GC Section. Astec, Agilent/J&W, SGE, Quadrex

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1 GC Section GC Columns Introduction Capillary Columns, Alltech Custom Columns Heliflex Econo-Cap EPA Methods Guide Capillary Columns, Other Astec, Agilent/J&W, SGE, Quadrex Packed Columns Packed Columns Custom Packings Empty Columns & Supports GC Accessories Capillary Accessories Packed Accessories Gas Management Gas Flow Purifiers Pressure Regulators Gas Sampling Ferrules Fittings & Tubing Injection Liners & Accessories Kits Septa Tools & Organizers Valves GC Instruments GC Systems & Data Collection Gas Generators Hydrogen Air Nitrogen Air Compressors

2 C O L U M N S Capillary Columns Introduction Alltech Capillary Columns What do I need to consider when selecting a GC column? Internal diameter - Selection is based on sample concentration and instrumentation. Narrow bore(0.1mm-0.2mm) are ideal for MS, and wide bore (.53mm) are ideal for purge and trap applications. Film thickness - Film thickness has a direct affect on retention of the compound. A thicker film thickness retains the compound longer, and a thinner film decreases retention. Column Length - The column length affects both the resolution and the rate of analysis. A longer column provides better resolution, but doubling the column length will double the time of analysis(isothermal conditions). Stationary Phase - The most important consideration is the stationary phase; this is dependent upon the polarity of the compound, property of the column, and standard methods referenced, - All Alltech columns are presented with their USP designations to help you easily make a selection. - The GC Application section (p ) offers proven methods for analysis.see for a complete listing. - Questions on stationary phase selection? Call Technical Service; we are ready to assist you with your application questions Alltech Capillary Column Families Econo-Cap Capillary Column Line Best value in capillary columns anywhere Batch tested to dramatically reduce price Ideal for aggressive applications Available in the most popular phases We ve taken our most popular capillary columns and perfected the manufacturing procedure to the point that reproducibility is assured. This allows us to test these columns in batches instead of individually, while still offering an unconditional guarantee. Batch testing significantly reduces cost in production without sacrificing quality. Each Econo-Cap Capillary Column comes with a copy of the batch test results, an instruction manual, and capillary end caps. If you are not completely satisfied with the quality of your Econo-Cap Capillary Column it will be replaced at no charge. Note: Column nuts and ferrules are not included. Heliflex Capillary Column Line High performance individually tested columns Choice of 5" or 7" rugged cage Most complete selection of phases Custom columns available to suit your specific application Heliflex Capillary Columns are manufactured from the highest quality polyimide coated synthetic fused silica. They are mounted on a rugged wear-resistant cage. Each Heliflex Column is individually tested to guarantee column performance and comes with a test chromatogram, instruction manual, capillary end caps, and a free ceramic column cutter. Note: Column nuts and ferrules are not included. If the column you need is not available in our standard offering, request a custom Heliflex Column made to your individual specifications. 329

3 Capillary Columns Introduction C O L U M N S Capillary Column Phase Cross Reference Use the chart below to cross reference manufacturers stationary phases as well as USP method designations to Alltech equivalent columns. Slight variations in selectivity may result between different manufacturers columns. Alltech Standard Phase Cross Reference Standard Phase Cross Reference COMPOSITION ALLTECH USP DESIGNATION 100% Dimethylpolysiloxane AT -1ms G1, G2, G38 100% Dimethylpolysiloxane AT -1ht, AT -1, G1, G2, EC -1 G38 5% Phenyl equivalent Polysilphenylene-Siloxane (5% Phenyl)- 95% methylpolysiloxane (20% Phenyl)- 80% methylpolysiloxane (35 Phenyl)- 65% Methylpolysiloxane (50 Phenyl)- 50% methylpolysiloxane (6% Cyanopropylphenyl)- 94% methylpolysiloxane (14% Cyanopropylphenyl)- 86% methylpolysiloxane Trifluoropropylmethyl polysiloxane (50% Cyanopropylphenyl)- 50% methylpolysiloxane (50% Cyanopropyl)- 50% methylpolysiloxane poly(80% bis cyanopropyl)- 20% cyanoproylphenyl siloxane poly(biscyanopropyl siloxane) Polyethyleneglycol Polyethyleneglycol Acid Modified AT -5ms AT -5, EC -5 G27, G36 SIMILIAR PHASES DB -1ms, HP -1ms, Rtx-1ms, CP-Sil,5CB low Bleed/ms 007-1, CP-Sil 5CB, DB -1, DB-1ht,HP -1,HP- 101, OV -1, RSL -150,RSL-160, Rtx -1, SE-30, SPB -1, SPB-Sulfur,ULTRA -1, SP-2100, BP-1, DC-200, PE-1, ZB-1 DB -5ms, Rtx -5Sil ms, BPX-5, 007-5ms, HP -5ms 007-2, CP-Sil 8CB, DB -5, D B-5.625, DB -5ht, HP -5, HP -5ms, OV -5, PTE-5, PTE-5QTM, PAS-5, RSL-200, Rtx -5,Rtx -5ms, SAC-5, SE-54, SPB-5, ULTRA-2, XTI-5, SE-52, BP-5, PE-2, ZB , Rtx -20, SPB-20, VOCOL, PE-7 AT -20, EC -20 G28, G32 AT -35ms G42 DB-35ms, Rtx-35, SPB-35, SUP-HERB, MDN-35, BPX-35 AT , DB -35, DB -35ms, HP -35, RSL-300, Rtx -35, SPB-35, SPB-608, OV -11, PE-35, Sup-Herb AT -50ms G3 DB 17ms, H5-50+, Rtx-50, SP-2250, SPB-50, SPB-17, BPX-50 AT -50ht DB-17ht, Rtx-65TG, BPX-50, CP-TAB-CB, AT , DB-17, DB-17ht, HP -17, HP -50+, Rtx -50 SP-50, SP-2250, SPB-50, CP Sil 24CB, PE-17, ZB-50 AT -624 G , DB -624, DB -1301, HP -1301, HP -624, AT Rtx -1301, Rtx -624, SPB-1301, SPB-624, , ZB-624 AT , CP-Sil 19CB, DB-1701, HP -1701, OV -1701, PAS-1701, Rtx -1701, SPB-1701, BP-10, ZB-1701 AT -210 G6 DB -210, RSL-400, Rtx -200, OV -202, OV -210, OV -215, QF-1, SP-2401 AT -225 G , CP-Sil43CB, DB -225, HP -225, OV -225, RSL-500,Rtx -225, BP-225, PE-225 AT -SILAR G5 DB -23, , PE-23, Rtx -2330, SP 2330 AT -SILAR-90 G8 DB-23, CP-Sil84, Rtx-2330, SP-2330 AT -SILAR-100 G5 CP-Sil88, Rtx-2330, SP-2340 AT -WAXms AT -WAX AT -AquaWax EC -WAX AT -1000, EC -1000, AT -AquaWax-DA G14,G15 G16,G20, G39 G25, G35 DB-WAX, Rtx-WAX, SUPELCOWAX CW, Carbowax 20M, CP-Wax 52CB, DB -WAXetr, DB -WAX, Rtx -WAX, HP-20M, HP -Wax, Innowax, Omegawax, Stabilwax, SUPELCOWAX -10, SUPEROX II, BP-20, ZB-WAX 007-FFAP, CP-Wax 58CB, DB -FFAP, HP -FFAP, Nukol, OV -351, SP-1000, Stabilwax-DA, SUPEROX-FA, BP-21 Polyethyleneglycol AT -CAM Stabilwax -DB, CAM, Carbowax Amine, CP Wax 51 Base Modified PONA Analysis AT -Petro F, CP-Sil PONA CB, DB -Petro100, Petrocol DH, PONA, Ttx-1PONA, HP-PONA ASTM Method 2887 AT V-1.0F, DB -2887, Petrocol 2887, Petrocol EX2887, Rtx- 2887, Sim-Dist-CB ASTM Method 3710 AT Petrocol

4 C O L U M N S Alltech Capillary Columns Alltech Specialty Columns Cross Reference Specialty Phases Cross Reference EPA Method 608 AT -Pesticide , DB -608, HP -608, SPB-608 EPA Method AT , , DB-502.2, DB -VRX, HP -624, Rtx -Volatiles, VOCOL Sulfur Analysis AT -Sulfur SPB-1 SULFUR FAME Analysis AT -FAME FAMEWAX, OmegaWAX Alltech Custom Capillary Columns A wide selection of stationary phases Lengths from 1 to 105 meters Wide selection of i.d. tubing Every column individually tested Custom Capillary Column Instructions 1. Stationary Choose a Phase in "Table 1: Custom Phase." 2. Length & Internal Diameter: Choose any length (1 to 105 meters) and internal diameter (0.10mm to 0.53mm) from in "Table 2: Custom Dimensions." 3. Film Thickness: Choose a film thickness; 0.01µm tolerance. 4. See Coiling and Guard Information for additional options. 5. Call Customer Service and they will confirm your order and provide exact prices. Table 1: Custom Phases Phases Available for Custom Capillary Columns Aquawax Dexsil 400 OV -17 Aquawax-DA Dexsil 410 OV AT -1 Di (2ethylhexyl OV -25 AT -5 phthalate OV -61 AT -20 Diisodecyl OV -73 phthalate AT -35 FFAP OV -101 AT Hi-Eff -1AP OV -105 AT Hi-Eff -1BP OV -210 AT Hi-Eff -2AP OV -351 AT -WAX Hi-Eff -2BP Polyvinylpyrrolidone AT -Amine Hi-Eff -3AP QF-1 Apiezon phases Hi-Eff -3BP Reoplex 400 Apolane -87 Hi-Eff -4BP SE-30 Butanediol succinate Hi-Eff -8BP Squalane (Craig s polyester) Hi-Eff -10BP Superox-FA Carbowax phases Igepal CO-880 XE-60 DC-550 OV -1 Dexsil 300 OV -11 HP -VOC,MST-502.2, MXT-624, MXT-Volatiles, OV-624, Rtx-502.2,Rtx -624, Table 2: Custom Dimensions ALLTECH HELIFLEX CUSTOM CAPILLARY COLUMNS LENGTH I.D. DESCRIPTION PART NO. PRICE 1-5m 0.10mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film m 0.10mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film m 0.10mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film m 0.18mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film m 0.25mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film mm Specify Phase & Film Custom Capillary All other Dimensions not specified Custom Capillary Coiling CUSTOM COILING DESCRIPTION PART NO. PRICE Custom Capillary on 4" Cage Custom Capillary on 5" Cage Custom Capillary Column with Integral Guard CUSTOM CAPILLARY COLUMN WITH INTEGRAL GUARD DESCRIPTION PART NO. PRICE Custom 0.25mm i.d. w/integral 5m Guard C-5400 Custom 0.32mm i.d. w/integral 5m Guard C-5500 Custom 0.53mm i.d. w/integral 5m Guard C

5 Alltech Capillary Columns C O L U M N S Heliflex AT -1ms Guaranteed low bleed characteristics Specifically designed for mass spec analysis Highly inert Similar to DB-1ms, HP-1ms, Rtx-1ms, CP-Sil 5 CB Low Bleed/MS, MDN-1. AT -1ms is a line of high-performance low bleed non-polar columns designed specifically for use with mass spectrometers. They are ideal for pharmaceutical, environmental, petrochemical, and food and fragrance analysis, or any GC/MS analysis requiring a 100% dimethylpolysiloxane-type polarity capillary column. Heliflex AT -1ht Shorten your analysis time with high temperature/low bleed columns Faster analysis time for high boiling compounds Better peak detection at lower concentrations Individually bleed tested at 380ºC Similar to 007-1, CP-Sil 5CB, DBTM-1, DB-1ht, HPTM- 1, HP-101,OVTM-1,RSLTM-150, RSL-160, RtxTM-1, SE-30TM, SPBTM-1, SPB-Sulfur,ULTRATM-1, SP-2100, BP-1, DC-200, PE-1, ZB-1 Max. Temp.: USP Designation: Ideal for: 100% Dimethylpolysiloxane Non-polar 340/360 C G1, G2, G38 Mass Spec Analysis for Environmental, PAH, CLP Pesticides, Steroids and Drugs Max. Temp.: USP Designation: Ideal for: 100% Dimethylpolysiloxane Non-polar 380/400 C G1, G2, G38 High Boiling Compounds Waxes, Crude Oils, and Trigylcerides Figure 1 - AT -1ms Low Bleed QC Test Chromatogram - Bleed Profile Column: Temp: Carrier Gas: Detector: Heliflex AT -1ms, 30m x 0.25mm x 0.25µm (Part No ) 135 C (20 min hold) to 320 C (10 min hold) at 20 C/min Helium at 0.65mL/min (23.1cm/sec) FID HELIFLEX AT -1MS CAPILLARY COLUMNS 15m 0.25mm 0.25µm -60/360 C mm 0.25µm -60/360 C m 0.25mm 0.10µm -60/360 C mm 0.25µm -60/360 C mm 0.25µm -60/360 C 15735* 0.32mm 0.10µm -60/360 C mm 0.25µm -60/360 C mm 0.25µm -60/360 C 15739* 60m 0.25mm 0.25µm -60/360 C mm 0.25µm -60/360 C *Equipped with uncoated 5m integral guard column. Total column length is 35 meters Ethylhexanoic Acid 2. 4-Chlorophenol 3. 1,7-Heptanediol 4. n-tridecane 5. 1-Undecanol 6. n-tetradecane 7. Dicyclohexylamine 8. Acenaphthylene 9. n-pentadecane Undecanol 2. Dicyclohexylamine pa 3. 4-Chlorophenol 4. n-pentadecane 5. Fluorene 6. Anthracene 7. n-heptadecane Min. Column: Heliflex AT -1ht, 30m x 0.25mm x 0.10µm (Part No ) Column Temp: 125ºC (hold 25 min) to 380ºC at 20ºC/min Carrier Gas: Helium at 26.3cm/sec Detector: FID at 390ºC HELIFLEX AT -1HT GC CAPILLARY COLUMNS 15m 0.25mm 0.1µm /400 C m 0.25mm 0.1µm /400 C m 0.25mm 0.1µm /400 C For more Capillary GC Applications, See the GC Applications Section p To view Alltech's complete chromatogram library, visit

6 C O L U M N S Alltech Capillary Columns Heliflex AT -1 Excellent general purpose columns Similar to DB -1, Rtx -1, SPB -1, SPB-Sulfur, SP , HP -1, HP -101, ULTRA -1, BP -1, CP-Sil - 5-CB, 007-1, OV -1, SE -30, DC -200, RSL -150, RSL-160, PE-1, ZB-1 USP Designation: Ideal for: 100% Dimethylpolysiloxane Non-polar General Purpose Column G1, G2, G38 General Purpose HELIFLEX AT -1 CAPILLARY COLUMNS 10m 0.25mm 0.20µm -60/350 C mm 0.25µm -60/350 C mm 0.10µm -60/350 C mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 0.30µm -60/350 C mm 0.25µm -60/350 C mm 1.20µm -60/350 C mm 2.65µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.10µm -60/350 C mm 0.20µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 0.30µm -60/350 C mm 1.00µm -60/350 C mm 3.00µm -60/350 C mm 5.00µm -60/300 C mm 0.15µm -60/350 C mm 0.25µm -60/350 C mm 0.50µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C mm 1.50µm -60/330 C mm 2.65µm -60/300 C mm 3.00µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.20µm -60/350 C mm 0.30µm -60/350 C mm 1.20µm -60/350 C m 0.25mm 0.10µm -60/350 C mm 0.20µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 0.30µm -60/350 C mm 1.00µm -60/350 C mm 3.00µm -60/300 C mm 5.00µm -60/300 C mm 0.50µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C mm 1.50µm -60/330 C HELIFLEX AT -1 CAPILLARY COLUMNS 30m 0.53mm 2.65µm -60/300 C mm 3.00µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.20µm -60/350 C mm 0.30µm -60/350 C mm 1.20µm -60/350 C m 0.25mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 3.00µm -60/300 C mm 5.00µm -60/300 C mm 0.50µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C mm 1.50µm -60/330 C mm 3.00µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.20µm -60/350 C HELIFLEX AT -1 CAPILLARY COLUMNS ON 5" CAGE 15m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.50µm -60/350 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.50µm -60/350 C Econo Cap EC-1 Batch tested to dramatically reduce price ECONO-CAP EC -1 CAPILLARY COLUMNS LENGTH I.D. FILM TEMP. LIMITS PART NO. 10m 0.53mm 2.65µm -60/350 C m 0.53mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C ECONO-CAP EC -1 CAPILLARY COLUMNS, SIX PACK LENGTH I.D. FILM TEMP. LIMITS PART NO. 30m 0.25mm.25µm -60/350 C m 0.32mm.25µm -60/350 C m 0.53mm 1.20µm -60/350 C PRICE PRICE 333

7 Alltech Capillary Columns C O L U M N S Heliflex AT -5ms Similar to DB -5ms, Rtx -5 Sil ms, HP -5TA, BPX-5, 007-5ms The AT -5ms capillaries are ideal for environmental, pharmaceutical, and petrochemical analysis, or any GC/MS analysis requiring a 5% phenyl-type polarity capillary column. Heliflex AT -5 Excellent general purpose columns Similar to DB -5, Rtx -5, SPB -5, HP -5, ULTRA -2, BP -5, CP-Sil -8-CB, 007-2, OV -5, SE -52, SE-54, RSL -200, ZB-5 USP Designation: Ideal for: (5% Phenyl)-95% Methoxpolysiloxane Non-polar G27, G36 Mass Spec Analysis-General Application Max. Temp.: USP Designation: Ideal for: (5% Phenyl)-95% Methylpolysiloxane Non-polar 380/400 C G27, G36 General Applications TEPP 2. Sulfotepp 3. Monocrotophos 4. Dimethoate 5. Dioxathion 6. Terbufos 7. Phosphamidon 8. Malathion 9. Parathion 10. cis-chlorfenvinphos 11. trans-chlorfenvinphos 12. Ethion Column: Temp: Carrier Gas: Detector: Organophosphorus Pesticides 13. Famphur 14. Carbophenothion 15. Phosmet Min. Heliflex AT -5ms, 30m x 0.25mm x 0.25µm (Part No ) 120 C (3min hold) to 285 C at 5 C/min (4min hold) Helium, 26 cm/sec MSD HELIFLEX AT -5MS CAPILLARY COLUMNS 15m 0.25mm 0.25µm /350 C m 0.25mm 0.10µm /350 C mm 0.25µm /350 C mm 0.25µm /350 C 15881* 0.25mm 0.50µm /350 C mm 0.50µm /350 C 15889* 0.25mm 1.00µm /350 C mm 0.10µm /350 C mm 0.25µm /350 C mm 0.25µm /350 C 15883* 0.32mm 1.00µm /350 C m 0.25mm 0.10µm /350 C mm 0.25µm /350 C mm 1.00µm /350 C mm 0.25µm /350 C EPN 17. Leptophos 18. Azinphos-ethyl *With 5 meter Integral Guard Columns. Total length of column is 35 meters HELIFLEX AT -5 CAPILLARY COLUMNS 10m 0.25mm 0.20µm -60/350 C mm 0.30µm -60/350 C mm 0.25µm -60/350 C mm 1.20µm -60/350 C mm 2.65µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.10µm -60/300 C mm 0.20µm -60/300 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 0.30µm -60/350 C mm 1.00µm -60/350 C mm 0.25µm -60/350 C mm 0.50µm -60/300 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C mm 1.50µm -60/330 C mm 3.00µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.20µm -60/350 C mm 0.30µm -60/350 C mm 1.20µm -60/350 C m 0.25mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 0.50µm -60/330 C mm 1.00µm -60/350 C mm 0.10µm -60/300 C mm 0.25µm -60/350 C mm 0.30µm -60/350 C mm 1.00µm -60/350 C mm 0.50µm -60/300 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C mm 1.50µm -60/330 C mm 2.65µm -60/300 C mm 5.00µm -60/300 C m 0.25mm 0.20µm -60/350 C mm 0.30µm -60/300 C mm 1.20µm -60/350 C 13942

8 C O L U M N S Alltech Capillary Columns HELIFLEX AT -5 CAPILLARY COLUMNS (CONTINUED) 60m 0.25mm 0.10um -60/350 C mm 0.20µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 0.10µm -60/350 C mm 0.25µm -60/350 C mm 0.30µm -60/350 C mm 1.00µm -60/350 C mm 0.50µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C mm 1.50µm -60/330 C mm 3.00µm -60/350 C mm 5.00µm -60/300 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.20µm -60/350 C HELIFLEX AT -5 CAPILLARY COLUMNS ON 5" CAGE 15m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.50µm -60/350 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.50µm -60/350 C Econo-Cap EC -5 Batch tested to dramatically reduce price Heliflex AT -20 Unique polarity between non-polar and mid-range. Similar to 007-7, Rtx -20, SPB-20, VOCOL, PE-7 USP Designation: Ideal for: (20% Phenyl)-80% Methylpolysiloxane Intermediate Polarity G28, G32 Volatile compounds and Solvents HELIFLEX AT -20 CAPILLARY COLUMNS 10m 0.53mm 1.20µm -20/320 C m 0.25mm 0.25µm -20/320 C mm 0.25µm -20/320 C mm 1.20µm -20/320 C mm 1.00µm -20/300 C m 0.53mm 1.20µm -20/320 C m 0.25mm 0.25µm -20/320 C mm 0.25µm -20/320 C mm 1.00µm -20/300 C mm 1.20µm -20/300 C m 0.53mm 1.20µm -20/320 C m 0.25mm 0.25µm -20/320 C mm 0.25µm -20/320 C mm 1.00µm -20/300 C mm 3.00µm -20/280 C Econo-Cap EC -20 Batch tested to dramatically reduce price ECONO-CAP EC -5 CAPILLARY COLUMNS LENGTH I.D. FILM TEMP. LIMITS PART NO. 15m 0.45mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.00µm -60/350 C mm 1.20µm -60/350 C PRICE ECONO-CAP EC -20 CAPILLARY COLUMNS LENGTH I.D. FILM TEMP. LIMITS PART NO. 15m 0.45mm 1.00µm -20/300 C mm 1.00µm -20/300 C mm 1.20µm -20/300 C m 0.25mm 0.25µm -20/300 C mm 0.25µm -20/300 C mm 1.00µm -20/300 C mm 1.00µm -20/300 C mm 1.20µm -20/300 C PRICE ECONO-CAP EC -5 CAPILLARY COLUMNS, SIX PACK LENGTH I.D. FILM TEMP. LIMITS PART NO. 15m 0.25mm 0.25µm -60/350 C m 0.25mm 0.25µm -60/350 C mm 0.25µm -60/350 C mm 1.20µm -60/350 C PRICE For a complete listing of Alltech Heliflex Capillary Columns, request data sheet PS. 335

9 Alltech Capillary Columns C O L U M N S Heliflex AT -35ms Guaranteed low bleed Specifically designed for mass spec analysis Similar to DB-35ms, Rtx-35, SPB-35, SUP-HERB, MDN-35, BPX-35 Heliflex AT -35 Ideal column for conformational analysis Similar to DB -35, DB -35ms, Rtx -35,BP X35, SPB - 35, SPB-608, thp -35, , OV -11, RSL -300, PE-35, Sup-Herb, ZB-35 USP Designation: Ideal for: (35% Phenyl)-65% Methylpolysiloxane Intermediate Polarity G42 Pesticides, Herbicides, Drugs, Aromatics USP Designation: Ideal for: (35% Phenyl)-65% Methylpolysiloxane Intermediate Polarity G42 Pesticides, Herbicides, Drugs, Aromatics AT -35MS CAPILLARY COLUMN LENGTH I.D. FILM TEMP. LIMIT PART NO. PRICE 15m 0.25mm 0.25µm -40 / 340 C m 0.25mm 0.25µm -40 / 340 C m 0.25mm 0.25µm -40 / 340 C Tocopherols Min. Column: Heliflex AT -35, 25m x 0.25mm x 0.20µm (Part No ) Temp: 310 C Carrier: Hydrogen at 40 cm/sec Detector: FID d-δ-tocopherol 2. d-β-tocopherol 3. d-γ-tocopherol 4. d-α-tocopherol For more Capillary GC Applications, See the GC Applications Section p AT -35 CAPILLARY COLUMNS 10m 0.25mm 0.25µm -20/320 C mm 0.10µm -20/350 C mm 0.25µm -20/300 C mm 0.10µm -20/350 C mm 0.20µm -20/280 C mm 1.20µm -20/300 C mm 2.65µm -20/280 C m 0.25mm 0.25µm -20/320 C mm 0.50µm -20/320 C mm 0.15µm -20/280 C mm 0.25µm -20/320 C mm 0.50µm -20/320 C mm 1.00µm -20/300 C mm 1.20µm -20/300 C m 0.25mm 0.20µm -20/320 C mm 0.30µm -20/320 C mm 1.20µm -20/300 C m 0.25mm 0.15µm -20/320 C mm 0.20µm -20/300 C mm 0.25µm -20/320 C mm 0.50µm -20/320 C mm 1.00µm -20/300 C mm 0.15µm -20/320 C mm 0.25µm -20/320 C mm 0.50µm -20/320 C mm 0.50µm -20/320 C mm 1.00µm -20/300 C mm 1.20µm -20/300 C mm 2.65µm -20/280 C m 0.25mm 0.20µm -20/320 C mm 0.30µm -20/320 C m 0.25mm 0.20µm -20/320 C mm 0.25µm -20/320 C mm 0.50µm -20/320 C mm 0.25µm -20/320 C mm 0.50µm -20/320 C mm 1.00µm -20/320 C

10 G C C O L U M N S Alltech Capillary Columns Heliflex AT -50ms Designed to provide low MS bleed Similar to DB -17ms, H5-50+, Rtx -50, SP-2250, SPB-50, SPB-17, BPX -50 Heliflex AT -50 General purpose column Similar to DB -17, DB -17ht, Rtx -50, BPX-50, SPB-50, SP-2250, HP -50+, HP -17, , OV -17, CP Sil 24CB, PE-17, ZB-50 (50% Phenyl)-Methylpolysiloxane Intermediate Polarity G3 Mass Spec Applications (50% Phenyl)-Methylpolysiloxane Intermediate Polarity G3 Pesticides, Herbicides, Phthalate Esters, Free Phenols, and Basic Drugs AT -50MS CAPILLARY COLUMNS 15m 0.25mm 0.25µm -40 /340 C m 0.25mm 0.25µm -40 /340 C m 0.25mm 0.25µm -40 /340 C m 0.32mm 0.25µm -40 /340 C m 0.32mm 0.25µm -40 /340 C AT -50 CAPILLARY COLUMNS 15m 0.25mm 0.25µm 40/325 C mm 0.25µm 40/325 C mm 1.00µm 40/280 C m 0.25mm 0.25µm 40/325 C mm 0.25µm 40/325 C mm 0.50µm 40/300 C mm 1.00µm 40/280 C Heliflex AT -50ht Specially tested for bleed at 340 C Higher temperatures mean faster analysis Similar to DB -17ht, Rtx -65TG, BPX-50, CP-TAB-CB Heliflex AT Unique polarity makes it ideal for a range of applications Similar to BP 624, DB -1301, Rtx -1301, Rtx -624, HP -1301,HP -624, DB -624, , , SPB-1301, SPB-624, ZB-624 (50% Phenyl)-Methylpolysiloxane Intermediate Polarity G3 High Boiling Compounds (6% Cyanopropylpenyl)-Methylpolysiloxane Intermediate Polarity G43 Volatile Organics, Pharmaceuticals, and EPA Method 612 AT -50HT CAPILLARY COLUMNS 15m 0.25mm 0.15µm -40 /340 C m 0.25mm 0.15µm -40 /340 C m 0.32mm 0.15µm -40 /340 C m 0.32mm 0.15µm -40 /340 C m 0.32mm 0.15µm -40 /340 C m 0.53mm 0.15µm -40 /340 C m 0.53mm 0.15µm -40 /340 C AT CAPILLARY COLUMNS 30m 0.25mm 0.25µm -20/280 C mm 1.00µm -20/260 C mm 0.25µm -20/280 C mm 1.00µm -20/260 C mm 3.00µm -20/260 C To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages

11 Alltech Capillary Columns G C C O L U M N S Heliflex AT -210 Similar to DB - 210, Rtx -200, OV - 202, OV -210, OV -215, QF-1, SP-2401, RSL-400 Heliflex AT Similar to DB -1701, OV -1701, SPB -1701, Rtx -1701, , PAS-1701, CP-Sil 19CB, HP -1701, BP-10, ZB-1701 Trifluoropropyl Methylpolysiloxane Polar G6 Ketones, Aldehydes, Silanes, Glycols, Nitro Aromatics, Herbicides, and Method 8140 and 609 (14% Cyanopropylphenyl)-86% Methylpolysiloxane Intermediate Polarity n/a Pesticides, PCB s, Drugs, Herbicides, and TMS Sugars 338 AT -210 CAPILLARY COLUMNS 10m 0.25mm 0.20µm 45/260 C mm 1.20µm 45/240 C m 0.25mm 0.25µm 45/260 C mm 0.20µm 45/260 C mm 0.50µm 45/260 C mm 0.15µm 45/260 C mm 0.25µm 45/260 C mm 1.00µm 45/240 C mm 1.20µm 45/240 C m 0.53mm 1.20µm 45/240 C m 0.25mm 0.25µm 45/260 C mm 0.50µm 45/260 C mm 0.15µm 45/260 C mm 0.25µm 45/260 C mm 0.50µm 45/260 C mm 1.00µm 45/240 C mm 1.20µm 45/240 C m 0.25mm 0.25µm 45/260 C mm 0.30µm 45/260 C Monochloroacetic Acid 2. Monobromoacetic Acid 3. Dalapon 4. Dichloroacetic Acid 5. Trichloroacetic Acid 6. Bromochloroacetic Acid 7. Dibromoacetic Acid 0 Column: Temp: Carrier Gas: Detector: EPA Method 552.1: Haloacetic Acids Heliflex AT -1701, 30m x 0.32mm x 0.25µm (Part No ) 50 C (10 min hold) to 120 C at 10 C/min Helium at 35cm/sec ECD Min. To view Alltech s complete chromatogram library, visit AT CAPILLARY COLUMNS 10m 0.25mm 0.20µm -20/280 C mm 1.20µm -20/280 C m 0.25mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 0.50µm -20/280 C mm 1.00µm -20/280 C mm 0.20µm -20/280 C mm 0.15µm -20/280 C mm 1.20µm -20/280 C m 0.25mm 0.20µm -20/280 C mm 0.30µm -20/280 C mm 1.20µm -20/280 C m 0.25mm 0.15µm -20/280 C mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 0.25µm -20/280 C mm 0.25µm -20/280 C 13106* 0.32mm 1.00µm -20/280 C mm 0.50µm -20/280 C mm 1.00µm -20/280 C mm 1.20µm -20/280 C m 0.25mm 0.20µm -20/280 C mm 0.30µm -20/280 C m 0.25mm 0.15µm -20/280 C mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 0.15µm -20/280 C mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 0.50µm -20/280 C mm 1.00µm -20/280 C *10 meter integral guard column. AT CAPILLARY COLUMNS ON 5" CAGE 15m 0.25mm 0.25µm -20/280 C mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 1.00µm -20/280 C mm 1.20µm -20/280 C m 0.25mm 0.25µm -20/280 C mm 0.25µm -20/280 C mm 1.00µm -20/280 C mm 1.00µm -20/280 C mm 1.20µm -20/280 C

12 G C C O L U M N S Alltech Capillary Columns Heliflex AT -WAXms Designed to provide low MS bleed Similar to DB -WAX, Rtx -WAX, Supelcowax -10 Heliflex AT -WAX Similar to DB -WAX, DB -WAXetr, Rtx -WAX, Stabilwax, Carbowax 20M, Supelcowax -10, Innowax, HP -20M, HP -Wax, BP -20, CP-Wax-52-CB, 007 -CW, Superox II, OmegaWAX, ZB-WAX 100% Polyethylene Glycol Polar G14, G15, G16, G39 Mass Spec Analysis AT -WAX CAPILLARY COLUMNS 15m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C mm 1.00µm 40/260 C m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C mm 1.00µm 40/260 C m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C % Polyethylene Glycol Polar G14, G15, G16, G39 FAMEs, Polar Solvents, BTEX, Flavor and Fragrances, Glycols, Alcohols, and Aromatics AT -WAX CAPILLARY COLUMNS CONTINUED 15m 0.32mm 2.50µm 40/260 C mm 0.50µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C mm 150µm 40/250 C mm 2.50µm 40/250 C mm 5.00µm 40/250 C m 0.25mm 0.20µm 40/280 C mm 0.30µm 40/280 C mm 1.20µm 40/260 C m 0.25mm 0.15µm 40/280 C mm 0.20µm 40/280 C mm 0.25µm 40/280 C mm 0.50µm 40/260 C mm 0.25µm 40/280 C mm 0.30µm 40/280 C mm 0.50µm 40/260 C mm 1.00µm 40/260 C mm 0.50µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C mm 1.50µm 40/260 C mm 2.00µm 40/250 C mm 2.50µm 40/250 C mm 5.00µm 40/250 C m 0.25mm 0.20µm 40/280 C mm 0.30µm 40/280 C mm 1.20µm 40/260 C m 0.25mm 0.20µm 40/280 C mm 0.25µm 40/280 C mm 0.50µm 40/260 C mm 0.25µm 40/280 C mm 0.30µm 40/280 C mm 0.50µm 40/260 C mm 0.50µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C mm 1.50µm 40/260 C AT -WAX CAPILLARY COLUMNS 10m 0.25mm 0.25µm 40/280 C mm 0.20µm 40/280 C mm 0.25µm 40/280 C mm 1.20µm 40/260 C m 0.25mm 0.15µm 40/280 C mm 0.20µm 40/280 C mm 0.25µm 40/280 C mm 0.50µm 40/260 C mm 1.00µm 40/260 C mm 0.25µm 40/280 C mm 0.30µm 40/280 C mm 0.50µm 40/260 C mm 1.00µm 40/260 C AT -WAX CAPILLARY COLUMNS ON 5" CAGE 15m 0.25mm 0.25µm 40/280 C mm 0.25µm 40/280 C mm 1.00µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C m 0.25mm 0.25µm 40/280 C mm 0.25µm 40/280 C mm 1.00µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C

13 Alltech Capillary Columns G C C O L U M N S Econo-Cap EC -WAX Batch tested to dramatically reduce price For phase specifications, see Heliflex AT version EC -WAX CAPILLARY COLUMNS 15m 0.45mm 1.00µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C m 0.25mm 0.25µm 40/280 C mm 0.25µm 40/280 C mm 1.00µm 40/260 C mm 1.00µm 40/260 C mm 1.20µm 40/260 C EC -WAX SIX-PACK CAPILLARY COLUMNS 30m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C mm 1.20µm 40/260 C For more information on the Econo-Cap Capillary Line, refer to page 329. Heliflex AT -AquaWax Designed and tested for aqueous injections Similar to DB -Wax, DB -Waxer, Rtx -WAX, Stabilwax, HP -Wax, HP -20M, HP -INNOwax, ZB-Wax and Supelcowax % Polyethylene Glycol Polar n/a Food and Beverage Analysis AT -AQUAWAX CAPILLARY COLUMNS 30m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C Heliflex AT - AquaWax-DA 0 Designed and tested for aqueous injections Eliminates the need for derivatization of acidic organic compounds Similar to DB -FFAP, Stabilwax, HP -FFAP-DA, ZB-FFAP, SPB-1000 and Nukol 1 100% Polyethylene Glycol - Nitroterephthal Acid Modified Polar n/a Analysis of Acidic Organic Compounds and Free Fatty Acids AT -AQUAWAX-DA CAPILLARY COLUMNS 30m 0.25mm 0.25µm 40/250 C mm 0.25µm 40/250 C mm 1.00µm 40/250 C m 0.25mm 0.25µm 40/250 C mm 0.25µm 40/250 C Free Fatty Acids Min Propionic Acid 2. Butyric Acid 3. Valeric Acid 4. Caproic Acid 5. Heptanoic Acid 6. Caprylic Acid 2528 Column: Heliflex AT -AquaWax-DA, 30m x 0.25mm x 0.25µm (Part No ) Temp: 180 C Carrier Gas: Helium at 22cm/sec Detector: FID For Capillary GC Applications, see the GC Applications Section, pages

14 G C C O L U M N S Alltech Capillary Columns Heliflex AT Similar to DB -FFAP, Stabilwax -DA, SPB -1000, Nukol, HP -FFAP, BP -21, CP-Wax -58-CB, 007 -FFAP, OV -351, FFAP, SUPEROX -FA, ZB-FFAP 100% Polyethylene Glycol - Acid Modified High Polarity G25, G35 Free Fatty Acids AT CAPILLARY COLUMNS 10m 0.25mm 0.20µm 40/250 C mm 0.30µm 40/250 C mm 1.20µm 40/250 C m 0.25mm 0.20µm 40/250 C mm 0.25µm 40/250 C mm 0.25µm 40/250 C mm 0.30µm 40/250 C mm 1.00µm 40/250 C mm 1.20µm 40/250 C m 0.25mm 0.20µm 40/250 C mm 0.30µm 40/250 C mm 1.20µm 40/250 C m 0.25mm 0.20µm 40/250 C mm 0.25µm 40/250 C mm 0.25µm 40/250 C mm 0.30µm 40/250 C mm 1.00µm 40/250 C mm 1.20µm 40/250 C mm 2.0µm 40/250 C m 0.25mm 0.20µm 40/250 C mm 0.30µm 40/250 C m 0.25mm 0.20µm 40/250 C mm 0.25µm 40/250 C mm 0.25µm 40/250 C mm 0.30µm 40/250 C mm 1.00µm 40/250 C mm 1.00µm 40/250 C Econo-Cap EC Batch tested to dramatically reduce price For phase specifications, see Heliflex AT version EC CAPILLARY COLUMNS 15m 0.45mm 1.00µm 40/250 C mm 1.00µm 40/250 C mm 1.20µm 40/250 C m 0.25mm 0.25µm 40/250 C mm 0.25µm 40/250 C mm 1.00µm 40/250 C mm 1.00µm 40/250 C mm 1.20µm 40/250 C EC SIX-PACK CAPILLARY COLUMNS 30m 0.25mm 0.25µm 40/250 C mm 0.25µm 40/250 C mm 1.20µm 40/250 C For more information on the Econo-Cap Capillary Line, refer to page 329. Heliflex AT -CAM Eliminates need for derivitazation Similar to Stabilwax -DB, Carbowax Amine, CAM, CP-WAX % Polyethylene Glycol-Base Modified High Polarity G25, G35 Basic Compounds, Amines AT -CAM CAPILLARY COLUMNS 30m 0.32mm 0.25µm 40/250 C mm 0.50µm 40/250 C mm 1.00µm 40/250 C Heliflex AT -FAME Similar to FAMEWAX and OmegaWAX Stable Bonded Polyethylene Glycol High Polarity G25, G35 Fatty Acid Methyl Esters AT -FAME CAPILLARY COLUMNS 30m 0.25mm 0.25µm 40/280 C mm 0.25µm 40/280 C

15 Alltech Capillary Columns G C C O L U M N S Heliflex AT -624 Specially tested for EPA Method 624 Similar to DB -1301, Rtx -1301, Rtx -624, HP -1301, HP -624, DB -624, , , SPB-1301, SPB-624, ZB-624 Heliflex AT -225 Similar to DB -225, HP -225, Rtx -225, OV -225, RSL-500, , CP-Sil 43CB, BP -225, PE-225 6% Cyanopropylphenyl-94% Methylpolysiloxane Intermediate Polarity G43 EPA Methods 524, 601, 602, 624, 8240 and 8260 and Solvent Analysis (50% Cyanopropylphenyl)-50% Methylpolysiloxane Mid to High Polarity G19 Carbohydrates and Solvents AT -624 CAPILLARY COLUMNS 30m 0.25mm 1.40µm -20/260 C mm 1.80µm -20/260 C mm 3.00µm -20/260 C mm 3.00µm -20/260 C m 0.25mm 1.40µm -20/260 C mm 1.80µm -20/260 C mm 3.00µm -20/260 C m 0.53mm 3.00µm -20/260 C AT -225 CAPILLARY COLUMNS 15m 0.25mm 0.20µm 40/240 C mm 0.25µm 40/240 C mm 0.25µm 40/240 C m 0.25mm 0.20µm 40/240 C mm 1.20µm 40/220 C m 0.25mm 0.25µm 40/240 C mm 0.25µm 40/240 C mm 0.30µm 40/240 C mm 1.20µm 40/220 C EPA Method Purgeable Aromatics Benzene 2. Toluene 3. Chlorobenzene 4. Ethylbenzene 5. 1,3-Dichlorobenzene 6. 1,4-Dichlorobenzene 7. 1,2-Dichlorobenzene Heliflex AT -Silar Similar to DB -23, , PE-23, Rtx -2330, SP (50% Cyanopropyl)-50% Methylpolysiloxane High Polarity G5 cis/trans Fatty Acids Methyl Esters Min. Column: Temp: Carrier Gas: Detector: Heliflex AT -624, 30m x 0.32mm x 1.80µm (Part No ) 90 C (7 min hold) to 180 C at 10 C/min Helium at 1.1mL/min FID AT -SILAR CAPILLARY COLUMNS 30m 0.25mm 0.25µm 40/260 C mm 0.25µm 40/260 C mm 0.50µm 40/260 C To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages

16 G C C O L U M N S Alltech Capillary Columns Heliflex AT -Silar-90 Designed and tested for FAME Similar to DB -23, CP-Sil84, Rtx -2330, SP-2330 Heliflex AT -Silar-100 Ideal for high and low temperature separation of samples containing geometric isomers of FAMEs Similar to CO-Sil88, Rtx -2330, SP-2340 Poly (90% bis Cyanopropyl)-10% Cyanopropyphenyl Siloxane High Polarity G8 Analysis of FAMEs Poly bis Cyanopropyl High Polarity Available G8 cis/trans Isomers of FAMEs, Dioxins and Furans SILAR-90 CAPILLARY COLUMNS 15m 0.25mm 0.20µm 0/250 C mm 0.20µm 0/250 C m 0.25mm 0.20µm 0/250 C mm 0.20µm 0/250 C SILAR-100 CAPILLARY COLUMNS 15m 0.25mm 0.20µm 0/250 C mm 0.20µm 0/250 C m 0.25mm 0.20µm 0/250 C mm 0.20µm 0/250 C Fatty Acid Methyl Esters Fatty Acid Methyl Esters in Rapeseed Oil C14:0 2. C16:0 3. C16:1 4. C18:1 5. C18:2 6. C18:3 7. C18: C20:1 9. C20:3 10. C20:4 11. C20:5 12. C20:5 13. C22:4 14. C22:5 15. C22: C14:0 2. C16:0 3. C18:0 4. C18:1 5. C18: C20:0 7. C20:1 8. C18:3 9. C22:0 10. C22: Min Min. Column: Heliflex AT -Silar-90, 30m x 0.25mm x 0.20µm (Part No ) Temp: 200 C Carrier Gas: Helium at 20cm/sec Detector: FID Column: Heliflex AT -Silar-100, 30m x 0.25mm x 0.20µm (Part No ) Temp: 190 C Carrier Gas: Helium at 20cm/sec Detector: FID Tips for Heliflex AT -Silar-90 and Silar-100 Silar-90 and Silar-100 are more susceptible to damage by oxygen, moisture, and HCL than other silicone phases. Avoid solvents such as water and methanol when using on-column injection techniques. Columns should not be rinsed. To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages

17 Alltech Capillary Columns G C C O L U M N S Heliflex Chirasil-Val Cross-linked for thermal stability Ideal for the determination of the optical purity of amino acids and the extent of ra ce m iza tion in peptide synthesis Heliflex AT -Amino Acid Separates all 20 essential amino acids Proprietary Intermediate - Chiral Separations n/a Optical Enantiomers Proprietary Intermediate n/a Amino Acids CHIRASIL-VAL CAPILLARY COLUMNS 20m 0.53mm 0.60µm 40/220 C m 0.25mm 0.16µm 40/220 C mm 0.20µm 40/220 C mm 0.20µm 40/220 C Test Kits Test Mixture*, 250µL Derivatization Kit** for Making Pentafluoropropyl Isopropyl Esters *TFA Isopropyl Esters of 5 Amino Acids **Contains 12.5 ml Acetyl Chloride, 20mL PFPA, and 50mL 2-Propanol AT -AMINO ACID CAPILLARY COLUMN 25m 0.53mm 1.20µm -20/350 C N(O,S)-Heptafluorobutyl-isobutyl Esters of Amino Acids from Soy Protein Hydrolysate 1. Alanine 2. Glycine 3. Valine 4. Threonine 5. Serine 6. Leucine 7. Isoleucine 8. Proline 9. Cystine 10. Methionine 11. Aspartic Acid 12. Phenylalanine 13. Glutamic Acid 14. Lysine 15. Tyrosine 16. Arginine 17. Histidine 18. Tryptophan 1241 R,S-Anticonvulsants S-Mephenytoin 2. R-Mephenytoin 3. S-3-Methyl-5-Isopropyl-5- Phenylhydantoin 4. R-3-Methyl-5-Isopropyl-5- Phenylhydantoin 5. S-5-Phenyl-5-Ethylhydantoin 6. R-5-Phenyl-5-Ethylhydantoin 7. S-5-Phenyl-5-Propylhydantoin 8. R-5-Phenyl-5-Propylhydantoin Min. Column: Heliflex Chirasil-Val, 25m x 0.32mm x 0.20µm (Part No ) Temp: 165 C Carrier Gas: Helium at 1.1mL/min Detector: FID Column: Temp: Carrier Gas: Detector: Heliflex AT -Amino Acid, 25m x 0.53mm x 1.20µm (Part No ) 80 C (2 min hold) to 230 C at 4 C/min Helium at 10mL/min FID To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages

18 G C C O L U M N S Alltech Capillary Columns Drug Analysis Capillaries No derivatization of sample necessary Specially tested for drugs Drug One is a non-polar column that will elute drugs in the same order as an OV -1 or OV -101 packed column. Drug Two is a moderately polar column that will give a retention order similar to OV-17. Drug Three is a special phase for mu lat ed for the analysis of anticonvulsants. Temp. Range: Column: Temp: Carrier Gas: Detector: Proprietary Drug I - Non-Polar, Drug 2 - Intermediate Polarity, Drug 3 - Polar 330 C Isothermal/350 C Programmed n/a Drug Analysis DRUG CAPILLARY COLUMNS LENGTH COATING I.D. FILM PART NO. PRICE 10m Drug One 0.53mm 1.20µm Drug Two 0.53mm 1.20µm Drug Three 0.53mm 1.20µm m Drug One 0.25mm 0.25µm Drug Two 0.25mm 0.25µm Drug One 0.32mm 0.25µm Drug Two 0.32mm 0.25µm Drug Mixture 1. Methylenedioxymethamphetamine ( MDMA) 2. Benzocaine 3. Meperidine 4. Phencyclidine ( PCP) 5. Caffeine 6. Procaine 7. Mepivacaine 8. Methadone 9. Atropine 10. Cocaine 11. Oxazepam 12. Codeine 13. Diazepam Heliflex Drug Two, 30m x 0.25mm x 0.25µm (Part No ) 230 C to 250 C at 5 C/min Helium at 0.64mL/min FID 0042 Heliflex USP 467 Capillary Kits Tested for organic volatile impurities Kits for Method I and V for Metod 467 Guard columns plus connector USP Method 467 deals with the determination of organic volatile impurities in pharmaceuticals, which results from sol vents commonly used in the manufacturing process. Method I Kit contains: AT -5, (USP G27) 30m x 0.53mm x 5.00µm; 5 x Universal FSOT Connectors; and 5 x 5m Deactivated Guard Columns (0.53mm i.d.). Method V Kit contains: AT -624, (USP G43) 30m x 0.53mm x 3.00µm; 5 x Universal FSOT Con nec tors; and 5 x 5m Deactivated Guard Columns (0.53mm i.d.). Temp. Range: Temp. Range: (5% Phenyl)-95% Methylpolysiloxane Non-Polar -60/350 C G27 Drug Analysis (6% Cyanopropylphenyl)-94% Methylpolysiloxane Intermediate 20/260 C G43 Drug Analysis USP CAPILLARY KITS DESCRIPTION PART NO. PRICE Capillary Kits USP 467/Method I Capillary Kit USP 467/Method V Capillary Kit Replacement Components AT -5, 30m x 0.53mm x 5.0µm AT -624, 30m x 0.53mm x 3.0µm Universal FSOT Connectors, 5/pk Deactivated Guard Columns, 5m x 0.53mm, 5/pk To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages For more information on Pharmaceutical analysis, request brochure #

19 Alltech Capillary Columns G C C O L U M N S Heliflex AT -Pesticide Unique selectivity for pesticide confirmation Pretested with pesticide mix Heliflex AT Separates early eluting gases at above ambient temperature Useful for volatile organics analysis, including EPA Methods 502.2, 524.2, 8260 Proprietary Intermediate n/a Chlorinated Pesticides, PCBs Proprietary Intermediate n/a Volatile Organics and EPA Methods 502.2, 524.2, and 8260 AT -PESTICIDE CAPILLARY COLUMNS 20m 0.53mm 0.60µm 40/240 C m 0.25mm 0.25µm 40/240 C mm 0.25µm 40/240 C mm 0.60µm 40/240 C AT CAPILLARY COLUMNS 30m 0.25mm 1.40µm 270 C mm 1.80µm 270 C mm 3.00µm 270 C m 0.25mm 1.40µm 270 C mm 1.80µm 270 C mm 3.00µm 270 C m 0.32mm 1.80µm 270 C mm 3.00µm 270 C Chlorinated Pesticides TCLP Volatiles Mix α-bhc 2. γ-bhc 3. β-bhc 4. δ-bhc 5. Heptachlor 6. Aldrin 7. Heptachlor Epoxide 8. Endosulfan I 9. p,p'-dde 10. Dieldrin 11. Endrin 12. p,p -DDD 13. Endosulfan II 14. p,p -DDT 15. Endrin Aldehyde 16. Endosulfan Sulfate Vinyl Chloride 2. 1,1-Dichloroethene 3. 2-Butanone 4. Chloroform 5. Carbon Tetrachloride 6. Benzene + 1,2-Dichloroethene 7. Trichloroethene 8. Tetrachloroethene 9. Chlorobenzene 10. 1, 4-Dichlorobenzene Min Min. Column: Temp: Carrier Gas: Detector: Heliflex AT -Pesticide, 30m x 0.25mm x 0.25µm (Part No ) 190 C to 240 C at 3 C/min Helium at 0.65mL/min ECD Column: Temp: Carrier Gas: Detector: Heliflex AT , 30m x 0.53mm x 3.00µm (Part No ) 40 C (10min hold) to 120 C at 4 C/min Helium at 22cm/sec FID To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages Need Sample Prep for Your Pesticide Analysis? Florisil -PR is pretested specifically chlorinated pesticides, see page

20 G C C O L U M N S Alltech Capillary Columns Heliflex AT For simulated distillation of petroleum products Heliflex AT -Sulfur Designed for the analysis of volatile sulfur-containing compounds in pe tro leum distillates 100% Methylpolysiloxane Non Polar n/a Petroleum Distillation 100% Methylpolysiloxane Non Polar n/a Volatile Sulfur Compounds AT CAPILLARY COLUMN 10m 0.53mm 1.20µm 350 C Test Mix for AT AT -SULFUR CAPILLARY COLUMNS 30m 0.32mm 4.00µm -20/350 C Heliflex AT For boiling range of gasoline samples Heliflex AT -Amine Separates underivatized amines with no tailing 100% Methylpolysiloxane Non Polar n/a Boiling Point of Gasoline Proprietary - Non bonded Intermediate n/a Amino Acids AT CAPILLARY COLUMN 15m 0.53mm 5.00µm 300 C Test Mix for AT Heliflex AT -Petro For high resolution of complex hydrocarbon mixtures 100% Methylpolysiloxane Non Polar n/a hydrocarbon Mixtures AT -AMINE CAPILLARY COLUMNS LENGTH I.D. FILM MAX. TEMP. PART NO. PRICE 30m 0.25mm 0.25µm 200 C mm 0.25µm 200 C mm 0.25µm 200 C m 0.25mm 0.25µm 200 C mm 0.25µm 200 C mm 0.25µm 200 C For more information about Petrochemical analysis, request brochure #478. To view Alltech s complete chromatogram library, visit AT -PETRO CAPILLARY COLUMN 100m 0.25mm 0.50µm 350 C For Capillary GC Applications, see the GC Applications Section, pages

21 Alltech Capillary Columns G C C O L U M N S PLOT Columns These PLOT (Porous Layer Open Tubular) columns can be used in capillary instruments, or in packed column instruments with a simple adapter kit, and are suitable for use with any detector appropriate for your application (FID, TCD, MSD, etc.). Heliflex AT -Q Porous divinylbenzene polymer Similar to GS-Q, PoraPLOT Q, PoraPLOT Q-HT, Rt-QPLOT, SupelQPLOT, HP-Q PLOT Heliflex AT -Alumina Faster and more efficient than packed alumina columns, with increased sensitivity Similar to GS-Alumina, Rt-Alumina, HP PLOT S, HP PLOT M, Aluminum Oxide Porous Divinylbenzene Polymer n/a Many gases and light hydrocarbons, and other applications currently using packed porous polymer columns Alumina n/a Light hydrocarbon analysis, separation of C1-C4 saturated and unsaturated hydrocarbons AT -Q CAPILLARY COLUMNS LENGTH I.D. TEMP. RANGE PART NO. PRICE 30m 0.53mm -60/250 C mm -60/250 C AT -ALUMINA CAPILLARY COLUMNS LENGTH I.D. TEMP. RANGE PART NO. PRICE 30m 0.53mm -60/200 C m 0.53mm -60/200 C Chlorofluorocarbons and Ethylene Oxide Light Hydrocarbons Min. 1. Methane 2. CF2Cl2 ( Freon -12) 3. Ethylene Oxide Methane 2. Ethane 3. Ethene 4. Propane 5. Propene Isobutane 7. Butene 8. Acetylene 9. trans-2-butene Butene 11. cis-2-butene 12. Isopentane 13. Pentane 14. 1,3-Butadiene 15. Propyne Column: Heliflex AT -Q, 30m x 0.53mm (Part No ) Temp: 180 C Carrier Gas: Helium at 4mL/min Detector: FID Column: Heliflex AT -Alumina, 50m x 0.53mm (Part No ) Temp: 100 C Carrier Gas: Helium at 7.1mL/min Detector: FID To view Alltech s complete chromatogram library, visit For Capillary GC Applications, see the GC Applications Section, pages Need to use 0.53 Columns in a Packed Column Instrument? Use Alltech s 0.53mm Conversion Kit. Kit includes deactivated injector and detector adapter, fittings, and instructions. 0.53MM CONVERSION KITS DESCRIPTION LENGTH PART NO. PRICE Direct Injection kits for 1/4" Ports 6" 5818 Expansion Liner Kit for 1/4" Ports 6"