STATE OF ILLINOIS ENVIRONMENTAL PROTECTION AGENCY NELAP - RECOGNIZED ENVIRONMENTAL LABORATORY ACCREDITATION. is hereby granted to

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STATE OF ILLINOIS ENVIRONMENTAL PROTECTION AGENCY NELAP - RECOGNIZED ENVIRONMENTAL LABORATORY ACCREDITATION is hereby granted to ALS GROUP USA CORP.

1 STATE OF ILLINOIS ENVIRONMENTAL PROTECTION AGENCY NELAP - RECOGNIZED ENVIRONMENTAL LABORATORY ACCREDITATION is hereby granted to ALS GROUP USA CORP. DBA ALS ENVIRONMENTAL - TX STANCLIFF ROAD, SUITE 210 HOUSTON, TX NELAP ACCREDITED ACCREDITATION NUMBER # According to the Illinois Administrative Code, Title 35, Subtitle A, Chapter II, Part 186, ACCREDITATION OF LABORATORIES FOR DRINKING WATER, WASTEWATER AND HAZARDOUS WASTES ANALYSIS, the State of Illinois formally recognizes that this laboratory is technically competent to perform the environmental analyses listed on the scope of accreditation detailed below. The laboratory agrees to perform all analyses listed on this scope of accreditation according to the Part 186 requirements and acknowledges that continued accreditation is dependent on successful ongoing compliance with the applicable requirements of Part 186. Please contact the Illinois EPA Environmental Laboratory Accreditation Program (IL ELAP) to verify the laboratory's scope of accreditation and accreditation status. Accreditation by the State of Illinois is not an endorsement or a guarantee of validity of the data generated by the laboratory. Primary Accrediting Authority: Texas Commission on Environmental Quality Celeste M. Crowley Acting Manager Environmental Laboratory Accreditation Program Rebecca Hambelton Accreditation Officer Environmental Laboratory Accreditation Program Expiration Date: 05/09/2018 Issued On: 03/31/2017 Page 1 of 13

2 to: According to the Illinois Administrative Code, Title 35, Subtitle A, Chapter II, Part 186, ACCREDITATION OF LABORATORIES FOR DRINKING WATER, WASTEWATER AND HAZARDOUS WASTES ANALYSIS, the State of Illinois formally recognizes that this laboratory is technically competent to perform the environmental analyses listed on the scope of accreditation detailed below. The laboratory agrees to perform all analyses listed on this scope of accreditation according to the Part 186 requirements and acknowledges that continued accreditation is dependent on successful ongoing compliance with the applicable requirements of Part 186. Please contact the Illinois EPA Environmental Laboratory Accreditation Program (IL ELAP) to verify the laboratory's scope of accreditation and accreditation status. Accreditation by the State of Illinois is not an endorsement or a guarantee of validity of the data generated by the laboratory. FOT Name: Drinking Water, Organic Method: USEPA1613RB Matrix Type: Potable Water Dioxin (2,3,7,8 TCDD) FOT Name: Non Potable Water, Organic Method: USEPA1613B 1,2,3,4,6,7,8-Heptachlorodibenzofuran 1,2,3,4,7,8,9-Heptachlorodibenzofuran 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin 1,2,3,7,8-Pentachlorodibenzo-p-dioxin 2,3,4,7,8-Pentachlorodibenzofuran 2,3,7,8-Tetrachlorodibenzo-p-dioxin Octachlorodibenzo-p-dioxin Total Heptachlorodibenzo-p-dioxin Total Hexachlorodibenzo-p-dioxin Total Pentachlorodibenzo-p-dioxin 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 1,2,3,4,7,8-Hexachlorodibenzofuran 1,2,3,6,7,8-Hexachlorodibenzofuran 1,2,3,7,8,9-Hexachlorodibenzofuran 1,2,3,7,8-Pentachlorodibenzofuran 2,3,4,6,7,8-Hexachlorodibenzofuran 2,3,7,8-Tetrachlorodibenzofuran Octachlorodibenzofuran Total Heptachlorodibenzofuran Total Hexachlorodibenzofuran Total Pentachlorodibenzofuran Total Tetrachlorodibenzofuran Total Tetrachlorodibenzo-p-dioxin Method: USEPA602 Benzene Ethylbenzene Toluene Method: USEPA608 4,4'-DDD 4,4'-DDT alpha-bhc Chlordane 4,4'-DDE Aldrin beta-bhc delta-bhc Thursday, March 30, 2017 Page 2 of 13

3 FOT Name: Non Potable Water, Organic Endosulfan I Endosulfan sulfate Method: USEPA608 Dieldrin Endosulfan II Endrin Endrin aldehyde Heptachlor Methoxychlor PCB-1221 PCB-1242 PCB-1254 gamma-bhc (Lindane) Heptachlor epoxide PCB-1016 PCB-1232 PCB-1248 PCB-1260 Toxaphene Method: USEPA624 1,1,1-Trichloroethane 1,1,2-Trichloroethane 1,1-Dichloroethene 1,2-Dichloroethane 1,3-Dichlorobenzene 2-Chloroethylvinyl ether Acrylonitrile Bromodichloromethane Bromomethane Chlorobenzene Chloroform cis-1,3-dichloropropene Dichloromethane (Methylene chloride) Methyl tert-butyl ether (MTBE) Toluene trans-1,3-dichloropropene Trichlorofluoromethane 1,1,2,2-Tetrachloroethane 1,1-Dichloroethane 1,2-Dichlorobenzene 1,2-Dichloropropane 1,4-Dichlorobenzene Acrolein (Propenal) Benzene Bromoform Carbon tetrachloride Chloroethane Chloromethane Dibromochloromethane Ethylbenzene Tetrachloroethene trans-1,2-dichloroethene Trichloroethene Vinyl chloride Xylenes (total) Method: USEPA625 1,2,4-Trichlorobenzene 1,3-Dichlorobenzene 1,2-Dichlorobenzene 1,4-Dichlorobenzene Thursday, March 30, 2017 Page 3 of 13

4 FOT Name: Non Potable Water, Organic Method: USEPA625 2,4,5-Trichlorophenol 2,4-Dichlorophenol 2,4-Dinitrophenol 2,6-Dinitrotoluene (2,6-DNT) 2-Chlorophenol 2-Nitrophenol 4-Bromophenyl phenyl ether 4-Chlorophenyl phenyl ether Acenaphthene Anthracene Benzo(a)anthracene Benzo(b)fluoranthene Benzo(k)fluoranthene Bis(2-chloroethoxy) methane Bis(2-ethylhexyl) phthalate Dibenz(a,h)anthracene Dimethyl phthalate Di-n-octyl phthalate Fluorene Hexachlorobutadiene Hexachloroethane Isophorone Nitrobenzene N-Nitrosodi-n-propylamine Pentachlorophenol Phenol 2,2-Oxybis (1-chloropropane) 2,4,6-Trichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene (2,4-DNT) 2-Chloronaphthalene 2-Methyl-4,6-dinitrophenol 3,3'-Dichlorobenzidine 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthylene Benzidine Benzo(a)pyrene Benzo(g,h,i)perylene Benzyl butyl phthalate Bis(2-chloroethyl) ether Chrysene Diethyl phthalate Di-n-butyl phthalate Fluoranthene Hexachlorobenzene Hexachlorocyclopentadiene Indeno(1,2,3-cd) pyrene Naphthalene N-Nitrosodimethylamine N-Nitrosodiphenylamine Phenanthrene Pyrene FOT Name: Solid and Chemical Materials, Inorganic Method: 1010A Ignitability Method: 1030 Matrix Type: SCM Ignitability of Solids Thursday, March 30, 2017 Page 4 of 13

5 FOT Name: Solid and Chemical Materials, Inorganic Method: 1311 TCLP (Organic and Inorganic) Method: 1312 Synthetic Precipitation Leaching Procedure Method: 6020A Aluminum Arsenic Beryllium Cadmium Chromium Copper Lead Manganese Nickel Selenium Sodium Vanadium Antimony Barium Boron Calcium Cobalt Iron Magnesium Molybdenum Potassium Silver Thallium Zinc Method: 7196A Chromium VI Method: 7470A Mercury Method: 7471B Matrix Type: SCM Mercury Method: 9012B Cyanide Method: 9014 Cyanide Thursday, March 30, 2017 Page 5 of 13

6 FOT Name: Solid and Chemical Materials, Inorganic Hydrogen Ion (ph) Method: 9045D Matrix Type: SCM Hydrogen Ion (ph) Method: 9050A Specific Conductance Method: 9056A Bromide Fluoride Nitrite Sulfate Method: 9060A Total Organic Carbon (TOC) Method: 9065 Phenolics Method: 9066 Phenolics Method: 9071B Matrix Type: SCM Oil and Grease Extractable Method: 9095B Matrix Type: SCM Paint Filter Method: 8011 Method: 9040C Chloride Nitrate Phosphate 1,2-Dibromo-3-chloropropane (DBCP) 1,2-Dibromoethane (EDB) Method: 8015C Thursday, March 30, 2017 Page 6 of 13

7 Method: 8015C 1-Propanol (n-propyl alcohol) Ethanol Isopropyl alcohol (2-Propanol) Diesel range organics (DRO) Gasoline range organics (GRO) Methanol t-butyl alcohol (TBA) Method: 8021B Benzene MTBE (Methyl-t-butyl ether) o-xylene Toluene Ethylbenzene m-xylene p-xylene Total Xylenes Method: 8081B Hexachlorobenzene 4,4'-DDD 4,4'-DDT alpha-bhc beta-bhc delta-bhc Endosulfan I Endosulfan sulfate Endrin aldehyde gamma-bhc (Lindane) Heptachlor Methoxychlor 4,4'-DDE Aldrin alpha-chlordane Chlordane - not otherwise specified Dieldrin Endosulfan II Endrin Endrin ketone gamma-chlordane Heptachlor epoxide Mirex Toxaphene Method: 8082A PCB-1016 PCB-1232 PCB-1248 PCB-1221 PCB-1242 PCB-1254 PCB-1260 Method: 8151A Thursday, March 30, 2017 Page 7 of 13

8 2,4,5-T 2,4-D Dalapon Dichloroprop MCPA Method: 8260C 2-Pentanone Method: 8151A 2,4,5-TP (Silvex) 2,4-DB Dicamba Dinoseb MCPP Allyl alcohol Diisopropyl ether (DIPE) Ethyl tert-butyl ether (ETBE) t-amyl methyl ether (TAME) 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 1,1-Dichloroethane 1,1-Dichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-Dibromoethane 1,2-Dichloroethane 1,3,5-Trimethylbenzene 1,3-Dichloropropane 1,4-Dioxane 1-Propanol 2-Butanone (MEK) 2-Chlorotoluene 2-Propanol 4-Methyl-2-pentanone (MIBK) Acetonitrile Acrylonitrile Benzene Bromobenzene Bromodichloromethane Bromomethane Carbon tetrachloride 1,1,1-Trichloroethane 1,1,2-Trichloroethane 1,1-Dichloroethene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2-Dibromo-3-chloropropane 1,2-Dichlorobenzene 1,2-Dichloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Chlorohexane 2,2-Dichloropropane 2-Chloroethyl vinyl ether 2-Hexanone 4-Chlorotoluene Acetone Acrolein (Propenal) Allyl chloride Benzyl chloride Bromochloromethane Bromoform Carbon disulfide Chlorobenzene Thursday, March 30, 2017 Page 8 of 13

9 Method: 8260C Chloroethane Chloromethane cis-1,2-dichloroethene Dibromomethane Diethyl ether Ethanol Ethyl methacrylate Ethylene oxide Iodomethane Isopropylbenzene Methyl acrylate Methyl tert-butyl ether (MTBE) Methylene chloride Naphthalene n-butylbenzene o-xylene p-isopropyltoluene p-xylene sec-butylbenzene t-butyl alcohol Tetrachloroethene trans-1,2-dichloroethene trans-1,4-dichloro-2-butene Trichlorofluoromethane Chlorodibromomethane Chloroform Chloroprene cis-1,3-dichloropropene Dichlorodifluoromethane Epichlorohydrin Ethyl acetate Ethylbenzene Hexachlorobutadiene Isobutyl alcohol Methacrylonitrile Methyl methacrylate Methylcyclohexane m-xylene n-butanol n-propylbenzene Pentachloroethane Propionitrile (ethyl cyanide) Pyridine Styrene tert-butylbenzene Toluene trans-1,3-dichloropropene Trichloroethene Vinyl acetate Vinyl chloride Method: 8270D 4-Nitrobiphenyl Captan Dimethylaminoazobenzene Ethion Maleic anhydride Phosmet Resorcinol 5-Chloro-2-methylaniline Coumaphos Dioxathion Famphur Naled Phthalic anhydride Trifluralin Thursday, March 30, 2017 Page 9 of 13

10 Method: 8270D 1,2,4,5-Tetrachlorobenzene 1,2-Dibromo-3-chloropropane (DBCP) 1,2-Dinitrobenzene 1,3,5-Trinitrobenzene (1,3,5-TNB) 1,3-Dinitrobenzene (1,3-DNB) 1,4-Dinitrobenzene 1,4-Phenylenediamine 1-Naphthylamine 2,3,4,6-Tetrachlorophenol 2,4,5-Trimethylaniline 2,4-Diaminotoluene 2,4-Dimethylphenol 2,4-Dinitrotoluene (2,4-DNT) 2,6-Dinitrotoluene (2,6-DNT) 2-Chloronaphthalene 2-Methylnaphthalene 2-Methylpyridine (2-Picoline) 2-Nitroaniline 3,3'-Dichlorobenzidine 3-Methylcholanthrene 3-Nitroaniline 4-Aminobiphenyl 4-Chloro-3-methylphenol 4-Chlorophenyl phenyl ether 4-Nitroaniline 4-Nitroquinoline-1-oxide 7,12-Dimethylbenz(a)anthracene Acenaphthylene alpha,alpha-dimethylphenethylamine Anthracene Azinphos-methyl Benzo(a)anthracene Benzo(b)fluoranthene Benzo(k)fluoranthene 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,2-Diphenylhydrazine 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Naphthoquinone 1-Chloronaphthalene 2,2-Oxybis (1-chloropropane) 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dinitrophenol 2,6-Dichlorophenol 2-Acetylaminofluorene 2-Chlorophenol 2-Methylphenol (o-cresol) 2-Naphthylamine 2-Nitrophenol 3,3'-Dimethylbenzidine 3-Methylphenol (m-cresol) 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether 4-Chloroaniline 4-Methylphenol (p-cresol) 4-Nitrophenol 5-Nitro-o-toluidine Acenaphthene Acetophenone Aniline Aramite Benzidine Benzo(a)pyrene Benzo(g,h,i)perlyene Benzoic acid Thursday, March 30, 2017 Page 10 of 13

11 Method: 8270D Benzyl alcohol Bis(2-chloroethoxy) methane Bis(2-ethylhexyl) phthalate Carbaryl (Sevin) Carbophenothion Chrysene Diallate Dibenz(a,j)acridine Dichlorovos Dimethoate Di-n-butyl phthalate Dinoseb Disulfoton Fluoranthene Hexachlorobenzene Hexachlorocyclopentadiene Hexachlorophene Indeno(1,2,3-cd) pyrene Isophorone Kepone Methapyrilene Methyl parathion Naphthalene Nitroquinoline-1-oxide N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosomethylethylamine N-Nitrosopiperidine O,O,O-Triethyl phosphorothioate o-cresol (2-Methylphenol) Parathion p-cresol (4-Methylphenol) Pentachloronitrobenzene Phenacetin Phenol Bis(2-chloroethyl) ether Butyl benzyl phthalate Carbazole Chlorobenzilate Demeton Dibenz(a,h)anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Diphenylamine Ethyl methanesulfonate Fluorene Hexachlorobutadiene Hexachloroethane Hexachloropropene Isodrin Isosafrole m-cresol (3-Methylphenol) Methyl methanesulfonate Mevinphos Nitrobenzene N-Nitrosodiethylamine N-Nitrosodi-n-butylamine (N-Nitrosodibutylamine) N-Nitrosodiphenylamine N-Nitrosomorpholine N-Nitrosopyrrolidine o-anisidine o-toluidine p-cresidine Pentachlorobenzene Pentachlorophenol Phenanthrene Phorate Thursday, March 30, 2017 Page 11 of 13

12 Pyrene Safrole Method: 8270D Pronamide Pyridine Terbufos Tetrachlorvinphos (Stirophos) Thiophenol (Benzenethiol) Thionazine (Zinophos) Toluene diisocyanate Matrix Type: SCM Dibenzo(a,e)pyrene Malathion Method: 8280B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF) 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF) 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF) 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF) 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF) 2,3,7,8-Tetrachlorodibenzofuran (TCDF) Total Heptachlorodibenzofuran (HpCDF) Total Hexachlorodibenzofuran (HxCDF) Total Pentachlorodibenzofuran (PeCDF) Total Tetrachlorodibenzofuran (TCDF) 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD) 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD) 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,6,7,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD) 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF) 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD) Total Heptachlorodibenzo-p-dioxin (HpCDD) Total Hexachlorodibenzo-p-dioxin (HxCDD) Total Pentachlorodibenzo-p-dioxin (PeCDD) Total Tetrachlorodibenzo-p-dioxin (TCDD) Method: 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF) 1,2,3,4,6,7,8-Heptachlorodibenzofuran (HpCDF) 1,2,3,4,7,8,9-Heptachlorodibenzofuran (HpCDF) 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,7,8-Pentachlorodibenzo-p-dioxin (PeCDD) 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF) 2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD) Total Heptachlorodibenzo-p-dioxin (HpCDD) Total Hexachlorodibenzo-p-dioxin (HxCDD) 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD) 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (HpCDD) 1,2,3,4,7,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,6,7,8-Hexachlorodibenzofuran (HxCDF) 1,2,3,7,8,9-Hexachlorodibenzofuran (HxCDF) 1,2,3,7,8-Pentachlorodibenzofuran (PeCDF) 2,3,4,6,7,8-Hexachlorodibenzofuran (HxCDF) 2,3,7,8-Tetrachlorodibenzofuran (TCDF) Total Heptachlorodibenzofuran (HpCDF) Total Hexachlorodibenzofuran (HxCDF) Total Pentachlorodibenzofuran (PeCDF) Thursday, March 30, 2017 Page 12 of 13

13 Method: 8290A Total Tetrachlorodibenzofuran (TCDF) Total Pentachlorodibenzo-p-dioxin (PeCDD) Total Tetrachlorodibenzo-p-dioxin (TCDD) Method: 8315A Formaldehyde Method: 8316 Acrylamide Method: 8330A 1,3,5-Trinitrobenzene (1,3,5-TNB) 2,4,6-Trinitrotoluene 2,4-Dinitrotoluene (2,4-DNT) 2-Amino-4,6-dinitrotoluene (2-Am-DNT) 3-Nitrotoluene (3-NT) 4-Nitrotoluene (4-NT) Methyl-2,4,6-trinitrophenylnitramine (Tetryl) 1,3-Dinitrobenzene (1,3-DNB) 2,4,6-Trinitrotoluene (2,4,6-TNT) 2,6-Dinitrotoluene (2,6-DNT) 2-Nitrotoluene (2-NT) 4-Amino-2,6-dinitrotoluene (4-Am-DNT) Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) Nitrobenzene Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine(HMX Thursday, March 30, 2017 Page 13 of 13

Methods and Analytes Requiring Laboratory Certification Attachment 3

Methods and Analytes Requiring Laboratory Certification Attachment 3 s and s Requiring Laboratory Certification Attachment 3 Current as of July 1, 2011 Laboratory Certificates need to accurately reflect the methods performed and reported by the laboratory, including the