Grace GC Capillary Column Families

Transcription

1 Grace GC Capillary Column Families Alltech Heliflex High-Performance, Widest Selection of Phases Alltech Econo-Cap Best Value, Popular Phases Grace offers two lines of capillary columns to suit every application and budget; Alltech Heliflex and Alltech Econo-Cap. Heliflex Columns are Grace s line of individually tested capillary columns. Econo-Cap Columns are batch tested to dramatically reduce the price without sacrificing quality. Both the Heliflex and Econo-Cap lines are manufactured under identical conditions using the same high-quality polyimide coated fused silica and immobilized stationary phases. In addition each are mounted on a rugged cage. Regardless of the capillary line you choose, every Grace manufactured capillary column has a guarantee of column performance. Alltech Heliflex Capillary Columns High-performance individually tested columns 7" rugged cage Most complete selection of phases Custom columns available to suit your specific application Heliflex Capillary Columns are manufactured from the highest quality polyimide coated synthetic fused silica. They are mounted on a rugged wear-resistant cage. Each Heliflex Column is individually tested to guarantee column performance and comes with a test chromatogram, instruction manual, capillary end caps, and a free ceramic column cutter. Note: Column nuts and ferrules are not included. If the column you need is not available in our standard offering, request a custom Heliflex Column made to your individual specifications. Alltech Econo-Cap Capillary Columns Best value in capillary columns anywhere Batch tested to dramatically reduce price value Ideal for aggressive applications Available in the most popular phases We ve taken our most popular capillary columns and perfected the manufacturing procedure to the point that reproducibility is assured. This allows us to test these columns in batches instead of individually, while still offering a guarantee. Batch testing significantly reduces cost in production without sacrificing quality. Each Econo-Cap Capillary Column comes with a copy of the batch test results, an instruction manual, and capillary end caps. If you are not completely satisfied with the quality of your Econo-Cap Capillary Column it will be replaced at no charge. Available Alltech Heliflex Phases Phase Page AT -ms 6 AT -ht 6 AT - 7 AT -5ms 8 AT -5 8 AT -0 9 AT -5ms 0 AT -5 0 AT -50 AT -6 6 AT -0 AT -70 AT -0 AT -5 6 AT -WAXms AT -WAX AT -AquaWax AT -AquaWax-DA AT AT -FAME 5 AT -CAM 5 AT -Amino Acid 8 Drug, Drug, and Drug 8 USP Method 67 Kits 9 AT -Pesticide 0 AT AT -Petro AT -887 AT -70 AT -Sulfur AT -Amine AT -Silar-90 7 AT -Silar-00 7 Available Alltech Econo-Cap Phases Phase Page EC - 7 EC -5 9 EC -0 9 EC -WAX EC tech tip Temperature limits Our GC capillary columns are temperature rated. In some cases, we list two maximum operating temperatures, the lower one is for isothermal condition and the higher one for temperatureprogrammed condition. 58 Note: Column nuts and ferrules are not included.

2 Capillary Column Phase Cross Reference Use the chart below to cross reference manufacturers stationary phases as well as USP method designations to Alltech equivalent columns. Slight variations in selectivity may result between different manufacturers columns. Alltech Standard Phase Cross Reference Standard Phase Cross Reference Composition Alltech Brand Usp Designation Similiar Phases 00% Dimethylpolysiloxane AT -ms G, G, G8 DB-ms, HP-ms, Rtx -ms, CP-Sil 5CB low-bleed/ms 00% Dimethylpolysiloxane AT -ht, AT -, EC - G, G, G8 007-, CP-Sil 5CB, DB-, DB-ht, HP-, HP-0, OV -, RSL-50, RSL-60, Rtx -, SE-0, SPB -, SPB -Sulfur, ULTRA-, SP-00, BP-, DC-00, PE-, ZB- 5% Phenyl equivalent Polysilphenylene-Siloxane AT -5ms DB-5ms, Rtx -5 Sil ms, BPX -5, 007-5ms, HP-5ms (5% Phenyl)- 95% methylpolysiloxane (0% Phenyl)- 80% methylpolysiloxane (5 Phenyl)- 65% Methylpolysiloxane (50 Phenyl)- 50% methylpolysiloxane (6% Cyanopropylphenyl)- 9% methylpolysiloxane (% Cyanopropylphenyl)- 86% methylpolysiloxane Trifluoropropylmethyl polysiloxane (50% Cyanopropylphenyl)- 50% methylpolysiloxane Poly(80% biscyanopropyl)- 0% cyanoproylphenyl siloxane Poly(biscyanopropyl siloxane) Polyethyleneglycol Polyethyleneglycol Acid Modified AT -5, EC -5 AT -0, EC -0 AT -5ms AT -5 G7, G6 G8, G G 007-, CP-Sil 8CB, DB-5, DB-5.65, DB-5ht, HP-5, HP-5ms, OV -5, PTE-5, PTE-5QTM, PAS-5, RSL-00, Rtx -5, Rtx -5ms, SAC-5, SE -5, SPB -5, ULTRA-, XTI-5, SE -5, BP-5, PE-, ZB , Rtx -0, SPB -0, VOCOL, PE-7 DB-5ms, Rtx -5, SPB -5, Sup-Herb, MDN-5, BPX , DB-5, DB-5ms, HP-5, RSL-00, Rtx -5, SPB -5, SPB -608, OV -, PE-5, Sup-HERB AT -50 G DB-7ms, H5-50+, Rtx -50, SP-50, SPB -50, SPB -7, BPX -50 DB-7ht, Rtx -65TG, BPX -50, CP-TAB-CB, 007-7, DB-7, DB-7ht, HP-7, HP-50+, Rtx -50 SP-50, SP-50, SPB -50, CP-Sil CB, PE-7, ZB-50 AT -6 G 007-0, DB-6, DB-0, HP-0, HP-6, AT -0 Rtx -0, Rtx -6, SPB -0, SPB -6, 007-6, ZB-6 AT , CP-Sil 9CB, DB-70, HP-70, OV -70, PAS-70, Rtx -70, SPB -70, BP-0, ZB-70 AT -0 G6 DB-0, RSL-00, Rtx -00, OV -0, OV -0, OV -5, QF-, SP-0 AT -5 G , CP-Sil CB, DB-5, HP-5, OV -5, RSL-500, Rtx -5, BP-5, PE-5 AT -SILAR-90 G8 DB-, CP-Sil 8, Rtx -0, SP-0 AT -SILAR-00 G5 CP-Sil 88, Rtx -0, SP-0 AT -WAXms AT -WAX AT -AquaWax EC -WAX AT -000, EC -000, AT -AquaWax-DA G, G5 G6, G0, G9 G5, G5 DB-WAX, Rtx -WAX, Supelcowax CW, Carbowax 0M, CP-Wax 5CB, DB-WAXetr, DB-WAX, Rtx -WAX, HP-0M, HP-Wax, Innowax, Omegawax, Stabilwax, Supelcowax -0, Superox II, BP-0, ZB-WAX 007-FFAP, CP-Wax 58CB, DB -FFAP, HP -FFAP, Nukol, OV -5, SP-000, Stabilwax -DA, Superox -FA, BP- Polyethyleneglycol AT -CAM Stabilwax -DB, CAM, Carbowax Amine, CP Wax 5 Base Modified PONA Analysis AT -Petro F, CP-Sil PONA CB, DB-Petro00, Petrocol DH, PONA, Ttx-PONA, HP-PONA ASTM Method 887 AT V-.0F, DB-887, Petrocol 887, Petrocol EX887, Rtx -887, Sim-Dist-CB ASTM Method 70 AT -70 Petrocol 70 Alltech Specialty Columns Cross Reference Specialty Phases Cross Reference EPA Method 608 AT -Pesticide , DB-608, HP-608, SPB -608 EPA Method 50. AT , , DB-50., DB-VRX, HP-6, HP-VOC, MST-50., MXT-6, MXT-Volatiles, OV -6, Rtx -50., Rtx -6, Rtx -Volatiles, VOCOL Sulfur Analysis AT -Sulfur SPB - Sulfur FAME Analysis AT -FAME FAMEWAX, OmegaWAX

3 Alltech Custom Capillary Columns A wide selection of stationary phases s from to 05 meters Wide selection of tubing Every column individually tested Custom Capillary Column Instructions. Stationary Choose a Phase in Table : Custom Phase.. & Internal Diameter: Choose any length ( 05 meters) and internal diameter (0.0mm ) in Table : Custom Dimensions.. Thickness: Choose a film thickness; 0.0µm tolerance.. See Coiling and Guard Information for additional options. 5. Call Customer Service and they will confirm your order and provide exact prices. Table : Custom Phases Phases Available for Custom Capillary Columns Aquawax DC-550 Igepal CO-880 Aquawax-DA Dexsil 00 OV - AT - Dexsil 00 OV - AT -5 Dexsil 0 OV -7 AT -0 Di (ethylhexyl OV -70 AT -5 phthalate OV -6 AT -000 Diisodecyl phthalate OV -0 AT -0 FFAP OV -05 AT -70 Hi-EFF -AP OV -0 AT -WAX Hi-EFF -BP OV -5 AT -Amine Hi-EFF -AP Polyvinylpyrrolidone Apiezon phases Hi-EFF -BP Reoplex 00 Apolane -87 Hi-EFF -AP SE-0 Butanediol succinate Hi-EFF -BP Squalane (Craig s polyester) Hi-EFF -BP Superox -FA Carbowax phases Hi-EFF -8BP XE-60 Table : Custom Dimensions Alltech Heliflex Custom Capillary Columns Description 5m 0.0mm Specify Phase and mm Specify Phase and Specify Phase and 9700 Specify Phase and mm Specify Phase and 9700 Specify Phase and m 0.0mm Specify Phase and mm Specify Phase and 970 Specify Phase and 9705 Specify Phase and mm Specify Phase and 9705 Specify Phase and m 0.0mm Specify Phase and mm Specify Phase and 9709 Specify Phase and 9700 Specify Phase and mm Specify Phase and 9700 Specify Phase and m 0.8mm Specify Phase and Specify Phase and Specify Phase and mm Specify Phase and Specify Phase and m Specify Phase and 9705 Specify Phase and mm Specify Phase and 9705 Specify Phase and Custom Capillary All other Dimensions not specified 970 Custom Capillary Coiling Custom Coiling Description Custom Capillary on " Cage 970 Custom Capillary Column with Integral Guard Custom Capillary Column with Integral Guard Description Custom with Integral 5m Guard C-500 Custom with Integral 5m Guard C-5500 Custom with Integral 5m Guard C

4 gas chromatography Heliflex AT -ms Heliflex AT -ht Guaranteed low-bleed characteristics Specifically designed for mass spec analysis Highly inert Similar to DB-ms, HP-ms, Rtx -ms, CP-Sil 5CB low-bleed/ms, MDN- AT -ms is a line of high-performance low bleed nonpolar columns designed specifically for use with mass spectrometers. They are ideal for pharmaceutical, environmental, petrochemical, and food and fragrance analysis, or any GC/MS analysis requiring a 00% dimethylpolysiloxane-type polarity capillary column. Heliflex AT -ms Specifications 00% Dimethylpolysiloxane Polarity: Non-polar Max. Temp.: 0/60 C USP Designation: G, G, G8 Ideal For: Mass Spec Analysis for Environmental, PAH, CLP Pesticides, Steroids, and Drugs Faster analysis time for high boiling compounds Better peak detection at lower concentrations Individually bleed tested at 80ºC Similar to 007-, CP-Sil 5CB, DB-, DB-ht, HP-, HP-0, OVTM-, RSL-50, RSL-60, Rtx -, SE-0, SPBTM-, SPBTM-Sulfur, ULTRA-, SP-00, BP-, DC-00, PE-, ZB- Heliflex AT -ht Specifications 00% Dimethylpolysiloxane Polarity: Non-polar Max. Temp.: 80/00 C USP Designation: G, G, G8 Ideal For: High Boiling Compounds Waxes, Crude Oils, and Trigylcerides Figure AT -ms Low Bleed QC Test Chromatogram Bleed Profile Ethylhexanoic Acid -Chlorophenol,7-Heptanediol n-tridecane -Undecanol n-tetradecane Dicyclohexylamine Acenaphthylene n-pentadecane pa m 60m Min. Column: Column Temp: Carrier Gas: Detector: Heliflex AT -ms Capillary Columns -Undecanol Dicyclohexylamine -Chlorophenol n-pentadecane Fluorene Anthracene n-heptadecane. pa 0 Min. Column: Heliflex AT -ms, 0m x x ( 5897) Temp: 5 C (0min hold) to 0 C (0min hold) at 0 C/min Carrier Gas: Helium at 0.65mL/min (.cm/sec) Detector: FID Shorten Your Analysis Time with High-Temperature/Low-Bleed Columns Heliflex AT -ht, 0m x x 0.0µm ( 668) 5ºC (5min hold) to 80ºC at 0ºC/min Helium at 6.cm/sec FID at 90ºC Heliflex AT -ht GC Capillary Columns min. max. 0.0µm C C C C C * min. max m 0m 60m 0.µm 0.µm 0.µm /00 C /00 C /00 C *Isothermal/Temp. program.

5 Heliflex AT - Excellent general purpose columns Similar to DB-, Rtx -, SPB -, SPB -Sulfur, SP-00, HP-, HP-0, ULTRA-, BP-, CP-Sil 5CB, 007-, OV-, SE -0, DC-00, RSL-50, RSL-60, PE-, ZB- Heliflex AT - Specifications 00% Dimethylpolysiloxane Polarity: Non-polar General Purpose Column USP Designation: G, G, G8 Ideal For: General Purpose Econo-Cap EC - Batch tested to dramatically reduce price value Econo-Cap EC - Capillary Columns 0m C C C µm C 9656 Heliflex AT - Capillary Columns 0m 0.0µm C µm C C µm C C 680.0µm C µm C µm C 68 5m 0.0µm C C C µm C C C µm C µm C 95.0µm C µm 60 0 C µm C µm C 685 5m 0.0µm C µm C 95 0m 0.0µm C C C C µm C C 6.00µm C µm C µm C C 55.0µm C µm 60 0 C 908 0m.65µm C µm C µm C 68 50m 0.0µm C m C C µm C C µm C µm C 70.00µm C µm C 80 00m C 97 best value Econo-Cap EC - Capillary Columns, Six Pack 0m C m C m.0µm C

6 gas chromatography Heliflex AT -5ms Heliflex AT -5 Similar to DB-5ms, Rtx -5 Sil ms, HP-5TA, BPX -5, 007-5ms Excellent general purpose columns Similar to DB-5, Rtx -5, SPB -5, HP-5, ULTRA-, BP-5, CP-Sil 8CB, 007-, OV -5, SE -5, SE -5, RSL-00, ZB-5 The AT -5ms capillaries are ideal for environmental, pharmaceutical, and petrochemical analysis, or any GC/MS analysis requiring a 5% phenyl-type polarity capillary column. Heliflex AT -5ms Specifications (5% Phenyl)-95% Methoxpolysiloxane Polarity: Non-polar USP Designation: G7, G6 Ideal For: Mass Spec Analysis General Application Heliflex AT -5 Specifications (5% Phenyl)-95% Methylpolysiloxane Polarity: Non-polar Max. Temp.: 80/00 C USP Designation: G7, G6 Ideal For: General Applications Organophosphorus Pesticides Heliflex AT -5 Capillary Columns TEPP. Famphur 6. EPN Sulfotepp. Carbophenothion 7. Leptophos Monocrotophos 5. Phosmet 8. Azinphos-ethyl Dimethoate 8 Dioxathion 9 Terbufos 6 Phosphamidon Malathion Parathion 6 cis-chlorfenvinphos 7 trans-chlorfenvinphos 5 8 Ethion 0m 5m 5m 0m Column: Temp: Carrier Gas: Detector: Min. Heliflex AT -5ms, 0m x x ( 5807) 0 C (min hold) to 85 C at 5 C/min (min hold) Helium, 6cm/sec MSD 60m Heliflex AT -5ms Capillary Columns 5m 0m 60m * min. max. 0.0µm 0.50µm 0.50µm 0.0µm 00m * * * min. max..65µm.0µm.50µm 0.0µm 0.0µm 0.50µm 0.50µm.0µm.50µm.65µm 5.00µm.0µm 5.00µm C 60 0 C 60 0 C C 60 0 C C C C C C C C C C Heliflex AT -0 Unique polarity between non-polar and mid-range Similar to 007-7, Rtx -0, SPBTM-0, VOCOLTM, PE-7 Heliflex AT -0 Specifications (0% Phenyl)-80% Methylpolysiloxane Polarity: Intermediate Polarity USP Designation: G8, G Ideal For: Volatile Compounds and Solvents Heliflex AT -0 Capillary Columns *Isothermal/Temp. program. 5m 0m 6 min. max..0µm 0 0 C 0 0 C 0 00 C 0 00 C

7 Econo-Cap EC -5 Batch tested to dramatically reduce price value Econo-Cap EC -5 Capillary Columns 5m.0µm C 965 0m C C C 967.0µm C 9657 best value Econo-Cap EC -5 Capillary Columns, Six Pack 0m C C µm C

8 gas chromatography Heliflex AT -5ms Heliflex AT -5 Guaranteed low-bleed Specifically designed for mass spec analysis Similar to DB-5ms, Rtx -5, SPBTM-5, Sup-HerbTM, MDN-5, BPX -5 Ideal column for conformational analysis Similar to DB-5, DB-5ms, Rtx -5, BPX -5, SPB -5, SPB -608, HP-5, 007-, OV -, RSL-00, PE-5, Sup-HerbTM, ZB-5 Heliflex AT -5ms Specifications (5% Phenyl)-65% Methylpolysiloxane Polarity: Intermediate Polarity USP Designation: G Ideal For: Pesticides, Herbicides, Drugs, Aromatics Heliflex AT -5 Specifications (5% Phenyl)-65% Methylpolysiloxane Polarity: Intermediate Polarity USP Designation: G Ideal For: Pesticides, Herbicides, Drugs, Aromatics Heliflex AT -5ms Capillary Column Heliflex AT -5 Capillary Columns min. max C -0 0 C 0m 60m m 5m 5m 0m Tocopherols m d-δ-tocopherol d-β-tocopherol d-γ-tocopherol d-α-tocopherol min. max..0µm.65µm.0µm.0µm 0.50µm.0µm.65µm C C C C -0 0 C C -0 0 C -0 0 C C C C -0 0 C -0 0 C Column: Temp: Carrier: Detector: 5 6 Min. Heliflex AT -5, 5m x x 0.0µm ( 9655) 0 C Hydrogen at 0cm/sec FID 8

9 Heliflex AT -50 General purpose column Similar to DB-7, DB-7ht, Rtx -50, BPX TM -50, SPB TM -50, SP-50, HP-50+, HP-7, 007-7, OV -7, CP-Sil CB, PE-7, ZB-50 Heliflex AT -0 Unique polarity makes it ideal for a range of applications Similar to BP6, DB-0, Rtx -0, Rtx -6, HP-0, HP-6, DB-6, 007-6, 007-0, SPB -0, SPB TM -6, ZB-6 Heliflex AT -50 Specifications (50% Phenyl)-Methylpolysiloxane Polarity: Intermediate Polarity USP Code: G Ideal For: Pesticides, Herbicides, Phthalate Esters, Free Phenols, and Basic Drugs Heliflex AT -0 Specifications (6% Cyanopropylpenyl)-Methylpolysiloxane Polarity: Intermediate Polarity USP Code: G Ideal For: Volatile Organics, Pharmaceuticals, and EPA Method 6 Heliflex AT -50 Capillary Columns 5m 0 5 C C 876 0m 0 5 C C µm 0 00 C C 878 Heliflex AT -0 Capillary Columns 0m C µm C

10 Heliflex AT -0 Similar to DB- 0, Rtx -00, OV - 0, OV -0, OV -5, QF-, SP-0, RSL-00 Heliflex AT -70 Similar to DB-70, OV -70, SPB -70, Rtx -70, , PAS-70, CP-Sil 9CB, HP-70, BP-0, ZB-70 Heliflex AT -0 Specifications Trifluoropropyl Methylpolysiloxane Polarity: Polar USP Code: G6 Ideal For: Ketones, Aldehydes, Silanes, Glycols, Nitro Aromatics, Herbicides, and Method 80 and 609 Heliflex AT -70 Specifications (% Cyanopropylphenyl)-86% Methylpolysiloxane Polarity: Intermediate Polarity USP Code: n/a Ideal For: Pesticides, PCB s, Drugs, Herbicides, and TMS Sugars Heliflex AT -0 Capillary Columns 5m 5 0 C 7.0µm 5 0 C m 5 0 C 6.0µm 5 0 C 9850 EPA Method 55.: Haloacetic Acids 05 Heliflex AT -70 Capillary Columns 5m C C 76 0m C C C C C 795.0µm C 80 60m C C C C C. Monochloroacetic Acid. Monobromoacetic Acid. Dalapon. Dichloroacetic Acid 5. Trichloroacetic Acid 6. Bromochloroacetic Acid 7. Dibromoacetic Acid Min. Column: Temp: Carrier Gas: Detector: Heliflex AT -70, 0m x x ( 690) 50 C (0min hold) to 0 C at 0 C/min Helium at 5cm/sec ECD 0

11 Heliflex AT -WAXms Designed to provide low MS bleed Similar to DB-WAX, Rtx -WAX, Supelcowax TM -0 Heliflex AT -WAX Similar to DB-WAX, DB-WAXetr, Rtx -WAX, Stabilwax, Carbowax 0M, Supelcowax TM -0, Innowax, HP-0M, HP-Wax, BP-0, CP-Wax 5-CB, 007-CW, Superox II, OmegaWAX, ZB-WAX Heliflex AT -WAXms Specifications 00% Polyethylene Glycol Polarity: Polar USP Code: G, G5, G6, G9 Ideal For: Mass Spec Analysis Heliflex AT -WAX Specifications 00% Polyethylene Glycol Polarity: Polar USP Code: G, G5, G6, G9 Ideal For: FAMEs, Polar Solvents, BTEX, Flavor and Fragrances, Glycols, Alcohols, and Aromatics Heliflex AT -WAXms Capillary Columns 0m 0 60 C C m 0 60 C 605 Heliflex AT -WAX Capillary Columns 0m.0µm 0 60 C m 0.50µm 0 60 C µm 0 60 C C 76 5m 0.50µm 0 60 C C 90.0µm 0 60 C m 0.0µm 0 80 C µm 0 80 C 995.0µm 0 60 C m 0.0µm 0 80 C C µm 0 60 C C µm 0 80 C µm 0 60 C C µm 0 60 C 0 60 C 907.0µm 0 60 C m 0.0µm 0 80 C µm 0 60 C 96 60m 0.0µm 0 80 C C C µm 0 80 C µm 0 60 C C 99.0µm 0 60 C 850

12 gas chromatography Econo-Cap EC -WAX Batch tested to dramatically reduce price For phase specifications, see Heliflex AT version Heliflex AT -AquaWax-DA Designed and tested for aqueous injections Eliminates the need for derivatization of acidic organic compounds Similar to DB-FFAP, Stabilwax, HP-FFAP-DA, ZB-FFAP, SPBTM-000, and Nukol value Econo-Cap EC -WAX Capillary Columns 5m 0m min. max..0µm.0µm 0 60 C 0 80 C 0 80 C 0 60 C Econo-Cap EC -WAX Six-Pack Capillary Columns 0m min. max..0µm 0 60 C 0 60 C 0 60 C Heliflex AT -AquaWax-DA Specifications 00% Polyethylene Glycol Nitroterephthal Acid Modified Polarity: Polar USP Code: n/a Ideal For: Analysis of Acidic Organic Compounds and Free Fatty Acids Heliflex AT -AquaWax-DA Capillary Columns best value m 60m min. max C 0 50 C 0 50 C 0 50 C more info Free Fatty Acids For more information on the Econo-Cap Capillary Line, refer to page. 58 Heliflex AT -AquaWax Designed and tested for aqueous injections Similar to DB-Wax, DB-Waxer, Rtx -WAX, Stabilwax, HP-Wax, HP-0M, HP-Innowax, ZB-Wax, and SupelcowaxTM-0 0 0m 60m min. max C 0 60 C 0 60 C 0 60 C Propionic Acid Butyric Acid Valeric Acid Caproic Acid Heptanoic Acid Caprylic Acid 0 Min. Column: Heliflex AT -AquaWax-DA, 0m x x ( 57) Temp: 80 C Carrier Gas: Helium at cm/sec Detector: FID Heliflex AT -AquaWax Capillary Columns Heliflex AT -AquaWax Specifications 00% Polyethylene Glycol Polarity: Polar USP Code: n/a Ideal For: Food and Beverage Analysis

13 Heliflex AT -000 Similar to DB -FFAP, Stabilwax -DA, SPB -000, Nukol, HP-FFAP, BP-, CP-Wax-58-CB, 007-FFAP, OV -5, FFAP, Superox -FA, ZB-FFAP Heliflex AT -000 Specifications 00% Polyethylene Glycol Acid Modified Polarity: High Polarity USP Code: G5, G5 Ideal For: Free Fatty Acids Heliflex AT -000 Capillary Columns 0m.0µm 0 50 C m 0 50 C 87.0µm 0 50 C m 0.0µm 0 50 C µm 0 50 C 975 0m 0 50 C C µm 0 50 C C 877.0µm 0 50 C µm 0 50 C 07 50m 0.0µm 0 50 C µm 0 50 C m 0 50 C C µm 0 50 C C C 879 Heliflex AT -FAME Similar to FAMEWAX and OmegaWAX Heliflex AT -FAME Specifications Stable Bonded Polyethylene Glycol Polarity: High Polarity USP Code: G5, G5 Ideal For: Fatty Acid Methyl Esters Heliflex AT -FAME Capillary Columns 0m 0 80 C C 8 Econo-Cap EC -000 Batch tested to dramatically reduce price For phase specifications, see Heliflex AT version value Econo-Cap EC -000 Capillary Columns 5m.0µm 0 50 C 968 0m 0 50 C C µm 0 50 C 9688 best value Econo-Cap EC -000 Six-Pack Capillary Columns 0m 0 50 C µm 0 50 C

14 Heliflex AT -6 Specially tested for EPA Method 6 Similar to DB -0, Rtx -0, Rtx -6, HP-0, HP-6, DB -6, 007-6, 007-0, SPB -0, SPB -6, ZB-6 Heliflex AT -5 Similar to DB -5, HP-5, Rtx -5, OV -5, RSL-500, 007-5, CP-Sil CB, BP-5, PE-5 Heliflex AT -6 Specifications 6% Cyanopropylphenyl-9% Methylpolysiloxane Polarity: Intermediate Polarity USP Code: G Ideal For: EPA Methods 5, 60, 60, 6, 80 and 860, and Solvent Analysis Heliflex AT -5 Specifications (50% Cyanopropylphenyl)-50% Methylpolysiloxane Polarity: Mid to High Polarity USP Code: G9 Ideal For: Carbohydrates and Solvents Heliflex AT -6 Capillary Columns 0m.0µm C 75.80µm C µm C µm C m.0µm C 50.80µm C µm C m.00µm C 97 EPA Method 60 Purgeable Aromatics Heliflex AT -5 Capillary Columns 5m 0 0 C 88 5m 0.0µm 0 0 C 955 0m 0 0 C C µm 0 0 C 90.0µm 0 0 C Benzene. Toluene. Chlorobenzene. Ethylbenzene 5.,-Dichlorobenzene 7 6.,-Dichlorobenzene 7.,-Dichlorobenzene Min. Column: Temp: Carrier Gas: Detector: Heliflex AT -6, 0m x x.80µm ( 756) 90 C (7min hold) to 80 C at 0 C/min Helium at.ml/min FID

15 Heliflex AT -Silar-90 Designed and tested for FAME Similar to DB -, CP-Sil 8, Rtx -0, SP-0 Heliflex AT -Silar-00 Ideal for high and low temperature separation of samples containing geometric isomers of FAMEs Similar to CO-Sil 88, Rtx -0, SP-0 Heliflex AT -Silar-90 Specifications Poly (90% bis Cyanopropyl)-0% Cyanopropyphenyl Siloxane Polarity: High Polarity USP Code: G8 Ideal For: Analysis of FAMEs Heliflex AT -Silar-00 Specifications Poly bis Cyanopropyl Polarity: High Polarity Available USP Code: G8 Ideal For: cis/trans Isomers of FAMEs, Dioxins, and Furans Heliflex AT -Silar-90 Capillary Columns 5m 0.0µm 0 50 C 67 0m 0.0µm 0 50 C µm 0 50 C Fatty Acid Methyl Esters C:0. C6:0. C6:. C8: 5. C8: 6. C8: 7. C8: 8. C0: 9. C0: C0:. C0:5. C:. C:5. C:6 Heliflex AT -Silar-00 Capillary Columns 5m 0.0µm 0 50 C 6 0m 0.0µm 0 50 C 6 0.0µm 0 50 C 6 Fatty Acid Methyl Esters in Rapeseed Oil C:0. C6:0. C8:0. C8: 5. C8: 6. C0: C0: 8. C8: 9. C:0 0. C: Min Min. Column: Heliflex AT -Silar-90, 0m x x 0.0µm ( 09) Temp: 00 C Carrier Gas: Helium at 0cm/sec Detector: FID Column: Heliflex AT -Silar-00, 0m x x 0.0µm ( 0) Temp: 90 C Carrier Gas: Helium at 0cm/sec Detector: FID 5

16 Heliflex AT -Amino Acid Separates all 0 essential amino acids Heliflex AT -Amino Acid Specifications Proprietary Polarity: Intermediate USP Code: n/a Ideal For: Amino Acids Heliflex AT -Amino Acid Capillary Column 5m.0µm C 686 N(O,S)-Heptafluorobutyl-isobutyl Esters of Amino Acids from Soy Protein Hydrolysate. Alanine. Glycine. Valine. Threonine 5. Serine 6. Leucine 7. Isoleucine 8. Proline 9. Cystine 0. Methionine. Aspartic Acid. Phenylalanine Glutamic Acid. Lysine 5. Tyrosine 6. Arginine 7. Histidine 8. Tryptophan Min. Column: Temp: Carrier Gas: Detector: Heliflex AT -Amino Acid, 5m x x.0µm ( 686) 80 C (min hold) to 0 C at C/min Helium at 0mL/min FID 6

17 Heliflex AT -50. Separates early eluting gases at above ambient temperature Useful for volatile organics analysis, including EPA Methods 50., 5., 860 Heliflex AT -50. Specifications Proprietary Polarity: Intermediate USP Code: n/a Ideal For: Volatile Organics and EPA Methods 50., 5., and 860 Heliflex AT -50. Capillary Columns Temp. Limit max. 60m.0µm 70 C µm 70 C µm 70 C 79 05m.80µm 70 C 79.00µm 70 C TCLP Volatiles Mix Vinyl Chloride.,-Dichloroethene. -Butanone. Chloroform 5. Carbon Tetrachloride 6. Benzene +,-Dichloroethene 7. Trichloroethene 8. Tetrachloroethene 9. Chlorobenzene 0.,-Dichlorobenzene Min. Column: Temp: Carrier Gas: Detector: Heliflex AT -50., 0m x x.00µm ( 79) 0 C (0min hold) to 0 C at C/min Helium at cm/sec FID 7

18 Heliflex AT -Sulfur Designed for the analysis of volatile sulfurcontaining compounds in petroleum distillates Heliflex AT -Sulfur Specifications 00% Methylpolysiloxane Polarity: Non-Polar USP Code: n/a Ideal For: Volatile Sulfur Compounds Heliflex AT -Sulfur Capillary Columns Temp. Limit min. max. 0m.00µm C 09 Heliflex AT -70 For boiling range of gasoline samples Heliflex AT -70 Specifications 00% Methylpolysiloxane Polarity: Non-Polar USP Code: n/a Ideal For: Boiling Point of Gasoline Heliflex AT -70 Capillary Column Temp. Limit max. 5m 5.00µm 00 C 99 Heliflex AT -Petro For high resolution of complex hydrocarbon mixtures Heliflex AT -Petro Specifications 00% Methylpolysiloxane Polarity: Non-Polar USP Code: n/a Ideal For: hydrocarbon Mixtures Heliflex AT -Petro Capillary Column Temp. Limit max. 00m 0.50µm 50 C

19 Alltech Column Guide to EPA Methods Alltech Guide to Capillary Columns for Environmental Analysis Method Description and Recommended Columns Comments 50. Trihalomethanes in Drinking Water Heliflex AT -6, 0m x x.00µm Volatile Halogenated Organics by Purge and Trap GC/ELCD Heliflex AT -6, 0m x x.00µm Subambient 6889 Heliflex AT -6, 60m x x.00µm Ambient Volatile Organics in Water by Purge and Trap GC/PID/ELCD Heliflex AT -50., 05m x x.00µm 79 Heliflex AT -6, 60m x x.00µm DBE and DBCP by Microextraction GC/ECD Econo-Cap EC -, 0m x x (Inexpensive, Batch QC ed Column) Organohalide Pesticides and PCBs by Microextraction and GC/ECD Heliflex AT -, 0m x x Primary Column Phthalate and Adipate Esters in Water (GC/PID) Heliflex AT -, 0m x x 60 Heliflex AT -5, 0m x x Nitrogen and Phosphorus Containing Pesticides by GC/NPD Heliflex AT -5, 0m x x Primary Column 656 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) 967 Heliflex AT -70, 0m x x Confirmation Column Chlorinated Pesticides by GC/ECD Heliflex AT -5, 0m x x Primary Column 656 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) 967 Heliflex AT -70, 0m x x Alternate Column Chlorinated Acids by GC/ECD Heliflex AT -5, 0m x x Primary Column 656 Econo-Cap EC -5 Econo-Cap, 0m x x (Inexpensive, batch QC ed column) 967 Heliflex AT -70, 0m x x Confirmation Column Purgeables by Purge and Trap GC/MS Heliflex AT -6, 0m x x.00µm Subambient (0 C) 6889 Heliflex AT -6, 60m x x.00µm Ambient 800 Heliflex AT -5, 0m x x Subambient, Cryofocusing 659 Heliflex AT -5, 0m x x Subambient, Cryofocusing Organic Compounds in Water by Liquid-Solid Extraction and Capillary GC/MS Heliflex AT -5ms, 0m x x 589 Heliflex AT -5ms, 0m x x Endothall in Drinking Water Heliflex AT -, 0m x x 68 Heliflex AT -5, 0m x x Chlorination Disinfection By-products and Chlorinated Solvents in Drinking Water Heliflex AT -, 0m x x 6 Econo-Cap EC -, 0m x x (Inexpensive, Batch QC ed Column) Haloacetic Acids in Drinking Water Heliflex AT -70, 0m x x

20 Alltech Column Guide to EPA Methods (continued) Alltech Guide to Capillary Columns for Environmental Analysis (continued) Method Description and Recommended Columns Comments 60 Purgeable Halocarbons by Purge and Trap ELCD Heliflex AT -6, 0m x x.00µm Subambient 6889 Heliflex AT -6, 60m x x.00µm Ambient Purgeable Aromatics by Purge and Trap GC/PID Heliflex AT -6, 0m x x.00µm 6889 Econo-Cap EC -WAX, 0m x x.0µm (Inexpensive, Batch QC ed Column) Acrolein and Acrylonitrile by GC/FID Heliflex AT -6, 0m x x.00µm Phenols by GC/FID and GC/ECD Heliflex AT -5, 0m x x.0µm 9550 Econo-Cap EC -5, 0m x x.0µm (Inexpensive, Batch QC ed Column) 9657 Heliflex AT -5, 0m x x 658 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) 966 Heliflex AT -5, 0m x x 656 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) Phthalate Esters by GC/ECD Heliflex AT -5, 5m x x.0µm 9555 Econo-Cap EC -5, 5m x x.0µm (Inexpensive, Batch QC ed Column) Nitrosamines Heliflex AT -5, 5m x x.0µm 9555 Econo-Cap EC -5, 5m x x.0µm (Inexpensive, Batch QC ed Column) Nitroaromatics and Isophorone by GC/FID and GC/ECD Heliflex AT -5, 5m x x.0µm (Capillary GC) Polynuclear Aromatic Hydrocarbons by GC/FID Heliflex AT -5, 0m x x.0µm 9550 Econo-Cap EC -5, 0m x x.0µm (Inexpensive, Batch QC ed Column) 9657 Heliflex AT -5, 0m x x Polynuclear Aromatic Hydrocarbons by HPLC and GC/FID Heliflex AT -5, 0m x x 658 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) 966 Heliflex AT -5, 0m x x 656 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) Haloethers by GC/HSD Heliflex AT -5, 5m x x.0µm 9555 Econo-Cap EC -5, 5m x x.0µm (Inexpensive, Batch QC ed Column) Chlorinated Hydrocarbons by GC/ECD Heliflex AT -5, 5m x x.0µm 9555 Econo-Cap EC -5, 5m x x.0µm (Inexpensive, Batch QC ed Column) Chlorinated Herbicides by GC/ECD/ELCD Heliflex AT -, 0m x x 60 Econo-Cap EC -, 0m x x (Inexpensive, Batch QC ed Column) Triazine Herbicides Heliflex AT -50, 0m x x Purgeables by Purge and Trap GC/MS Heliflex AT -6, 0m x x.00µm Subambient (0 C) 6889 Heliflex AT -6, 60m x x.00µm Ambient 800 Heliflex AT -5, 0m x x Subambient, Cryofocusing 659 Heliflex AT -5, 0m x x Subambient, Cryofocusing Base/Neutral and Acids by GC/MS See Method Pesticides and PCBs in Water and Soil/Sediment by GC/MS Heliflex AT -5ms, 0m x x EDB and DBCP by Microextraction Using GC Heliflex AT -, 0m x x

21 Alltech Column Guide to EPA Methods (continued) Alltech Guide to Capillary Columns for Environmental Analysis (continued) Method Description and Recommended Columns Comments 805 Nonhalogenated Volatile Organics Heliflex AT -WAX, 0m x x 907 Heliflex AT -5, 0m x x.50µm Acrylamide by GC/ECD Heliflex AT -000, 5m x x.0µm Acetonitrile by GC/NPD Heliflex AT -WAX, 5m x x Phenols by GC/FID/(ECD) Heliflex AT -5, 0m x x.50µm 909 Heliflex AT -70, 0m x x Nitrosamines Heliflex AT -5, 5m x x.0µm 9555 Econo-Cap EC -5, 5m x x.0µm (Inexpensive, Batch QC ed Column) Organochlorine Pesticides by GC/ECD Heliflex AT -5, 0m x x 657 Heliflex AT -5, 0m x x 796 Heliflex AT -70, 0m x x 795 Heliflex AT -5, 0m x x.50µm Polychlorinated Biphenyls (PCBs) by GC/ECD or GC/ELCD Heliflex AT -5, 0m x x 657 Heliflex AT -5, 0m x x 796 Heliflex AT -70, 0m x x 795 Heliflex AT -5, 0m x x.50µm Nitroaromatics and Cyclic Ketones by GC/ECD or GC/NPD Heliflex AT -5, 0m x x.50µm 909 Heliflex AT -70, 0m x x Polynuclear Aromatic Hydrocarbons by GC/FID Heliflex AT -5, 0m x x.0µm 9550 Econo-Cap EC -5, 0m x x.0µm (Inexpensive, Batch QC ed Column) 9657 Heliflex AT -5, 0m x x 658 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) 966 Heliflex AT -5, 0m x x 656 Econo-Cap EC -5, 0m x x (Inexpensive, Batch QC ed Column) Haloethers by GC/ECD Heliflex AT -5, 0m x x.50µm 909 Heliflex AT -70, 0m x x.0µm 80 8 Organophosphorus Pesticides by GC/NPD/FPD/ELCD Heliflex AT -0, 5m x x.0µm Column 9855 Heliflex AT -5, 5m x x.0µm Column 9555 Econo-Cap EC -5, 5m x x.0µm (Inexpensive, Batch QC ed Column) Chlorinated Herbicides by GC/ECD Using Methylation and Pentafluorobenzylation Derivatization Heliflex AT -5, 0m x x 656 Heliflex AT -5, 0m x x 659 Heliflex AT -5, 0m x x 6 Heliflex AT -70, 0m x x 686 Heliflex AT -70, 0m x x Volatile Organics by GC/MS: Capillary Column Technique Heliflex AT -6, 0m x x.00µm Subambient (0 C) 6889 Heliflex AT -6, 60m x x.00µm Ambient 800 Heliflex AT -5, 0m x x Subambient, Cryofocusing 659 Heliflex AT -5, 0m x x Subambient, Cryofocusing 657 Heliflex AT -50., 60m x x.00µm Ambient 79 Heliflex AT -50., 05m x x.00µm Ambient 79