TEST REPORT Facility: CAPPIO TESSUTI Country: ITALY Address: VIA PIAVE 44-46, FAGNANO OLONA (VA) Date of report: 29/07/2016
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1 TEST REPORT Facility: CAPPIO TESSUTI Country: ITALY Address: VIA PIAVE 44-46, FAGNANO OLONA (VA) Date of report: 29/07/2016 INTRODUCTION Benetton Group has a relevant experience of environmentally responsible business practices and is putting significant resources and passion on its environmental program with the objective to minimize the impact of all its activities and preserve the natural resources for present and future generations. Benetton Group Restricted Substances List (RSL) contains the complete list of banned or restricted chemical substances. In line with the Company s commitment to zero discharges of hazardous substances by 2020, chemical investigations are regularly conducted by independent external auditors considering the following groups of hazardous chemical substances and using the lowest detection limits currently available with the best in class chemical laboratories around the world: PRIORITY CHEMICAL GROUPS 1. Alkylphenols 2. Phthalates 3. Brominated and chlorinated flame retardants 4. Azo dyes 5. Organotin compounds 6. Perfluorinated chemicals 7. Chlorobenzenes 8. Chlorinated solvents 9. Chlorophenols 10. Short chain chlorinated paraffins 11. Heavy metals such as cadmium, lead, mercury and chromium (VI). 12. Cyanide The findings are meant to highlight the current level of use (at times also unintentional) of the above chemical groups through a comparison of the incoming, UNTREATED wastewaters (i.e. samples are collected upstream of any wastewaters treatment plant) and treated wastewater (if there is. i.e. samples are collected downstream of self-owned Effluent Treatment Plant). The comparison is in fact a valuable tool to identify if and in which formulations, used by the Page 1 of 11
2 facility, the above chemical groups might be contained, helping to subsequently identify potential alternatives of assessed lower impact. For every specific situation an action plan is designed and a monitoring procedure is put in place to avoid non viable substitutions. Page 2 of 11
3 Facility details and analysis results Facility Name: CAPPIO TESSUTI Address: VIA PIAVE 44,46 FAGNANO OLONA (VA) Activity: Dyeing Sample Description: Three(3)Samples: (1)Transparent Liquid, Incoming Water, Tap Water, Collected During Operating Hours on Jul. 12, 2016; (2)Dark Blue Liquid, Wastewater before treatment, Collected During Operating Hours on Jul. 12, 2016; (3)Transparent (with solids) Liquid, Wastewater after treatment, Collected During Operating Hours on Jul The water samples were collected and tested by PH SRL. SUMMARY Test Items Result (3) Azodyes (Banned Aromatic Amines) - - Chlorinated Solvents Phthalates - - Brominated and Chlorinated Flame - - Retardants Organic Tin Compounds - - Chlorophenols - - Short-Chain Chlorinated Paraffins (C C 13) Heavy Metals Alkylphenol - ethoxylates/alkylphenols(apeos/aps) Perfluorinated Chemicals (PFCs) - - Chlorinated Benzenes - - Cyanide - - Note/ Key Detected Not Detected - Not Tested Page 3 of 11
4 1 Detection Of Amines Derived From Azocolourants And Azodyes With Reference To MPC EN 14362:1&3, By Gas Chromatographic - Mass Spectrometric (GC-MS) And High Performance Liquid Chromatographic - Diode Array Detector(HPLC-DAD) Analysis. Compound(s) Cas No. Result (µg/l) 1,4-Phenylenediamine N.D. 2,4,5-Trimethylaniline N.D. 2,4-Diaminoanisole N.D. 2,4-Diaminotoluene N.D. 2,4-Xylidine N.D. 2,6-Xylidine N.D. 2-Chloroaniline N.D. 2-Naphthylamine N.D. 3,3'-Dichlorobenzidine N.D. 3,3'-Dimethoxybenzidine N.D. 3,3'-Dimethyl-4,4'-diaminodiphenylmethane N.D. 3,3'-Dimethylbenzidine N.D. 4,4'-Diaminodiphenylmethane N.D. 4,4'-Methylene-bis(2-chloroaniline) N.D. 4,4'-Oxydianiline N.D. 4,4'-Thiodianiline N.D. 4-Aminobiphenyl N.D. 4-Chloroaniline N.D. 4-Chloro-o-toluidine N.D. 5-Nitro-o-anisidine N.D. 5-Nitro-o-toluidine N.D. 4-Aminoazobenzene N.D. Aniline N.D. Benzidine N.D. m-toluidine N.D. n,n-diethylanaline N.D. n-ethylaniline N.D. n-methylaniline N.D. o-aminoazotoluene N.D. o-anisidine N.D. o-toluidine N.D. p-cresidine N.D. p-toluidine N.D. Remark: ND= Not detected Detection limit = 0.1µg/L Page 4 of 11
5 2 Chlorinated Solvents By Headspace Gas Chromatography Mass Spectrometric (HS-GC/MS) Analysis. Compound(s) Cas No. Result (µg/l) Detection Limit (3) (µg/l) Carbon tetrachloride N.D. N.D. N.D Pentachloroethane N.D. N.D. N.D ,1,1-trichloroethane N.D. N.D ,1,1,2-tetrachloroethane N.D. N.D. N.D ,1,2,2-tetrachloroethane N.D. N.D. N.D Chloroform N.D ,1,2-trichloroethane N.D. N.D. N.D ,1-dichloroethylene N.D. N.D. N.D Trichloroethylene N.D. N.D Tetrachloroethylene N.D. N.D ,2-dichloroethane N.D. N.D. N.D Dichloromethane N.D. N.D. N.D Remark: ND= Not detected Page 5 of 11
6 3 Phthalates Solvent Extraction And By Gas Chromatography-Mass Spectrometry (GC-MS) Analysis. Compound(s) Cas No. Result (µg/l) Di-iso-butyl-phthalate(DIBP) N.D. Di-butyl-phthalate(DBP) N.D. Benzyl-butyl-phthalate(BBP) N.D. Di-(2-ethyl-hexyl)-phthalate(DEHP) N.D. Di-n-octyl-phthalate(DNOP) N.D. Di-iso-nonyl-phthalate(DINP) N.D. Di-iso-decyl-phthalate(DIDP) N.D. Di-methyl-phthalate(DMP) N.D. Di-ethyl-phthalate(DEP) N.D. Di-n-propyl-phthalate(DPrP / DPP) N.D. Di-iso-pentyl-phthalate(DIPP) N.D. Di-n-hexyl-phthalate(DNHP) N.D. Di-cyclo-hexyl-phthalate(DCHP) N.D. Di-iso-heptyl-phthalate(DIHP) N.D. Di-iso-octyl-phthalate(DIOP) N.D. Di-nonyl-phthalate(DNP) N.D. Bis-(2-methoxy-ethyl)-phthalate(DMEP) N.D. 1,2-Benzene-di-carboxylic acid di-pentyl-esters, branched and linear N.D. N-iso-pentyl-iso-pentyl-phthalate(PIPP) N.D. 1,2-Benzene-di-carboxylic acid, di-c 7, 11-branched and linear alkyl esters(dhnup) N.D. Remark: ND= Not detected Detection limit = 1µg/L Page 6 of 11
7 4 Brominated And Chlorinated Flame Retardants Solvent Extraction And By Liquid Chromatography - Mass Spectrometry (LC-MS) And Gas Chromatography - Mass Spectrometry (GC-MS) Analysis. Compound(s) Cas No. Result (µg/l) Detection Limit (µg/l) Polybrominated Biphenyles(PBBs) various Bromo-biphenyl - N.D Di-bromo-biphenyl - N.D Tri-bromo-biphenyl - N.D Tetra-bromo-biphenyl - N.D Penta-bromo-biphenyl - N.D Hexa-bromo-biphenyl - N.D Hepta-bromo-biphenyl - N.D Octa-bromo-biphenyl - N.D Nona-bromo-biphenyl - N.D Deca-bromo-biphenyl N.D Polybrominated Diphenyl ethers(pbdes) various N.D. Bromo-diphenyl-ether - N.D Di-bromo-diphenyl-ether - N.D Tri-bromo-diphenyl-ether - N.D Tetra-bromo-diphenyl-ether - N.D Penta-bromo-diphenyl-ether - N.D Hexa-bromo-diphenyl-ether - N.D Hepta-bromo-diphenyl-ether - N.D Octa-bromo-diphenyl-ether - N.D Nona-bromo-diphenyl-ether - N.D Deca-bromo-diphenyl-ether N.D Hexa-bromo-cyclo-dodecan(HBCDD) N.D. 0.5 Tri-(2,3-di-bromo-propyl)-phosphate(TRIS) N.D. 0.5 Tetra-bromo-bisphenol-A(TBBPA) N.D. 0.5 Tetra-bromo-bisphenol A bis-(d-ibromopropyl-ether)(tbbpa-bdpe) N.D. 0.5 Bis-(2,3-di-bromo-propyl)-phosphate N.D. 0.5 Tris-(2-chloro-ethyl)-phosphate(TCEP) N.D Tris-(1,3-di-chloro-iso-propyl)- phosphate(tdcpp) N.D Tris-(2-chloroisopropyl)-phosphate(TCPP) N.D. 0.5 Remark: ND= Not detected Page 7 of 11
8 5 Organic Tin Compounds With Reference To US EPA , By Gas Chromatography-Mass Spectrometry (GC-MS) Analysis. Compound(s) Result (µg/l) Detection Limit (µg/l) Monobutyltin (MBT) N.D Dibutyltin (DBT) N.D Tributyltin (TBT) N.D Triphenyltin (TPhT) N.D Dioctyltin (DOT) N.D Monooctyltin (MOT) N.D Tetrabutyltin (TeBT) N.D Trioctyltin(TriOT) N.D Tricyclohexyltin(TCyHT) N.D Tripropyltin (TPT) N.D Remark: ND= Not Detected 6 Chlorophenols Solvent Extraction And Acetylated By Acetic Anhydride, And Analyzed By Gas Chromatography-Mass Spectrometry (GC-MS). Compound(s) Cas No. Result (µg/l) Pentachlorophenol (PCP) N.D. Tetrachlorophenols (TeCP) N.D. Trichlorophenols (TriCP) Various N.D. Dichlorophenol (DiCP) Various N.D. Monochlorophenol Various N.D. Remark: ND = Not detected Detection limit = 0.5µg/L Page 8 of 11
9 7 Short-Chain Chlorinated Paraffins (C 10-C 13) Solvent Extraction And By Liquid Chromatography - Mass Spectrometry (LC-MS) Analysis. Compound(s) Cas No. Result (µg/l) Short-chain chlorinated paraffins (C 10-C 13) N.D. Remark: ND = Not detected Detection limit = 90 µg/l 8 Heavy Metals By Inductively Coupled Argon Plasma-Mass Spectrometry(ICP-MS) Analysis And By Ion Chromatography- Inductively Coupled Argon Plasma-Mass Spectrometry(IC-ICP-MS) Analysis. Compound(s) CAS No. Result (µg/l) Detection Limit (µg/l) (3) Total Cadmium(Cd) N.D Total Lead(Pb) Total Mercury(Hg) N.D. N.D. N.D Total Hexavalent Chromium(Cr-VI) Total Arsenic (As) Total Antimony (Sb) N.D. N.D Total Cobalt (Co) N.D Total Nickel (Ni) Total Copper (Cu) Total Zinc (Zn) Total Manganese (Mn) N.D Total Chromium (Cr) Remark: ND = Not detected 9 Alkylphenol ethoxylates/alkylphenols(apeos/aps) Solvent Extraction And By Gas Chromatography-Mass Spectrometry (GC-MS) And By Liquid Chromatography-Mass Spectrometry (LC-MS/MS) Analysis. Compound(s) Cas No. Result (µg/l) Detection Limit (µg/l) Nonylphenols N.D Octylphenols N.D. 6 Nonylphenolethoxylates N.D. 2 Octylphenolethoxylates N.D. 2 Nonylphenolethoxylates N.D. 2 Octylphenolethoxylates N.D. 2 Remark: ND = Not detected Page 9 of 11
10 10 Perfluorinated Chemicals (PFCs) By Liquid Chromatography Mass Spectrometry (LC-MS/MS) Analysis. Compound(s) Cas No. Result (µg/l) Detection Limit (µg/l) Perfluorooctane sulphonates (PFOS) N.D Perfluoro-octane-sulfon- amide(pfosa) N.D N-Methyl-Perfluoro-octane-sulfon-amide(N-Me- N.D FOSA) N-Ethyl-Perfluoro-octane-sulfon-amide(N-Et- N.D FOSA) N-Methyl-Perfluoro-octane-sulfon-amidoethanol(N-Me-FOSE alcohol) N.D N-Ethyl-Perfluoro-octane-sulfon-amido-ethanol(N- N.D Et-FOSE alcohol) Perfluoro-octane acid N.D Perfluoro-butanoic acid N.D Perfluoro-pentanoic acid N.D Perfluoro-hexanoic acid N.D Perfluoro-heptanoic acid N.D Perfluoro-nonanoic acid N.D Perfluoro-decanoic acid N.D Perfluoro-undecanoic acid N.D. 0.5 Perfluoro-dodecanoic acid N.D. 0.5 Perfluoro-tridecanoic acid N.D. 0.5 Perfluoro-tetradecanoic acid N.D. 0.5 Perfluoro-butane-sulfonic acid N.D / N.D Perfluoro-hexane-sulfonic acid Perfluoro-heptane-sulfonic acid N.D. 0.5 Perfluor-decane-sulfonic acid N.D H,1H,2H,2H-Perfluoro-octane-sulphonic acid N.D H,2H,3H,3H-Perfluoro-undecanoic acid N.D Perfluoro-3-7-dimethyl octane carboxylate N.D H-Dodecafluoro heptane carboxylate N.D Remark: ND = Not detected Page 10 of 11
11 11 Chlorinated Benzenes Solvent Extraction And Followed By Gas Chromatography-Mass Spectrometry (GC-MS) Analysis. Compound(s) Detection Limit Cas No. Result(µg/L) (µg/l) Dichlorobenzene various N.D Trichlorobenzenes various N.D Tetrachlorobenzenes various N.D Pentachlorobenzenes N.D Hexachlorobenes N.D Chlorobenzene N.D Remark: ND = Not detected 12 Cyanide EPA 9014 with IC. Compound(s) Cyanide Result(ug/L) (3) N.D. Remarks: Detection limit = 1 ug/l ND = Not detected Testing Period: Jun. 21, 2015 To Jul. 04, 2015 End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. PH SRL does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing PH SRL's provision of services to you. PH SRL makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. Page 11 of 11
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