Analytical Services for Innovative Materials Research
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1 Applied and Analytical Chemistry Analytical Services for Innovative Materials Research Prof. Dr. Robert Carleer, Dr. ir. Pieter Samyn Contact : Pieter.Samyn@uhasselt.be Agoralaan Gebouw D B-3590 Diepenbeek Belgium
2 Institute of Materials Research IMO - IMOMEC focusses on the study of advanced material systems to contribute by innovation to the societal drivers of our time and region, develops synergies between fundamental/basic research and applied research until achieving technological innovation with economic valorization potential.
3 Institute of Materials Research IMO - IMOMEC Inorganic and physical chemistry Design and synthesis of organic semiconductors Biomolecule design group NMR spectroscopy Applied and Analytical Chemistry Functional materials manufacturing Packaging technology center Polymer Reaction design group Chemistry Electrical & physical characterization Engineering Energy Systems Engineering Biomedical Device Engineering Battery Technology Nanobionics and soft matter interfaces Nano structure physics Physics Wide bandgap materials Nanophotonis and nanofabrication Organic and nanostructured electronics Energy and materials interfaces
4 Applied & Analytical Chemistry (TANC) Development of analytical strategies and dedicated analytical methods for the study of advanced material systems with focus on (bio)polymers, rubbers, resins and coatings using complementary (hyphenated) analytical techniques. Fundamental & Applied & Contract Research on new applications, processing, performance, sustainability Environmentally-oriented Research: contaminants & side-stream valorization Chemical Analysis Material Composition Material Processing Physical Analysis Mechanical Analysis Structure vs. Property Relationships Application Optimization through definition of expert systems Prof. Dr. Robert Carleer Dr. Ir. Pieter Samym Prof. Dr. Em. Jan Yperman Prof. Dr. Peter Adriaensens (NMR spectroscopy) 6 Ph.D. students 6 Sr. Researchers 6 Sr Technicians
5 Analytical Expertise Elemental Analysis Chromatography Spectroscopy Rheology AAS ICP-OES ICP-MS XRF IC GC GC-MS HPLC GPC LC-MS NMR FTIR UV-VIS-NIR MS Raman Plate Cone Thermal Analysis DSC TGA DMA TMA Coupled Techniques Headspace-, thermal desorption-, pyrolysis GC-MS, IC-ICP-MS FT-IR microscopy TG coupled techniques TG-FT-IR,TG-MS, TG-TD-GC-MS
6 Case Studies Particle detection and characterization Real-time single nanoparticle ICP-MS (µs measuring times!) - elemental composition (< ppb) - number of particles - particle size - particle size distribution Traditional Particle size & stability - micro- to nanometer particle size - field flow fractionation - zetapotential measurements Applications - drinkwater, waste-water - blood, urine - processing liquids - corrosion - extracts of solid materials - slurries of abrasive polishing - cosmetics
7 Case Studies Processing behaviour and composition of polymers Study of thermal features and properties of polymers (VOC, cure behaviour, degradation, fogging, ) Material failure analysis & troubleshooting (die and mould contamination, adhesion problems, processing problems) Analysis of additives as a function of the emission of volatile components Doublesided tape with recycling abilities TG-FTIR Wastefree degreasing proces with guaranteed high degreasing speed and -quality Low formaldehyde emitting glues for wood Delamination of PVC on MDF board Phenolic resins, UF resins, foams Adhesion problems Contaminants Coating defects Rheological instability in polymer coatings TG-MS
8 Core Research Topics: Pyrolysis Valorization of materials from contaminated biomass (with heavy metals) or organic rest streams (biomass/biopolymers) into value-added products by using (co-) pyrolysis techniques (biochar, activated carbon, electrodes) Chemical and energetical valorization of pyrolysis products (recycling heavy metals): - upgrade bio-oil as a secondary feedstock with added value for the preparation of chemicals - validate the bio-oil as a bio-fuel with higher heating value and to obtain a more homogeneous composition, free of heavy metals and with low concentration of pyrolyitc water Improving yields of bio-oil Char residue where all heavy metals are accumulated and concentrated.
9 Core Research Topics: Bio-based Materials Valorization of side-products from paper and pulp industry: Nanocellulose (CNW/MFC) and lignin products Paper products with engineering properties (bio-based barrier coatings, surface properties, high-strength papers, functional papers) Rheology, Processing and characterization of bio-based nanocomposites (PHB, PLA) Organic nanoparticles with encapsulation & controlled release
10 Contact us Applied & Analytical Research Group (TANC) University Hasselt Prof. Dr. Robert Carleer Dr. ir. Pieter Samyn Agoralaan Gebouw D Campus Diepenbeek tel +32 (0) fax +32 (
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