RESEARCH LABORATORIES

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RESEARCH LABORATORIES LABORATORY OF SOLID STATE CHEMISTRY AND CATALYSIS Head: Prof. Lionel Montagne, lionel.montagne@univ-lille1.fr Team 1 : SOLID STATE CHEMISTRY Team director : Prof.

1 RESEARCH LABORATORIES LABORATORY OF SOLID STATE CHEMISTRY AND CATALYSIS Head: Prof. Lionel Montagne, Team 1 : SOLID STATE CHEMISTRY Team director : Prof. Rose-Noëlle VANNIER (rose-noelle.vannier@ensc-lille.fr) Phone : École Nationale Supérieure de Chimie de Lille Avenue Mendeleïev Bâtiment C7a BP VILLENEUVE D ASCQ CEDEX Research Fields: Solid State Chemistry Ionic, electronic and mixed conductors, ferroelectric Precursors and new routes for oxide synthesis Solid Oxide Fuel Cell, Electrochemical separation of gas Glasses Materials for nuclear applications Solid State NMR Scientific equipment: X-ray diffraction platform (powder diffractometers, Four circle and CCD X-ray single crystal diffractometers, High temperature X-ray diffraction (up to 1200 C with controlled atmospheres) Thermal analysis Impedance spectroscopy, Ionic transport number measurements Solid State NMR Electron microscopy Key-words : Ceramics Fuel cells Crystal structure determination Electrical properties Magnetic properties Glasses Solid State NMR Main fields of applications: Gas separation Energy storage and savings Electrochemical membranes Refractory materials and glasses Environment

2 Team 2 : HETEROGENEOUS CATALYSIS Team director : Prof. Pascal GRANGER (pascal.granger@univ-lille1.fr ) Phone : Addresses : Université des Sciences et Technologies de Lille Bâtiment C3 École Nationale Supérieure de Chimie de Lille Bâtiment C7 Ecole Centrale de Lille Cité Scientifique VILLENEUVE D ASCQ Research Fields: Novel synthesis of ordered mesoporous functionalized catalysts with controlled nanosized metallic and oxidic particles. Advanced surface analysis and operando spectroscopic characterization Molecular modelling and reaction mechanisms Chemical engineering kinetics and reactor modelling, structured reactors, powder technologies All those competencies are profitably used in various practical applications dedicated to the production of clean fuels (hydrotreating and Fischer-Tropsch reactions), biomass and light alkanes conversion for the production of valuables intermediates and environmental catalysis (denox, den 2 O, COV) Surface analysis: XPS/LEIS/Tof-SIMS coupled to a catalytic cell working under controlled atmosphere up to 800 C. Raman and infrared spectrometers for in situ and operando investigations Thermal analysis (Thermogravimetry, DSC TPR/TPO, adsorption of probe molecules/therodesorpion) Catalytic reactor (CSTR, plug flow slurry reactors running under atmospheric at high pressure with online analytical systems. Devices for the preparation and analysis of powder catalysts. Key words : Hydrocarbon activation, biomass conversion, Fischer-Tropsch, hydrotreating reaction catalytic depollution, molecular modelling, surface analysis Main fields of applications: Petrochemistry, fine chemistry, energy production, atmospheric pollutant abatement

3 Team 3: Catalysis and Molecular Chemistry Team director: Dr Francine AGBOSSOU-NIEDERCORN ) Phone: École Nationale Supérieure de Chimie de Lille Avenue Mendeleïev Bâtiment C7a BP VILLENEUVE D ASCQ CEDEX Research Fields: Synthesis and application of homogeneous organometallic catalysts Hydrogenation, carbonylation, hydroformylation, C-C, C-O and C-N bond formation, oligomerization and polymerization Organic synthesis Surface organometallic complexes and catalysts Supramolecular catalysis Polymerization catalysis These research fields aim at applying homogeneous catalysis to the production of fine chemicals, clean processes, and polymeric materials. Catalytic reactors (high pressure autoclaves, multiclaves, polymerisation reactors) Glove-boxes and synthesis under controlled atmosphere equipments GC and HPLC chromatographs, FTIR, elemental analysis Key words : Homogeneous catalysis, fine chemistry, organometallic complexes, polymerization, organic synthesis Main fields of applications: Fine chemistry, polymeric materials, pharmaceutical industry

4 UNITE MATERIAUX ET TRANSFORMATIONS UMR CNRS 8207 Director : Prof. Alexandre LEGRIS (alexandre.legris@univ-lille1.fr) Phone : Fax : Université des Sciences et Technologies de Lille Bâtiment C Villeneuve d Ascq Team 1 : «ENGINEERING POLYMERS» Director: Prof. Jean-Marc LEFEBVRE (jean-marc.lefebvre@univ-lille1.fr) Phone : +33 (0) Fax : +33 (0) Thematics Engineering of flame retardancy of materials (Prof. S. Bourbigot) Engineering and processing of filled polymers and nanocomposites: Intumescent systems, ceramization, synergy, synthesis of FRs Polymer nanocomposites (organomodified clays, LDH, carbon nanotubes, POSS, metal oxides ) Reactive extrusion Modeling and simulation of flame retarded materials: Development of experimental protocol at the small scale Kinetic analysis Modeling (burning polymer, heat barrier) Sustainable materials Recycling Biopolymer, bionanocomposite Engineering of surface treatment (Prof. M. Traisnel) Biomaterials Surface modification/coating by chemical way (sol-gel + chemisorption of corrosion inhibitors) Surface modification /Coating by physical way (cold plasma + flaming) Adhesion Equipment Processing Twin screw extruder Single screw extruder Mixers (350 cc, 50cc) equipped with N 2 chamber Micro extruder equipped for making film and monofilament (Film, Micro melt spinning machine) Fire testing Limiting oxygen index UL-94 Mass loss calorimeter Small furnace Heat radiator test

5 Thermal analyses DSC and MDSC (including k = f(t)) TGA at high temperature (1550 C) Very high heating rate TGA (up to 500 C/min) Simultaneous TGA/DSC TC probe (thermal effusivity) Surface treatment Cold plasma (radiofrequency and microwave) equipped with different chambers Spraying machine Coating machine Padding machine Contact angle meter Microscopies Optical microscopes Electronic microprobe SEM with EDX TEM AFM Spectroscopy Liquid/solid state NMR (100, 300, 400, 800 MHz) XRD XPS ESR FTIR To summarize Reaction and resistance to fire Anti-corrosion Biocompatibility Adhesion Modification and functionalisation of surfaces Surface treatment Properties Characterization Field of expertise Materials Spectroscopy: NMR, FTIR, ESR, XPS. Microscopy: Optical, SEM, TEM, AFM, microprobe Thermal analyses: TGA, DTA, DSC, DMA Fire testing Modeling and simulation Processing of polymers (including reactive extrusion) Material (bulk and surface) chemistry

6 Team 2: PHYSICAL METALLURGY AND MATERIALS ENGINEERING Team director: Prof. Alexandre LEGRIS Phone : Université des Sciences et Technologies de Lille Bâtiment C VILLENEUVE D ASCQ CEDEX Erasmus contact : Prof. Jean-Bernard VOGT (jean-bernard.vogt@ensc-lille.fr) Research Fields : Physical mechanisms of phase transformations in metallic alloys, near or far from thermodynamical equilibrium, with or without presence of external solicitations (impact, irradiation, mechanical stress). Reliability of metallic alloys with or without presence of corrosive environment (fatigue, liquid metal embrittlement, environmentally assisted damage). Simulation and Modelling of radiation damage Processing and characterization of ceramics through non stand procedures : 1. composite coating by sol-gel process on metals and ceramics 2. structural and thermo mechanical characterisations of ceramics obtained by Spark Plasma Sintering (SPS) X Ray diffractometer Transmission and reflection Mössbauer Spectrometer Scanning electron microscope equipped with EDX and EBSD detectors Atomic Force Microscopes Optical microscope and image collection system Dilatometer Electrochemical equipment Micro- and macro-indentation Tensile and fatigue machines equipped with extensometers, furnaces and environmental cells Experimental set-up for testing metallic alloys in liquid metals (lead, sodium...) Nitriding facilities and galvanisation unit High energy mill, cold roller Heat treatment furnaces Keys-words : Mechanical tests and fracture analysis Microscopies -metallography Mössbauer spectroscopy Corrosion Microstructure-galvanisation Structural alloys Main fields of applications : Metallurgy Steel making Nuclear industry Energy Transportation industry Battery

7 Laboratory of Organic and Macromolecular Chemistry Director and Erasmus contact : Prof. Jean-Marie AUBRY (jean-marie.aubry@ensc-lille.fr) Phone : Fax : Equipe d Accueil Chimie Moléculaire et Formulation BP Bâtiment C7, Cité Scientifique Villeneuve d Ascq cedex, France Research Fields : Pro and anti oxidant molecules Organic synthesis, reactivity, functionnalization Water soluble polymers with complexing properties Photo and radiochemistry on polymers Studies of photochemical reactions by NMR Singlet Oxygen Free radicals Formulation Polyphenols UV, Visible, IR and IRTF spectrophotometers Spectrofluorimetry Phosphorimeter Photoreactive cells Chromatographic devices Potentiostat. Galvanostat Electron beam (175kV) UV sources Dynamometers Goniometry Specific area measurements Treatments of textile EPR NMR Key-words : Alcaloïds Macromolecules Antioxidant molecules Singlet oygen Pro-oxidant complexes - Photochemistry Water soluble polymers Free radicals Main fields of applications : Polymeric materials Pharmaceutical industry Surfactants Cosmetics Paints and varnishes

MICROSTRUCTURE-BASED PROCESS ENGINEERING AND CATALYSIS

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