Tüver Boya Kimya Tekstil San. Tic. Ltd. Şti.

Transcription

1 Form LG.044/Rev:0.0 TEST REORT REORT NUMBER : ALICANT NAME : TURA Tüver Boya Kimya Tekstil San. Tic. Ltd. Şti. ADDRESS : İkitelli Organize San. Böl. Çevre San. Sit. 10. Blok No:6 İkitelli İstanbul / TÜRKİYE TEL: FAX: Attention : Sami Eskinazi ( sami@tuverboya.com ) SAMLE DESCRITION : One sample of White printed ink knitted fabric DATE IN : 25 April,2014 ( 15:05) DATE OUT : 2 May,2014 BUYER'S NAME : COLOUR : UMA AQUA WHITE SAMLE TEST 1 AEO Test Detection of Amines Derived From Azocolourants and Azodyes Determination of Free and Hydrolised Formaldehyde Test (Water extraction method) F Heavy Metals Analysis for print age 1 of 5 = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT ERFORMED / NA = NOT ALICABLE / LS = LACK OF SAMLE / NC = NO COMMENT / I = INCONCLUSIVE The test results relate only to the items tested. The whole and/or the part of this test report shall not be reproduced and shall not be shared with third parties, nor to be used for R activities without the written permission of INTERTEK Test Hizmetleri A.S. The reported uncertainty is based on a standard uncertainty multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainty evaluation has been carried out in accordance with ISO/IEC and TÜRKAK accreditation requirements. Unless otherwise is specified, all ass or Fail results are given without uncertainty considered. When uncertainty is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer s decision. Opinions and interpretations expressed herein are outside the scope of TÜRKAK accreditation. Tests marked (*) in this test report are not included in the TÜRKAK accreditation schedule for this laboratory. Aşkın GÜNERİ COORDINATOR Neslihan Sözer Chemical Laboratory Manager

2 R E S U L T S age 2 of 5 AEO Test INTERTEK IHTM AL Determination of AEO by Liquid Chromotography-Mass Spectrometry (LC-MS-MS) Analysis White print Alkylphenols Nonylphenol (N) Not Detected Not Detected Octylphenol (O) Not Detected Alkylphenol Ethoxylates Nonylphenolethoxylates (NEO) Not Detected 100 ppm Octylphenolethoxylates (OEO) Not Detected Detection Limit : 20 ppm Estimated Total Uncertainity=( lastic:±4% ; Textile:±3%)

3 R E S U L T S age 3 of 5 Detection of Amines Derived From Azocolourants and Azodyes Test Method : BS EN : 2012 for Textile Material By Gas Chromatographic - Mass Spectrometric (GC-MS) And High erformance Liquid Chromatographic (HLC) Analysis. 1)White print (without extraction) <20 ppm RESULTS FORBIDDEN AMINE CAS NO 1 4-AMINOBIHENYL N BENZIDINE N CHLORO-O-4-CHLOR-O-TOLUIDINE N 2-NAHTHYLAMINE N *O-AMINOAZOTOLUENE N *2-AMINO-4-NITROTOLUENE N -CHLOROANILINE N 2,4-DIAMINOANISOLE N 4,4 -DIAMINOBIHENYLMETHANE N 3,3 -DICHLOROBENZIDINE N 3,3 -DIMETHOXYBENZIDINE N 3,3 -DIMETHYLBENZIDINE N 3,3 -DİMETHYL-4,4 DIAMINOBIHENYLMETHANE N -CRESIDINE N 4,4 -METHYLENE-BIS-(2 CHLOROANILINE) N 4,4 -OXYDIANILINE N 4,4 -THIODIANILINE N O-TOLUIDINE N 2,4-TOLUENDIAMINE N 2,4,5-TRIMETHYLANILINE N O-ANISIDINE N **-AMINOAZOBENZENE N 2,4 XYLIDINE N 2,6 XYLIDINE N Note: 1)The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. 2)Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine. The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used. 3)According to EN :2012, separate test is suggested to ascertain the compliance for result of mixed test in the range between 5 ppm and 30 ppm. 4)Azocolourants Content Requirement In Annex XVII Item 43 Of The REACH Regulation (EC) NO. 1907/2006 & Amendment No. 552/2009 and 126/2013 (Formerly Known As Directive 2002/61/EC ppm : part per million (mg/kg) Detection Limit: 5 ppm < = Less Than N: Not Detected NC : No Comment Estimated Total Uncertainity=( ±9%)

4 R E S U L T S age 4 of 5 Determination of Free and Hydrolised Formaldehyde Test (Water extraction method) BS EN ISO :2011 Free and Hydrolized Formaldehyde by UV-VIS Analysis White print 30 ppm 16 ppm ppm (part per million) =mg / kg Detection Limit =5 ppm < =Less Than Estimated Total Uncertainity=( ±6%) Note :Sample was received unsealed Heavy Metals Analysis for print INTERTEK IHTM AL with refer to ISO 105 E-04 Extractable with artificial perspiration solution and Determination by IC-MS Result Requirement Lead (b) <0.1 ppm 0.2 ppm Mercury (Hg) <0.01 ppm 0.02 ppm ppm : part per million (mg/kg) < =Less Than Estimated Total Uncertainity=( ±8%)

5 R E S U L T S age 5 of 5 ## END OF TEST REORT ##