Test Report. As per applicant s request
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1 Applicant: Sigma Ink Corporation Date : Nov 19, Via De La Valle Ste 100, Solana Beach, CA USA Sample Description: One (1) group of submitted samples said to be : Sample Description : UV Series Pad Printing Ink Style / Item No. : (1)UV310 (black) (2)UV320 (white) Series No. : UV Supplier s Name : Sigma Ink Corporation Date Sample Received : Nov 10, 2014 Date Test Started : Nov 10, 2014 : As requested by the applicant, for details please refer to attached pages. Conclusion: Tested Sample Standard Result Submitted Samples Restriction Of Hazardous Substances (RoHS) Test - As per applicant s request with reference to 2011/65/EU Pass As per applicant s request - Total Arsenic (As) Content - Total Barium (Ba) Content - Total Antimony (Sb) Content - Total Selenium (Se) Content - Phthalates See See See See See Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director *THJ * Page 1 of 10
2 Test Result Summary: Heavy Metal Cadmium (Cd) Content Lead (Pb) Content Mercury (Hg) Content Arsenic (As) Content Barium (Ba) Content Antimony (Sb) Content Selenium (Se) Content Test Item Unit Test Method Chromium VI (Cr 6+ ) Content With reference to IEC : 2013, by microwave or acid digestion and determined by ICP-OES. With reference to IEC : 2013, by microwave or acid digestion and determined by ICP-OES. With reference to IEC : 2013, by microwave or acid digestion and determined by ICP-OES. With reference to USEPA 3052, by microwave digestion and determined by ICP-OES. With reference to USEPA 3052, by microwave digestion and determined by ICP-OES. With reference to USEPA 3052, by microwave digestion and determined by ICP-OES. With reference to USEPA 3052, by microwave digestion and determined by ICP-OES. With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer. Result (1) (2) RL ND ND 1 *THJ * Page 2 of 10
3 Test Item Unit Test Method Result (1) (2) RL Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) Dibrominated Biphenyls (DiBB) Tribrominated Biphenyls (TriBB) Tetrabrominated Biphenyls (TetraBB) With reference to IEC 62321: Pentabrominated Biphenyls 2008, by solvent extraction ND ND 5 (PentaBB) and determined by GC-MS and Hexabrominated Biphenyls further HPLC-DAD confirmation ND ND 5 (HexaBB) when necessary. Heptabrominated Biphenyls (HeptaBB) Octabrominated Biphenyls (OctaBB) Nonabrominated Biphenyls (NonaBB) Decabrominated Biphenyl (DecaBB) ND ND 5 Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) Dibrominated Diphenyl Ethers (DiBDE) Tribrominated Diphenyl Ethers (TriBDE) Tetrabrominated Diphenyl Ethers (TetraBDE) With reference to IEC 62321: Pentabrominated Diphenyl Ethers 2008, by solvent extraction ND ND 5 (PentaBDE) and determined by GC-MS and Hexabrominated Diphenyl Ethers further HPLC-DAD confirmation ND ND 5 (HexaBDE) when necessary. Heptabrominated Diphenyl Ethers (HeptaBDE) Octabrominated Diphenyl Ethers (OctaBDE) Nonabrominated Diphenyl Ethers (NonaBDE) Decabrominated Diphenyl Ether (DecaBDE) ND ND 5 *THJ * Page 3 of 10
4 Test Item Unit Test Method Result (1) (2) RL Phthalates Di(2-ethylhexyl) Phthalate (DEHP) 0 Dibutyl Phthalate (DBP) 0 With reference to EN 14372: Benzyl Butyl Phthalate (BBP) , by solvent extraction Di-(Iso-Nonyl) Phthalate (DINP) 0 and determined by GC-MS. Di-(Iso-Decyl) Phthalate (DIDP) 0 Di-(N-Octyl) Phthalate (DNOP) ND ND 50 Remarks: = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample Responsibility of Chemist: Pelny Hsiao/ Vico Lin Date Sample Received : Nov 10, 2014 Test Period : Nov 10, 2014 to Nov 13, 2014 RoHS Limit Restricted Substances Cadmium (Cd) content Lead (Pb) content Mercury (Hg) content Chromium VI (Cr 6+ ) content Polybrominated Biphenyls (PBBs) Polybrominated Diphenyl Ethers (PBDEs) Limits 0.01% (100) 0.1% (1000) 0.1% (1000) 0.1% (1000) 0.1% (1000) 0.1% (1000) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material. *THJ * Page 4 of 10
5 Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard:Cd/Pb: IEC :2013; Hg: IEC :2013; Chromium (VI)/PBBs/PBDEs : IEC 62321:2008 Sampling Cd/Pb/Hg Metal Cr 6+ Polymers / electronics PBBs/PBDEs For different material, digest the sample with appropriate acid *1 By spot test Weigh sample and add alkaline solution Weigh sample and add organic solvent Negative *2 Confirm the tested samples are totally dissolved Get 50cm 2 sample Definite temp. extraction By solvent extraction Make up with deionized water By boiling water extraction Cool and filter the extract Concentrate the extract and make up with organic solvent Analyzed by ICP-OES Make up with deionized water and add diphenyl-carbazide solution Analyzed by GC-MS Analyzed by UV-VIS Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO 3,HCl,HF,H 2 O 2,H 3 BO 3 Metals HNO 3,HCl,HF Electronics HNO 3,HCl,H 2 O 2,HBF 4 *2: If the result of spot test is positive, Chromium VI would be determined as detected. *THJ * Page 5 of 10
6 Measurement Flowchart: Test for Heavy Metal Contents Reference Method:USEPA 3052 Sampling Weigh sample and digest in microwave digestion oven with suitable acid Confirm the tested samples are totally dissolved Transfer the digested solution and make up with deionized water Analyzed by ICP-OES *THJ * Page 6 of 10
7 Measurement Flowchart: Test for Phthalates Content Reference Method: EN 14372: 2004 Sampling Weigh sample and add organic solvent By solvent extraction Concentrate the extract and make up with organic solvent Analyzed by GC-MS *THJ * Page 7 of 10
8 End of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct. *THJ * Page 8 of 10
9 *THJ * Page 9 of 10
10 *THJ * Page 10 of 10
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