How to Use the Devices in the Analytical Instrument Laboratory

Transcription

1 How to Use the Devices in the Analytical Instrument Laboratory 1. Eligible users To be eligible, the user must be a member of the faculty or staff, a researcher, or a Waseda University student. If the user is a student, the student is required to obtain the supervising faculty member s approval stamp. 2. Available hours of use Weekdays from 9:00 to 17:00. However, it is closed during the lunch break (12:30 to 13:30). 3. Procedures for making a reservation (If the reservation date is a weekend or holiday, the following weekday will be set as the reservation date) Requests for a reservation will be accepted at the Analytical Instrument Staff Room (Room 304 on the 3rd floor of Building ). Analyzers (excluding the focused ion beam machining device [FIB]) (for 2 weeks) Assemble at 9:30 Users must discuss with other users the date of use for each device they wish to use (No one is granted exclusive use of any device) Fill out the required items on the Application for the Use of a Device and receive a Reservation Slip. Appear at the Staff Room on the day of use. Make sure to bring along the Reservation Slip. (The supervising faculty member s approval stamp is required) After using the device, fill out the required items on the Device Usage Record and the Reservation Slip. Promptly submit the Reservation Slip. (Do not forget the supervising faculty member s approval stamp.) Caution: The Staff Room will only accept requests to process using FIB. The request must be made in person, bringing your sample, during opening hours. Requests made by phone and other similar means will not be accepted.

2 4. Out-of-hours use (As a general rule, no one is allowed to use any of the devices out of hours.) Only users approved by the said Staff Room can use the device out of hours. Before using any device out of hours, the user is required to submit an All-night, Extended, Weekend, or Holiday Use Notification (the supervising faculty member's approval stamp is required) to the appropriate Staff Room. In addition, when using out of hours, it must be used by two or more people to minimize the danger that might result from unexpected accidents, etc. Caution: Any problems arising during out-of-hours use will be the full responsibility of the lab team that was using the room at the time. As a general rule, users from research labs outside Zaiken will not be allowed to use the devices out of hours. If a user from a research lab outside Zaiken wishes to use the devices out of hours for a special reason (for example, for a series of experiments), please submit the Request for Out-of-Hours Use of a Facility in advance. 5. Cautions No smoking, eating, or drinking in the laboratories. No one will be allowed to use more than one device at the same time. When cancelling, make sure to always notify the Staff Room in advance. These are joint use devices. Please clean the device after use. When you have finished, promptly report the fact to the Staff Room. Do not bring any chemicals, high pressure gases, experimental, or other objects into the laboratory without permission.

3 List of Joint-Use Facilities c. Analytical Instrument Laboratory Reception 304, the 3 rd Floor of Building the Analytical Instrument Lab. Staff Room (ext ) Device name High-resolution scanning electron microscope: Hitachi HR-FE-SEM S-5500 Thermal field emission type scanning electron microscope(fe-sem) Analysis on request JEOL JSM-7800F PRIME Automatic gas adsorption measurement [AUTOSORB] Quantachrome Instruments IMP/wk3:, iq2mpxr: Focused ion beam machining device (FIB) Processing on request JEOL JIB-4000 Scanning electron microscope (with low vacuum capability)(lv-sem) JEOL JSM-5500 LV 3D digital microscope KEYENCE VHX-5000 Optical microscope (with camera attached): Nikon L150 Thermal field emission type scanning electron microscope(fe-sem) 001B 001B 001B 202 JEOL JSM-7001F 203 Energy dispersive X-ray analyzer(eds) JEOL JED-2300F Transmission electron microscope (TEM 200 kev) JEOL JEM-2010 License required. If you do not have a license: Thermal field emission type scanning electron microscope (FE-SEM) JEOL JSM-6500F Energy-dispersive X-ray analyzer (EDS) JEOL JED-2300F Cathode luminescence analyzer (CL) GATAN MonoCL3 Cooling stage Shared darkroom (development, enlargement, etc.) Mihou Nakajima Every other Monday Anytime Every other Monday Analytical Instrument Staff Room s bulletin board and webpage See Attachment 5-2 for the procedures for using the devices Consultation on the use of devices: Usually on Mondays 1,500 /hour 5,000 /hour Consumables: 1,000, 1,500, or 3,000 Plus 250 /hour Plus 250 /hour Plus 250 /hour (excluding consumables) Electron probe microanalyzer (EPMA) JEOL JXA (W) 1,000 /hour (LaB6) 1,500 /hour

4 Device name Sample preparation devices Automatic polisher, hot mounting press, cold mounting press, Handy-lap (precise surface polisher), polishing machine, ultrasonic disc cutter, precision cutting machine, dimple grinder, electronic balance, belt grinder, laboratory hotplate, gas burner, ultrasonic cleaner, optical microscope, etc. 208 Field emission Auger electron spectroscopy (AES) JEOL JAMP-9500F Imaging plate reader (IP READER) FUJIFILM FDL-5000 Image analyzers Electron backscattering diffraction device(ebsp) TSL OIM 7 OIM Analysis 4 Analysis Station DigitalMicrograph Image-Pro PLUS Photoshop (For reading TEM films) Premiere Origin Pro 9.0J Mac Tempas Crystal Kit Image Gauge L-Process etc. PDXL (for searching the ICDD database and for X-ray powder diffraction, qualitative) Photoelectron spectrometer(esca) JEOL JPS-9010 Field emission scanning transmission electron microscope(fe-stem) JEOL JEM-2100F Energy-dispersive X-ray analyzer(eds) JEOL JED-2300T Mihou Nakajima Analytical Instrument Staff Room s bulletin 1,500 /hour 1,500 /hour See Attachment 5-2 for the procedures 2,000 /hour Plus Transmission electron microscope (TEM 300 kev) JEOL JEM-3010 License required. If you do not have a license: / full film 150 / half film 200 / imaging plate

5 Device name Ultraviolet and visible spectrophotometer (UV VIS) PerkinElmer Lambda 650 Micro-Fourier transform infrared spectrometer (MICRO FT-IR) PerkinElmer AutoIMAGE Dynamic light scattering particle size distribution analyzer [DLSPSA] HORIBA LB-550 Surface roughness tester HORIBA Dektak 6M Epifluorescence microscope Olympus BX Focused ion beam machining device (FIB) Processing per request SII SMI 2050 Transmission electron microscope 302A (TEM100 kev) JEOL JEM-1010 Electropolisher Struers TenuPol-3 Carrier concentration measuring device ACCENT PN4400 Hall Effect measurement system ACCENT HL5500 Dual ion milling GATAN Model 600N Ion milling Hitachi E-300 Ion polishing GATAN Model 691 PIPS Cryo Ion Slicer JEOL Cryo IS Cross Section Polisher JEOL CP 302B Mihou Nakajima Analytical Instrument Staff Room s bulletin See Attachment 5-2 for the procedures Anytime Analytical Instrument Staff Room s bulletin See Attachment 5-2 for the procedures Normal : When accessories are used: 100 /hour 2,500 /hour Consumables: 1,000 or 1, / half film See Attachment 5-3 Submit the Application for the Use of Chemical Pretreatment Room beforehand and obtain a Permission to Use the Chemical Pretreatment Room. 100 /hour When cryo is used: Each user must purchase his/her own sample holder Flat ion milling Sanyu Electron SVM-730 Vacuum deposition device (exclusively for carbon) Vacuum Device VE 2020

6 Device name Curved imaging plate X-ray diffractometer (MDG) Rigaku RINT RAPID-S Nanoscale X-ray structure evaluation device (SAXS) Rigaku NANO-Viewer X-ray diffractometer for thin film structure analysis (XRD) Rigaku ATX-G Fully automatic horizontal multi-purpose X-ray diffractometer (XRD) Rigaku SmartLab Extremely low temperature attachment for SmartLab Temperature variable between 4 K and 300 K High temperature attachment for SmartLab Temperature variable between 25 C and 1200 C Mihou Nakajima Analytical Instrument Staff Room s bulletin See Attachment 5-2 for the procedures 600 /hour 600 /hour d. Chemical Pretreatment Room Reception 304, the 3rd Floor of Building the Analytical Instrument Lab. Staff Room (ext ) Device name Chemical Pretreatment Room 302B Shinpei See Attachment 5-3 Submit the Application for the Use of Chemical Pretreatment Room beforehand and obtain a Permission to Use the Chemical Pretreatment Room. Related devices: Fume hood, electronic balance, ultrademineralizer, ultrasonic cleaning machine, and poison cabinet Because chemicals cannot be carried from one campus to another, only the research labs located in Zaiken (research labs that can purchase chemicals through Zaiken) can use these devices.