X-Ray & Thermal Analysis Unit. Unit Pengurusan Makmal Universiti Blok T03 Bangunan UIRL Universiti Teknologi Malaysia Skudai Johor
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1 X-Ray & Thermal Analysis Unit Unit Pengurusan Makmal Universiti Blok T03 Bangunan UIRL Universiti Teknologi Malaysia Skudai Johor
2 Contents Introduction Team Members Laboratory Instrument XPS XRD TGA DSC TGA FTIR RAMAN AFM Operating Hours Contact Us
3 Introduction 5 staff 6 Laboratories 11 Instruments
4 Team Members
5 Laboratories Laboratory : Advanced X-ray Photoelectron Spectroscopy Laboratory ( Room no : ) Instrument : X-Ray Photoelectron Spectroscopy (XPS) Laboratory : Advanced X-ray Spectroscopy Laboratory (Room no : ) Instrument : Small Angle X-Ray Scattering (SAXS) Laboratory : Advanced X-ray Diffractometer Laboratory ( ) Instrument : X-Ray Diffraction (XRD) Laboratory : Advanced Optical Microscope & Nano Raman Photoluminescene Laboratory (( ) Instrument : Raman Xplora Plus (Raman- AFM) Laboratory : Advanced Optical Microscope & Nano Raman Photoluminescene Laboratory (( ) Instrument : Atomic Force Microscopy (AFM) Laboratory : Advanced Optical Microscope & Nano Raman Photoluminescene Laboratory (( ) Instrument : Raman LabRAM HR Evolution (Raman) Laboratory : Thermal Analysis Laboratory (T ) Instrument : Thermogravimetry Analyzer Interface With FTIR (TGA-IR) Laboratory : Thermal Analysis Laboratory (T ) Instrument : Thermogravimetry Analyzer With DSC (TGA-DSC)
6 X-Ray Photoelectron Spektroscopy ( XPS) Brand : Shimadzu Model : AXIS ULTRA DLD Location : Advanced X-ray Photoelectron Spectroscopy Laboratory Person In Charge : Amy Zuria amyzuria@utm.my Siti Zhahara szhahara@utm.my
7 Function Chemical element detection C 1s, O 1s, Cu 2p, N 1s Composition of chemical element Binding energy
8 Type of sample Non Organic Metal Semiconducter Polymer Ceramic Sample size : Not more than 2cm x 2cm for solid. Thickness not more than 1cm. Amount required : Small amount (about 5g only).
9 Rigaku Smartlab Brand Model : Rigaku Smartlab : Smartlab Location : Advanced X-ray Diffraction Laboratory Person In Charge : Amy Zuria amyzuria@utm.my Mohd Izzam m.izzam@utm.my
10
11 Type of sample 20 x 20 x 0.5 mm Fine Powder Sample Stage Film Thin Film Powder Solid Film
12 Thermogravimetry With Fourier Transform Infrared Brand : TA Instrument Model : Q500 Location : Molecular Spectroscopy Laboratory Person In Charge : Amy Zuria amyzuria@utm.my Mr Muhamad Arif m.arifmislet@utm.my
13 Function Spectrum of absorption Emission Functional Group Weight Loss
14 Type of sample Solid Powder Liquid 5 to 25 mg
15 Thermogravimetry With DSC Brand : Pelkin Elmer Model : STA8000 (Simultaneous Thermal Analysis) Location : Molecular Spectroscopy Laboratory Person In Charge : Amy Zuria amyzuria@utm.my Mr Muhamad Arif m.arifmislet@utm.my
16 Function Weight change and heatflow measured under perfect identical test conditions with a TGA/DSC deliver more information about composition, phase transitions and chemical reactions. Measures both heat flow (Differential Scanning Calorimetry) and weight changes (thermogravimetry) in a material as a function of temperature or time in a controlled atmosphere.
17 Type of sample Solid Powder Liquid 5 to 25 mg
18 Labram Hr Evolution Brand : Horiba Scientific Model : Labram hr evolution Location : Advanced Nano Raman Photolumeniscence laboratory Person In Charge : Md Razali Rehat -mdrazali@utm.my Amy Zuria amyzuria@utm.my
19 Type of sample Solid (1 x 1 cm) Powder (1 mg) Liquid (10 ml) Laser Type Visible (633 nm): Helium Neon Ultra violet (325 nm) : He-Cd
20 XpLoRA PLUS Brand : Horiba Scientific Model : XpLoRA PLUS Location : Advanced Nano Raman Photolumeniscence laboratory Person In Charge : Md Razali Rehat -mdrazali@utm.my Amy Zuria amyzuria@utm.my
21 Type of sample Solid Powder (1 x 1 cm) 1 mg Laser Type 532 nm, 20-25mW 785 nm, 100mW
22 Function
23 Atomic Force Microscopy Brand : Zeiss Model : JPK Instrument Location : Advanced Nano Raman Photolumeniscence laboratory Person In Charge : Mohd Izzam Bin Idrus m.izzam@utm.my Amy Zuria amyzuria@utm.my
24 Type of sample Solid Powder (Max : 2 x 7 cm X 4mm) 1 mg Dry Sample Non Sticky
25 Function To measure a roughness of a sample surface at a high resolution, in order to distinguish a sample based on its mechanical properties.
26 Operating Hours Sun- Wed : 08.30am-05.00pm (Run & Analysis Sample ) Thursday : 08.30am-03.30pm (For appointment & consultation only)
27 Contact us For more inquiries & details, you can contact : Pn Amy Zuria Binti Abdul Ajid Senior Science Officer University Industry Research Laboratory Universiti Teknologi Malaysia. Ext : amyzuria@utm.my Laboratory : XPS & XRD : RAMAN AFM : TGA : SAXS :
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