European Energy Materials Development Platform. Awareness Building
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1 European Energy Materials Development Platform Awareness Building
2 STRUCTURES FOR MATERIAL RESEARCH IN HORIZON EUROPE What do we want? How could a larger material researcher community benefit from missions? Could we get may be 2 or three missions or is it possible to have one mission integrating all our research efforts? What kind of other structural funding schemes could we further think of? How to raise the awareness of member states? Should we push for a SET-PLAN Implementation working group? Missions should have innovative potentials. Missions need to interesting for the public. If we want to be successful, we need to team up and build an interesting concept in 1, 2 or 3 years from now.
3 Autonomous Material Development Platform (AMDP)
4 TARGET : COST REDUCTION FOR CLEAN ENERGY DEVICES Material cost share is > 50% for many energy technologies Industry 4.0 and large scale production will reduce the costs for energy devices Long-term job security by highly specialized products, which are realized in small and medium charges by Industry 4.0 production processes In general higher performing materials enable access to larger markets Study on battery costs : ( MOBI Research Group, Vrije Universiteit Brussel,2017) Cathode: Lithium Nickel Manganese Cobalt Oxide (NMC) Anode : Silicon alloy intended to be state of the art in years from now
5 GENERAL IDEA Costs reduction by modern AI and High Throughput robotic technologies Costs reduction by sample centric approaches
6 ENABLER : BIG DATA Specialized data cloud: HPC, HP-network Meso-scaling techniques ( data mining, AI) Big data technologies will enable energy systems management This figure comes from Reizman, Bandon, J.; Jensen, K. F. Acct. Chem. Res. 2016, 49 (9), pp
7 2016 : SYSTEMS ARE UP AND GROWING Virtual characterisation of new materials : HPC software requirements are investigated Infrastructure optimisation Indication for large acceleration of materials development. Target is to present a small sub-set of user cases where scientists utilize BEAM across for broad range of analytical techniques and analysis modes. This figure comes from Reizman, Bandon, J.; Jensen, K. F. Acct. Chem. Res. 2016, 49 (9), pp
8 MISSION INNOVATION INTERNATIONAL CO-OPERATION Participating countries promised to double the research and innovation efforts in next 5 years European partners are supporting Innovation Challenge 6 Materials Accelerator Project pushed by US, Mex. and Can
9 Ångström Advanced Battery Centre - Uppsala Roughly 60 scientists from three different departments: -Chemistry, Physics and Engineering Sciences -Modeling and experiment Batterifondsprogrammet
10 Established battery chemistries: EVs, grids Novel materials: Li-ion and Solid State Future Concepts Anode Cathode Electrolytes/separators Interfaces New concepts Synthesis of new electrode and electrolyte materials New characterisation methods Fundamental processes (life time, energy, power, etc.) EV batteries, large scale storage, medical applications, automation, etc. Recycling Beyond Li-jon Organic electrodes Li-O 2 Na-O 2 Li-S Li-metal Uppsala University a research overview New chemistries: Na, K, Mg, Ca, Al
11 Infrastructure Material synthesis plattform all kinds of furnaces, polymer synthesis X-ray diffraction plattform laboratory instruments for powder, thin film and single crystal. Special designed sample holders for in situ XRD in transmission mode on batteries Material characterisation plattform SEM, TEM, FIB, AFM, XPS, Raman spectroscopy, FTIR, BET, etc. More than 200 battery cycling channels for different cell designs Potentiostats, etc. An in house small pilot line for battery production Trained in using synchrotron and neutron scattering methods
12 HELMHOLTZ ENERGY MATERIALS CHARACTERIZATION PLATFORM (HEMCP)
13 HEMF - HEMPC
14 Charakterisierungstools am KIT Focus: Energy Materials Prof. Helmut Ehrenberg INSTITUTE for APPLIED MATERIALS ENERGY STORAGE SYSTEMS & Inorganic Chemistry 30. January 2017 Prof. Dr. Helmut Ehrenberg Batteries
15 Characterization Length scales: nuclei atoms/ions cluster nanodomains / crystals primary / secondary particles composite electrodes components cells battery packs applications
16 Characterization overview: List of analytical tools: TG-DTA SPM-XPS BET FIB RDE DSC SAM DLS TEM CV QMB FT-IR SEM APT EIS KFT MBS XRD AFM PITT DEMS TERS NPD SCM GITT QMS NMR UPS n-tomo SQUID ToF-SIMS EPR XAS STM All necessary methods are available + dedicated techniques.
17 Characterization in situ/in operando methods: X-Ray Diffraction, XRD X-ray Absorption Spectroscopy, XAS Synchrotron Diffraction Neutron Powder Diffraction, NPD Neutron Tomography, NT Scanning Electron Microscopy, SEM Transmission Electron Microscopy, TEM Mößbauer spectroscopy Magnetisation measurements, SQUID Mechanical tests, Substrate Curvature Measurements, SCM Raman spectroscopy Solid ElectroIyte Interface analytics by combined DTA/TG & FT-IR Differential Electrochemical Mass Spectroscopy, DEMS Nuclear Magnetic Resonance spectroscopy, NMR Electron Paramagnetic Resonance spectroscopy, EPR
18 KIT Battery Technical Centre Cell manufacturing and system integration of Li-ion and post-li batteries Electrode coating and flexible cell processing Stationary and mobile applications Process technology for all-solid state batteries Showroom for battery research and development at KIT Compilation of battery engineering within CELEST Helmholtz Energy Materials Foundry (HEMF) Electrode Application Lab KIT Battery Technical Centre / KIT Batterietechnikum KIT Cell Assembly Batteries in Applications
19 High throughput Experiments with Inorganic materials 04. JUNI 2018 I SVEN UHLENBRUCK Forschungszentrum Jülich GmbH, Institute of Energy and Climate Research: Materials Synthesis and Processing (IEK-1), Jülich, Germany
20 HIGH THROUGHPUT SYNTHESIS BY PHYSICAL VAPOR DEPOSITION (PVD) Sputter source material 1 Sputter source material 2 PVD cluster system 3 sputter sources confocal arrangement Sputter source material 3 A. Rar et al., Meas. Sci. Technol. 16 (2005) 46 Compositional gradient
21 CREATION OF TERNARY PHASE DIAGRAMS S. Guerin and B.E. Hayden, J. Combinatorial Chemistry 8 (2006) 66)
22 HIGH THROUGHPUT ANALYSIS: PHASE MAPPING BY RAMAN MICROSCOPY Solid-state lithium battery: Mixture of solid-state electrolyte (Li 5 La 3 Ta 2 O 12 ; yellow) and cathode active material (LiCoMnO 4 ; red); blue: organic material (resin) Max sample size: 100 mm x 70 mm Sub micrometer resolution Up to 1000 spectra per second (depending on the sample)
23 HORIZON EUROPE (HE) POSSIBILITIES The upcoming FET-Flagships will be implemented as HE Mission Funding will be taken from the pillar global challenges ( overall budget 52b ) Missions will be implemented as co-funding actions ( like European Technology Platform with funding support from EU and member states ) European Strategic Research Infrastructure ( ESFRI) - next list will be discussed in 2-3 years from now - but the idea needs some preparation to be successful FP9 will support research infrastructure activities: - efforts to develop new infrastructures - establishing an European Open Science Cloud (EOSC), open data (as a scalable and sustainable environment for data-driven research;) For the Sustainable Development Goal (SDGs) in part: SDG 7 Affordable and Clean Energy; SDG 9 Industry Innovation and Infrastructure
24 DISTRIBUTED EUROPEAN RESEARCH INFRASTRUCTURES EMBRC - European Marine Biological Resource Centre The EMBRC is a distributed RI aiming at providing a strategic delivery mechanism for excellent and large-scale marine science. EMBRC offers services to users from academia, industry, technology and education in all sectors in the fields of marine biology and ecology, particularly supporting the development of blue biotechnologies. EMPHASIS European Infrastructure for multi-scale Plant Phenomics and Simulation for food security in a changing climate
25 EUROPEAN ENERGY MATERIALS DEVELOPMENT PLATFORM Europe has already elements of a materials development platform, But a systematic approach for setting up an automised platform is not available. What do we need to coordinate our efforts better for speeding up materials development? - Mission ( Affordable Clean Energy ) - ESFRI infrastructure How could we mobilise our resources? Should we aim to set up a platform roadmap? Request, if you are aware of facilities or installation as presented, please let me know! ( holger.ihssen@helmholtz.de )
26 ADDITIONAL SLIDES
27 SEM : SCANNING ELECTRON MICROSCOP TEM : TRANSMISSION ELECTRON MICROSCOP FIB : FOCUSED ION BEAM AFM : ATOMIC FORCE MICROSCOPE XPS : X-RAY PHOTOELECTRON SPECTROSCOPY RAMAN SPECTROSCOPY : FTIR : FOURIER-TRANSFORM INFRARED SPECTROSCOPY BET : BRUNAUER, EMMETT AND TELLER ( DETERMINES SURFACE AREA )
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