Page 2 of 5 REPORT OF ANALYSIS Delta Water PBC dba/delta Water Mr. Jereme Cavallo 1400 Union Ave. Report Date : 09/21/2017

Transcription

1 21146 Delta Water PBC dba/delta Water Mr. Jereme Cavallo 1400 Union Ave Memphis, TN Project Information : Analytical Testing Report Date : 09/21/2017 Received : 9/14/2017 Report Number : REPORT OF ANALYSIS Lab No : Matrix: Aqueous Sample ID : Delta Water Non-Ozonated Sampled: 9/14/ :15 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Coliform <1 MPN/100mL /14/17 14:10 SBA 9223B-2004 Conductivity 491 µs/cm /15/17 09:05 SBA 2510B-2011 E-coli <1 MPN/100mL /14/17 14:10 SBA 9223B-2004 Nitrate (NO3-N) 2.89 mg/l /14/17 13:45 BKN EPA ph 7.8 s.u. 1 09/14/17 15:35 TSP 4500H+B-2011 Total Dissolved Solids 314 mg/l /15/17 09:05 SBA 2510B-2011 Total Calcium 55.3 mg/l /20/17 23:39 CCR EPA Total Copper <0.005 mg/l /20/17 23:39 CCR EPA Hardness as CaCO3(SM-2340B) 202 mg/l /20/17 23:39 EPA Total Iron <0.100 mg/l /20/17 23:39 CCR EPA Total Lead <0.006 mg/l /20/17 23:39 CCR EPA Total Magnesium 15.6 mg/l /20/17 23:39 CCR EPA Qualifiers/ Definitions DF Dilution Factor MQL Method Quantitation Limit Page 2 of 5

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b[.!Wb&0)NBc%5Db2N)Bc%9?b5X*?33N&c%[DbA4Nc%f?b %%%%f?32&nnc%8[bann3&4233 9",<"%9'aIa$F DF"7K-<E"7%T"G%9"F"#$,

3 <<<<< =C=.D1E! 6) "#$%&'()*+,#&(-./ /.!"#$!%&$'&()(*+,-, "42GK(6L%+4M.&%/#0'(=424N#&.&%/#0'(( 123%&+4'5%2(- "#$%&'(F4'#(- :8HIJHI:9J "#0#5A#G(- 8H9<HI:9J O4,()%(- E4+$B#(1F( &9:;5<86&=875<&,><:;? =4'&5P- (FG5HGI Test Results Units MQL DF Date / Time By Analytical Analyzed Method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age 2 of 4

4 12/20/2016 Delta Water PBC dba/delta Water Mr. Jereme Cavallo 1400 Union Ave Memphis, TN, Ref: Analytical Testing Lab Report Number: Client Project Description: Analysis Required for Source Approval Dear Mr. Jereme Cavallo: Waypoint Analytical, Inc. received sample(s) on 11/28/2016 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-nelap) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '~' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, ph, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an asreceived basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Andy Parrish Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.!"#$#%# &'()*( +,-./.#0# &('(1* 2! 34+!5 &'6(171 89:#/ &81(')('17( 11 6!;<#0/#/ &77 (6*( =.//.//.>>.?#".@,;0.# &AB(' 3? &'1* C<"#D,%# &BE11 2.;F.0.# &((1(6 G90H-I<J &B((') 89009//99 &83(A(A) 45! &83(((1A G90H-I<J KL8 &'1 Page 1 of 39

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age 3 of 39

6 <99;= H&I(J#&#+#(B4G4??% 9;::(E25%2(FG# H#+$K5L! 6) 789:; F24?ML5L("#N*5&#C(3%&(O%*&0#(F$$&%G4? "#$%&'()*+,#&(-./ !"#$!%&$'&()(*+,-,.&%/#0'(( 123%&+4'5%2(- "#$%&'(>4'#(- 9<D<:D<:9= "#0#5G#C(- 99D<8D<:9= P4,()%(- O4+$?#(1>( &:986;&(<97=>?>&. H4'&5Q- (DE6FE> O4+$?#C-..A34A32./&.2BC2 Test Results Units MQL DF Date / Time By Analytical Analyzed Method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`)5'&5'#Y) 1G.. +RDP :I9:: 9 99D<8D9=(9W-7[ \.FY7::I: UC%& )F<6 9 99D<XD9=(97-WX JAA 9;:I9 $a /GI LI*I 9 ;W::a`AY<:99 6%'4?(>5LL%?G#C(O%?5CL 3C2 +RDP 9: 9 99D7:D9=(9:-:: BJ" <W;:BY<:99 O*&340'42'L(THAFOV Z:I<:: +RDP :I<:: 9 99D<XD9=(97-7: 6JO WW;:BY<:99 6%'4?(F?*+52*+ Z9:: brdp 9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(F2'5+%2M Z9I:: brdp 9I:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(F&L#250 Z:IW:: brdp :IW:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(A4&5*+ /HGC brdp 9I:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(A#&M??5*+ Z:IW:: brdp :IW:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 JE97?K?6;>A 56K?<?8?F<> >^ >5?*'5%2(^40'%& HcP H#'K%C(c*42'5'4'5%2(P5+5' Page 4 of 39

7 <99;= H&I(J#&#+#(B4G4??% 9;::(E25%2(FG# H#+$K5L! 6) 789:; F24?ML5L("#N*5&#C(3%&(O%*&0#(F$$&%G4? "#$%&'()*+,#&(-./ !"#$!%&$'&()(*+,-,.&%/#0'(( 123%&+4'5%2(- "#$%&'(>4'#(- 9<D<:D<:9= "#0#5G#C(- 99D<8D<:9= P4,()%(- O4+$?#(1>( &:986;&(<97=>?>&. H4'&5Q- (DE6FE> O4+$?#C-..A34A32./&.2BC2 Test Results Units MQL DF Date / Time By Analytical Analyzed Method 6%'4?(B4C+5*+ Z:I9:: brdp :I9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(B4?05*+ 12C22 brdp 9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(BK&%+5*+ Z9I:: brdp 9I:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(B%$$#& Z:IW:: brdp :IW:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 a4&c2#ll(4l(b4bu7tohy<7;:av.1@222 brdp 9:: 9 99D<XD9=(9=-WW \.FY<::I8 6%'4?(1&%2 Z9:: brdp 9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(P#4C Z:IW:: brdp :IW:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(H4R2#L5*+.I122 brdp 9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(H42R42#L# Z9I:: brdp 9I:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 H#&0*&M(T6%'4?V Z:I:::<: +RDP :I:::<: 9 99D<XD9=(97-:= ]]H \.FY<;WI9 6%'4?()50S#? Z:IW:: brdp :IW:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(O#?#25*+ Z9I:: brdp 9I:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(O5?G#& Z:I9:: brdp :I9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(O%C5*+ 3C422 brdp 9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(6K4??5*+ Z:I9:: brdp :I9:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6%'4?(d520 1HG1 brdp WI:: 9 99D<XD9=(9=-WW A]) \.FY<::I8 6*&,5C5'M Z9I: )6E 9I: 9 99D<XD9=(9:-<W >A< <97:AY<:99 O*?34'#.1GC +RDP 9I:: 9 99D<8D9=(9W-7[ A]) \.FY7::I: JE97?K?6;>A 56K?<?8?F<> >^ >5?*'5%2(^40'%& HcP H#'K%C(c*42'5'4'5%2(P5+5' Page 5 of 39

8 #=CL# LIMS USE: FR - PROJECT MANAGER LIMS OBJECT ID: December 20, 2016 Project Manager Waypoint 2790 Whitten Road Memphis, TN RE: Dear Project Manager: Enclosed are the analytical results for sample(s) received by the laboratory on November 29, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sakina Mckenzie sakina.mckenzie@pacelabs.com Project Manager Enclosures cc: Accounts Payable, Waypoint Mr. Nathan A. Pera, Waypoint Page 1 of 32 Page 6 of 39

9 #=CP# CERTIFICATIONS Pennsylvania Certification IDs 1638 Roseytown Rd Suites 2,3&4, Greensburg, PA L-A-B DOD-ELAP Accreditation #: L2417 Alabama Certification #: Arizona Certification #: AZ0734 Arkansas Certification California Certification #: 04222CA Colorado Certification Connecticut Certification #: PH-0694 Delaware Certification Florida/TNI Certification #: E87683 Georgia Certification #: C040 Guam Certification Hawaii Certification Idaho Certification Illinois Certification Indiana Certification Iowa Certification #: 391 Kansas/TNI Certification #: E Kentucky Certification #: Louisiana DHH/TNI Certification #: LA Louisiana DEQ/TNI Certification #: 4086 Maine Certification #: PA00091 Maryland Certification #: 308 Massachusetts Certification #: M-PA1457 Michigan/PADEP Certification Missouri Certification #: 235 Ormond Beach Certification IDs, Alabama Certification #: Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: Maryland Certification: #346 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Montana Certification #: Cert 0082 Nebraska Certification #: NE Nevada Certification #: PA New Hampshire/TNI Certification #: 2976 New Jersey/TNI Certification #: PA 051 New Mexico Certification #: PA01457 New York/TNI Certification #: North Carolina Certification #: North Dakota Certification #: R-190 Oregon/TNI Certification #: PA Pennsylvania/TNI Certification #: Puerto Rico Certification #: PA01457 Rhode Island Certification #: South Dakota Certification Tennessee Certification #: TN2867 Texas/TNI Certification #: T Utah/TNI Certification #: PA USDA Soil Permit #: P Vermont Dept. of Health: ID# VT-0282 Virgin Island/PADEP Certification Virginia/VELAP Certification #: Washington Certification #: C868 West Virginia DEP Certification #: 143 West Virginia DHHR Certification #: 9964C Wisconsin Certification Wyoming Certification #: 8TMS-L Nebraska Certification: NE-OS Nevada Certification: FL NELAC Reciprocity New York Certification #: North Carolina Environmental Certificate #: 667 North Carolina Certification #: Oklahoma Certification #: D9947 Pennsylvania Certification #: Puerto Rico Certification #: FL01264 South Carolina Certification: # Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: Wyoming Certification: FL NELAC Reciprocity West Virginia Certification #: 9962C Wisconsin Certification #: Wyoming (EPA Region 8): FL NELAC Reciprocity Page 2 of 32 Page 7 of 39

10 #=SS# SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received Water 11/28/16 10:40 11/29/16 10:20 Page 3 of 32 Page 8 of 39

11 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA SMH 2 PASI-O EPA JTJ 21 PASI-O EPA SMH 7 PASI-O EPA JLR 49 PASI-O SM7500RnB-07 NJV 1 PASI-PA EPA NEG 1 PASI-PA EPA ACM 1 PASI-PA EPA JLW 1 PASI-PA ASTM D LAL 1 PASI-PA EPA WRR 1 PASI-PA ASTM D RMK 1 PASI-PA EPA TK1 1 PASI-O Page 4 of 32 Page 9 of 39

12 #=HO# SUMMARY OF DETECTION Lab Sample ID Method Client Sample ID s Result Units Report Limit Analyzed Qualifiers SM7500RnB-07 EPA EPA EPA ASTM D EPA ASTM D EPA Radon ± 73.6 (71.9) C:NA T:NA pci/l 12/02/16 21:55 1p Gross Alpha 1.64U ± pci/l 12/06/16 21: (1.64) C:NA T:NA Radium U ± pci/l 12/15/16 10: (0.584) C:NA T:92% Radium U ± pci/l 12/16/16 11: (1.04) C:68% T:84% Strontium U ± pci/l 12/08/16 20:17 N (0.465) C:97% T:NA Tritium ± 138 pci/l 12/09/16 17:32 (251) C:NA T:NA Total Uranium 0.193U ± ug/l 12/19/16 16: (0.193) C:NA T:NA Phenolics, Total Recoverable mg/l /15/16 14:49 Page 5 of 32 Page 10 of 39

13 #=AR# ANALYTICAL RESULTS Sample: Lab ID: 001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water Comments: Split off 500 ml amber un-preserved bottle for Tritium analysis. Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the sample preservation requirement of ph <2 for radiochemistry analysis. s Results Units PQL MDL DF Prepared Analyzed CAS No. Qual GCS EDB and DBCP Analytical Method: EPA Preparation Method: EPA ,2-Dibromo-3-chloropropane U ug/l /05/16 17:04 12/06/16 04: ,2-Dibromoethane (EDB) U ug/l /05/16 17:04 12/06/16 04: GCS Pesticides Analytical Method: EPA Preparation Method: EPA Alachlor 0.034U ug/l /30/16 10:15 12/05/16 17: Atrazine 0.061U ug/l /30/16 10:15 12/05/16 17: gamma-bhc (Lindane) U ug/l /30/16 10:15 12/05/16 17: Chlordane (Technical) 0.045U ug/l /30/16 10:15 12/05/16 17: Endrin U ug/l /30/16 10:15 12/05/16 17: Heptachlor 0.012U ug/l /30/16 10:15 12/05/16 17: Heptachlor epoxide U ug/l /30/16 10:15 12/05/16 17: Hexachlorobenzene 0.018U ug/l /30/16 10:15 12/05/16 17: L3 Hexachlorocyclopentadiene 0.031U ug/l /30/16 10:15 12/01/16 17: L3 Methoxychlor 0.049U ug/l /30/16 10:15 12/05/16 17: PCB-1016 (Aroclor 1016) 0.077U ug/l /30/16 10:15 12/05/16 17: PCB-1221 (Aroclor 1221) 0.028U ug/l /30/16 10:15 12/05/16 17: PCB-1232 (Aroclor 1232) 0.028U ug/l /30/16 10:15 12/05/16 17: PCB-1242 (Aroclor 1242) 0.049U ug/l /30/16 10:15 12/05/16 17: PCB-1248 (Aroclor 1248) 0.060U ug/l /30/16 10:15 12/05/16 17: PCB-1254 (Aroclor 1254) 0.022U ug/l /30/16 10:15 12/05/16 17: PCB-1260 (Aroclor 1260) 0.063U ug/l /30/16 10:15 12/05/16 17: PCB, Total 0.077U ug/l /30/16 10:15 12/05/16 17: Simazine 0.066U ug/l /30/16 10:15 12/05/16 17: Toxaphene 0.58U ug/l /30/16 10:15 12/05/16 17: Surrogates Decachlorobiphenyl (S) 56 % /30/16 10:15 12/05/16 17: S Haloacetic Acids Analytical Method: EPA Preparation Method: EPA Dibromoacetic Acid U mg/l /30/16 11:25 12/02/16 14: Dichloroacetic Acid U mg/l /30/16 11:25 12/02/16 14: Haloacetic Acids (Total) U mg/l /30/16 11:25 12/02/16 14:49 Monobromoacetic Acid U mg/l /30/16 11:25 12/02/16 14: Monochloroacetic Acid U mg/l /30/16 11:25 12/02/16 14: Trichloroacetic Acid U mg/l /30/16 11:25 12/02/16 14: Surrogates 2,3-Dibromopropanoic Acid (S) 102 % /30/16 11:25 12/02/16 14: MSV Analytical Method: EPA Benzene 0.25U ug/l /09/16 17: Bromobenzene 0.25U ug/l /09/16 17: Bromodichloromethane 0.25U ug/l /09/16 17: Bromoform 0.25U ug/l /09/16 17: Bromomethane 0.25U ug/l /09/16 17: Date: 12/20/ :20 AM Page 6 of 32 Page 11 of 39

14 #=AR# ANALYTICAL RESULTS Sample: Lab ID: 001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water Comments: Split off 500 ml amber un-preserved bottle for Tritium analysis. Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the sample preservation requirement of ph <2 for radiochemistry analysis. s Results Units PQL MDL DF Prepared Analyzed CAS No. Qual MSV Analytical Method: EPA Carbon tetrachloride 0.25U ug/l /09/16 17: Chlorobenzene 0.25U ug/l /09/16 17: Chloroethane 0.28U ug/l /09/16 17: L3 Chloroform 0.25U ug/l /09/16 17: Chloromethane 0.46U ug/l /09/16 17: Chlorotoluene 0.25U ug/l /09/16 17: Chlorotoluene 0.25U ug/l /09/16 17: Dibromochloromethane 0.25U ug/l /09/16 17: Dibromomethane 0.25U ug/l /09/16 17: ,2-Dichlorobenzene 0.25U ug/l /09/16 17: ,3-Dichlorobenzene 0.25U ug/l /09/16 17: ,4-Dichlorobenzene 0.25U ug/l /09/16 17: Dichlorodifluoromethane 0.49U ug/l /09/16 17: L3 1,1-Dichloroethane 0.25U ug/l /09/16 17: ,2-Dichloroethane 0.25U ug/l /09/16 17: ,1-Dichloroethene 0.25U ug/l /09/16 17: cis-1,2-dichloroethene 0.25U ug/l /09/16 17: trans-1,2-dichloroethene 0.25U ug/l /09/16 17: ,2-Dichloropropane 0.25U ug/l /09/16 17: ,3-Dichloropropane 0.25U ug/l /09/16 17: ,2-Dichloropropane 0.25U ug/l /09/16 17: ,1-Dichloropropene 0.25U ug/l /09/16 17: ,3-Dichloropropene 0.25U ug/l /09/16 17: N2 Ethylbenzene 0.25U ug/l /09/16 17: Methylene Chloride 0.44U ug/l /09/16 17: Methyl-tert-butyl ether 0.25U ug/l /09/16 17: L3 Styrene 0.25U ug/l /09/16 17: ,1,1,2-Tetrachloroethane 0.25U ug/l /09/16 17: Tetrachloroethene 0.25U ug/l /09/16 17: Toluene 0.25U ug/l /09/16 17: Total Trihalomethanes (Calc.) 0.25U ug/l /09/16 17:00 1,2,4-Trichlorobenzene 0.41U ug/l /09/16 17: ,1,1-Trichloroethane 0.25U ug/l /09/16 17: ,1,2-Trichloroethane 0.25U ug/l /09/16 17: Trichloroethene 0.25U ug/l /09/16 17: Trichlorofluoromethane 0.25U ug/l /09/16 17: L3 1,2,3-Trichloropropane 0.43U ug/l /09/16 17: Vinyl chloride 0.39U ug/l /09/16 17: Xylene (Total) 0.25U ug/l /09/16 17: m&p-xylene 0.25U ug/l /09/16 17: o-xylene 0.25U ug/l /09/16 17: Surrogates 4-Bromofluorobenzene (S) 86 % /09/16 17: Toluene-d8 (S) 96 % /09/16 17: Date: 12/20/ :20 AM Page 7 of 32 Page 12 of 39

15 #=AR# ANALYTICAL RESULTS Sample: Lab ID: 001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water Comments: Split off 500 ml amber un-preserved bottle for Tritium analysis. Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the sample preservation requirement of ph <2 for radiochemistry analysis. s Results Units PQL MDL DF Prepared Analyzed CAS No. Qual MSV Analytical Method: EPA Surrogates 1,2-Dichloroethane-d4 (S) 111 % /09/16 17: Phenolics, Total Analytical Method: EPA Phenolics, Total Recoverable mg/l /15/16 14:49 Date: 12/20/ :20 AM Page 8 of 32 Page 13 of 39

16 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA MSV METHOD BLANK: Associated Lab Samples: 001 Units Blank Result Matrix: Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/l 0.25U /09/16 15:32 1,1,1-Trichloroethane ug/l 0.25U /09/16 15:32 1,1,2-Trichloroethane ug/l 0.25U /09/16 15:32 1,1-Dichloroethane ug/l 0.25U /09/16 15:32 1,1-Dichloroethene ug/l 0.25U /09/16 15:32 1,1-Dichloropropene ug/l 0.25U /09/16 15:32 1,2,3-Trichloropropane ug/l 0.43U /09/16 15:32 1,2,4-Trichlorobenzene ug/l 0.41U /09/16 15:32 1,2-Dichlorobenzene ug/l 0.25U /09/16 15:32 1,2-Dichloroethane ug/l 0.25U /09/16 15:32 1,2-Dichloropropane ug/l 0.25U /09/16 15:32 1,3-Dichlorobenzene ug/l 0.25U /09/16 15:32 1,3-Dichloropropane ug/l 0.25U /09/16 15:32 1,3-Dichloropropene ug/l 0.25U /09/16 15:32 N2 1,4-Dichlorobenzene ug/l 0.25U /09/16 15:32 2,2-Dichloropropane ug/l 0.25U /09/16 15:32 2-Chlorotoluene ug/l 0.25U /09/16 15:32 4-Chlorotoluene ug/l 0.25U /09/16 15:32 Benzene ug/l 0.25U /09/16 15:32 Bromobenzene ug/l 0.25U /09/16 15:32 Bromodichloromethane ug/l 0.25U /09/16 15:32 Bromoform ug/l 0.25U /09/16 15:32 Bromomethane ug/l 0.25U /09/16 15:32 Carbon tetrachloride ug/l 0.25U /09/16 15:32 Chlorobenzene ug/l 0.25U /09/16 15:32 Chloroethane ug/l 0.28U /09/16 15:32 Chloroform ug/l 0.25U /09/16 15:32 Chloromethane ug/l 0.46U /09/16 15:32 cis-1,2-dichloroethene ug/l 0.25U /09/16 15:32 Dibromochloromethane ug/l 0.25U /09/16 15:32 Dibromomethane ug/l 0.25U /09/16 15:32 Dichlorodifluoromethane ug/l 0.49U /09/16 15:32 Ethylbenzene ug/l 0.25U /09/16 15:32 m&p-xylene ug/l 0.25U /09/16 15:32 Methyl-tert-butyl ether ug/l 0.25U /09/16 15:32 Methylene Chloride ug/l 0.44U /09/16 15:32 o-xylene ug/l 0.25U /09/16 15:32 Styrene ug/l 0.25U /09/16 15:32 Tetrachloroethene ug/l 0.25U /09/16 15:32 Toluene ug/l 0.25U /09/16 15:32 Total Trihalomethanes (Calc.) ug/l 0.25U /09/16 15:32 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 9 of 32 Page 14 of 39

17 #=QC# QUALITY CONTROL DATA METHOD BLANK: Associated Lab Samples: 001 Units Blank Result Matrix: Water Reporting Limit MDL Analyzed trans-1,2-dichloroethene ug/l 0.25U /09/16 15:32 Trichloroethene ug/l 0.25U /09/16 15:32 Trichlorofluoromethane ug/l 0.25U /09/16 15:32 Vinyl chloride ug/l 0.39U /09/16 15:32 Xylene (Total) ug/l 0.25U /09/16 15:32 1,2-Dichloroethane-d4 (S) % /09/16 15:32 4-Bromofluorobenzene (S) % /09/16 15:32 Toluene-d8 (S) % /09/16 15:32 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: Units Spike Conc LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,1-Dichloropropene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trichlorobenzene ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloropropane ug/l ,3-Dichlorobenzene ug/l ,3-Dichloropropane ug/l ,3-Dichloropropene ug/l N2 1,4-Dichlorobenzene ug/l ,2-Dichloropropane ug/l Chlorotoluene ug/l Chlorotoluene ug/l Benzene ug/l Bromobenzene ug/l Bromodichloromethane ug/l Bromoform ug/l Bromomethane ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l L0 Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Dichlorodifluoromethane ug/l L0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Max RPD Qualifiers Date: 12/20/ :20 AM Page 10 of 32 Page 15 of 39

18 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE & LCSD: Units Spike Conc LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Ethylbenzene ug/l m&p-xylene ug/l Methyl-tert-butyl ether ug/l L0 Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l Total Trihalomethanes (Calc.) ug/l trans-1,2-dichloroethene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l L0 Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 11 of 32 Page 16 of 39

19 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA EDB DBCP METHOD BLANK: Associated Lab Samples: 001 Units Blank Result Matrix: Water Reporting Limit MDL Analyzed 1,2-Dibromo-3-chloropropane ug/l U /06/16 03:52 1,2-Dibromoethane (EDB) ug/l U /06/16 03:52 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: Units Spike Conc LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD 1,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l Max RPD Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,2-Dibromo-3- ug/l U chloropropane 1,2-Dibromoethane (EDB) ug/l U Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 12 of 32 Page 17 of 39

20 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA GCS Pesticide METHOD BLANK: Associated Lab Samples: 001 Units Blank Result Matrix: Water Reporting Limit MDL Analyzed Alachlor ug/l 0.035U /01/16 06:28 Atrazine ug/l 0.063U /01/16 06:28 Chlordane (Technical) ug/l 0.047U /01/16 06:28 Endrin ug/l U /01/16 06:28 gamma-bhc (Lindane) ug/l U /01/16 06:28 Heptachlor ug/l 0.012U /01/16 06:28 Heptachlor epoxide ug/l U /01/16 06:28 Hexachlorobenzene ug/l 0.019U /01/16 06:28 Hexachlorocyclopentadiene ug/l 0.032U /01/16 06:28 Methoxychlor ug/l 0.051U /01/16 06:28 PCB-1016 (Aroclor 1016) ug/l 0.080U /01/16 06:28 PCB-1221 (Aroclor 1221) ug/l 0.029U /01/16 06:28 PCB-1232 (Aroclor 1232) ug/l 0.029U /01/16 06:28 PCB-1242 (Aroclor 1242) ug/l 0.051U /01/16 06:28 PCB-1248 (Aroclor 1248) ug/l 0.062U /01/16 06:28 PCB-1254 (Aroclor 1254) ug/l 0.023U /01/16 06:28 PCB-1260 (Aroclor 1260) ug/l 0.066U /01/16 06:28 Simazine ug/l 0.069U /01/16 06:28 Toxaphene ug/l 0.61U /01/16 06:28 Decachlorobiphenyl (S) % /01/16 06:28 Qualifiers LABORATORY CONTROL SAMPLE: Units Spike Conc. LCS Result LCS % Rec % Rec Limits Alachlor ug/l Atrazine ug/l Chlordane (Technical) ug/l 0.047U Endrin ug/l gamma-bhc (Lindane) ug/l Heptachlor ug/l Heptachlor epoxide ug/l Hexachlorobenzene ug/l L0 Hexachlorocyclopentadiene ug/l L0 Methoxychlor ug/l PCB-1016 (Aroclor 1016) ug/l 0.080U PCB-1221 (Aroclor 1221) ug/l 0.029U PCB-1232 (Aroclor 1232) ug/l 0.029U PCB-1242 (Aroclor 1242) ug/l 0.051U PCB-1248 (Aroclor 1248) ug/l 0.062U PCB-1254 (Aroclor 1254) ug/l 0.023U Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 13 of 32 Page 18 of 39

21 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Units Spike Conc. LCS Result LCS % Rec % Rec Limits PCB-1260 (Aroclor 1260) ug/l 0.066U Simazine ug/l Toxaphene ug/l 0.61U Decachlorobiphenyl (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Alachlor ug/l ND Atrazine ug/l ND Chlordane (Technical) ug/l ND 0.10U 0.10U 40 Endrin ug/l ND gamma-bhc (Lindane) ug/l ND Heptachlor ug/l ND Heptachlor epoxide ug/l ND Hexachlorobenzene ug/l ND Hexachlorocyclopentadiene ug/l ND Methoxychlor ug/l ND PCB-1016 (Aroclor 1016) ug/l ND 0.18U 0.18U 40 PCB-1221 (Aroclor 1221) ug/l ND 0.064U 0.064U 40 PCB-1232 (Aroclor 1232) ug/l ND 0.064U 0.064U 40 PCB-1242 (Aroclor 1242) ug/l ND 0.11U 0.11U 40 PCB-1248 (Aroclor 1248) ug/l ND 0.14U 0.14U 40 PCB-1254 (Aroclor 1254) ug/l ND 0.051U 0.051U 40 PCB-1260 (Aroclor 1260) ug/l ND 0.15U 0.15U 40 Simazine ug/l ND Toxaphene ug/l ND 1.4U 1.4U 40 Decachlorobiphenyl (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 14 of 32 Page 19 of 39

22 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA Haloacetic Acids METHOD BLANK: Associated Lab Samples: 001 Units Blank Result Matrix: Water Reporting Limit MDL Analyzed Dibromoacetic Acid mg/l U /02/16 09:52 Dichloroacetic Acid mg/l U /02/16 09:52 Haloacetic Acids (Total) mg/l U /02/16 09:52 Monobromoacetic Acid mg/l U /02/16 09:52 Monochloroacetic Acid mg/l U /02/16 09:52 Trichloroacetic Acid mg/l U /02/16 09:52 2,3-Dibromopropanoic Acid (S) % /02/16 09:52 Qualifiers LABORATORY CONTROL SAMPLE: Units Spike Conc. LCS Result LCS % Rec % Rec Limits Dibromoacetic Acid mg/l Dichloroacetic Acid mg/l Haloacetic Acids (Total) mg/l Monobromoacetic Acid mg/l Monochloroacetic Acid mg/l Trichloroacetic Acid mg/l ,3-Dibromopropanoic Acid (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Dibromoacetic Acid mg/l 5.1 ug/l Dichloroacetic Acid mg/l 2.5 ug/l M1 Haloacetic Acids (Total) mg/l 8.7 ug/l Monobromoacetic Acid mg/l 0.37U ug/l Monochloroacetic Acid mg/l 0.37U M1,R1 ug/l Trichloroacetic Acid mg/l 1.2 ug/l ,3-Dibromopropanoic Acid (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 15 of 32 Page 20 of 39

23 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Dibromoacetic Acid mg/l 0.37U ug/l Dichloroacetic Acid mg/l 3.1 ug/l M1 Haloacetic Acids (Total) mg/l 10 ug/l Monobromoacetic Acid mg/l 0.37U ug/l Monochloroacetic Acid mg/l 0.37U M1 ug/l Trichloroacetic Acid mg/l 6.9 ug/l ,3-Dibromopropanoic Acid (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 16 of 32 Page 21 of 39

24 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 Analysis Method: Analysis Description: EPA Phenolics METHOD BLANK: Associated Lab Samples: 001 Units Blank Result Matrix: Water Reporting Limit MDL Analyzed Phenolics, Total Recoverable mg/l U /15/16 14:44 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: Units Spike Conc LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Phenolics, Total Recoverable mg/l Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 12/20/ :20 AM Page 17 of 32 Page 22 of 39

25 #=ARR# ANALYTICAL RESULTS - RADIOCHEMISTRY Sample: Lab ID: 001 Collected: 11/28/16 10:40 Received: 11/29/16 10:20 Matrix: Water PWS: Site ID: Sample Type: Comments: Split off 500 ml amber un-preserved bottle for Tritium analysis. Upon receipt at the laboratory, the 12 mls of nitric acid were added to the 1 gallol sample container to meet the sample preservation requirement of ph <2 for radiochemistry analysis. s Method Act ± Unc (MDC) Carr Trac Units Analyzed CAS No. Qual Radon SM7500RnB ± 73.6 (71.9) C:NA T:NA Gross Alpha EPA U ± (1.64) C:NA T:NA Radium-226 EPA U ± (0.584) C:NA T:92% Radium-228 EPA U ± (1.04) C:68% T:84% Strontium-90 ASTM D U ± (0.465) C:97% T:NA Tritium EPA ± 138 (251) C:NA T:NA Total Uranium ASTM D U ± (0.193) C:NA T:NA pci/l 12/02/16 21: p pci/l 12/06/16 21: pci/l 12/15/16 10: pci/l 12/16/16 11: pci/l 12/08/16 20: N2 pci/l 12/09/16 17: ug/l 12/19/16 16: Page 18 of 32 Page 23 of 39

26 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water EPA Radium 228 Act ± Unc (MDC) Carr Trac Units Analyzed Radium ± (0.857) C:66% T:81% pci/l 12/16/16 11:35 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 19 of 32 Page 24 of 39

27 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: SM7500RnB-07 Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water SM7500RnB Rn B Radon Act ± Unc (MDC) Carr Trac Units Analyzed Radon 23.8 ± 19.9 (32.0) C:NA T:NA pci/l 12/02/16 21:22 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 20 of 32 Page 25 of 39

28 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water EPA Radium-226 Act ± Unc (MDC) Carr Trac Units Analyzed Radium ± (0.701) C:NA T:95% pci/l 12/15/16 10:09 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 21 of 32 Page 26 of 39

29 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: ASTM D Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water ASTM D ASTM D5811 Sr 89/90 Eichrom Act ± Unc (MDC) Carr Trac Units Analyzed Strontium ± (1.30) C:96% T:NA pci/l 12/08/16 13:29 N2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 22 of 32 Page 27 of 39

30 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water EPA Tritium Act ± Unc (MDC) Carr Trac Units Analyzed Tritium 82.6 ± 148 (252) C:NA T:NA pci/l 12/09/16 16:30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 23 of 32 Page 28 of 39

31 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: EPA Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water EPA Gross Alpha/Beta Act ± Unc (MDC) Carr Trac Units Analyzed Gross Alpha ± (1.63) C:NA T:NA pci/l 12/07/16 09:29 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 24 of 32 Page 29 of 39

32 #=QCR# QUALITY CONTROL - RADIOCHEMISTRY QC Batch: QC Batch Method: ASTM D Associated Lab Samples: 001 METHOD BLANK: Associated Lab Samples: 001 Analysis Method: Analysis Description: Matrix: Water ASTM D D Total Uranium KPA Act ± Unc (MDC) Carr Trac Units Analyzed Total Uranium ± (0.193) C:NA T:NA ug/l 12/19/16 15:55 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Page 25 of 32 Page 30 of 39

33 #=QL# QUALIFIERS DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Act - Activity Unc - Uncertainty: SDWA = 1.96 sigma count uncertainty, all other matrices = Expanded Uncertainty (95% confidence interval). Gamma Spec = Expanded Uncertainty (95.4% Confidence Interval) (MDC) - Minimum Detectable Concentration Trac - Tracer Recovery (%) Carr - Carrier Recovery (%) Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-O PASI-PA Pace Analytical Services - Ormond Beach Pace Analytical Services - Greensburg ANALYTE QUALIFIERS 1p Sample 001 from this analytical project was analyzed outside of the recommended Radon-222 hold time of four days. Results reported are decay corrected to the sample collection date and time supplied by the client. L0 Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter. R1 RPD value was outside control limits. S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis). Date: 12/20/ :20 AM Page 26 of 32 Page 31 of 39

34 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch EPA EPA EPA EPA EPA EPA EPA SM7500RnB EPA EPA EPA ASTM D EPA ASTM D EPA Date: 12/20/ :20 AM Page 27 of 32 Page 32 of 39

35 Page 33 of 39 Page 28 of 32

36 Page 34 of 39 Page 29 of 32

37 Page 35 of 39 Page 30 of 32

38 Page 36 of 39 Page 31 of 32

39 Page 37 of 39 Page 32 of 32

40 Page 39 of 39

41

42

43

44