Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 2 of 20 Test Result(s) PART NAME No.1 : GOLDEN COLORED METAL WIRE Cadmium (Cd) Lead (Pb) Merc
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1 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 1 of 20 The following sample(s) was/were submitted and identified by/on behalf of the applicant as : Sample Submitted By Sample Description Style/Item No. Sample Receiving Date Testing Period : : : : : GOLD WIRE 4N 2014/10/ /10/15 TO 2014/10/22 ============================================================================================ Test Result(s) : Please refer to next page(s). Conclusion : Based on the performed tests on submitted samples, the test results of Cadmium, Lead, Mercury, Hexavalent Chromium Cr(VI), PBBs and PBDEs comply with the limits as set by RoHS Directive 2011/65/EU Annex II; recasting 2002/95/EC.
2 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 2 of 20 Test Result(s) PART NAME No.1 : GOLDEN COLORED METAL WIRE Cadmium (Cd) Lead (Pb) Mercury (Hg) Hexavalent Chromium Cr(VI) Phosphorus (P) Antimony (Sb) Beryllium (Be) PVC Test Item(s) Polychlorinated Biphenyls (PCBs) (CAS No.: ) Polychlorinated Naphthalene (PCNs) Polychlorinated Terphenyls (PCTs) Unit mg/kg With reference to IEC : 2013 and performed by ICP-AES. mg/kg With reference to IEC : 2013 and performed by ICP-AES. mg/kg With reference to IEC : 2013 and performed by ICP-AES. ** With reference to IEC 62321: 2008 and performed by Boiling water extraction Method.# mg/kg mg/kg mg/kg mg/kg With reference to IEC 62321: 2008 and performed by UV-VIS. With reference to US EPA Method 3050B. Analysis was performed by ICP-AES. With reference to US EPA Method 3050B. Analysis was performed by ICP-AES. With reference to US EPA Method 3050B. Analysis was performed by ICP-AES. ** Analysis was performed by FTIR and FLAME Test. mg/kg mg/kg mg/kg Method With reference to US EPA 3540C method. Analysis was performed by GC/MS. With reference to US EPA 3540C method. Analysis was performed by GC/MS. With reference to US EPA 3540C method. Analysis was performed by GC/MS. MDL Result No.1 Limit 2 n.d n.d n.d # Negative # 2 n.d. - 2 n.d. - 2 n.d Negative n.d. - 5 n.d n.d. -
3 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 3 of 20 Test Item(s) Alkanes, C10-13, chloro (Short Chain Chlorinated Paraffins) (CAS No.: ) Perfluorooctane sulfonates (PFOS-Acid, Metal Salt, Amide) PFOA (CAS No.: ) Hexabromocyclododecane (HBCDD) and all major diastereoisomers identified (α- HBCDD, β- HBCDD, γ- HBCDD) (CAS No.: and ( , , )) Medium-Chained Chlorinated Paraffins (C14-C17) (MCCP) (CAS No.: ) Sulfur Hexafluoride (SF6) (CAS No.: ) DEHP (Di- (2-ethylhexyl) phthalate) (CAS No.: ) DBP (Dibutyl phthalate) (CAS No.: ) BBP (Butyl Benzyl phthalate) (CAS No.: ) DIBP (Di-isobutyl phthalate) (CAS No.: ) DNOP (Di-n-octyl phthalate) (CAS No.: ) DINP (Di-isononyl phthalate) (CAS No.: ; ) DIDP (Di-isodecyl phthalate) (CAS No.: ; ) DNHP (Di-n-hexyl phthalate) (CAS No.: ) Unit Method MDL Result No.1 Limit mg/kg With reference to US EPA 3540C method. Analysis was performed by GC/MS. 100 n.d. - mg/kg With reference to US EPA 3550C: Analysis was performed by LC/MS. mg/kg With reference to US EPA 3550C: Analysis was performed by LC/MS. mg/kg With reference to IEC 62321: 2008 method. Analysis was performed by GC/MS. mg/kg With reference to US EPA 3540C & 8270D method. Analysis was performed by GC/MS. mg/kg With reference to US EPA 5021 method. Analysis was performed by % With reference to EN Analysis % With reference to EN Analysis % With reference to EN Analysis % With reference to EN Analysis % With reference to EN Analysis % With reference to EN Analysis % With reference to EN Analysis % With reference to EN Analysis 10 n.d n.d. - 5 n.d n.d. - 1 n.d n.d n.d n.d n.d n.d n.d n.d n.d. -
4 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 4 of 20 Test Item(s) Unit Method MDL Result No.1 Limit % With reference to EN Analysis 0.01 n.d. - DIHP (1,2-Benzenedicarboxylic acid, di-c6-8-branched alkyl esters, C7-rich) (CAS No.: ) DHNUP (1,2-Benzenedicarboxylic acid, di-c7-11-branched and linear alkyl esters) (CAS No.: ) DMEP (Bis (2-methoxyethyl) phthalate) (CAS No.: ) Sum of PBBs Monobromobiphenyl Dibromobiphenyl Tribromobiphenyl Tetrabromobiphenyl Pentabromobiphenyl Hexabromobiphenyl Heptabromobiphenyl Octabromobiphenyl Nonabromobiphenyl Decabromobiphenyl Sum of PBDEs Monobromodiphenyl ether Dibromodiphenyl ether Tribromodiphenyl ether Tetrabromodiphenyl ether Pentabromodiphenyl ether Hexabromodiphenyl ether Heptabromodiphenyl ether Octabromodiphenyl ether Nonabromodiphenyl ether Decabromodiphenyl ether % With reference to EN Analysis % With reference to EN Analysis 0.01 n.d n.d. - mg/kg - n.d mg/kg With reference to IEC 62321: 2008 and 5 n.d. - mg/kg performed by GC/MS. - n.d. 1000
5 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 5 of 20 Result Test Item(s) Unit Method MDL Limit No.1 Organic-tin compounds Tributyl Tin (TBT) Triphenyl Tin (TphT) Dibutyl Tin (DBT) Dioctyl Tin (DOT) Tributyl Tin Oxide (TBTO)*** (CAS No.: ) Halogen Halogen-Fluorine (F) (CAS No.: ) Halogen-Chlorine (Cl) (CAS No.: ) Halogen-Bromine (Br) (CAS No.: ) Halogen-Iodine (I) (CAS No.: ) mg/kg 0.03 n.d. - mg/kg 0.03 n.d. - mg/kg With reference to ISO Analysis 0.03 n.d. - mg/kg was performed by GC/FPD n.d. - mg/kg - n.d. - mg/kg With reference to BS EN 14582:2007. Analysis was performed by IC. mg/kg With reference to BS EN 14582:2007. Analysis was performed by IC. mg/kg With reference to BS EN 14582:2007. Analysis was performed by IC. mg/kg With reference to BS EN 14582:2007. Analysis was performed by IC. 50 n.d n.d n.d n.d. - Note: 1. mg/kg = ppm;0.1wt% = 1000ppm 2. n.d. = Not Detected 3. MDL = Method Detection Limit 4. " - " = Not Regulated 5. ** = Qualitative analysis (No Unit) 6. Negative = Undetectable / Positive = Detectable 7. # = a. Positive means the presence of CrVI on the tested areas b. Negative means the absence of CrVI on the tested areas The detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm² tested areas. 8. ***: The substance was calculated by the test result of Tributyl Tin. The MDL was evaluated for Tributyl Tin. 9. Parameter Conversion Table:Please refer to PFOS Reference Information : POPs - (EU) 757/2010 Outlawing PFOS as substances or preparations in concentrations above 0.001% (10ppm), in semi-finished products or articles or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1µg/m².
6 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 6 of 20 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr 6+ test method excluded) 2) Name of the person who made measurement: Climbgreat Yang 3) Name of the person in charge of measurement: Troy Chang Cutting / Preparation Sample Measurement Pb Cd Acid digestion by suitable acid depended on different sample material (as below table) Hg Microwave digestion with HNO 3 /HCl/HF Cr 6+ (Note**) Add appropriate amount of digestion reagent Filtration Solution ICP-AES Sample Material Residue 1) Alkali Fusion 2) HCl to dissolve Digestion Acid Heat to appropriate temperature to extract Cool, filter digestate through filter Add diphenyl-carbazide for color development Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2 O 2 Glass Gold, platinum, palladium, ceramic HNO 3 /HF Aqua regia Silver HNO 3 Plastic Others H 2 SO 4, H 2 O 2, HNO 3, HCl Added appropriate reagent to total digestion measure the absorbance at 540 nm by UV-VIS Note** (For IEC 62321) (1) For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2) For metallic material, add pure water and heat to boiling.
7 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 7 of 20 1) These samples were dissolved totally by pre-conditioning method according to below flow chart. 2) Name of the person who made measurement: Climbgreat Yang 3) Name of the person in charge of measurement: Troy Chang Flow Chart of digestion for the elements analysis performed by ICP-AES Cutting / Preparation Sample Measurement Acid digestion by suitable acid depended on different sample material (as below table) Filtration Solution Residue 1) Alkali Fusion 2) HCl to dissolve ICP-AES Steel, copper, aluminum, solder Aqua regia, HNO 3, HCl, HF, H 2 O 2 Glass Gold, platinum, palladium, ceramic HNO 3 /HF Aqua regia Silver HNO 3 Plastic Others H 2 SO 4, H 2 O 2, HNO 3, HCl Added appropriate reagent to total digestion
8 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 8 of 20 HBCDD analytical flow chart Name of the person who made measurement: Roman Wong Sample pretreatment Sample extraction / Ultrasonic method Concentrate/Dilute Extracted solution Filter Analysis was performed by GC/MS Data
9 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 9 of 20 Analytical flow chart of phthalate content Name of the person who made measurement: Roman Wong Sample pretreatment/separation Sample extraction by soxhlet method Concentrate/Dilute Extracted solution Analysis was performed by GC/MS Data
10 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 10 of 20 Analysis flow chart for determination of PVC in material Name of the person who made measurement: Roy Lin Sample pre-treatment Flame test Sample analyzed by FTIR Check wave-number of C-Cl bonding Data
11 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 11 of 20 PFOA/PFOS analytical flow chart of Ultrasonic extraction (LC/MS) procedure Name of the person who made measurement: Roman Wong Sample pretreatment Sample extraction by Ultrasonic extraction (Reference method: US EPA 3550C) Concentrate/Dilute Extracted solution Analysis was performed by LC/MS Data
12 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 12 of 20 Analytical flow chart of halogen content Name of the person who made measurement: Rita Chen Sample pretreatment / Separation Weighting and putting sample in cell Oxygen Bomb Combustion / Absorption Dilution to fixed volume Analysis was performed by IC
13 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 13 of 20 Analytical flow chart of Organic-Tin content Name of the person who made measurement: Roy Lin Sample pretreatment Sample extraction by organic solvent Derived by Sodium tetraethylborate Concentrate/Dilute Extracted solution Analysis was performed by GC/FPD Data
14 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 14 of 20 Chlorinated Paraffins analytical flow chart Name of the person who made measurement: Barry Tseng Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the extracted solution Analysis was performed by GC/MS Data
15 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 15 of 20 PCTs analytical flow chart Name of the person who made measurement: Barry Tseng Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the extracted solution Analysis was performed by GC/MS Data
16 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 16 of 20 PCNs analytical flow chart Name of the person who made measurement: Barry Tseng Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the extracted solution Analysis was performed by GC/MS Data
17 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 17 of 20 PCBs analytical flow chart Name of the person who made measurement: Barry Tseng Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute the extracted solution Analysis was performed by GC/MS Data
18 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 18 of 20 PBB/PBDE analytical FLOW CHART Name of the person who made measurement: Roman Wong First testing process Optional screen process Confirmation process Sample Sample pretreatment Screen analysis Sample extraction/ Soxhlet method Concentrate/Dilute Extracted solution Filter Analysis by GC/MS Issue Report
19 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 19 of 20 Analytical flow chart of volatile organic compounds (VOCs) Name of the person who made measurement:chun Wu Name of the person in charge of measurement:shinjyh Chen Reference method:us EPA 5021 Sample pretreatment Take sample and put it into headspace glassware and seal. Bake the sample in the oven Emitted gas was performed by GC/MS Data
20 Test Report No. : CE/2014/A2569 Date : 2014/10/22 Page : 20 of 20 * The tested sample / part is marked by an arrow if it's shown on the photo. * ** End of Report **
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