/..0 /1/1.. // // /1/1.. Responsive Resourceful Reliable

22 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE GROUN WATER ELEVATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA TOC Screened epth to Ground Water Well I.. Elevation Interval ate Water Elevation (ft NAV) (ft NAV) (ft btoc) (ft NAV) MW- (Abandoned) MW-R (Piezometer) 0. NA /0/ // // // /0/0 1.. /1/0 1.. /1/ /1/0.. /1/0 1.. //0.. //0.1.1 //0.. // // /1/0.1. // //0 1.. //0.0. //0.. //0..0 //.. /1/.. // 1..1 /1/ 1.. //.1. //..1 //..1 //.. //1 1.. //1..1 //1.. /1/1.1. //.. // //.0. /0/ 1.1. /1/1.. //1.0. //1..1 /1/1.1. Responsive Resourceful Reliable

23 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE GROUN WATER ELEVATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA TOC Screened epth to Ground Water Well I.. Elevation Interval ate Water Elevation (ft NAV) (ft NAV) (ft btoc) (ft NAV) MW- (Compliance) /0/0 0.. /1/0 1.. /1/0..1 /1/0.. /1/0 1.. //0.. // //0.0. //0.. // /1/ //0 1.. //0 1.. // // //0 1.. //.. /1/.0. // 1.1. /1/ 1.. // 1..0 // 1.0. // 1.. // 1..1 // //1.0. //1..0 /1/ //.0. // 1.. //..00 /0/..1 /1/1.1. 0//1 1.. // /1/1.1. Responsive Resourceful Reliable

24 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE GROUN WATER ELEVATIONS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA TOC Screened epth to Ground Water Well I.. Elevation Interval ate Water Elevation (ft NAV) (ft NAV) (ft btoc) (ft NAV) MW- (etection) Notes: NM = not measured. ft NAV = feet North American Vertical atum (1). ft btoc = feet below top-of-casing. //0 1.. // // /1/ 1..1 //.. /1/.. //.0.0 //..0 // 1.. //.. //1.. // //1 1.. /1/1.. // 1.. //.. // 1..1 /0/ 1.1. /1/ //1.0.0 //1.. /1/1 1.. Responsive Resourceful Reliable

25 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE SUMMARY OF ETECTE GROUN WATER CONSTITUENTS BACKGROUN MONITOR WELL MW-1 PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA Constituent s Standard // 1/0/00 /0/0 /1/0 //0 /1/0 /1/0 //0 //0 //0 //0 //0 //0 /1/0 //0 //0 //0 //0 //0 // /1/ // // // // //1 //1 //1 /1/1 // // // /0/ /1/1 //1 //1 /1/1 Mod. Renewal Semi Semi Semi Semi Semi Semi Semi Renewal Semi Semi Semi Semi Semi Resample Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi FIEL PARAMETERS ph units NS Conductivity umhos/cm None NS Temperature egrees C None 1 1 NS NM.1. issolved Oxygen mg/l None NS Turbidity NTUs None NT NS Redox Potential Millivolts None NT NT NT NT NT NT NT NT NS NT GENERAL & MINERAL TS mg/l NS NT 0 Sodium mg/l 0 NT NS. NT Chloride mg/l NT. NS.1 NT Sulfide mg/l None NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL 0.0 BL BL BL 0.0 BL Hydrogen sulfide mg/l 0.01 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL 0.0 BL BL BL 0.0 BL* Sulfate mg/l 0 NT BL NT NS NT Ammonia-N mg/l. 1. BL BL BL BL 0.0 BL 0.0 BL BL BL NS 0.00 NT BL BL BL BL 0.0 BL BL 0.0 BL BL 0.1 BL BL BL BL BL BL BL BL BL Nitrate-N mg/l NS 1. NT METALS Aluminum, Total mg/l 0. NT BL BL NT NS BL BL BL BL BL Aluminum, issolved mg/l 0. NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL 0.0 BL 0.0 BL 0.00 BL BL BL BL BL BL BL BL BL Arsenic mg/l 0.01 BL BL BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Barium mg/l.0 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT 0.0 NT NT NT NT NT NT NT NT Boron mg/l 1. NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Cadmium mg/l 0.00 BL BL BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Chromium mg/l BL BL BL BL BL BL BL NS 0.00 NT BL BL 0.00 BL BL BL BL BL BL Iron, Total mg/l 0. NT 0. BL BL BL BL 0.01 BL BL NS BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0.0 BL BL Iron, issolved mg/l 0. NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL 0.0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Mercury mg/l 0.00 BL BL BL BL BL BL BL BL BL BL BL NT BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Lead mg/l 0.0 BL BL BL BL BL BL BL 0.00 BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Selenium mg/l 0.0 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT 0.00 NT NT NT NT NT NT NT NT Strontium mg/l. NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT VOLATILE ORGANIC COMPOUNS Benzene ug/l 1 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL BL BL Bromoform ug/l. BL BL BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL BL BL BL BL Carbon isulfide ug/l 00 BL NT NT NT NT NT NT NT BL 0. NT BL NT NS NT NT BL NR BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Chloroform ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL 0.1 BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL Chloromethane ug/l. BL BL BL BL BL BL BL BL 0.1 BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL ichlorodifluoromethane ug/l 0 BL BL BL BL BL BL BL BL BL NT 0.1 BL BL NS BL NT BL BL NR NR NR NR NR NR NR NR NR BL BL BL BL BL BL BL BL BL BL Ethylbenzene ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL BL BL -Hexanone ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL.0 BL BL BL BL BL BL MTBE ug/l 0 BL BL BL BL BL BL BL BL BL BL BL NT NT NS 0.1 NT BL BL NR NR NR NR NR NR NR NR NR BL BL BL BL BL BL BL BL BL BL Toluene ug/l 0 BL BL BL BL BL BL BL BL BL BL 1.1 BL NT NS 0. NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Xylenes ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL.1 BL BL BL BL BL BL BL BL BL BL BL PHENOLS Total Phenols ug/l None BL BL BL BL BL BL BL BL BL NT BL BL BL NS BL NT BL BL BL BL NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Notes: NT = Not tested. BL = Below laboratory detection limits. NM = Not Measured (instrument malfunctioning) NR = Not reported. Shading denotes value outside the applicable water quality standard. NS = Well was not sampled by the consultant. * lab detection limit 0.0 mg/l. Responsive Resourceful Reliable

26 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 Table SUMMARY OF ETECTE GROUN WATER CONSTITUENTS COMPLIANCE MONITOR WELL MW- PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA Constituent s Standard 1/0/00 /0/0 /1/0 //0 /1/0 /1/0 //0 //0 //0 //0 //0 /1/0 //0 //0 //0 //0 //0 // /1/ // // // // //1 //1 //1 /1/1 // // // /0/ /1/1 //1 //1 //1 Renewal Semi Semi Semi Semi Semi Semi Semi Renewal Semi Semi Semi Semi Resample Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi FIEL PARAMETERS ph units NS Conductivity umhos/cm None NS Temperature egrees C None NS NM issolved Oxygen mg/l None NS Turbidity NTUs None NS Redox Potential Millivolts None NT NT NT NT NT NT NS NT GENERAL & MINERAL TS mg/l NS NT Sodium mg/l NS. NT Chloride mg/l NS NT Sulfide mg/l None NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0.01 BL 0.0 BL Hydrogen sulfide mg/l 0.01 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0.01 BL 0.0 BL Sulfate mg/l NT. NS 1. NT Ammonia-N mg/l. BL BL BL BL BL BL 0.0 BL BL NS 0.00 NT 0.00 BL BL BL BL 0.0 BL BL BL BL BL BL BL BL BL BL BL BL Nitrate-N mg/l NS. NT METALS Aluminum, Total mg/l 0. BL BL NT NS BL BL Aluminum, issolved mg/l 0. NT NT NT NT NT NT NT NT NT NT NT NS NT BL BL Arsenic mg/l 0.01 BL BL BL BL BL BL BL BL BL BL BL NS 0.00 NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Boron mg/l 1. NT NT NT NT NT NT NT NT NT NT NT NS NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Cadmium mg/l 0.00 BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Chromium mg/l BL BL BL BL BL BL BL BL 0.00 NS NT BL BL BL BL BL BL BL 0.00 BL BL BL BL BL 0.0 BL BL Iron, Total mg/l 0. BL BL BL 0. BL NS BL BL BL BL BL BL BL 0.0 BL BL BL BL 0.0 BL 0. BL BL Iron, issolved mg/l 0. NT NT NT NT NT NT NT NT NT NT NT NS NT BL BL 0.0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Mercury mg/l 0.00 BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL ###### BL BL ###### BL BL Lead mg/l 0.0 BL BL BL BL BL BL 0.00 BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Strontium mg/l. NT NT NT NT NT NT NT NT NT NT NT NS NT NT NT NT NT NT VOLATILE ORGANIC COMPOUNS Acetone ug/l 00 BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL. BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Bromoform ug/l. BL BL BL BL BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL 0..1 BL BL BL BL BL BL BL BL BL BL BL BL Chloroform ug/l 0 BL BL BL BL BL BL BL NS. NT BL 0.0 BL BL ichlorodifluoromethane ug/l 0 BL BL BL BL BL BL BL BL NT 0.1 BL NS BL NT BL BL NR NR BL NR NR NR NR NR NR BL BL BL BL BL BL BL BL BL BL Ethylbenzene ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL BL BL BL Methylene chloride ug/l BL BL BL 1. BL BL BL BL BL BL BL NS BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Toluene ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0.1 BL BL BL BL BL BL BL BL BL BL BL BL Xylenes ug/l 0 BL BL BL BL BL BL BL BL BL 0. NT NS BL NT BL BL BL BL BL BL BL BL 1. BL BL BL BL BL BL BL BL BL BL BL BL PHENOLS Total Phenols ug/l None BL BL BL BL BL BL BL BL NT BL BL NS BL NT BL BL BL BL NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Notes: NT = Not tested. BL = Below laboratory detection limits. NM = Not Measured (instrument malfunctioning) NR = Not reported. Shading denotes value outside the applicable water quality standard. NS = Well was not sampled by the consultant. * lab detection limit 0.0 mg/l. Responsive Resourceful Reliable

27 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE SUMMARY OF ETECTE GROUN WATER CONSTITUENTS COMPLIANCE MONITOR WELL MW- PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA Constituent s Standard //0 //0 //0 //0 /1/0 //0 //0 //0 //0 //0 // /1/ // // // // //1 //1 //1 /1/1 // // // /0/ /1/1 //1 //1 /1/1 Semi Renewal Semi Semi Semi Semi Resample Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi FIEL PARAMETERS ph units Conductivity umhos/cm None Temperature egrees C None 1 NM.. issolved Oxygen mg/l None Turbidity NTUs None Redox Potential Millivolts None NT NT NT NT GENERAL & MINERAL TS mg/l 00 0 NT Sodium mg/l NT Chloride mg/l 0.0. NT..0. NT Sulfide mg/l None NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0.0 BL Hydrogen sulfide mg/l 0.01 NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0.0 BL Sulfate mg/l 0. NT. BL BL BL NT Ammonia-N mg/l BL BL BL 0.00 NT 0.0 BL BL BL BL 0.0 BL BL BL BL BL BL BL BL BL BL BL BL BL Nitrate-N mg/l NT METALS Aluminum, Total mg/l NT BL BL BL BL BL BL Aluminum, issolved mg/l 0. NT NT NT NT NT NT BL 0.0 BL BL BL BL BL BL 0.01 BL BL BL BL BL BL 0.01 BL 0.0 BL BL BL 0.0 Arsenic mg/l 0.01 BL BL BL BL 0.00 BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Boron mg/l 1. NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL 0.0 BL BL BL BL BL Cadmium mg/l 0.00 BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Chromium mg/l 0.1 BL BL BL NT BL BL 0.00 BL BL BL 0.00 BL BL Iron, Total mg/l BL BL BL BL BL 0.0 BL BL Iron, issolved mg/l 0. NT NT NT NT NT NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Mercury mg/l 0.00 BL BL NT BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Lead mg/l 0.0 BL BL BL BL 0.01 BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Strontium mg/l. NT NT NT NT NT NT NT NT NT NT NT VOLATILE ORGANIC COMPOUNS Bromoform ug/l. BL BL BL BL BL BL NT BL BL BL BL BL BL BL 0.0 BL BL BL BL BL BL BL BL BL BL BL BL BL Chloroform ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Ethylbenzene ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL BL BL MTBE ug/l 0 BL BL BL BL BL 0.1 NT 0.0 BL NR NR NR NR NR NR NR NR NR BL BL BL BL BL BL BL BL BL BL Toluene ug/l 0 BL BL BL BL BL 0.0 NT BL BL BL BL BL BL BL BL BL 1.1 BL BL BL BL BL BL BL BL BL BL BL Xylenes ug/l 0 BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL 1. BL BL BL BL BL BL BL BL BL BL BL PHENOLS Total Phenols ug/l None BL NT BL BL BL BL NT BL BL BL BL NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Notes: NT = Not tested. BL = Below laboratory detection limits. NM = Not Measured (instrument malfunctioning) NR = Not reported. Shading denotes value outside the applicable water quality standard. * lab detection limit 0.0 mg/l. Responsive Resourceful Reliable

28 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE SUMMARY OF ETECTE GROUN WATER CONSTITUENTS COMPLIANCE MONITOR WELL MW- PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA Constituent s /0/0 /1/0 //0 /1/0 /1/0 //0 //0 //0 //0 //0 //0 /1/0 //0 //0 //0 //0 //0 // /1/ // // // // // //1 //1 //1 /1/1 // // // /0/ /1/1 //1 //1 /1/1 Standard Semi Semi Semi Semi Semi Semi Semi Renewal Semi Semi Semi Semi Semi Resample Semi Semi Semi Semi Semi Semi Semi Semi Resample Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi FIEL PARAMETERS ph units Conductivity umhos/cm None Temperature egrees C None NR 1 NM.. issolved Oxygen mg/l None Turbidity NTUs None Redox Potential Millivolts None NT NT NT NT 1 10 NT NT NT NT GENERAL & MINERAL TS mg/l NT NT Sodium mg/l NT NT..... Chloride mg/l BL.... NT 1 NT NT Sulfide mg/l None NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL Hydrogen sulfide mg/l 0.01 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL Sulfate mg/l NT. 1 BL 1 NT 1 NT 0 0 Ammonia-N mg/l. BL 0. BL BL BL 0.0 BL 0.0 BL BL BL NT NT BL 0. BL BL Nitrate-N mg/l NT NT METALS Aluminum, Total mg/l 0. BL 0.1. BL NT BL BL BL BL BL NT BL BL BL Aluminum, issolved mg/l 0. NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL BL BL BL BL NT BL 0.00 BL BL BL BL BL BL BL BL BL BL BL Arsenic mg/l 0.01 BL BL BL BL BL BL BL BL BL BL BL BL 0.00 NT BL BL BL BL BL BL BL BL NT BL BL 0.00 BL BL BL Boron mg/l 1. NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL BL 0.0 NT BL BL 0.0 BL BL BL Cadmium mg/l 0.00 BL BL BL BL BL BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL Chromium mg/l 0.1 BL 0.00 BL BL BL BL BL BL 0.00 BL NT BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL 0.00 BL 0.00 Iron, Total mg/l 0. BL BL 0.1 BL BL BL Iron, issolved mg/l 0. NT NT NT NT NT NT NT NT NT NT NT NT NT BL BL Mercury mg/l 0.00 BL BL BL BL BL BL BL BL BL NT BL BL BL NT BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL Lead mg/l 0.0 BL BL BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL Strontium mg/l. NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT VOLATILE ORGANIC COMPOUNS Bromoform ug/l. BL BL BL BL BL BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL 0. NT BL BL BL BL BL BL BL BL BL BL BL BL BL Chloroform ug/l 0 BL BL BL BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL NT BL BL BL 0.0 BL BL BL BL BL BL BL BL BL Methylene chloride ug/l BL BL BL BL BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL Toluene ug/l 0 BL BL BL BL BL BL BL BL 0. BL NT NT BL NT BL BL BL BL BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL PHENOLS Total Phenols ug/l None BL BL BL BL BL BL BL NT BL BL BL BL BL NT BL BL BL BL NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Notes: NT = Not tested. BL = Below laboratory detection limits. NM = Not Measured (instrument malfunctioning) NR = Not reported. Shading denotes value outside the applicable water quality standard. 1 Methylene chloride detected in method blank at 0.0 ug/l. Bromoform detected in method blank and trip blank at 0. ug/l and 0. ug/l, respectively. Iron detected in method blank at 0.0 mg/l. Chloroform detected in method blank and trip blank at 0. ug/l and 0. ug/l, respectively. Responsive Resourceful Reliable

29 Summer 01 Semi-Annual Monitoring Report Persimmon Hollow C Santa Rosa County, Florida Terracon Project Number: EA0001 TABLE SUMMARY OF ETECTE GROUN WATER CONSTITUENTS ETECTION MONITOR WELL MW- PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA Constituent s Standard //0 // /1/ // /1/ // // // //1 //1 //1 /1/1 // // // /0/ /1/1 //1 //1 /1/1 Initial Semi Semi Semi Re-Sample Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi Semi FIEL PARAMETERS ph units Conductivity umhos/cm None Temperature egrees C None NM.. issolved Oxygen mg/l None Turbidity NTUs None Redox Potential Millivolts None GENERAL & MINERAL TS mg/l NT Sodium mg/l NT Chloride mg/l 0 1 NT Sulfide mg/l None BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL 0. BL Hydrogen sulfide mg/l 0.01 BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL 0.0 BL Sulfate mg/l 0 0 NT Ammonia-N mg/l. 0. BL BL BL BL 0.0 BL BL 0.1 BL Nitrate-N mg/l NT METALS Aluminum, Total mg/l 0. BL BL BL BL NT BL BL BL BL BL 0. BL BL BL BL BL BL BL BL 0.0 Aluminum, issolved mg/l 0. BL BL BL BL NT BL 0.0 BL BL BL BL BL BL BL BL BL BL BL BL BL Arsenic mg/l 0.01 BL BL BL BL NT BL BL BL BL BL 0.00 BL BL BL BL BL BL BL BL Boron mg/l 1. NT NT NT Cadmium mg/l 0.00 BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Chromium mg/l 0.1 BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL Cobalt mg/l 0.1 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Iron, Total mg/l 0. BL BL BL BL BL BL 0.0 BL 0. Iron, issolved mg/l 0. BL BL BL. 0. BL BL BL BL BL BL BL BL BL BL Mercury mg/l 0.00 BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL Lead mg/l 0.0 BL BL BL BL NT BL BL BL BL BL BL BL BL BL BL BL BL BL BL BL Selenium mg/l 0.0 NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Strontium mg/l. NT NT NT VOLATILE ORGANIC COMPOUNS Bromoform ug/l. BL BL BL BL NT BL 0. 1 BL BL BL BL BL BL BL BL BL BL BL BL BL Chloroform ug/l 0 BL 0. BL BL NT BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL cis-1,-ichloroethene ug/l 0.00 BL BL BL 1. NT BL BL BL BL BL BL BL BL BL BL BL Styrene ug/l 0.00 BL BL BL BL BL BL BL BL 0. BL BL BL BL BL BL BL BL BL BL BL Toluene ug/l 0.00 BL BL BL BL NT BL BL 0. BL BL BL BL BL BL BL BL BL BL BL BL PHENOLS Total Phenols ug/l None BL BL NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT NT Notes: NT = Not tested. BL = Below laboratory detection limits. NM = Not Measured (instrument malfunctioning) Shading denotes value outside the applicable water quality standard. 1 Bromoform detected in method blank and trip blank at 0. ug/l and 0. ug/l, respectively. Iron detected in method blank at 0.0 mg/l. Chloroform detected in method blank and trip blank at 0. ug/l and 0. ug/l, respectively. Responsive Resourceful Reliable

30 ATTACHMENT 1 SUMMER 01 LABORATORY ANALYTICAL REPORT AN FIEL SAMPLING LOGS PERSIMMON HOLLOW C& EBRIS ISPOSAL FACILITY SANTA ROSA COUNTY, FLORIA - sampling and analysis by - TESTAMERCIA TALLAHASSEE, FL Sample Organization Comp QAP #: 0G Analytical lab Certification #: 0G/E0

31 1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola McLemore rive Pensacola, FL 1 Tel: (0)-01 TestAmerica Job I: Client Project/Site: Persimmon Landfill For: Anderson Columbia Company Anderson Columbia PO BOX 1 Lake City, Florida 0 Attn: Mr. Scott Cleveland Authorized for release by: /1/01 ::0 PM Kathryn Smith, Manager of Project Management ()0-0 kathy.smith@testamericainc.com esignee for Noel Savoie, Project Manager I (0)- noel.savoie@testamericainc.com 1 1 The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

32 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Table of Contents TestAmerica Job I: Cover Page Table of Contents Case Narrative etection Summary Sample Summary Client Sample Results efinitions Surrogate Summary QC Association QC Sample Results Chronicle Method Summary Certification Summary Subcontract ata Chain of Custody Field ata Sheets Page of TestAmerica Pensacola /1/01

33 Case Narrative Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Job I: Laboratory: TestAmerica Pensacola Narrative Comments No additional comments. Job Narrative Receipt The samples were received on /1/01 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was.º C. GC/MS VOA No analytical or quality issues were noted, other than those described in the efinitions/glossary page. HPLC/IC No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Metals No analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. Field Service / Mobile Lab No analytical or quality issues were noted, other than those described in the efinitions/glossary page. General Chemistry Method(s) Nitrate by calc: This method requires one to analyze the combination of Nitrate plus Nitrite and then analyze Nitrite. The Nitrate is obtained by subtracting the Nitrite from the Nitrate plus Nitrite results. Although the Nitrate plus Nitrite hold time is days the Nitrite Hold time is hours. Since the Nitrite result is critical in determining the Nitrate concentration the hold time for Nitrate result is effectively hours and the Nitrite analysis date/time is therefore reported for the calculated result: MW- (00--1), MW- (00--), MW- (00--) and MW-1 (00--) No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Subcontract Work Method SM00S-Sulfide/SM00SH-HS,Unionized: This method was subcontracted to Benchmark EnviroAnalytical, Inc.. The subcontract laboratory certification is different from that of the facility issuing the final report. TestAmerica Pensacola Page of /1/01

34 Client: Anderson Columbia Company Project/Site: Persimmon Landfill etection Summary TestAmerica Job I: Client Sample I: MW- Lab Sample I: PQL ML il Fac Method Prep Type Sulfate mg/l Total/NA Chloride mg/l Total/NA Mercury 0.0 I ug/l 1.1 Total/NA Boron I 0 ug/l 1 0C Total Recoverable Strontium ug/l 1 0C Total Recoverable Aluminum 1 ug/l 00 Total Recoverable Iron 0 ug/l 00 Total Recoverable Sodium mg/l 00 Total Recoverable Nitrate Nitrite as N mg/l 1. Total/NA Nitrate as N mg/l 1 Nitrate by calc Total/NA Total issolved Solids.0. mg/l 1 SM 0C Total/NA Color Clear Color s 1 Field Sampling Total/NA Field ph. SU 1 Field Sampling Total/NA Field Temperature. Centigrade 1 Field Sampling Total/NA Odor None NONE 1 Field Sampling Total/NA Oxidation Reduction Potential 1. millivolts 1 Field Sampling Total/NA Oxygen, issolved 1.0 mg/l 1 Field Sampling Total/NA Specific Conductance umhos/cm 1 Field Sampling Total/NA Turbidity.1 NTU 1 Field Sampling Total/NA epth to Water (ft from MP) 1.1 ft 1 Field Sampling Total/NA Client Sample I: MW- Lab Sample I: PQL ML il Fac Method Prep Type Sulfate mg/l Total/NA Chloride mg/l Total/NA Mercury 0.0 I ug/l 1.1 Total/NA Boron I 0 ug/l 1 0C Total Recoverable Strontium ug/l 1 0C Total Recoverable Iron, issolved 00 ug/l 00 issolved Aluminum 0 1 ug/l 00 Total Recoverable Arsenic ug/l 00 Total Recoverable Chromium ug/l 00 Total Recoverable Iron 00 ug/l 00 Total Recoverable Sodium mg/l 00 Total Recoverable Ammonia (as N) mg/l Total/NA Nitrate Nitrite as N mg/l 1. Total/NA Nitrate as N mg/l 1 Nitrate by calc Total/NA Total issolved Solids 0.0. mg/l 1 SM 0C Total/NA Color Clear Color s 1 Field Sampling Total/NA Field ph.1 SU 1 Field Sampling Total/NA This etection Summary does not include radiochemical test results. TestAmerica Pensacola Page of /1/01

35 Client: Anderson Columbia Company Project/Site: Persimmon Landfill etection Summary TestAmerica Job I: Client Sample I: MW- (Continued) Lab Sample I: 00-- PQL ML il Fac Method Prep Type Field Temperature. Centigrade 1 Field Sampling Total/NA Odor None NONE 1 Field Sampling Total/NA Oxidation Reduction Potential. millivolts 1 Field Sampling Total/NA Oxygen, issolved. mg/l 1 Field Sampling Total/NA Specific Conductance umhos/cm 1 Field Sampling Total/NA Turbidity.1 NTU 1 Field Sampling Total/NA epth to Water (ft from MP).0 ft 1 Field Sampling Total/NA Client Sample I: MW- Lab Sample I: 00-- PQL ML il Fac Method Prep Type Sulfate mg/l Total/NA Chloride mg/l Total/NA Strontium ug/l 1 0C Total Recoverable Aluminum, issolved 0 1 ug/l 00 issolved Aluminum 0 1 ug/l 00 Total Recoverable Chromium ug/l 00 Total Recoverable Iron 0 ug/l 00 Total Recoverable Sodium mg/l 00 Total Recoverable Nitrate Nitrite as N mg/l 1. Total/NA Nitrate as N mg/l 1 Nitrate by calc Total/NA Total issolved Solids.0. mg/l 1 SM 0C Total/NA Color Clear Color s 1 Field Sampling Total/NA Field ph. SU 1 Field Sampling Total/NA Field Temperature. Centigrade 1 Field Sampling Total/NA Odor None NONE 1 Field Sampling Total/NA Oxidation Reduction Potential.1 millivolts 1 Field Sampling Total/NA Oxygen, issolved. mg/l 1 Field Sampling Total/NA Specific Conductance umhos/cm 1 Field Sampling Total/NA Turbidity.1 NTU 1 Field Sampling Total/NA epth to Water (ft from MP). ft 1 Field Sampling Total/NA Client Sample I: MW-1 Lab Sample I: 00-- PQL ML il Fac Method Prep Type Sulfate mg/l Total/NA Chloride mg/l Total/NA Mercury 0.0 I ug/l 1.1 Total/NA Strontium ug/l 1 0C Total Recoverable Aluminum 1 ug/l 00 Total Recoverable Chromium ug/l 00 Total Recoverable Sodium mg/l 00 Total Recoverable Nitrate Nitrite as N mg/l 1. Total/NA Nitrate as N mg/l 1 Nitrate by calc Total/NA This etection Summary does not include radiochemical test results. TestAmerica Pensacola Page of /1/01

36 Client: Anderson Columbia Company Project/Site: Persimmon Landfill etection Summary TestAmerica Job I: Client Sample I: MW-1 (Continued) Lab Sample I: 00-- PQL ML il Fac Method Prep Type Total issolved Solids.0. mg/l 1 SM 0C Total/NA Color Clear Color s 1 Field Sampling Total/NA Field ph. SU 1 Field Sampling Total/NA Field Temperature. Centigrade 1 Field Sampling Total/NA Odor None NONE 1 Field Sampling Total/NA Oxidation Reduction Potential.1 millivolts 1 Field Sampling Total/NA Oxygen, issolved. mg/l 1 Field Sampling Total/NA Specific Conductance umhos/cm 1 Field Sampling Total/NA Turbidity 1. NTU 1 Field Sampling Total/NA epth to Water (ft from MP) 1. ft 1 Field Sampling Total/NA Client Sample I: T Blank Lab Sample I: 00-- No etections. Client Sample I: MW-R Lab Sample I: 00-- PQL ML il Fac Method Prep Type epth to Water (ft from MP).1 ft 1 Field Sampling Total/NA 1 1 This etection Summary does not include radiochemical test results. TestAmerica Pensacola Page of /1/01

37 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received MW- Water 0/1/1 0:01 0/1/1 : 00-- MW- Water 0/1/1 0: 0/1/1 : 00-- MW- Water 0/1/1 0: 0/1/1 : 00-- MW-1 Water 0/1/1 : 0/1/1 : 00-- T Blank Water 0/1/1 00:00 0/1/1 : 00-- MW-R Water 0/1/1 00:00 0/1/1 : TestAmerica Pensacola Page of /1/01

38 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0:01 ate Received: 0/1/1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: Analyzed Acetone U ug/l 0/0/1 1: 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 U 0. U 1. U 0. U 0. U 0. U 1.0 U 0. U.1 U 0.0 U.0 U 1. U 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1. ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1.1 ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1 1. ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1.0 ug/l 0/0/1 1: ug/l 0/0/1 1: TestAmerica Pensacola Page of /1/01

39 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0:01 ate Received: 0/1/1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: Analyzed Xylenes, Total 1. U 1. ug/l 0/0/1 1: 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) /0/1 1: 1 Analyzed 1,-ichloroethane-d (Surr) - 1 0/0/1 1: 1 Method: Anions, Ion Chromatography PQL Sulfate mg/l 0/0/1 0:0 1 Chloride mg/l 0/0/1 0:0 1 Method:.1 - Mercury (CVAA) PQL ML ML Analyzed Analyzed Mercury 0.0 I ug/l 0/0/1 1: 0//1 1:0 1 Method: 0C - Metals (ICP) - Total Recoverable PQL Boron I 0 ug/l 0/0/1 : 0/0/1 1:1 1 Strontium ug/l 0/0/1 : 0/0/1 1:1 1 Method: 00 - issolved Metals by ICP-MS - issolved PQL ML ML Analyzed Analyzed Aluminum, issolved 1 U 1 ug/l 0//1 : 0//1 : Iron, issolved U Method: 00 - Metals (ICP/MS) - Total Recoverable il Fac il Fac il Fac il Fac il Fac il Fac ug/l 0//1 : 0//1 : PQL Aluminum 1 ug/l 0//1 : 0//1 : Arsenic 0. U ug/l 0//1 : 0//1 : Cadmium Chromium 0. U 1.1 U Iron 0 Sodium.1 Lead 0. U ML Analyzed il Fac. 0. ug/l 0//1 : 0//1 :. 1.1 ug/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : mg/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : General Chemistry PQL ML Analyzed il Fac Ammonia (as N) 0.0 U mg/l 0//1 : 1 Nitrate Nitrite as N mg/l 0/1/1 : 1 Nitrate as N mg/l 0/01/1 0: 1 Total issolved Solids.0. mg/l 0/0/1 : 1 Nitrite as N 0.01 U mg/l 0/01/1 0: 1 Method: Field Sampling - Field Sampling PQL ML Analyzed il Fac Color Clear Color s 0/1/1 0:00 1 Field ph. SU 0/1/1 0:00 1 Field Temperature. Centigrade 0/1/1 0:00 1 Odor None NONE 0/1/1 0:00 1 Oxidation Reduction Potential 1. millivolts 0/1/1 0:00 1 Oxygen, issolved 1.0 mg/l 0/1/1 0:00 1 TestAmerica Pensacola Page of /1/01

40 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0:01 ate Received: 0/1/1 : Method: Field Sampling - Field Sampling (Continued) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: Analyzed Specific Conductance umhos/cm 0/1/1 0:00 1 Turbidity.1 NTU 0/1/1 0:00 1 epth to Water (ft from MP) 1.1 ft 0/1/1 0:00 1 il Fac TestAmerica Pensacola Page of /1/01

41 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Acetone U ug/l 0/0/1 1:1 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 U 0. U 1. U 0. U 0. U 0. U 1.0 U 0. U.1 U 0.0 U.0 U 1. U 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1:1 1. ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1:1 1.1 ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1:1 1.0 ug/l 0/0/1 1: ug/l 0/0/1 1: TestAmerica Pensacola Page of /1/01

42 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Xylenes, Total 1. U 1. ug/l 0/0/1 1:1 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) 0-0 0/0/1 1:1 1 Analyzed 1,-ichloroethane-d (Surr) - 1 0/0/1 1:1 1 Method: Anions, Ion Chromatography PQL Sulfate mg/l 0/0/1 0: 1 Chloride mg/l 0/0/1 0: 1 Method:.1 - Mercury (CVAA) PQL ML ML Analyzed Analyzed Mercury 0.0 I ug/l 0/0/1 1: 0//1 1:0 1 Method: 0C - Metals (ICP) - Total Recoverable PQL Boron I 0 ug/l 0/0/1 : 0/0/1 1: 1 Strontium ug/l 0/0/1 : 0/0/1 1: 1 Method: 00 - issolved Metals by ICP-MS - issolved PQL ML ML Analyzed Analyzed Aluminum, issolved 1 U 1 ug/l 0//1 : 0/1/1 00:0 Iron, issolved 00 Method: 00 - Metals (ICP/MS) - Total Recoverable il Fac il Fac il Fac il Fac il Fac il Fac ug/l 0//1 : 0/1/1 00:0 PQL Aluminum 0 1 ug/l 0//1 : 0//1 : Arsenic ug/l 0//1 : 0//1 : Cadmium 0. U. 0. ug/l 0//1 : 0//1 : Chromium. Iron 00 Sodium Lead 0. U ML Analyzed il Fac. 1.1 ug/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : mg/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : General Chemistry PQL ML Analyzed il Fac Ammonia (as N) mg/l 0//1 : 1 Nitrate Nitrite as N mg/l 0/1/1 : 1 Nitrate as N mg/l 0/01/1 0: 1 Total issolved Solids 0.0. mg/l 0/0/1 : 1 Nitrite as N 0.01 U mg/l 0/01/1 0: 1 Method: Field Sampling - Field Sampling PQL ML Analyzed il Fac Color Clear Color s 0/1/1 0: 1 Field ph.1 SU 0/1/1 0: 1 Field Temperature. Centigrade 0/1/1 0: 1 Odor None NONE 0/1/1 0: 1 Oxidation Reduction Potential. millivolts 0/1/1 0: 1 Oxygen, issolved. mg/l 0/1/1 0: 1 TestAmerica Pensacola Page of /1/01

43 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Method: Field Sampling - Field Sampling (Continued) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Specific Conductance umhos/cm 0/1/1 0: 1 Turbidity.1 NTU 0/1/1 0: 1 epth to Water (ft from MP).0 ft 0/1/1 0: 1 il Fac TestAmerica Pensacola Page 1 of /1/01

44 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Acetone U ug/l 0/0/1 1:1 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 U 0. U 1. U 0. U 0. U 0. U 1.0 U 0. U.1 U 0.0 U.0 U 1. U 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1:1 1. ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1:1 1.1 ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1:1 1.0 ug/l 0/0/1 1: ug/l 0/0/1 1: TestAmerica Pensacola Page 1 of /1/01

45 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Xylenes, Total 1. U 1. ug/l 0/0/1 1:1 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) 0-0 0/0/1 1:1 1 Analyzed 1,-ichloroethane-d (Surr) - 1 0/0/1 1:1 1 Method: Anions, Ion Chromatography PQL Sulfate mg/l 0/0/1 0:1 1 Chloride mg/l 0/0/1 0:1 1 Method:.1 - Mercury (CVAA) PQL ML ML Analyzed Analyzed Mercury 0.00 U ug/l 0/0/1 1: 0//1 1:0 1 Method: 0C - Metals (ICP) - Total Recoverable PQL Boron U 0 ug/l 0/0/1 : 0/0/1 1: 1 Strontium 1 Method: 00 - issolved Metals by ICP-MS - issolved ML Analyzed il Fac il Fac il Fac il Fac il Fac ug/l 0/0/1 : 0/0/1 1: 1 PQL Aluminum, issolved 0 1 ug/l 0//1 : 0/1/1 00:0 Iron, issolved U ug/l 0//1 : 0/1/1 00:0 Method: 00 - Metals (ICP/MS) - Total Recoverable PQL ML ML Analyzed Analyzed Aluminum 0 1 ug/l 0//1 : 0//1 :1 Arsenic 0. U ug/l 0//1 : 0//1 :1 Cadmium 0. U Chromium. Iron 0 Sodium.0 Lead 0. U il Fac il Fac. 0. ug/l 0//1 : 0//1 : ug/l 0//1 : 0//1 :1 ug/l 0//1 : 0//1 : mg/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : General Chemistry PQL ML Analyzed il Fac Ammonia (as N) 0.0 U mg/l 0//1 : 1 Nitrate Nitrite as N mg/l 0/1/1 :00 1 Nitrate as N mg/l 0/01/1 0: 1 Total issolved Solids.0. mg/l 0/0/1 : 1 Nitrite as N 0.01 U mg/l 0/01/1 0: 1 Method: Field Sampling - Field Sampling PQL ML Analyzed il Fac Color Clear Color s 0/1/1 0: 1 Field ph. SU 0/1/1 0: 1 Field Temperature. Centigrade 0/1/1 0: 1 Odor None NONE 0/1/1 0: 1 Oxidation Reduction Potential.1 millivolts 0/1/1 0: 1 Oxygen, issolved. mg/l 0/1/1 0: 1 TestAmerica Pensacola Page of /1/01

46 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Method: Field Sampling - Field Sampling (Continued) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Specific Conductance umhos/cm 0/1/1 0: 1 Turbidity.1 NTU 0/1/1 0: 1 epth to Water (ft from MP). ft 0/1/1 0: 1 il Fac TestAmerica Pensacola Page of /1/01

47 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW-1 ate Collected: 0/1/1 : ate Received: 0/1/1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Acetone U ug/l 0/0/1 1: 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 U 0. U 1. U 0. U 0. U 0. U 1.0 U 0. U.1 U 0.0 U.0 U 1. U 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1. ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1.1 ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1 1. ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: ug/l 0/0/1 1: 1.0 ug/l 0/0/1 1: ug/l 0/0/1 1: TestAmerica Pensacola Page 1 of /1/01

48 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW-1 ate Collected: 0/1/1 : ate Received: 0/1/1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Xylenes, Total 1. U 1. ug/l 0/0/1 1: 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) 0-0 0/0/1 1: 1 Analyzed 1,-ichloroethane-d (Surr) - 1 0/0/1 1: 1 Method: Anions, Ion Chromatography PQL Sulfate mg/l 0/0/1 1:1 1 Chloride mg/l 0/0/1 1:1 1 Method:.1 - Mercury (CVAA) PQL ML ML Analyzed Analyzed Mercury 0.0 I ug/l 0/0/1 1: 0//1 1: 1 Method: 0C - Metals (ICP) - Total Recoverable PQL Boron U 0 ug/l 0/0/1 : 0/0/1 1: 1 Strontium Method: 00 - issolved Metals by ICP-MS - issolved ML Analyzed il Fac il Fac il Fac il Fac il Fac ug/l 0/0/1 : 0/0/1 1: 1 PQL Aluminum, issolved 1 U 1 ug/l 0//1 : 0/1/1 00: Iron, issolved U Method: 00 - Metals (ICP/MS) - Total Recoverable ML Analyzed il Fac ug/l 0//1 : 0/1/1 00: PQL Aluminum 1 ug/l 0//1 : 0//1 : Arsenic 0. U ug/l 0//1 : 0//1 : Cadmium 0. U Chromium. Iron U Sodium. Lead 0. U ML Analyzed il Fac. 0. ug/l 0//1 : 0//1 :. 1.1 ug/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : mg/l 0//1 : 0//1 : ug/l 0//1 : 0//1 : General Chemistry PQL ML Analyzed il Fac Ammonia (as N) 0.0 U mg/l 0//1 : 1 Nitrate Nitrite as N mg/l 0/1/1 :01 1 Nitrate as N mg/l 0/01/1 0: 1 Total issolved Solids.0. mg/l 0/0/1 : 1 Nitrite as N 0.01 U mg/l 0/01/1 0: 1 Method: Field Sampling - Field Sampling PQL ML Analyzed il Fac Color Clear Color s 0/1/1 : 1 Field ph. SU 0/1/1 : 1 Field Temperature. Centigrade 0/1/1 : 1 Odor None NONE 0/1/1 : 1 Oxidation Reduction Potential.1 millivolts 0/1/1 : 1 Oxygen, issolved. mg/l 0/1/1 : 1 TestAmerica Pensacola Page 1 of /1/01

49 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW-1 ate Collected: 0/1/1 : ate Received: 0/1/1 : Method: Field Sampling - Field Sampling (Continued) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Specific Conductance umhos/cm 0/1/1 : 1 Turbidity 1. NTU 0/1/1 : 1 epth to Water (ft from MP) 1. ft 0/1/1 : 1 il Fac TestAmerica Pensacola Page 1 of /1/01

50 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: T Blank ate Collected: 0/1/1 00:00 ate Received: 0/1/1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Acetone U ug/l 0/0/1 : 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 U 0. U 1. U 0. U 0. U 0. U 1.0 U 0. U.1 U 0.0 U.0 U 1. U 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1. ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1.1 ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1 1. ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1.0 ug/l 0/0/1 : ug/l 0/0/1 : TestAmerica Pensacola Page 0 of /1/01

51 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: T Blank ate Collected: 0/1/1 00:00 ate Received: 0/1/1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Xylenes, Total 1. U 1. ug/l 0/0/1 : 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) 0-0 0/0/1 : 1 Analyzed 1,-ichloroethane-d (Surr) - 1 0/0/1 : 1 il Fac il Fac TestAmerica Pensacola Page 1 of /1/01

52 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW-R ate Collected: 0/1/1 00:00 ate Received: 0/1/1 : Method: Field Sampling - Field Sampling Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed epth to Water (ft from MP).1 ft 0/0/1 00:00 1 il Fac TestAmerica Pensacola Page of /1/01

53 Client: Anderson Columbia Company Project/Site: Persimmon Landfill efinitions/glossary TestAmerica Job I: Qualifiers GC/MS VOA Qualifier Qualifier escription U Indicates that the compound was analyzed for but not detected. HPLC/IC Qualifier Qualifier escription U Indicates that the compound was analyzed for but not detected. Metals Qualifier Qualifier escription I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. U Indicates that the compound was analyzed for but not detected. General Chemistry Qualifier U I Glossary Abbreviation Qualifier escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid ER uplicate Error Ratio (normalized absolute difference) il Fac ilution Factor L etection Limit (o/oe) L, RA, RE, IN Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision Level Concentration (Radiochemistry) EL Estimated etection Limit (ioxin) LO Limit of etection (o/oe) LOQ Limit of Quantitation (o/oe) MA Minimum etectable Activity (Radiochemistry) MC Minimum etectable Concentration (Radiochemistry) ML Method etection Limit ML Minimum Level (ioxin) NC Not Calculated N Not etected at the reporting limit (or ML or EL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) 1 1 TestAmerica Pensacola Page of /1/01

54 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Surrogate Summary Method: 0B - Volatile Organic Compounds (GC/MS) TOL CA Lab Sample I Client Sample I (0-0) (-1) MW MW MW MW T Blank LCS 00-/0 MB 00-/ Surrogate Legend TOL = Toluene-d (Surr) Lab Control Sample Method Blank CA = 1,-ichloroethane-d (Surr) 0 0 TestAmerica Job I: Percent Surrogate Recovery (Acceptance Limits) Prep Type: Total/NA TestAmerica Pensacola Page of /1/01

55 Client: Anderson Columbia Company Project/Site: Persimmon Landfill GC/MS VOA Analysis : QC Association Summary TestAmerica Job I: Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water 0B 00-- MW- Total/NA 00-- MW- Total/NA 00-- MW-1 Total/NA 00-- T Blank Total/NA MB 00-/ Method Blank Total/NA LCS 00-/0 Lab Control Sample Total/NA HPLC/IC Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water MW- Total/NA 00-- MW- Total/NA 00-- MW-1 Total/NA MB 00-/ Method Blank Total/NA LCS 00-/ Lab Control Sample Total/NA LCS 00-/ Lab Control Sample up Total/NA Metals Prep : Water Water Water Water Water Water 0B 0B 0B 0B 0B 0B Water 00.0 Water 00.0 Water 00.0 Water 00.0 Water 00.0 Water 00.0 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total Recoverable Water 00A 00-- MW- Total Recoverable 00-- MW- Total Recoverable 00-- MW-1 Total Recoverable MB 00-/1-A Method Blank Total Recoverable LCS 00-/-A Lab Control Sample Total Recoverable Water Water Water Water Water 00A 00A 00A 00A 00A Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total Recoverable Water 0C 00-- MW- Total Recoverable 00-- MW- Total Recoverable 00-- MW-1 Total Recoverable MB 00-/1-A Method Blank Total Recoverable LCS 00-/-A Lab Control Sample Total Recoverable Prep : Water 0C Water 0C Water 0C Water 0C Water 0C Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water MW- Total/NA 00-- MW- Total/NA 00-- MW-1 Total/NA MB 00-/1-A Method Blank Total/NA LCS 00-/1-A Lab Control Sample Total/NA Water.1 Water.1 Water.1 Water.1 Water.1 TestAmerica Pensacola Page of /1/01

56 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Metals (Continued) Analysis : 0 QC Association Summary TestAmerica Job I: Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water MW- Total/NA 00-- MW- Total/NA 00-- MW-1 Total/NA MB 00-/1-A Method Blank Total/NA LCS 00-/1-A Lab Control Sample Total/NA Prep : 1 Water.1 Water.1 Water.1 Water.1 Water.1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- issolved Water 00A MW- Total Recoverable 00-- MW- issolved 00-- MW- Total Recoverable 00-- MW- issolved 00-- MW- Total Recoverable 00-- MW-1 issolved 00-- MW-1 Total Recoverable MB 00-1/1-A ^ Method Blank Total Recoverable LCS 00-1/-A Lab Control Sample Total Recoverable Analysis : 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- issolved Water MW- Total Recoverable 00-- MW- issolved 00-- MW- Total Recoverable 00-- MW- issolved 00-- MW- Total Recoverable 00-- MW-1 issolved 00-- MW-1 Total Recoverable MB 00-1/1-A ^ Method Blank Total Recoverable LCS 00-1/-A Lab Control Sample Total Recoverable Water Water Water Water Water Water Water Water Water 00A 00A 00A 00A 00A 00A 00A 00A 00A Water 00 1 Water 00 1 Water 00 1 Water 00 1 Water 00 1 Water 00 1 Water 00 1 Water 00 1 Water General Chemistry Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water SM 00 NO B 00-- MW- Total/NA Water SM 00 NO B 00-- MW- Total/NA Water SM 00 NO B 00-- MW-1 Total/NA Water SM 00 NO B MB 00-/ Method Blank Total/NA Water SM 00 NO B LCS 00-/ Lab Control Sample Total/NA Water SM 00 NO B MRL 00-/ Lab Control Sample Total/NA Water SM 00 NO B MS MW- Total/NA Water SM 00 NO B MS MW- Total/NA Water SM 00 NO B Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water SM 0C TestAmerica Pensacola Page of /1/01

57 Client: Anderson Columbia Company Project/Site: Persimmon Landfill General Chemistry (Continued) Analysis : (Continued) QC Association Summary TestAmerica Job I: Lab Sample I Client Sample I Prep Type Matrix Method Prep 00-- MW- Total/NA Water SM 0C 00-- MW- Total/NA 00-- MW-1 Total/NA MB 00-/1 Method Blank Total/NA LCS 00-/ Lab Control Sample Total/NA Analysis : 1 Water Water Water Water SM 0C SM 0C SM 0C SM 0C Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water MW- Total/NA 00-- MW- Total/NA 00-- MW-1 Total/NA MB 00-1/ Method Blank Total/NA LCS 00-1/ Lab Control Sample Total/NA MRL 00-1/ Lab Control Sample Total/NA 00-- MS MW- Total/NA 00-- MS MW- Total/NA Analysis : Water 0.1 Water 0.1 Water 0.1 Water 0.1 Water 0.1 Water 0.1 Water 0.1 Water 0.1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water MW- Total/NA 00-- MW- Total/NA 00-- MW-1 Total/NA MB 00-/1 Method Blank Total/NA LCS 00-/ Lab Control Sample Total/NA MRL 00-/1 Lab Control Sample Total/NA Water. Water. Water. Water. Water. Water Analysis : 1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water Nitrate by calc 00-- MW- Total/NA Water Nitrate by calc 00-- MW- Total/NA Water Nitrate by calc 00-- MW-1 Total/NA Water Nitrate by calc Field Service / Mobile Lab Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water Field Sampling 00-- MW- Total/NA Water Field Sampling 00-- MW- Total/NA Water Field Sampling 00-- MW-1 Total/NA Water Field Sampling Analysis : 0 Lab Sample I Client Sample I Prep Type Matrix Method Prep 00-- MW-R Total/NA Water Field Sampling TestAmerica Pensacola Page of /1/01

58 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 00-/ Analysis : MB MB PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Acetone U ug/l 0/0/1 : 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate il Fac 0. U ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : ug/l 0/0/1 : U ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : 1. U. ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : 1.0 U.0.0 ug/l 0/0/1 : U ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : ug/l 0/0/1 : 1 1. U.0 1. ug/l 0/0/1 : ug/l 0/0/1 : 1 0. U.0 0. ug/l 0/0/1 : ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : U ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1.1 U.1 ug/l 0/0/1 : U ug/l 0/0/1 : 1.0 U.0.0 ug/l 0/0/1 : 1 1. U 1. ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : U ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : U ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : ug/l 0/0/1 : 1 0. U ug/l 0/0/1 : 1 0. U.0 0. ug/l 0/0/1 : 1.0 U.0 ug/l 0/0/1 : TestAmerica Pensacola Page of /1/01

59 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MB 00-/ Analysis : MB MB PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Vinyl chloride ug/l 0/0/1 : 1 Xylenes, Total Surrogate %Recovery il Fac 1. U 1. ug/l 0/0/1 : 1 MB MB Qualifier Limits Analyzed Toluene-d (Surr) 0-0 0/0/1 : 1 1,-ichloroethane-d (Surr) 0-1 0/0/1 : 1 Lab Sample I: LCS 00-/0 Analysis : Spike Added LCS LCS il Fac Client Sample I: Lab Control Sample Prep Type: Total/NA Acetone 00 ug/l - 0 Benzene ug/l Chlorobromomethane ug/l ichlorobromomethane 0.0. ug/l - 1 Bromoform ug/l - Bromomethane 0.0. ug/l - 0 -Butanone (MEK) 00 0 ug/l 1 - Carbon disulfide 0.0. ug/l 1-1 Carbon tetrachloride 0.0. ug/l 1-1 Chlorobenzene ug/l Chloroethane 0.0. ug/l 1 - -Chloroethyl vinyl ether ug/l - 0 Chloroform ug/l - Chloromethane 0.0. ug/l - 1 Chlorodibromomethane ug/l - 1,-ibromo--Chloropropane 0.0. ug/l - Ethylene ibromide 0.0. ug/l 0 - ibromomethane 0.0. ug/l 0-1,-ichlorobenzene ug/l - 1,-ichlorobenzene ug/l 0-1,-ichlorobenzene ug/l 0 - trans-1,-ichloro--butene 0.0. ug/l - ichlorodifluoromethane ug/l 1-1,1-ichloroethane ug/l 0-1,-ichloroethane ug/l - cis-1,-ichloroethene ug/l 1 - trans-1,-ichloroethene ug/l 0-1,1-ichloroethene ug/l - 1 1,-ichloropropane ug/l cis-1,-ichloropropene 0.0. ug/l - trans-1,-ichloropropene 0.0. ug/l - Ethylbenzene ug/l 0 - -Hexanone 00 1 ug/l - 1 Iodomethane ug/l - Methylene Chloride 0.0. ug/l - -Methyl--pentanone (MIBK) 00 0 ug/l 1-1 %Rec %Rec. Limits TestAmerica Pensacola Page of /1/01

60 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 00-/0 Analysis : Spike Added LCS LCS TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Total/NA Methyl tert-butyl ether 0.0. ug/l 1 - Styrene 0.0. ug/l 0-1,1,1,-Tetrachloroethane 0.0. ug/l - 1,1,,-Tetrachloroethane 0.0. ug/l 0 - Tetrachloroethene 0.0. ug/l 1 - Toluene ug/l 0-1,1,1-Trichloroethane 0.0. ug/l - 1,1,-Trichloroethane ug/l 0 - Trichloroethene 0.0. ug/l 0 - Trichlorofluoromethane ug/l 0-1 1,,-Trichloropropane ug/l 0 - Vinyl acetate 0 1 ug/l 1-0 Vinyl chloride 0.0. ug/l 0 - Xylenes, Total 0. ug/l 0 - Surrogate %Recovery LCS LCS Qualifier Limits Toluene-d (Surr) 0-0 1,-ichloroethane-d (Surr) 0-1 Method: Anions, Ion Chromatography Lab Sample I: MB 00-/ Analysis : MB MB PQL ML %Rec %Rec. Limits Client Sample I: Method Blank Prep Type: Total/NA Analyzed Sulfate 0.0 U mg/l 0/0/1 0: 1 Chloride il Fac 0. U mg/l 0/0/1 0: Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : Spike LCS LCS %Rec. Added %Rec Limits Sulfate.0. mg/l 0-0 Chloride.0.0 mg/l 0-0 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample up Prep Type: Total/NA Analysis : Spike LCS LCS %Rec. RP Added %Rec Limits RP Limit Sulfate.0. mg/l Chloride.0.1 mg/l TestAmerica Pensacola Page 0 of /1/01

61 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method:.1 - Mercury (CVAA) QC Sample Results TestAmerica Job I: Lab Sample I: MB 00-/1-A Client Sample I: Method Blank Prep Type: Total/NA Analysis : 0 Prep : MB MB PQL Mercury 0.00 U ug/l 0/0/1 1: 0//1 1: 1 ML Analyzed Lab Sample I: LCS 00-/1-A Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 0 Prep : Spike LCS LCS %Rec. Added Mercury ug/l 1-1 Method: 0C - Metals (ICP) Lab Sample I: MB 00-/1-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : Prep : MB MB PQL Boron U 0 ug/l 0/0/1 : 0/0/1 :1 1 Strontium ML %Rec Limits Analyzed il Fac il Fac 1.0 U ug/l 0/0/1 : 0/0/1 :1 1 Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : Prep : Spike LCS LCS %Rec. Added Boron 00 0 ug/l 0-0 Strontium 00 0 ug/l 0-0 %Rec Limits Method: 00 - Metals (ICP/MS) Lab Sample I: MB 00-1/1-A ^ Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : 0 Prep : 1 MB MB PQL Aluminum 1 U 1 ug/l 0//1 : 0//1 : Aluminum, issolved Arsenic Cadmium Chromium Iron Iron, issolved Sodium Lead ML Analyzed il Fac 1 U 1 ug/l 0//1 : 0//1 : 0. U ug/l 0//1 : 0//1 : 0. U. 0. ug/l 0//1 : 0//1 : 1.1 U. 1.1 ug/l 0//1 : 0//1 : U ug/l 0//1 : 0//1 : U ug/l 0//1 : 0//1 : 0.1 U mg/l 0//1 : 0//1 : 0. U ug/l 0//1 : 0//1 : TestAmerica Pensacola Page 1 of /1/01

62 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method: 00 - Metals (ICP/MS) (Continued) QC Sample Results TestAmerica Job I: Lab Sample I: LCS 00-1/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : 0 Prep : 1 Spike LCS LCS %Rec. Added Aluminum 00 0 ug/l Aluminum, issolved 00 0 ug/l Arsenic ug/l 0-0 Cadmium ug/l 0-0 Chromium 0.0. ug/l 0-0 Iron ug/l Iron, issolved ug/l Sodium.00. mg/l Lead ug/l 0-0 Method: Nitrogen, Ammonia Lab Sample I: MB 00-1/ Analysis : 1 MB MB PQL ML %Rec Limits Client Sample I: Method Blank Prep Type: Total/NA Analyzed Ammonia (as N) 0.0 U mg/l 0//1 : 1 Lab Sample I: LCS 00-1/ Analysis : 1 Spike Added LCS LCS il Fac Client Sample I: Lab Control Sample Prep Type: Total/NA Ammonia (as N).00.1 mg/l 0-0 %Rec %Rec. Limits Lab Sample I: MRL 00-1/ Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 1 Spike MRL MRL %Rec. Added %Rec Limits Ammonia (as N) I mg/l 0-0 Lab Sample I: 00-- MS Analysis : 1 Sample Client Sample I: MW- Prep Type: Total/NA Sample Spike MS MS %Rec. Added %Rec Limits Ammonia (as N) 0.0 U mg/l Lab Sample I: 00-- MS Client Sample I: MW- Prep Type: Total/NA Analysis : 1 Sample Sample Spike MS MS %Rec. RP Added %Rec Limits RP Limit Ammonia (as N) 0.0 U mg/l TestAmerica Pensacola Page of /1/01

63 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/1 Analysis : MB MB QC Sample Results PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Nitrate Nitrite as N 0.01 U mg/l 0/1/1 : 1 Lab Sample I: LCS 00-/ Analysis : Spike Added LCS LCS il Fac Client Sample I: Lab Control Sample Prep Type: Total/NA Nitrate Nitrite as N mg/l 0-0 Lab Sample I: MRL 00-/1 Analysis : Spike Added MRL MRL %Rec %Rec. Limits Client Sample I: Lab Control Sample Prep Type: Total/NA Nitrate Nitrite as N I mg/l 0-0 Method: SM 0C - Solids, Total issolved (TS) Lab Sample I: MB 00-/1 Analysis : MB MB PQL ML %Rec %Rec. Limits Client Sample I: Method Blank Prep Type: Total/NA Analyzed Total issolved Solids. U.0. mg/l 0/0/1 : 1 il Fac Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : Spike LCS LCS %Rec. Added %Rec Limits Total issolved Solids mg/l 1 - Method: SM 00 NO B - Nitrogen, Nitrite Lab Sample I: MB 00-/ Client Sample I: Method Blank Prep Type: Total/NA Analysis : MB MB PQL ML Analyzed il Fac Nitrite as N 0.01 U mg/l 0/01/1 0: 1 Lab Sample I: LCS 00-/ Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : Spike LCS LCS %Rec. Added %Rec Limits Nitrite as N mg/l 0-0 TestAmerica Pensacola Page of /1/01

64 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: SM 00 NO B - Nitrogen, Nitrite (Continued) Lab Sample I: MRL 00-/ Analysis : Spike Added MRL MRL TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Total/NA Nitrite as N mg/l Lab Sample I: MS Analysis : Sample Sample Result Qualifier Spike Added MS MS Nitrite as N 0.01 U mg/l 0 - Lab Sample I: MS Analysis : Sample Sample Result Qualifier Spike Added MS MS %Rec %Rec %Rec. Limits Client Sample I: MW- Prep Type: Total/NA %Rec. Limits Client Sample I: MW- Prep Type: Total/NA Nitrite as N 0.01 U mg/l %Rec %Rec. Limits RP RP Limit TestAmerica Pensacola Page of /1/01

65 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: MW- Lab Sample I: ate Collected: 0/1/1 0:01 ate Received: 0/1/1 : Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 1: RS TAL PEN Total/NA Initial Final Number Analysis /0/1 0:0 JAW TAL PEN Total/NA Prep.1 0 ml 0 ml 0/0/1 1: N1 TAL PEN Total/NA Analysis //1 1:0 N1 TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 0/0/1 : KWN TAL PEN Total Recoverable Analysis 0C 1 0/0/1 1:1 CWF TAL PEN issolved Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN issolved Analysis //1 : RE TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN Total Recoverable Analysis //1 : RE TAL PEN Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Total/NA Analysis. 1 ml ml 0/1/1 : KJR TAL PEN Total/NA Analysis Nitrate by calc 1 1 0/01/1 0: RRC TAL PEN Total/NA Analysis SM 0C 1 0 ml 0 ml 0/0/1 : EK TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Total/NA Analysis Field Sampling 1 0/1/1 0:00 FS TAL PEN Client Sample I: MW- Lab Sample I: 00-- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Lab Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 1:1 RS TAL PEN Total/NA Initial Final Number Analysis /0/1 0: JAW TAL PEN Total/NA Prep.1 0 ml 0 ml 0/0/1 1: N1 TAL PEN Total/NA Analysis //1 1:0 N1 TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 0/0/1 : KWN TAL PEN Total Recoverable Analysis 0C 1 0/0/1 1: CWF TAL PEN issolved Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN issolved Analysis /1/1 00:0 RE TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN Total Recoverable Analysis //1 : RE TAL PEN Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Total/NA Analysis. 1 ml ml 0/1/1 : KJR TAL PEN Total/NA Analysis Nitrate by calc 1 1 0/01/1 0: RRC TAL PEN Total/NA Analysis SM 0C 1 0 ml 0 ml 0/0/1 : EK TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Total/NA Analysis Field Sampling 1 0/1/1 0: FS TAL PEN Lab TestAmerica Pensacola Page of /1/01

66 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: MW- Lab Sample I: 00-- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 1:1 RS TAL PEN Total/NA Initial Final Number Analysis /0/1 0:1 JAW TAL PEN Total/NA Prep.1 0 ml 0 ml 0/0/1 1: N1 TAL PEN Total/NA Analysis //1 1:0 N1 TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 0/0/1 : KWN TAL PEN Total Recoverable Analysis 0C 1 0/0/1 1: CWF TAL PEN issolved Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN issolved Analysis /1/1 00:0 RE TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN Total Recoverable Analysis //1 :1 RE TAL PEN Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Total/NA Analysis. 1 ml ml 0/1/1 :00 KJR TAL PEN Total/NA Analysis Nitrate by calc 1 1 0/01/1 0: RRC TAL PEN Total/NA Analysis SM 0C 1 0 ml 0 ml 0/0/1 : EK TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Total/NA Analysis Field Sampling 1 0/1/1 0: FS TAL PEN Client Sample I: MW-1 Lab Sample I: 00-- ate Collected: 0/1/1 : ate Received: 0/1/1 : Lab Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 1: RS TAL PEN Total/NA Initial Final Number Analysis /0/1 1:1 JAW TAL PEN Total/NA Prep.1 0 ml 0 ml 0/0/1 1: N1 TAL PEN Total/NA Analysis //1 1: N1 TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 0/0/1 : KWN TAL PEN Total Recoverable Analysis 0C 1 0/0/1 1: CWF TAL PEN issolved Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN issolved Analysis /1/1 00: RE TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN Total Recoverable Analysis //1 : RE TAL PEN Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Total/NA Analysis. 1 ml ml 0/1/1 :01 KJR TAL PEN Total/NA Analysis Nitrate by calc 1 1 0/01/1 0: RRC TAL PEN Total/NA Analysis SM 0C 1 0 ml 0 ml 0/0/1 : EK TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Total/NA Analysis Field Sampling 1 0/1/1 : FS TAL PEN Lab TestAmerica Pensacola Page of /1/01

67 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: T Blank Lab Sample I: 00-- ate Collected: 0/1/1 00:00 ate Received: 0/1/1 : Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 : RS TAL PEN Initial Final Number Client Sample I: MW-R Lab Sample I: 00-- ate Collected: 0/1/1 00:00 ate Received: 0/1/1 : Prep Type Total/NA Type Method Run il Factor Initial or Analyzed Analyst Analysis Field Sampling 1 0 0/0/1 00:00 FS TAL PEN Final Number Client Sample I: Method Blank Lab Sample I: MB 00-/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Initial Final Number Lab Lab Lab Lab Sample I: MB 00-/1-A or Analyzed Analyst Total Recoverable Prep 00A 0 ml 0 ml 0/0/1 : KWN TAL PEN Total Recoverable Initial Final Number Analysis 0C 1 0/0/1 :1 CWF TAL PEN Lab Client Sample I: Method Blank Lab Sample I: MB 00-/ ate Collected: N/A ate Received: N/A Prep Type Total/NA il Initial Final Type Method Run Factor Number or Analyzed Analyst Lab Analysis /0/1 0: JAW TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 : RS TAL PEN Initial Final Number Lab TestAmerica Pensacola Page of /1/01

68 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Method Blank Lab Sample I: MB 00-/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis SM 0C 1 0 ml 0 ml 0/0/1 : EK TAL PEN Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Initial Final Number Lab Lab Sample I: MB 00-/1-A or Analyzed Analyst Total/NA Prep.1 0 ml 0 ml 0/0/1 1: N1 TAL PEN Total/NA Initial Final Number Analysis //1 1: N1 TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-1/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Initial Final Number Lab Lab Lab Sample I: MB 00-1/1-A ^ il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total Recoverable Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN Total Recoverable Analysis //1 : RE TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis. 1 ml ml 0/1/1 : KJR TAL PEN Initial Final Number Lab Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Initial Final Number Lab TestAmerica Pensacola Page of /1/01

69 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Lab Sample I: LCS 00-/-A or Analyzed Analyst Total Recoverable Prep 00A 0 ml 0 ml 0/0/1 : KWN TAL PEN Total Recoverable Initial Final Number Analysis 0C 1 0/0/1 :0 CWF TAL PEN Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Prep Type Total/NA Type Method Run il Factor Initial or Analyzed Analyst Analysis /0/1 0: JAW TAL PEN Final Number Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/0 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml 0/0/1 : RS TAL PEN Initial Final Number Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Lab Lab Lab il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis SM 0C 1 0 ml 0 ml 0/0/1 : EK TAL PEN Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Lab Sample I: LCS 00-/1-A il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep.1 0 ml 0 ml 0/0/1 1: N1 TAL PEN Total/NA Analysis //1 1: N1 TAL PEN Client Sample I: Lab Control Sample Lab Sample I: LCS 00-1/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis ml ml 1 0//1 :1 KJR TAL PEN Initial Final Number Lab TestAmerica Pensacola Page of /1/01

70 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Lab Sample I: LCS 00-1/-A or Analyzed Analyst Total Recoverable Prep 00A 0 ml 0 ml 1 0//1 : RE TAL PEN Total Recoverable Initial Final Number Analysis //1 :1 RE TAL PEN Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis. 1 ml ml 0/1/1 : KJR TAL PEN Initial Final Number Client Sample I: Lab Control Sample up Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Prep Type Total/NA Type Method Run il Factor Initial or Analyzed Analyst Analysis /0/1 0:0 JAW TAL PEN Final Number Client Sample I: Lab Control Sample Lab Sample I: MRL 00-/ ate Collected: N/A ate Received: N/A Lab Lab Lab il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Client Sample I: Lab Control Sample Lab Sample I: MRL 00-1/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Initial Final Number Lab Client Sample I: Lab Control Sample Lab Sample I: MRL 00-/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis. 1 ml ml 0/1/1 : KJR TAL PEN Initial Final Number Lab TestAmerica Pensacola Page 0 of /1/01

71 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0/1/1 0:01 ate Received: 0/1/1 : Prep Type Type Method Run il Factor Lab Sample I: MS or Analyzed Analyst Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Client Sample I: MW- ate Collected: 0/1/1 0:01 ate Received: 0/1/1 : Prep Type Type Method Run il Factor Initial Final Number Lab Lab Sample I: MS or Analyzed Analyst Total/NA Analysis SM 00 NO B 1 ml ml 0/01/1 0: BAB TAL PEN Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Prep Type Type Method Run il Factor Initial Final Number Lab Lab Sample I: 00-- MS or Analyzed Analyst Total/NA Analysis ml ml 1 0//1 :0 KJR TAL PEN Client Sample I: MW- ate Collected: 0/1/1 0: ate Received: 0/1/1 : Prep Type Type Method Run il Factor Initial Final Number Lab Lab Sample I: 00-- MS or Analyzed Analyst Total/NA Analysis ml ml 1 0//1 : KJR TAL PEN Initial Final Number Lab Laboratory References: BMEA = Benchmark EnviroAnalytical, Inc., 1 th St E., Palmetto, FL 1, TEL (1)- TAL PEN = TestAmerica Pensacola, McLemore rive, Pensacola, FL 1, TEL (0)-01 TestAmerica Pensacola Page 1 of /1/01

72 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory 0B Volatile Organic Compounds (GC/MS) SW TAL PEN 00.0 Anions, Ion Chromatography MCAWW TAL PEN.1 Mercury (CVAA) EPA TAL PEN 0C Metals (ICP) SW TAL PEN 00 issolved Metals by ICP-MS SW TAL PEN 00 Metals (ICP/MS) SW TAL PEN 0.1 Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN Nitrate by calc Nitrogen, Nitrate SM TAL PEN SM 0C Solids, Total issolved (TS) SM TAL PEN SM 00 NO B Nitrogen, Nitrite SM TAL PEN Field Sampling Field Sampling EPA TAL PEN Subcontract SM00S-Sulfide/SM00SH-HS,Unionized None BMEA.1 Preparation, Mercury EPA TAL PEN 00A Preparation, Total Recoverable or issolved Metals SW TAL PEN 00B Purge and Trap SW TAL PEN Protocol References: EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March 1 And Subsequent Revisions. None = None SM = "Standard Methods For The Examination Of Water And Wastewater" SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1 And Its Updates. Laboratory References: BMEA = Benchmark EnviroAnalytical, Inc., 1 th St E., Palmetto, FL 1, TEL (1)- TAL PEN = TestAmerica Pensacola, McLemore rive, Pensacola, FL 1, TEL (0) TestAmerica Pensacola Page of /1/01

73 Accreditation/Certification Summary Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Laboratory: TestAmerica Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program EPA Region Identification Number Expiration ate Florida NELAP E The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Field Sampling Water Color Field Sampling Water epth to Water (ft from MP) Field Sampling Water Field ph Field Sampling Water Field Temperature Field Sampling Water Odor Field Sampling Water Oxidation Reduction Potential Field Sampling Water Oxygen, issolved Field Sampling Water Specific Conductance Field Sampling Water Turbidity Nitrate by calc Water Nitrate as N TestAmerica Pensacola Page of /1/01

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83 1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Pensacola McLemore rive Pensacola, FL 1 Tel: (0)-01 TestAmerica Job I: Client Project/Site: Persimmon Landfill For: Anderson Columbia Company Anderson Columbia PO BOX 1 Lake City, Florida 0 Attn: Mr. Scott Cleveland Authorized for release by: /1/01 :: AM Noel Savoie, Project Manager I (0)- noel.savoie@testamericainc.com 1 1 The test results in this report meet all 00 NELAC and 00 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

84 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Table of Contents TestAmerica Job I: Cover Page Table of Contents Case Narrative etection Summary Sample Summary Client Sample Results efinitions Surrogate Summary QC Association QC Sample Results Chronicle Method Summary Certification Summary Subcontract ata Chain of Custody Field ata Sheets Page of TestAmerica Pensacola /1/01

85 Case Narrative Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Job I: Laboratory: TestAmerica Pensacola Narrative Comments No additional comments. Job Narrative Receipt The samples were received on //01 : AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 0.º C. GC/MS VOA Method 0B: The laboratory control sample (LCS) for analytical batch recovered outside control limits for the following analytes: -Hexanone, Chloromethane and methyl isobutyl ketone. These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported. Method 0B: The matrix spike duplicate (MS) associated with batch recovered outside advisory control limits for Chloromethane. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) met acceptance criteria; therefore, the results have been reported and qualified. No additional analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. HPLC/IC No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Metals No analytical or quality issues were noted, other than those described in the efinitions/glossary page Field Service Field results have been included in the report. General Chemistry No analytical or quality issues were noted, other than those described above or in the efinitions/glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the efinitions/glossary page. Subcontract Work Method SM00S-Sulfide/SM00SH-HS,Unionized: This method was subcontracted to Benchmark EnviroAnalytical, Inc.. The subcontract laboratory certification is different from that of the facility issuing the final report. Report attached. TestAmerica Pensacola Page of /1/01

86 Client: Anderson Columbia Company Project/Site: Persimmon Landfill etection Summary TestAmerica Job I: Client Sample I: MW- Lab Sample I: PQL ML il Fac Method Prep Type Chloroform 0.0 I ug/l 1 0B Total/NA Sulfate mg/l Total/NA Chloride mg/l Total/NA Strontium ug/l 1 0C Total Recoverable Aluminum, issolved 0 1 ug/l 00 issolved Aluminum 1 ug/l 00 Total Recoverable Sodium mg/l 00 Total Recoverable Nitrate Nitrite as N mg/l 1. Total/NA Nitrate as N mg/l 1 Nitrate by calc Total/NA Total issolved Solids.0. mg/l 1 SM 0C Total/NA Color Clear Color s 1 Field Sampling Total/NA Field ph. SU 1 Field Sampling Total/NA Field Temperature 1. Centigrade 1 Field Sampling Total/NA Odor None NONE 1 Field Sampling Total/NA Oxidation Reduction Potential. millivolts 1 Field Sampling Total/NA Oxygen, issolved 1. mg/l 1 Field Sampling Total/NA Specific Conductance 1 umhos/cm 1 Field Sampling Total/NA Turbidity. NTU 1 Field Sampling Total/NA Client Sample I: T Blank Lab Sample I: 00-- No etections This etection Summary does not include radiochemical test results. TestAmerica Pensacola Page of /1/01

87 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Sample Summary TestAmerica Job I: Lab Sample I Client Sample I Matrix Collected Received MW- Water 0//1 : 0//1 : 00-- T Blank Water 0//1 00:00 0//1 : TestAmerica Pensacola Page of /1/01

88 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0//1 : ate Received: 0//1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: Analyzed Acetone U ug/l /0/1 1: 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 I 0. U J 1. U 0. U 0. U 0. U 1.0 U J 0. U.1 U J 0.0 U.0 U 1. U J 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: 1. ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: 1.1 ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: 1 1. ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: ug/l /0/1 1: 1.0 ug/l /0/1 1: ug/l /0/1 1: TestAmerica Pensacola Page of /1/01

89 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0//1 : ate Received: 0//1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: Analyzed Xylenes, Total 1. U 1. ug/l /0/1 1: 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) 0-0 /0/1 1: 1 Analyzed 1,-ichloroethane-d (Surr) - 1 /0/1 1: 1 Method: Anions, Ion Chromatography PQL Sulfate mg/l 0//1 : 1 Chloride mg/l 0//1 : 1 Method:.1 - Mercury (CVAA) PQL ML ML Analyzed Analyzed Mercury 0.00 U ug/l /0/1 : /0/1 1: 1 Method: 0C - Metals (ICP) - Total Recoverable PQL Boron U 0 ug/l /01/1 : /0/1 0: 1 Strontium Method: 00 - issolved Metals by ICP-MS - issolved ML Analyzed il Fac il Fac il Fac il Fac il Fac ug/l /01/1 : /0/1 0: 1 PQL Aluminum, issolved 0 1 ug/l /1/1 0: /1/1 : Iron, issolved U ug/l /1/1 0: /1/1 : Method: 00 - Metals (ICP/MS) - Total Recoverable PQL ML ML Analyzed Analyzed Aluminum 1 ug/l //1 : //1 : Arsenic 0. U ug/l //1 : //1 : Cadmium Chromium Iron 0. U 1.1 U U Sodium.0 Lead 0. U il Fac il Fac. 0. ug/l //1 : //1 :. 1.1 ug/l //1 : //1 : ug/l //1 : //1 : mg/l //1 : //1 : ug/l //1 : //1 : General Chemistry PQL ML Analyzed il Fac Ammonia (as N) 0.0 U mg/l /01/1 : 1 Nitrate Nitrite as N mg/l /01/1 1: 1 Nitrate as N mg/l 0//1 0:1 1 Total issolved Solids.0. mg/l /0/1 0: 1 Nitrite as N 0.01 U mg/l 0//1 0:1 1 Method: Field Sampling - Field Sampling PQL ML Analyzed il Fac Color Clear Color s 0//1 : 1 Field ph. SU 0//1 : 1 Field Temperature 1. Centigrade 0//1 : 1 Odor None NONE 0//1 : 1 Oxidation Reduction Potential. millivolts 0//1 : 1 Oxygen, issolved 1. mg/l 0//1 : 1 TestAmerica Pensacola Page of /1/01

90 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: MW- ate Collected: 0//1 : ate Received: 0//1 : Method: Field Sampling - Field Sampling (Continued) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: Analyzed Specific Conductance 1 umhos/cm 0//1 : 1 Turbidity. NTU 0//1 : 1 il Fac TestAmerica Pensacola Page of /1/01

91 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: T Blank ate Collected: 0//1 00:00 ate Received: 0//1 : Method: 0B - Volatile Organic Compounds (GC/MS) Client Sample Results PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Acetone U ug/l /0/1 :1 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate Vinyl chloride 0. U 0. U 0.1 U 0. U. U 0. U.0 U 0.0 U 0. U J 1. U 0. U 0. U 0. U 1.0 U J 0. U.1 U J 0.0 U.0 U 1. U J 0. U 1.0 U 0. U 0. U 0.0 U 0. U 0. U.0 U il Fac ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 :1 1. ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 :1 1.1 ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 :1 1.0 ug/l /0/1 : ug/l /0/1 : TestAmerica Pensacola Page of /1/01

92 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Client Sample I: T Blank ate Collected: 0//1 00:00 ate Received: 0//1 : Client Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) PQL ML TestAmerica Job I: Lab Sample I: 00-- Analyzed Xylenes, Total 1. U 1. ug/l /0/1 :1 1 Surrogate %Recovery Qualifier Limits Toluene-d (Surr) 0-0 /0/1 :1 1 Analyzed 1,-ichloroethane-d (Surr) - 1 /0/1 :1 1 il Fac il Fac TestAmerica Pensacola Page of /1/01

93 Client: Anderson Columbia Company Project/Site: Persimmon Landfill efinitions/glossary TestAmerica Job I: Qualifiers GC/MS VOA Qualifier Qualifier escription U Indicates that the compound was analyzed for but not detected. J Estimated value; value may not be accurate. Spike recovery or RP outside of criteria. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. HPLC/IC Qualifier Qualifier escription U Indicates that the compound was analyzed for but not detected. Metals Qualifier Qualifier escription U Indicates that the compound was analyzed for but not detected. General Chemistry Qualifier U I Glossary Abbreviation Qualifier escription Indicates that the compound was analyzed for but not detected. The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. These commonly used abbreviations may or may not be present in this report. Listed under the "" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid ER uplicate Error Ratio (normalized absolute difference) il Fac ilution Factor L etection Limit (o/oe) L, RA, RE, IN Indicates a ilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample LC ecision Level Concentration (Radiochemistry) EL Estimated etection Limit (ioxin) LO Limit of etection (o/oe) LOQ Limit of Quantitation (o/oe) MA Minimum etectable Activity (Radiochemistry) MC Minimum etectable Concentration (Radiochemistry) ML Method etection Limit ML Minimum Level (ioxin) NC Not Calculated N Not etected at the reporting limit (or ML or EL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RP Relative Percent ifference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (ioxin) TEQ Toxicity Equivalent Quotient (ioxin) 1 1 TestAmerica Pensacola Page of /1/01

94 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Surrogate Summary Method: 0B - Volatile Organic Compounds (GC/MS) TOL CA Lab Sample I Client Sample I (0-0) (-1) MW MS MW MS MW T Blank LCS 00-/0 MB 00-/ Surrogate Legend TOL = Toluene-d (Surr) Lab Control Sample Method Blank CA = 1,-ichloroethane-d (Surr) 1 TestAmerica Job I: Percent Surrogate Recovery (Acceptance Limits) Prep Type: Total/NA TestAmerica Pensacola Page of /1/01

95 Client: Anderson Columbia Company Project/Site: Persimmon Landfill GC/MS VOA Analysis : QC Association Summary TestAmerica Job I: Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water 0B 00-- T Blank Total/NA MB 00-/ Method Blank Total/NA LCS 00-/0 Lab Control Sample Total/NA MS MW- Total/NA MS MW- Total/NA HPLC/IC Analysis : Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water 00.0 MB 00-/1 Method Blank Total/NA LCS 00-/1 Lab Control Sample Total/NA LCS 00-/ Lab Control Sample up Total/NA Metals Prep : 00 Water Water Water Water Water 0B 0B 0B 0B 0B Water 00.0 Water 00.0 Water 00.0 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total Recoverable Water 00A MB 00-00/1-A Method Blank Total Recoverable LCS 00-00/-A Lab Control Sample Total Recoverable Prep : Water Water 00A 00A Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water.1 MB 00-/1-A Method Blank Total/NA LCS 00-/1-A Lab Control Sample Total/NA Analysis : 1 Water.1 Water.1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total Recoverable Water 0C 00 MB 00-00/1-A Method Blank Total Recoverable LCS 00-00/-A Lab Control Sample Total Recoverable Analysis : 1 Water 0C 00 Water 0C 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water.1 MB 00-/1-A Method Blank Total/NA LCS 00-/1-A Lab Control Sample Total/NA Prep : 10 Water.1 Water.1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total Recoverable Water 00A MB 00-10/1-A ^ Method Blank Total Recoverable LCS 00-10/-A Lab Control Sample Total Recoverable MS MW- Total Recoverable MS MW- Total Recoverable Water Water Water Water 00A 00A 00A 00A TestAmerica Pensacola Page 1 of /1/01

96 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Metals (Continued) Analysis : 1 QC Association Summary TestAmerica Job I: Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total Recoverable Water MB 00-10/1-A ^ Method Blank Total Recoverable LCS 00-10/-A Lab Control Sample Total Recoverable MS MW- Total Recoverable MS MW- Total Recoverable Prep : Water Water Water Water Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- issolved Water 00A MB 00-/1-A ^ Method Blank Total Recoverable LCS 00-/-A Lab Control Sample Total Recoverable Analysis : 1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- issolved Water 00 MB 00-/1-A ^ Method Blank Total Recoverable LCS 00-/-A Lab Control Sample Total Recoverable General Chemistry Analysis : 10 Water Water 00A 00A Water 00 Water 00 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water SM 00 NO B MB 00-10/ Method Blank Total/NA LCS 00-10/ Lab Control Sample Total/NA MRL 00-10/1 Lab Control Sample Total/NA MS MW- Total/NA MS MW- Total/NA Water Water Water Water Water SM 00 NO B SM 00 NO B SM 00 NO B SM 00 NO B SM 00 NO B Analysis : 1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water 0.1 MB 00-1/1 Method Blank Total/NA LCS 00-1/ Lab Control Sample Total/NA MRL 00-1/1 Lab Control Sample Total/NA Analysis : Water 0.1 Water 0.1 Water 0.1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water. MB 00-/1 Method Blank Total/NA LCS 00-/ Lab Control Sample Total/NA Analysis : 1 Water. Water. Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water Nitrate by calc Analysis : 1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water SM 0C MB 00-1/1 Method Blank Total/NA Water SM 0C TestAmerica Pensacola Page 1 of /1/01

97 Client: Anderson Columbia Company Project/Site: Persimmon Landfill General Chemistry (Continued) Analysis : 1 (Continued) QC Association Summary TestAmerica Job I: Lab Sample I Client Sample I Prep Type Matrix Method Prep LCS 00-1/ Lab Control Sample Total/NA Water SM 0C Field Service / Mobile Lab Analysis : 1 Lab Sample I Client Sample I Prep Type Matrix Method Prep MW- Total/NA Water Field Sampling TestAmerica Pensacola Page of /1/01

98 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) Lab Sample I: MB 00-/ Analysis : MB MB PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Acetone U ug/l /0/1 : 1 Benzene Chlorobromomethane ichlorobromomethane Bromoform Bromomethane -Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane -Chloroethyl vinyl ether Chloroform Chloromethane Chlorodibromomethane 1,-ibromo--Chloropropane Ethylene ibromide ibromomethane 1,-ichlorobenzene 1,-ichlorobenzene 1,-ichlorobenzene trans-1,-ichloro--butene ichlorodifluoromethane 1,1-ichloroethane 1,-ichloroethane cis-1,-ichloroethene trans-1,-ichloroethene 1,1-ichloroethene 1,-ichloropropane cis-1,-ichloropropene trans-1,-ichloropropene Ethylbenzene -Hexanone Iodomethane Methylene Chloride -Methyl--pentanone (MIBK) Methyl tert-butyl ether Styrene 1,1,1,-Tetrachloroethane 1,1,,-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,-Trichloroethane Trichloroethene Trichlorofluoromethane 1,,-Trichloropropane Vinyl acetate il Fac 0. U ug/l /0/1 : 1 0. U ug/l /0/1 : ug/l /0/1 : U ug/l /0/1 : 1 0. U ug/l /0/1 : 1. U. ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : 1 0. U ug/l /0/1 : 1.0 U.0.0 ug/l /0/1 : U ug/l /0/1 : 1 0. U ug/l /0/1 : ug/l /0/1 : 1 1. U.0 1. ug/l /0/1 : ug/l /0/1 : 1 0. U.0 0. ug/l /0/1 : ug/l /0/1 : 1 0. U ug/l /0/1 : 1 0. U ug/l /0/1 : U ug/l /0/1 : 1 0. U ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : 1.1 U.1 ug/l /0/1 : U ug/l /0/1 : 1.0 U.0.0 ug/l /0/1 : 1 1. U 1. ug/l /0/1 : 1 0. U ug/l /0/1 : U ug/l /0/1 : 1 0. U ug/l /0/1 : ug/l /0/1 : 1 0. U ug/l /0/1 : U ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : ug/l /0/1 : 1 0. U ug/l /0/1 : 1 0. U.0 0. ug/l /0/1 : 1.0 U.0 ug/l /0/1 : TestAmerica Pensacola Page of /1/01

99 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MB 00-/ Analysis : MB MB PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Vinyl chloride ug/l /0/1 : 1 Xylenes, Total Surrogate %Recovery il Fac 1. U 1. ug/l /0/1 : 1 MB MB Qualifier Limits Analyzed Toluene-d (Surr) 0-0 /0/1 : 1 1,-ichloroethane-d (Surr) - 1 /0/1 : 1 Lab Sample I: LCS 00-/0 Analysis : Spike Added LCS LCS il Fac Client Sample I: Lab Control Sample Prep Type: Total/NA Acetone 00 ug/l 1-0 Benzene 0.0. ug/l 0 - Chlorobromomethane ug/l ichlorobromomethane ug/l - 1 Bromoform ug/l - Bromomethane ug/l - 0 -Butanone (MEK) 00 1 ug/l 1 - Carbon disulfide ug/l 1-1 Carbon tetrachloride 0.0. ug/l 1-1 Chlorobenzene 0.0. ug/l 0 - Chloroethane 0.0. ug/l - -Chloroethyl vinyl ether 0.0. ug/l 1-0 Chloroform 0.0. ug/l - Chloromethane 0.0. J ug/l - 1 Chlorodibromomethane ug/l 0-1,-ibromo--Chloropropane 0.0. ug/l 0 - Ethylene ibromide 0.0. ug/l 0 - ibromomethane 0.0. ug/l 0-1,-ichlorobenzene 0.0. ug/l - 1,-ichlorobenzene 0.0. ug/l 0-1,-ichlorobenzene 0.0. ug/l 0 - trans-1,-ichloro--butene 0.0. ug/l 1 - ichlorodifluoromethane ug/l 1-1,1-ichloroethane ug/l 0-1,-ichloroethane 0.0. ug/l - cis-1,-ichloroethene 0.0. ug/l - trans-1,-ichloroethene 0.0. ug/l 0-1,1-ichloroethene 0.0. ug/l - 1 1,-ichloropropane 0.0. ug/l 0 - cis-1,-ichloropropene 0.0. ug/l - trans-1,-ichloropropene 0.0. ug/l - Ethylbenzene 0.0. ug/l 0 - -Hexanone 00 1 J ug/l - 1 Iodomethane 0.0. ug/l 1 - Methylene Chloride 0.0. ug/l - -Methyl--pentanone (MIBK) 00 0 J ug/l - 1 %Rec %Rec. Limits TestAmerica Pensacola Page 1 of /1/01

100 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: LCS 00-/0 Analysis : Spike Added LCS LCS TestAmerica Job I: Client Sample I: Lab Control Sample Prep Type: Total/NA Methyl tert-butyl ether 0.0. ug/l 0 - Styrene 0.0. ug/l 0-1,1,1,-Tetrachloroethane 0.0. ug/l - 1,1,,-Tetrachloroethane 0.0. ug/l 0 - Tetrachloroethene 0.0. ug/l - Toluene 0.0. ug/l 0-1,1,1-Trichloroethane 0.0. ug/l - 1,1,-Trichloroethane 0.0. ug/l Trichloroethene 0.0. ug/l Trichlorofluoromethane 0.0. ug/l - 1 1,,-Trichloropropane 0.0. ug/l 0 - Vinyl acetate 0 ug/l - 0 Vinyl chloride 0.0. ug/l - Xylenes, Total 0.1 ug/l 0 - Surrogate %Recovery LCS LCS Qualifier Limits Toluene-d (Surr) 0-0 1,-ichloroethane-d (Surr) 1-1 Lab Sample I: MS Analysis : Sample Sample Result Qualifier Spike Added MS MS Acetone U ug/l 1-0 Benzene 0. U ug/l 0 - Chlorobromomethane 0. U 0.0. ug/l - ichlorobromomethane ug/l - 1 Bromoform 0.1 U 0.0. ug/l 0 - Bromomethane 0. U 0.0. ug/l - 0 -Butanone (MEK). U 00 ug/l - 0 Carbon disulfide ug/l - 0 Carbon tetrachloride ug/l 0 - Chlorobenzene 0.0. ug/l - Chloroethane 0. U 0.0. ug/l 0-0 -Chloroethyl vinyl ether.0 U 0.0. ug/l - 0 Chloroform 0.0 I ug/l 0 - Chloromethane 0. U J ug/l - 1 Chlorodibromomethane 0.0. ug/l - 1 1,-ibromo--Chloropropane 1. U ug/l 1 - Ethylene ibromide 0.0. ug/l - ibromomethane 0. U ug/l 1-1 1,-ichlorobenzene 0.0. ug/l - 1 1,-ichlorobenzene 0. U 0.0. ug/l - 1,-ichlorobenzene 0. U 0.0. ug/l - trans-1,-ichloro--butene 1.0 U J 0.0. ug/l - 1 ichlorodifluoromethane 0. U 0.0. ug/l 1-0 1,1-ichloroethane 0.0. ug/l 1-1 %Rec %Rec %Rec. Limits Client Sample I: MW- Prep Type: Total/NA %Rec. Limits TestAmerica Pensacola Page 1 of /1/01

101 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MS Analysis : Sample Sample Result Qualifier Spike Added MS MS TestAmerica Job I: ,-ichloroethane 0.0. ug/l 0 - cis-1,-ichloroethene 0.0. ug/l - 1 trans-1,-ichloroethene 0.0. ug/l 1-1 1,1-ichloroethene 0.0. ug/l - 1 1,-ichloropropane 0.0. ug/l - 1 cis-1,-ichloropropene 0.0. ug/l - trans-1,-ichloropropene ug/l - 1 Ethylbenzene 0.0. ug/l - -Hexanone.1 U J 00 ug/l - Iodomethane 0.0 U 0.0. ug/l 0-0 Methylene Chloride.0 U ug/l 0 - -Methyl--pentanone (MIBK) 1. U J 00 1 ug/l 1 - Methyl tert-butyl ether 0. U 0.0. ug/l - 1 Styrene 1.0 U 0.0. ug/l 0-1,1,1,-Tetrachloroethane 0. U 0.0. ug/l - 1 1,1,,-Tetrachloroethane ug/l - Tetrachloroethene 0. U ug/l 1-1 Toluene 0.0 U 0.0. ug/l 1-1,1,1-Trichloroethane 0.0. ug/l - 1,1,-Trichloroethane ug/l - Trichloroethene 0.0. ug/l - Trichlorofluoromethane 0. U ug/l - 0 1,,-Trichloropropane 0. U 0.0. ug/l - 1 Vinyl acetate.0 U 0 0. ug/l 0-0 Vinyl chloride 0.0. ug/l - 0 Xylenes, Total 1. U 0. ug/l - %Rec Client Sample I: MW- Prep Type: Total/NA %Rec. Limits Surrogate %Recovery MS MS Qualifier Limits Toluene-d (Surr) 0-0 1,-ichloroethane-d (Surr) - 1 Lab Sample I: MS Analysis : Sample Sample Result Qualifier Spike Added MS MS Client Sample I: MW- Prep Type: Total/NA Acetone U 00 ug/l Benzene 0. U ug/l 1-0 Chlorobromomethane 0. U ug/l ichlorobromomethane 0.0. ug/l Bromoform 0.1 U ug/l Bromomethane 0. U 0.0. ug/l Butanone (MEK). U 00 1 ug/l Carbon disulfide 0.0. ug/l Carbon tetrachloride 0.0. ug/l 0-0 Chlorobenzene 0.0. ug/l - 0 Chloroethane 0. U ug/l Chloroethyl vinyl ether.0 U 0.0. ug/l %Rec %Rec. Limits RP RP Limit TestAmerica Pensacola Page 1 of /1/01

102 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: 0B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample I: MS Analysis : Sample Sample Result Qualifier Spike Added MS MS TestAmerica Job I: Client Sample I: MW- Prep Type: Total/NA Chloroform 0.0 I 0.0. ug/l 0-0 Chloromethane 0. U J 0.0. J ug/l Chlorodibromomethane 0.0. ug/l ,-ibromo--Chloropropane 1. U 0.0. ug/l Ethylene ibromide 0.0. ug/l - 0 ibromomethane 0. U ug/l ,-ichlorobenzene 0.0. ug/l ,-ichlorobenzene 0. U 0.0. ug/l - 0 1,-ichlorobenzene 0. U 0.0. ug/l - 0 trans-1,-ichloro--butene 1.0 U J 0.0. ug/l ichlorodifluoromethane 0. U 0.0. ug/l ,1-ichloroethane 0.0. ug/l ,-ichloroethane ug/l cis-1,-ichloroethene 0.0. ug/l trans-1,-ichloroethene 0.0. ug/l ,1-ichloroethene 0.0. ug/l ,-ichloropropane 0.0. ug/l cis-1,-ichloropropene ug/l trans-1,-ichloropropene 0.0. ug/l Ethylbenzene 0.0. ug/l - 0 -Hexanone.1 U J 00 ug/l - 0 Iodomethane 0.0 U ug/l Methylene Chloride.0 U 0.0. ug/l 0 - -Methyl--pentanone (MIBK) 1. U J 00 1 ug/l - 0 Methyl tert-butyl ether 0. U 0.0. ug/l Styrene 1.0 U ug/l - 0 1,1,1,-Tetrachloroethane 0. U 0.0. ug/l ,1,,-Tetrachloroethane 0.0. ug/l - 0 Tetrachloroethene 0. U 0.0. ug/l Toluene 0.0 U ug/l 1-0 1,1,1-Trichloroethane 0.0. ug/l 0-0 1,1,-Trichloroethane 0.0. ug/l - 0 Trichloroethene ug/l - 0 Trichlorofluoromethane 0. U 0.0. ug/l ,,-Trichloropropane 0. U 0.0. ug/l Vinyl acetate.0 U 0 1 ug/l 1-0 Vinyl chloride ug/l Xylenes, Total 1. U 0.0 ug/l %Rec %Rec. Limits RP RP Limit Surrogate %Recovery MS MS Qualifier Limits Toluene-d (Surr) 0-0 1,-ichloroethane-d (Surr) - 1 TestAmerica Pensacola Page 0 of /1/01

103 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method: Anions, Ion Chromatography Lab Sample I: MB 00-/1 Analysis : MB MB QC Sample Results PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Sulfate 0.0 U mg/l 0//1 1: 1 Chloride Lab Sample I: LCS 00-/1 Analysis : il Fac 0. U mg/l 0//1 1: 1 Spike Added LCS LCS Client Sample I: Lab Control Sample Prep Type: Total/NA Sulfate.0. mg/l 0-0 Chloride.0. mg/l 0-0 Lab Sample I: LCS 00-/ Analysis : Spike Added LCS LCS %Rec %Rec. Limits Client Sample I: Lab Control Sample up Prep Type: Total/NA Sulfate.0. mg/l Chloride.0.0 mg/l Method:.1 - Mercury (CVAA) Lab Sample I: MB 00-/1-A Client Sample I: Method Blank Prep Type: Total/NA Analysis : 1 Prep : MB MB PQL Mercury 0.00 U ug/l /0/1 0: /0/1 1: 1 ML %Rec %Rec. Limits Analyzed RP RP Limit il Fac Lab Sample I: LCS 00-/1-A Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 1 Prep : Spike LCS LCS %Rec. Added Mercury ug/l - 1 Method: 0C - Metals (ICP) Lab Sample I: MB 00-00/1-A Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : 1 Prep : 00 MB MB PQL Boron U 0 ug/l /01/1 : /0/1 1: 1 Strontium ML %Rec Limits Analyzed il Fac 1.0 U ug/l /01/1 : /0/1 1: 1 TestAmerica Pensacola Page 1 of /1/01

104 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method: 0C - Metals (ICP) (Continued) QC Sample Results TestAmerica Job I: Lab Sample I: LCS 00-00/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : 1 Prep : 00 Spike LCS LCS %Rec. Added Boron 00 0 ug/l 0-0 Strontium 00 1 ug/l 0-0 Method: 00 - Metals (ICP/MS) Lab Sample I: MB 00-10/1-A ^ Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : 1 Prep : 10 MB MB PQL Aluminum 1 U 1 ug/l //1 : //1 :0 Arsenic Cadmium Chromium Iron Sodium Lead ML %Rec Limits Analyzed il Fac 0. U ug/l //1 : //1 :0 0. U. 0. ug/l //1 : //1 :0 1.1 U. 1.1 ug/l //1 : //1 :0 U ug/l //1 : //1 :0 0.1 U mg/l //1 : //1 :0 0. U ug/l //1 : //1 :0 Lab Sample I: LCS 00-10/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : 1 Prep : 10 Spike LCS LCS %Rec. Added Aluminum 00 ug/l 0-0 Arsenic 0.0. ug/l 0-0 Cadmium ug/l Chromium 0.0. ug/l 0-0 Iron ug/l 0-0 Sodium.00.0 mg/l Lead ug/l %Rec Limits Lab Sample I: MS Client Sample I: MW- Prep Type: Total Recoverable Analysis : 1 Prep : 10 Sample Sample Spike MS MS %Rec. Added %Rec Limits Aluminum 00 0 ug/l - Arsenic 0. U 0.0. ug/l - Cadmium 0. U ug/l - Chromium 1.1 U 0.0. ug/l - Iron U ug/l 1 - Sodium mg/l 1 - Lead 0. U ug/l - TestAmerica Pensacola Page of /1/01

105 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method: 00 - Metals (ICP/MS) (Continued) QC Sample Results TestAmerica Job I: Lab Sample I: MS Client Sample I: MW- Prep Type: Total Recoverable Analysis : 1 Prep : 10 Sample Sample Spike MS MS %Rec. RP Result Qualifier Added Aluminum 00 ug/l 0-0 Arsenic 0. U ug/l Cadmium 0. U ug/l Chromium 1.1 U 0.0. ug/l Iron U ug/l Sodium mg/l - 0 Lead 0. U ug/l Method: 00 - issolved Metals by ICP-MS Lab Sample I: MB 00-/1-A ^ Client Sample I: Method Blank Prep Type: Total Recoverable Analysis : 1 Prep : MB MB PQL Aluminum, issolved 1 U 1 ug/l /1/1 0: /1/1 :1 Iron, issolved ML %Rec Limits Analyzed RP Limit il Fac U ug/l /1/1 0: /1/1 :1 Lab Sample I: LCS 00-/-A Client Sample I: Lab Control Sample Prep Type: Total Recoverable Analysis : 1 Prep : Spike LCS LCS %Rec. Added Aluminum, issolved 00 0 ug/l 0-0 Iron, issolved ug/l 0-0 %Rec Limits Method: Nitrogen, Ammonia Lab Sample I: MB 00-1/1 Client Sample I: Method Blank Prep Type: Total/NA Analysis : 1 MB MB PQL ML Analyzed il Fac Ammonia (as N) 0.0 U mg/l /01/1 :1 1 Lab Sample I: LCS 00-1/ Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 1 Spike LCS LCS %Rec. Added %Rec Limits Ammonia (as N).00.0 mg/l 0-0 Lab Sample I: MRL 00-1/1 Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 1 Spike MRL MRL %Rec. Added %Rec Limits Ammonia (as N) I mg/l 0-0 TestAmerica Pensacola Page of /1/01

106 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method:. - Nitrogen, Nitrate-Nitrite Lab Sample I: MB 00-/1 Analysis : MB MB QC Sample Results PQL ML TestAmerica Job I: Client Sample I: Method Blank Prep Type: Total/NA Analyzed Nitrate Nitrite as N 0.01 U mg/l /01/1 1: 1 Lab Sample I: LCS 00-/ Analysis : Spike Added LCS LCS il Fac Client Sample I: Lab Control Sample Prep Type: Total/NA Nitrate Nitrite as N mg/l 0-0 Method: SM 0C - Solids, Total issolved (TS) Lab Sample I: MB 00-1/1 Analysis : 1 MB MB PQL ML %Rec %Rec. Limits Client Sample I: Method Blank Prep Type: Total/NA Analyzed Total issolved Solids. U.0. mg/l /0/1 0: 1 Lab Sample I: LCS 00-1/ Analysis : 1 Spike Added LCS LCS il Fac Client Sample I: Lab Control Sample Prep Type: Total/NA Total issolved Solids mg/l - %Rec %Rec. Limits Method: SM 00 NO B - Nitrogen, Nitrite Lab Sample I: MB 00-10/ Client Sample I: Method Blank Prep Type: Total/NA Analysis : 10 MB MB PQL ML Analyzed il Fac Nitrite as N 0.01 U mg/l 0//1 0:1 1 Lab Sample I: LCS 00-10/ Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 10 Spike LCS LCS %Rec. Added %Rec Limits Nitrite as N mg/l 0-0 Lab Sample I: MRL 00-10/1 Client Sample I: Lab Control Sample Prep Type: Total/NA Analysis : 10 Spike MRL MRL %Rec. Added %Rec Limits Nitrite as N mg/l 0-0 TestAmerica Pensacola Page of /1/01

107 Client: Anderson Columbia Company Project/Site: Persimmon Landfill QC Sample Results Method: SM 00 NO B - Nitrogen, Nitrite (Continued) Lab Sample I: MS Analysis : 10 Sample Sample Result Qualifier Spike Added MS MS TestAmerica Job I: Nitrite as N 0.01 U mg/l 0 - Lab Sample I: MS Analysis : 10 Sample Sample Result Qualifier Spike Added MS MS %Rec Client Sample I: MW- Prep Type: Total/NA %Rec. Limits Client Sample I: MW- Prep Type: Total/NA Nitrite as N 0.01 U mg/l 0-0 %Rec %Rec. Limits RP RP Limit TestAmerica Pensacola Page of /1/01

108 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: MW- Lab Sample I: ate Collected: 0//1 : ate Received: 0//1 : Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml /0/1 1: CAR TAL PEN Total/NA Initial Final Number Analysis //1 : JAW TAL PEN Total/NA Prep.1 0 ml 0 ml /0/1 : JAP TAL PEN Total/NA Analysis /0/1 1: JAP TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 00 /01/1 : KWN TAL PEN Total Recoverable Analysis 0C 1 1 /0/1 0: GESP TAL PEN issolved Prep 00A 0 ml 0 ml /1/1 0: RE TAL PEN issolved Analysis 00 1 /1/1 : RE TAL PEN Total Recoverable Prep 00A 0 ml 0 ml 10 //1 : RE TAL PEN Total Recoverable Analysis 00 1 //1 : RE TAL PEN Total/NA Analysis ml ml 1 /01/1 : KJR TAL PEN Total/NA Analysis. 1 ml ml /01/1 1: KJR TAL PEN Total/NA Analysis Nitrate by calc 1 1 0//1 0:1 RRC TAL PEN Total/NA Analysis SM 0C 1 0 ml 0 ml 1 /0/1 0: CLB TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 10 0//1 0:1 BAB TAL PEN Total/NA Analysis Field Sampling 1 1 0//1 : FS TAL PEN Client Sample I: T Blank Lab Sample I: 00-- ate Collected: 0//1 00:00 ate Received: 0//1 : Lab il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 0B 1 ml ml /0/1 :1 CAR TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-/1 ate Collected: N/A ate Received: N/A Prep Type Total/NA il Initial Final Type Method Run Factor Number or Analyzed Analyst Lab Analysis //1 1: JAW TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-10/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis SM 00 NO B 1 ml ml 10 0//1 0:1 BAB TAL PEN Initial Final Number Lab TestAmerica Pensacola Page of /1/01

109 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Method Blank Lab Sample I: MB 00-1/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis ml ml 1 /01/1 :1 KJR TAL PEN Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Initial Final Number Lab Lab Sample I: MB 00-00/1-A or Analyzed Analyst Total Recoverable Prep 00A 0 ml 0 ml 00 /01/1 : KWN TAL PEN Total Recoverable Initial Final Number Analysis 0C 1 1 /0/1 1: GESP TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis. 1 ml ml /01/1 1: KJR TAL PEN Initial Final Number Client Sample I: Method Blank Lab Sample I: MB 00-/ ate Collected: N/A ate Received: N/A Lab Lab il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 0B 1 ml ml /0/1 : CAR TAL PEN Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Lab Sample I: MB 00-/1-A il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep.1 0 ml 0 ml /0/1 0: JAP TAL PEN Total/NA Analysis /0/1 1: JAP TAL PEN Client Sample I: Method Blank Lab Sample I: MB 00-1/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis SM 0C 1 0 ml 0 ml 1 /0/1 0: CLB TAL PEN Initial Final Number Lab TestAmerica Pensacola Page of /1/01

110 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Lab Sample I: MB 00-10/1-A ^ or Analyzed Analyst Total Recoverable Prep 00A 0 ml 0 ml 10 //1 : RE TAL PEN Total Recoverable Initial Final Number Analysis 00 1 //1 :0 RE TAL PEN Client Sample I: Method Blank ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Lab Lab Sample I: MB 00-/1-A ^ or Analyzed Analyst Total Recoverable Prep 00A 0 ml 0 ml /1/1 0: RE TAL PEN Total Recoverable Initial Final Number Analysis 00 1 /1/1 :1 RE TAL PEN Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/1 ate Collected: N/A ate Received: N/A Prep Type Total/NA Type Method Run il Factor Initial or Analyzed Analyst Analysis //1 1: JAW TAL PEN Final Number Client Sample I: Lab Control Sample Lab Sample I: LCS 00-10/ ate Collected: N/A ate Received: N/A Lab Lab il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis SM 00 NO B 1 ml ml 10 0//1 0:1 BAB TAL PEN Client Sample I: Lab Control Sample Lab Sample I: LCS 00-1/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis ml ml 1 /01/1 : KJR TAL PEN Initial Final Number Lab Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Lab Sample I: LCS 00-00/-A il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total Recoverable Prep 00A 0 ml 0 ml 00 /01/1 : KWN TAL PEN Total Recoverable Analysis 0C 1 1 /0/1 1: GESP TAL PEN TestAmerica Pensacola Page of /1/01

111 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis. 1 ml ml /01/1 1: KJR TAL PEN Initial Final Number Client Sample I: Lab Control Sample Lab Sample I: LCS 00-/0 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml /0/1 : CAR TAL PEN Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor Initial Final Number Lab Lab Lab Sample I: LCS 00-/1-A or Analyzed Analyst Total/NA Prep.1 0 ml 0 ml /0/1 0: JAP TAL PEN Total/NA Initial Final Number Analysis /0/1 1: JAP TAL PEN Client Sample I: Lab Control Sample Lab Sample I: LCS 00-1/ ate Collected: N/A ate Received: N/A Lab il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis SM 0C 1 0 ml 0 ml 1 /0/1 0: CLB TAL PEN Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Lab Sample I: LCS 00-10/-A il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total Recoverable Prep 00A 0 ml 0 ml 10 //1 : RE TAL PEN Total Recoverable Analysis //1 : RE TAL PEN Client Sample I: Lab Control Sample ate Collected: N/A ate Received: N/A Lab Sample I: LCS 00-/-A il Initial Final Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total Recoverable Prep 00A 0 ml 0 ml /1/1 0: RE TAL PEN Total Recoverable Analysis /1/1 : RE TAL PEN TestAmerica Pensacola Page of /1/01

112 Lab Chronicle Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Client Sample I: Lab Control Sample up Lab Sample I: LCS 00-/ ate Collected: N/A ate Received: N/A Prep Type Total/NA Type Method Run il Factor Initial or Analyzed Analyst Analysis //1 1: JAW TAL PEN Final Number Client Sample I: Lab Control Sample Lab Sample I: MRL 00-10/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis SM 00 NO B 1 ml ml 10 0//1 0:1 BAB TAL PEN Initial Final Number Client Sample I: Lab Control Sample Lab Sample I: MRL 00-1/1 ate Collected: N/A ate Received: N/A Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis ml ml 1 /01/1 : KJR TAL PEN Client Sample I: MW- ate Collected: 0//1 : ate Received: 0//1 : Prep Type Type Method Run il Factor Initial Final Number Lab Lab Lab Lab Sample I: MS or Analyzed Analyst Total/NA Analysis 0B 1 ml ml /0/1 1:0 CAR TAL PEN Initial Final Number Total Recoverable Prep 00A 0 ml 0 ml 10 //1 : RE TAL PEN Total Recoverable Analysis 00 1 //1 : RE TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 10 0//1 0:1 BAB TAL PEN Lab Client Sample I: MW- ate Collected: 0//1 : ate Received: 0//1 : Lab Sample I: MS Prep Type Type Method Run il Factor or Analyzed Analyst Total/NA Analysis 0B 1 ml ml /0/1 1: CAR TAL PEN Initial Final Number Total Recoverable Prep 00A 0 ml 0 ml 10 //1 : RE TAL PEN Total Recoverable Analysis 00 1 //1 :1 RE TAL PEN Total/NA Analysis SM 00 NO B 1 ml ml 10 0//1 0:1 BAB TAL PEN Lab Laboratory References: BMEA = Benchmark EnviroAnalytical, Inc., 1 th St E., Palmetto, FL 1, TEL (1)- TAL PEN = TestAmerica Pensacola, McLemore rive, Pensacola, FL 1, TEL (0)-01 TestAmerica Pensacola Page 0 of /1/01

113 Client: Anderson Columbia Company Project/Site: Persimmon Landfill Method Summary TestAmerica Job I: Method Method escription Protocol Laboratory 0B Volatile Organic Compounds (GC/MS) SW TAL PEN 00.0 Anions, Ion Chromatography MCAWW TAL PEN.1 Mercury (CVAA) EPA TAL PEN 0C Metals (ICP) SW TAL PEN 00 issolved Metals by ICP-MS SW TAL PEN 00 Metals (ICP/MS) SW TAL PEN 0.1 Nitrogen, Ammonia MCAWW TAL PEN. Nitrogen, Nitrate-Nitrite MCAWW TAL PEN Nitrate by calc Nitrogen, Nitrate SM TAL PEN SM 0C Solids, Total issolved (TS) SM TAL PEN SM 00 NO B Nitrogen, Nitrite SM TAL PEN Field Sampling Field Sampling EPA TAL PEN Subcontract SM00S-Sulfide/SM00SH-HS,Unionized None BMEA.1 Preparation, Mercury EPA TAL PEN 00A Preparation, Total Recoverable or issolved Metals SW TAL PEN 00B Purge and Trap SW TAL PEN Protocol References: EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-00/--00, March 1 And Subsequent Revisions. None = None SM = "Standard Methods For The Examination Of Water And Wastewater" SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1 And Its Updates. Laboratory References: BMEA = Benchmark EnviroAnalytical, Inc., 1 th St E., Palmetto, FL 1, TEL (1)- TAL PEN = TestAmerica Pensacola, McLemore rive, Pensacola, FL 1, TEL (0) TestAmerica Pensacola Page 1 of /1/01

114 Accreditation/Certification Summary Client: Anderson Columbia Company TestAmerica Job I: Project/Site: Persimmon Landfill Laboratory: TestAmerica Pensacola Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program EPA Region Identification Number Expiration ate Florida NELAP E The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Field Sampling Water Color Field Sampling Water Field ph Field Sampling Water Field Temperature Field Sampling Water Odor Field Sampling Water Oxidation Reduction Potential Field Sampling Water Oxygen, issolved Field Sampling Water Specific Conductance Field Sampling Water Turbidity Nitrate by calc Water Nitrate as N TestAmerica Pensacola Page of /1/01

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