The performance you demand... the service you deserve... from the company you trust. Updated with:

Transcription

1 Equity Capillary GC Columns The performance you demand... the service you deserve... from the company you trust. Updated with: NEW Equity-0 columns New Applications sigma-aldrich.com/supelco

2 The performance you demand... the service you deserve... from the company you trust. Choose Equity for consistent, reproducible performance with: Special Purpose GC/MS Analyses Demanding Environmental Methods General Purpose Applications Table of Contents Equity Column Quick Look-Up Guide... The Resolution You Need... The Analyte Response You Require... The Low Bleed You Expect... The Column Life You Count On... 0 Equity Applications Alcohols Blood Alcohol (SPME/GC)... Hydrocarbons and Alcohols (GC)... Fusel Oils in Vodka (GC)... Alditol Acetates (GC)... Amines (GC)... Low Molecular Weight (GC)... Anilines (GC)... BAMEs Bacterial Acid Methyl Esters (GC)... Dioxin and Furans (GC/MS)... Drugs Drug Screen on Equity- (GC/MS)... Drug Screen on Equity-0 (GC/MS)... Foods, Flavors and Fragrances Distilled Lime Oil (GC)... 0 Cold Pressed Lemon Oil (GC)... Fuels Fuel Oils, (GC)... Fuel Oils,, (GC)... Glycols Glycols and Diols (GC)... Haloacetic Acids US EPA Method. Haloacetic Acids (GC)... Herbicides US EPA Method Chlorinated Acids (GC)... Hydrocarbons Simple Hydrocarbons (GC)... Hydrocarbons and Alcohols (GC)... Diesel Fuel (GC)... Unleaded Gasoline (GC)... Ketones Impurities in Methyl Ethyl Ketone (GC)... Odors Trace Odors in Drinking Water (SPME/GC)... PCBs US EPA Method 0 Polychlorinated Biphenyls (GC)... 0 US EPA Method 0 Polychlorinated Biphenyls (Fast GC)... Pesticides US EPA Method 0 Chlorinated Pesticides (GC)... US EPA Method 0 Chlorinated Pesticides (Fast GC)... US EPA Method 0 Chlorinated Pesticides (GC)... US EPA Method Organophosphorus Pesticides (GC)... US EPA Method Organophosphorus Pesticides (GC/MS)... Phenols US EPA Method 0 Phenols (GC)... US EPA Method 0 Methylated Phenols (GC)... Semivolatiles Phthalate Esters (GC)... US EPA Method 0 Semivolatile Compounds (GC/MS), Primary Analyte List... US EPA Method 0 Semivolatile Compounds (GC/MS), Supplemental Appendix IX List... Solvents Industrial Solvents (GC)... 0 Pharmaceutical Solvents, Class (GC)... Pharmaceutical Solvents, Class (GC)... Pharmaceutical Solvents, Class (GC)... Residual Solvents (GC)... Volatiles Indoor Air (GC/MS)... Popular GC Accessories Agilent Technologies Instruments... PerkinElmer Instruments... Varian Instruments... Services and Support... 0 Ordering Information...

3 Supelco s new and improved line of capillary GC columns consistently deliver the resolution you need, the low bleed you expect, and the column life you count on. Supelco s new and improved Equity Capillary GC Columns deliver the capillary GC column performance you demand for your nonpolar applications. Significant improvements in the polymer chemistry are at the heart of the enhanced performance you will receive with our new Equity Capillary GC Columns. The polymer improvements result in better cross-linking, higher thermal stability, and superior product reproducibility. The consistent resolution, analyte response, low bleed, and column life from one Equity column to the next will allow you to reliably transfer methods between sites or instruments within the same site. Also, maintain the expected column performance over time within the same instrument when you need to replace your column. The reproducible performance Equity provides will minimize time consuming method adjustments and troubleshooting with column changes. This equals more tests run with higher confidence. Equity Capillary GC Column Quick Look-Up Guide The following table provides an overview of the current capillary GC columns available in the new Equity line. For more detailed ordering information please refer to page of this brochure. Equity- Equity- Equity-0 Phase bonded; poly(dimethylsiloxane) bonded; poly (% diphenyl/ bonded; poly (% cyanopropylphenyl/ % dimethylsiloxane) % dimethylsiloxane) Temperature Limits 0. and 0.mm ID: 0. and 0.mm ID: 0. and 0.mm ID: -0 C to /0 C -0 C to /0 C subambient to 0 C 0.mm ID: 0.mm ID: 0.mm ID: -0 C to 00/0 C (<=.µm df) -0 C to 00/0 C (<=.µm df) subambient to 0 C -0 C to 0/0 C (>.µm df) -0 C to 0/0 C (>.µm df) Column IDs 0.0, 0., 0., 0.0, 0.0, 0., 0., 0.0, 0., 0., and 0.mm IDs, and 0.mm IDs and 0.mm IDs Column Lengths varies; 0 to 00 meters varies; to 0 meters varies; to 0 meters Column Film Thickness varies; 0.0 to.0µm varies; 0.0 to.0µm varies; 0. to.µm Custom Dimensions yes; please inquire for details on yes; please inquire for details on yes; please inquire for details on custom dimensions custom dimensions custom dimensions

4 The Resolution You Need Equity- Resolution of Aromatics Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C, 0 C/min to 00 C ( min) Inj.: 00 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, 00: split Sample: UST Modified Gasoline Range Organics (Cat. No. ) Excellent baseline separation. Methyl tert-butyl ether. Benzene. Toluene. Ethylbenzene. m/p-xylene. o-xylene.,,-trimethylbenzene.,,-trimethylbenzene. Naphthalene 0 G00 Equity- Resolution of Pesticides Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), C/min to 00 C ( min) Inj.: C Det.: ECD, 00 C Carrier Gas: Helium, 00 C Injection: µl, splitless Sample: 0pg on-column of a component EPA Method 0 pesticide standard Excellent baseline separation 0. g-chlordane. Endosulfan I. a-chlordane., -DDE. Dieldrin. Endrin. Endosulfan II., -DDD. Endrin aldehyde 0. Endosulfan sulfate., -DDT G000 Equity-0 Resolution of Pesticides Column: 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 00 C ( min), C/min to 0 C, C/min to 0 C (0 min) Inj.: C Det.: ECD, 0 C Carrier Gas: Helium, C Injection: µl, splitless (0. min) Sample: 0ppb of a component chlorinated pesticide standard (Cat. No. -U) 0 Peak ID s on page.0.0 G000

5 For accurate identification, reliable quantitation, and confidence in your results, choose Equity Capillary GC columns. The consistently high resolution you demand and the service you deserve. Equity- Reproducible Resolution Across Phase Lots and Manufacturing Batches Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C, 0 C/min to 00 C ( min) Inj.: 00 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, 00: split Sample: UST Modified Gasoline Range Organics (Cat. No. ). Ethylbenzene. m/p-xylene. o-xylene.,,-trimethylbenzene.,,-trimethylbenzene Phase Lot Phase Lot Phase Lot G00,, Equity- Reproducible Resolution Across Phase Lots and Manufacturing Batches Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to C ( min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier Gas: Helium, 0 C Injection: µl, splitless Sample: ng on-column of a component semivolatile standard. Benzo(b)fluoranthene. Benzo(k)fluoranthene Phase Lot Phase Lot Phase Lot G0000, 0, 0 Equity-0 Reproducible Resolution Across Phase Lots and Manufacturing Batches.,,,-Tetrachlorom-xylene (surr.). a-bhc. g-bhc. Heptachlor. Aldrin. b-bhc. d-bhc. Heptachlor epoxide. Endosulfan I 0. g-chlordane. a-chlordane., -DDE. Dieldrin. Endrin., -DDD. Endosulfan II., -DDT. Endrin aldehyde. Methoxychlor 0. Endosulfan sulfate. Endrin ketone. Decachlorobiphenyl (surr.) Run conditions same as page. 0 0 Excellent peak shape, resolution and analyte response Phase Lot Phase Lot Phase Lot G00 G00 G000

6 The Analyte Response You Require Equity- Excellent Analyte Response Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C, C/min to 0 C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, 0: split Sample: Grob Test Mix (Cat. No. 0),-Butanediol: Excellent response and peak symmetry 0.,-Butanediol. Decane. Octanol.,-Dimethylphenol. Nonanal. Undecane. -Ethyl hexanoic acid.,-dimethylaniline. Methyl decanoate Methyl undecanoate. Methyl dodecanoate G000 Equity- Excellent Analyte Response Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to C ( min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier Gas: Helium, 0 C Injection: µl, splitless Sample: ng on-column of a component semivolatile standard Excellent response and peak symmetry for pentachlorophenol and benzidine. Pentachlorophenol. Phenanthrene. Anthracene. Benzidine G000 Equity-0 Excellent Analyte Response 0 Column: 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 00 C ( min), C/min to 0 C, C/min to 0 C (0 min) Inj.: C Det.: ECD, 0 C Carrier Gas: Helium, C Injection: µl, splitless (0. min) Sample: 0ppb of a component chlorinated pesticide standard (Cat. No. -U) Excellent response Peak ID s on page G000

7 For lower detection limits and less instrument downtime, you can depend on Equity Capillary GC columns. The reproducible analyte response you demand and the service you deserve. Equity- Reproducible Analyte Response Across Phase Lots and Manufacturing Batches Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection:.0µL, 00: split Sample: Nonpolar Column Test Mix (Cat. No. 00-U) % Response: Calculated relative to the predicted hydrocarbon response at the same retention time % Response % % % % % % % % % % % Consistent Response for -Octanol % 0% % % % % % % % % % % 0 Different Phase Lots and Manufacturing Batches G000 Equity- Reproducible Analyte Response Across Phase Lots and Manufacturing Batches % Consistent Response for,-dimethylaniline Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, 00: split Sample: Nonpolar Column Test Mix (00-U) %Response: Calculated relative to the predicted hydrocarbon response at the same retention time % Response % % % % % 0% % % 0% 0% % % % Different Phase Lots and Manufacturing Batches G000 Equity-0 Reproducible Analyte Response Across Phase Lots and Manufacturing Batches.,,,-Tetrachloro-m-xylene (surr.). a-bhc. g-bhc. Heptachlor. Aldrin. b-bhc. d-bhc. Heptachlor epoxide. Endosulfan I 0. g-chlordane. a-chlordane., -DDE. Dieldrin. Endrin., -DDD. Endosulfan II., -DDT. Endrin aldehyde 0 0 Excellent peak shape, resolution and analyte response Phase Lot Phase Lot Phase Lot. Methoxychlor 0. Endosulfan sulfate. Endrin ketone. Decachlorobiphenyl (surr.) G00 G00 G000

8 The Low Bleed You Expect Equity- Reproducible Low Column Bleed Across Phase Lots and Manufacturing Batches Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, 00: split Sample: Nonpolar Column Test Mix (Cat. No. 00-U) pa pa pa Phase Lot Phase Lot Phase Lot FID C G000, 0, 0 Equity- Reproducible Low Column Bleed Across Phase Lots and Manufacturing Batches Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, 00: split Sample: Nonpolar Column Test Mix (Cat. No. 00-U) pa pa pa Phase Lot Phase Lot Phase Lot FID C G00,, Equity-0 Reproducible Low Column Bleed Across Phase Lots and Manufacturing Batches Column: 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: C (0 min), C/min to 0 C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: µl, 00: split Sample: Modified intermediate polarity test mix.0pa Phase Lot.pA Phase Lot.pA Phase Lot FID Bleed at 0 C G00 G00 G00

9 For great sensitivity, reliable identification, and increased sample throughput, rely on Equity Capillary GC columns. The consistent low bleed performance you demand and the service you deserve. Equity- Low GC/MS Column Bleed Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to 00 C ( min), C/min to C ( min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier Gas: Helium, 0 C Injection: µl, pulsed splitless (pulsed to 0psi for 0. min) Sample: ng on-column of a component EPA Method 0 standard Superb GC/MS signal-to-noise ratio at nanograms Clean Mass Spectrum (unsubtracted for background) nanograms Benzo(g,h,i)perylene (m/z ) 0 0 G00 Equity Low GC/MS Column Bleed Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to 00 C ( min), C/min to C ( min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier Gas: Helium, 0 C Injection: µl, pulsed splitless (pulsed to 0psi for 0. min) Sample: ng on-column of a component EPA Method 0 semivolatile standard Superb GC/MS signal-to-noise ratio at nanograms Clean Mass Spectrum (unsubtracted for background) nanograms Benzo(g,h,i)- perylene (m/z ) 0 G00 Equity-0 Low ECD Column Bleed Column: 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 0 C, C/min to 0 C ( min) Inj.: 0 C Det.: ECD, 0 C Carrier Gas: Helium, 0 C Injection: µl, splitless (0. min) Liner: mm ID double taper Sample: Custom mix in MTBE diluted and derivatized with diazomethane. Dalapon.,-Dichlorobenzoate. -Nitrophenol. Dicamba. Dichloroprop.,-D. Pentachlorophenol.,,-TP. Chloramben 0.,,-T. Dinoseb.,-DB. Bentazon. Picloram. Dacthal. Acifluorfen G00, 0 Low ECD Bleed

10 The Column Life You Count On Equity- Durability Challenge Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), 0 C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: µl, 00: split Sample: Test Mix. to ng on-column of a component semivolatile standard; the column challenge mix is a high concentration waste sample. Response factor is calculated relative to the internal standard, -Difluorobiphenyl Relative Response Factor Final response after clipping one loop off the column. Benzidine Very consistent response throughout the durability challenge test Pentachlorophenol Durability Test The column durability and life were challenged for over 0 injections by alternating injections of the µl test mix followed by consecutive Number of Injections µl splitless injections of the high concentration waste sample. Column maintenance was performed at the end of the test before a final test mix was injected. G000 0 Equity- Durability Challenge Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), 0 C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: µl, 00: split Sample: Test Mix. to ng on-column of a component semivolatile standard; the column challenge mix is a high concentration waste sample. Response factor is calculated relative to the internal standard, -Difluorobiphenyl Durability Test Relative Response Factor Response recovered well after clipping one loop from the column Pentachlorophenol Benzoic acid The column durability and life were challenged for over 0 injections by alternating injections of the µl test mix followed by consecutive µl splitless injections of the high concentration waste sample. Number of Injections Column maintenance was performed at the end of the test before a final test mix was injected. G00 Equity-0 Durability Challenge Column: 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: C ( min), C/min to 0 C Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: µl, 00: split Sample: Test Mix-% each solvent by weight in methanol Durability Test The column durability and life were challenged by repeatedly ramping the GC oven up to 0 C and holding for four hours. After each four-hour increment, a solvent standard was analyzed. This sequence was repeated until the column had experienced a total of hours at 0 C. First injection after hours Last injection after hours Isopropyl acetate.,-dichloroethane. Isobutanol. -Methoxyethanol. Trichloroethene. -Ethoxyethyl acetate. -Butoxyethanol G00 Consistent performance throughout the challenge G00

11 To increase your productivity and reduce your instrument downtime, use Equity Capillary GC columns. The durable, consistent column life you demand and the service you deserve. Equity- Durable Analyte Response Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), 0 C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: µl, 00: split Sample: Test Mix. to ng on-column of a component semivolatile standard; the column challenge mix is a high concentration waste sample. Response factor is calculated relative to the internal standard, -Difluorobiphenyl Durability Test The column durability and life were challenged for over 0 injections by alternating injections of the µl test mix followed by consecutive µl splitless injections of the high concentration waste sample. Column maintenance was performed at the end of the test before a final test mix was injected.. Pentachlorophenol. Phenanthrene. Anthracene Last injection after column maintenance 0th Injection First Injection G00,, Equity- Durable Analyte Response Column: 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), 0 C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: µl, 00: split Sample: Test Mix. to ng on-column of a component semivolatile standard; the column challenge mix is a high concentration waste sample.. Pentachlorophenol. Phenanthrene. Anthracene Last injection after column maintenance Response factor is calculated relative to the internal standard, -Difluorobiphenyl 0th Injection Durability Test The column durability and life were challenged for over 0 injections by alternating injections of the µl test mix followed by consecutive µl splitless injections of the high concentration waste sample. Column maintenance was performed at the end of the test before a final test mix was injected. First Injection G00,, Equity-0 Durable Analyte Response Column: 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 00 C ( min), C/min to 0 C, C/min to 0 C (0 min) Inj.: C Det.: ECD, 0 C Carrier Gas: Helium, C Injection: µl, splitless (0. min) Sample: 0ppb of a component chlorinated pesticide standard (Cat. No. -U).,,,-Tetrachlorom-xylene (surr.). a-bhc. g-bhc. Heptachlor. Aldrin. b-bhc. d-bhc. Heptachlor epoxide. Endosulfan I 0. g-chlordane. a-chlordane., -DDE. Dieldrin. Endrin., -DDD. Endosulfan II., -DDT. Endrin aldehyde. Methoxychlor 0. Endosulfan sulfate. Endrin ketone. Decachlorobiphenyl (surr.) 0 0 Excellent peak shape, resolution and analyte response Phase Lot Phase Lot Phase Lot G00 G00 G000

12 Alcohols - Blood Alcohol (SPME/GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Oven: C (. min), 0 C/min to 0 C ( min) Sample: Blood alcohols in ml serum in ml vial, all analytes at 0.% or 00mg/dL SPME Fiber: Carbowax-DVB Stableflex Cat. No.: -U Extraction: Heated headspace, 0 C, min Desorption: minutes at 0 C Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, C Injection: SPME fiber, split 0: Liner: 0.mm SPME liner. Acetaldehyde. Methanol. Ethanol. Acetone. Isopropanol. n-propanol (internal standard) Excellent Peak Symmetry for Alcohols 0 G00 Alcohols - Hydrocarbons and Alcohols (GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C (0 min) Inj.: 0 C Det.: FID, C Carrier Gas: Helium, 0 C Injection: 0.0µL, split 00: Liner: Split, cup design Sample: component mixed solvent sample, equal by weight. Methanol. Ethanol. Isopropanol. t-butanol. Propanol. -Butanol. Hexane. Isobutanol U. Unknown. Butanol 0. -Methyl--butanol. -Pentanol. -Pentanol. Heptane. -Methyl--butanol. -Methyl--butanol. -Methyl--pentanol. -Methyl--pentanol. Pentanol. Octane 0. -Methyl--pentanol. Hexanol. Nonane. Heptanol. Decane. Octanol. Undecane. Dodecane. Decanol. Tridecane 0. Tetradecane. Pentadecane. Hexadecane Excellent Peak Shapes and Resolutions 0, 0 0 U G000

13 Alcohols - Fusel Oils in Vodka (GC) Column: Equity-0, 0m x 0.mm ID,.0µm Cat. No.: -U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, split 00: Liner: mm ID single tapered Sample: 000ppm in % undenatured ethanol. Acetaldehyde. Methanol. n-propanol. Ethyl acetate. Isobutanol. Isoamyl alcohol All compounds resolved from solvent peak G0000

14 Alditol Acetates (GC) Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 0 C isothermal Inj: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: µl, : split Liner: split cup design Sample: Alditol acetate 00ppm in methylene chloride (Cat. Nos. 0-U & ). Rhamnitol. Fucitol. Ribitol. Arabinitol. Inositol. Mannitol. Glucitol. Galactitol Key Resolution Achieved G0000

15 Amines (GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Oven: C ( min), C/min to C Inj.: 0 C Det.: FID, 00 C Carrier Gas: Helium, C Injection: µl, split 00: Liner: mm ID, straight Sample: 00ppm each amine in methanol Excellent Response and Peak Shape. Propionitrile. Diethylamine. Diisopropylamine. -Methyl-pyrrolidine. Triethylamine. Pyridine. Acrylamide. Benzonitrile. Benzylamine 0. Octylamine. Nonylamine. Decylamine. Unknown impurity. Toluenediamine. Dicyclohexylamine G000 Amines - Low Molecular Weight (GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Oven: C ( min), 0 C/min to C Inj.: 0 C Det.: FID, 00 C Carrier Gas: Helium, C Injection: µl, split 00: Liner: mm ID, straight Sample: 00ppm each amine in methanol Solvent. Methylamine. Dimethylamine. Ethylamine. Trimethylamine Complete Amine Separation at C Initial Temperature.0.0 G000

16 Anilines (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to 00 C, C/min to C ( min) Inj.: 0 C Det.: FID, C Carrier Gas: Helium,.mL/min, constant Injection:.0µL, splitless (0. min) Liner: Splitless, mm ID single taper Sample: 0ng on-column of a custom anilines mix. Aniline. -Aminobenzotrifluoride. o-toluidine. N,N-Dimethylaniline. -Chloroaniline.,-Dimethylaniline. -Chloro--fluoroaniline. -Isopropylaniline. -Methyl--ethylaniline 0. -Chloro--methylaniline.,-Diethylaniline.,-Diaminotoluene.,-Dichloroaniline.,,-Trichloroaniline. -Chloro--nitroaniline.,'-Dichlorobenzidine Excellent Peak Shapes and Resolutions 0 Low FID Bleed C 0 0 G000

17 BAMEs - Bacterial Acid Methyl Esters (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to 0 C ( min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection:.0µL, split 00: Liner: Split, cup design Sample: 00ng on-column of a component BAME standard (Cat. No. 00-U) Solvent. Me. Undecanoate (C:0). Me. -Hydroxydecanoate (-OH-C0:0). Me. Dodecanoate (C:0). Me. Tridecanoate (C:0). Me. -Hydroxydodecanoate (-OH-C:0). Me. -Hydroxydodecanoate (-OH-C:0). Me. Tetradecanoate (C:0). Me. -Methyltetradecanoate (i-c:0). Me. -Methyltetradecanoate (a-c:0) 0. Me. Pentadecanoate (C:0). Me. -Hydroxytetradecanoate (-OH-C:0). Me. -Hydroxytetradecanoate (-OH-C:0). Me. -Methylpentadecanoate (i-c:0). Me. cis--hexadecenoate (C: ). Me. Hexadecanoate (C:0). Me. -Methylhexadecanoate (i-c:0). Me. cis-,0-methylenehexadecanoate (C:0D). Me. Heptadecanoate (C:0D). Me. -Hydroxyhexadecanoate (-OH-C:0) 0. Me. cis, -Octadecadienoate (C:, ). Me. cis--octadecanoate (C: Cis). Me. trans--octadecanoate (C: trans). Me. Octadecanoate (C:0). Me. cis-,0-methyleneoctadecanoate (C:0D). Me. Nonadecanoate (C:0). Me. Eicosanoate (C0:0) Excellent Peak Shape and Response Solvent 0 0 G Dioxin and Furans (GC/MS) Separation of all Target Analytes Column: Equity-, 0m x 0.mm ID x 0.µm Cat. No.: 00-U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C MSD Interface: C Scan Range: SIM Carrier Gas: Helium, cm/sec, constant Injection: µl, splitless ( min) Liner: mm ID, single taper Sample: Dioxin standard, 00-00ppb in octane,, % Resolution Between Peaks and. C-,,,-TCDF.,,,-TCDF. C-,,,-TCDD. C-,,,-TCDD.,,,-TCDD.,,,,-PCDF.,,,,-PCDF.,,,,-PCDD, 0,,.,,,,,-HxCDF 0.,,,,,-HxCDF.,,,,,-HxCDF.,,,,,-HxCDD. C-,,,,,-HxCDD.,,,,,-HxCDD. C-,,,,,-HxCDD.,,,,,-HxCDD.,,,,,-HxCDF. C-,,,,,,-HpCDF.,,,,,,-HpCDF 0.,,,,,,-HpCDD.,,,,,,-HpCDF. C-OCDD. OCDD. OCDF 0, 0 G0000

18 Drugs - Drug Screen (GC/MS) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), C/min to 0 C, C/min to 00 C, C/min to 0 C ( min) Inj.: 0 C MSD Interface: C Scan Range: 0-0m/z Carrier Gas: Helium, C Injection: 0.µL pulsed splitless (pulsed to 0psi until 0. min) split open at 0. min Liner: mm ID, straight Sample: ~ng on-column of a component drug standard. Amphetamine. Methamphetamine. Nicotine. Caffeine. Diphenhydramine. Lidocaine. Phenobarbital. Methadone. Amitriptyline 0. Cocaine. Desipramine. Codeine. Morphine. Diazepam. Heroin. Fentenyl Amphetamine: Excellent Response and Peak Symmetry 0 Key Resolutions Achieved 0 0 G00

19 Drugs - Drug Screen (GC/MS) Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: C ( min), C/min to 0 C, C/min to 00 C, C/min to 0 C ( min) Inj.: 0 C MSD Interface: 0 C Scan Range: 0-0m/z Carrier Gas: Helium, 0.mL/min constant flow Injection: 0.µL pulsed splitless (pulsed to 0psi for 0. min) split open at 0. min Liner: mm ID straight Sample: 0ppm drug standard in methanol. Amphetamine. Methamphetamine. Nicotine. Diphenhydramine. Caffeine. Lidocaine. Methadone. Phenobarbital. Amitriptyline 0. Cocaine. Desipramine. Codiene. Diazepam. Heroin. Fentenyl Key Resolutions Achieved 0 Low MS Bleed G0000

20 Foods, Flavors and Fragrances - Distilled Lime Oil (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), C/min to 00 C (0 min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: Wet needle, split 00: Liner: Split, cup design Sample: Distilled lime oil. a-pinene. Camphene. b-pinene. Myrcene. a-phellandrene.,-cineole. a-terpinene. p-cymene. d-limonene 0. g-terpinene. Terpinolene. Linalool. a-fenchyl alcohol. Terpinen--ol. b-terpineol. Borneol. Terpinen--ol. a-terpineol. g-terpineol 0. Decanal. Neral. Geranial. Neral acetate. Geranyl acetate. Dodecanal. b-caryophyllene. trans-a-bergamotene. trans-a-farnesen. b-bisabolene Equity- 0 Excellent Peak Shapes and Resolution G0000 Equity- 0 Excellent Peak Shapes and Resolution G000

21 Foods, Flavors and Fragrances - Cold Pressed Lemon Oil (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: C ( min), C/min to 00 C (0 min) Inj.: 0 C Det.: FID, 0 C Carrier Gas: Helium, 0 C Injection: Wet needle, split 00: Liner: Split, cup design Sample: Cold pressed lemon oil. Heptanal. a-thujene. a-pinene. Camphene. Sabinene. b-pinene. -Methy--heptene--one. Myrcene. Octanal 0. a-phellandrene. -Carene. a-terpinene. p-cymene. d-limonene. g-terpinene. Octanol. Terpinolene. Linalool. Nonanal 0. Citronellal. Terpinen--ol. a-terpineol. Decanal. Octyl acetate. Nerol. Neral. Carvone. Geraniol. Geranial 0. Nonyl acetate. Citronellyl acetate. Neryl acetate. Geranyl acetate. Dodecanal. b-caryophyllene. trans-a-bergamotene. a-humelene. b-bisabolene Equity- Excellent Peak Shapes and Resolution Equity- Excellent Peak Shapes and Resolution G000, G

22 Fuels - Fuel Oils, (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C /min to C (0 min) Inj.: C Det.: FID, C Carrier Gas: Helium, 0cm/sec, constant Injection:.0µL, split 00: Liner: mm ID single taper Fuel Oil No. Sample: 00ng on-column of Fuel Oil No. (Cat. No. -U) Excellent Peak Shapes and Response Low FID Bleed G00 Fuel Oil No. Sample: 00ng on-column of Fuel Oil No. (Cat. No. -U) Low FID Bleed G00

23 Fuels - Fuel Oils,, (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C /min to C (0 min) Inj.: C Det.: FID, C Carrier Gas: Helium, 0cm/sec, constant Injection:.0µL, split 00: Liner: mm ID single taper Excellent Peak Shapes and Response Fuel Oil No. Sample: 00ng on-column of Fuel Oil No. (Cat. No. -U) Low FID Bleed G00 Fuel Oil No. Sample: 00ng on-column of Fuel Oil No. (Cat. No. -U) Low FID Bleed G00 Fuel Oil No. Sample: 00ng on-column of Fuel Oil No. (Cat. No. -U) Low FID Bleed G00

24 Glycols - Glycols and Diols (GC) Column: Equity-, 0m x 0.mm ID,.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to 00 C ( min) Inj.: 0 C Det.: FID, 00 C Carrier gas: Helium, cm/sec, constant Injection: µl, pulsed splitless, (pulsed to 0psi until 0.0 min) split open at 0. min Liner: mm ID, straight Sample: 00ppm glycol standard in methanol. -Methoxyethanol (Methyl cellosolve). Ethylene glycol. -Ethoxyethanol (Cellosolve). Propylene glycol.,-butanediol.,-propanediol. -Butoxyethanol (Butyl cellosolve).,-butanediol. -(-Ethoxyethoxy) ethanol (Carbitol) 0. Dipropylene glycol. -(-Butoxyethoxy) ethanol (Butyl carbitol) Excellent Peak Shape Low ppm for ethylene(eg) and propylene glycol(pg) G00 Haloacetic Acids - US EPA Method. Haloacetic Acids (GC) Column: Equity-0, 0m x 0.mm ID, 0.mm Cat. No.: -U Oven: 0 C (0 min), C/min to C ( min), 0 C/min to 0 C ( min) Inj.: 00 C Det.: ECD, 0 C Carrier gas: Helium, C Injection: µl, splitless (0. min) Liner: mm ID single taper Sample: component mix, 0-00ppb in MTBE (Cat. Nos.: -, 0-U, -U, -U) Key resolution achieved. Monochloroacetic acid (MCAA). Monobromoacetic acid (MBAA). Dalapon. Dichloroacetic acid (DCAA). Trichloroacetic acid (TCAA).,,-Trichloropropane (internal standard). Bromochloroacetic acid (BCAA). Bromodichloroacetic acid (BDCAA). Dibromoacetic acid (DBAA) 0. Chlorodibromoacetic acid (CDBAA).,-Dibromopropionic acid (surrogate). Tribromoacetic acid (TBAA) (all compounds except internal standard were methylated) G0000

25 Herbicides - US EPA Method Chlorinated Acids (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 0 C, C/min to 00 C Inj.: 0 C Det.: ECD, 0 C Carrier gas: Helium, 0 C Injection: µl, splitless (0. min) Liner: mm ID double taper Sample: Custom mix in MTBE diluted and derivatized with diazomethane Equity-. Dalapon.,-Dichlorobenzoate. -Nitrophenol. Dicamba. Dichloroprop.,-D. Pentachlorophenol.,,-TP. Chloramben 0.,,-T. Dinoseb.,-DB. Bentazon. Picloram. Dacthal. Acifluorfen, Excellent Peak Shapes and Resolution 0 Stable Baseline No Bleed G000 Equity-0 program ends at 0 C, G00

26 Hydrocarbons - Simple Hydrocarbons (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: Track oven Det.: FID, C Carrier gas: Helium,.mL/min, constant Injection: 0.0µL, cold on column Liner: Not applicable Sample: 00ng on-column of a component n-hydrocarbon standard (Cat. No. -U). C. C0. C. C. C. C. C0. C. C 0. C. C. C0. C. C. C. C. C0 Equity- Equity Excellent Peak Shape and Response 0 Low FID Bleed G000 Low FID Bleed G000 Hydrocarbons - Hydrocarbons and Alcohols (GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: 0 C Det.: FID, C Carrier gas: Helium, 0 C Injection: 0.0µL, split 00: Liner: Split, cup design Sample: component mixed solvent sample, equal by weight Excellent Peak Shapes. Methanol. Ethanol. Isopropanol. t-butanol. Propanol. -Butanol. Hexane. Isobutanol U. Unknown. Butanol 0. -Methyl--butanol. -Pentanol. -Pentanol. Heptane. -Methyl--butanol. -Methyl--butanol. -Methyl--pentanol. -Methyl--pentanol. Pentanol. Octane 0. -Methyl--pentanol. Hexanol. Nonane. Heptanol. Decane. Octanol. Undecane. Dodecane. Decanol. Tridecane 0. Tetradecane. Pentadecane. Hexadecane 0, 0 0 U G000

27 Hydrocarbons - Diesel Fuel (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to C ( min) Inj.: C Det.: FID, C Carrier gas: Helium, 0cm/sec, constant Injection:.0µL, split 00: Liner: mm ID single taper Sample: 00ng on-column of a No. Fuel Oil standard (Cat. No. -U) Excellent Peak Shapes and Response Low FID Bleed C G00 Hydrocarbons - Unleaded Gasoline (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C (0 min), C/min to 00 C Inj.: 0 C Det.: FID, 0 C Carrier gas: Helium, 0 C Injection: µl, 00: split Liner: Split, cup design Sample: Unleaded gasoline, neat. Methyl-t-butyl ether. Benzene. Toluene. Octane. Ethylbenzene. m/p-xylenes. o-xylene.,,-trimethylbenzene.,,-trimethylbenzene 0. Decane. Naphthalene. Dodecane G00

28 Ketones - Impurities in Methyl Ethyl Ketone (GC) Column: Equity-0, 0m x 0.mm ID,.µm Cat. No.: -U Oven: C (0 min), C/min to 00 C Inj.: 0 C Det.: FID, 0 C Carrier gas: Helium, C Injection: µl, 0: split Liner: mm ID cup style Sample: Methyl ethyl ketone of various purity levels ACS Reagent Grade 0. Methanol. Ethanol. Acetone. Isopropanol. t-butanol. n-propanol. n-butanol. Ethyl acetate. Diethoxymethane 0. sec-butanol. Methyl isobutyl ketone. Isopropyl acetate. Isobutanol. Toluene. -Methyl--pentanone. -Octene 0 0 G00000 Commercial Grade G0000 Laboratory Standard G0000

29 Odors - Trace Odors in Drinking Water (SPME/GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Sample: ml of water containing % NaCl and drinking water odors kit, Cat. No. -U SPME Fiber: cm StableFlex coated with 0/0µm DVB/Carboxen/PDMS Cat. No.: -U Extraction: headspace, C (0 min) Desorption: min at 0 C Oven: 0 C ( min), C/min to 00 C Liner: 0.mm SPME liner MSD Interface: 0 C Scan Range: Selected m/z (SIM),,,, Carrier gas: Helium, ml/min, constant Injection: SPME fiber, splitless, opened after 0mL/min. -Isopropyl--methoxypyrazine, ppt. -Isobutyl--methoxypyrazine, ppt. -Methylisoborneol, ppt.,,-trichloroanisole (Internal Standard), ppt. (±)Geosmin, ppt Excellent Analyte Response at ppt G00

30 PCBs - US EPA Method 0 Polychlorinated Biphenyls (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 00 C ( min), C/min to 0 C, C/min to 00 C (0 min) Inj.: C Det.: ECD, 0 C Carrier gas: Helium, 00 C Injection:.0µL, splitless (0. min) Liner: mm ID double taper Sample: ppb of Aroclors 0 & 0 with surrogates at.ppb (Cat. No. -U).,,,-Tetrachloro-m-xylene (surr.),.ppb. Aroclor 0, ppb. Aroclor 0, ppb. Decachlorobiphenyl (surr.),.ppb Equity- Excellent Peak Shape and Resolution Stable Baseline, Low Bleed G000 Equity-0 program ends at 0 C Excellent Peak Shape and Resolution Stable Baseline, Low Bleed G0000

31 PCBs - US EPA Method 0 Polychlorinated Biphenyls (Fast GC) Column: Equity-, m x 0.0mm ID, 0.0µm Cat. No.: 0-U Oven: 00 C, 0 C/min to 00 C, C/min to 0 C ( min) Inj.: C Det.: ECD, 0 C Carrier gas: Hydrogen, 0cm/sec, constant Injection: µl, splitless (0. min) Liner: mm ID single taper Sample: 00ppb of Aroclors 0 & 0 with surrogates at 0ppb (Cat. No. -U).,,,-Tetrachloro-m-xylene (surr.), 0ppb. Aroclor 0, 00ppb. Aroclor 0, 00ppb. Decachlorobiphenyl (surr.), 0ppb G00

32 Pesticides - US EPA Method 0 Chlorinated Pesticides (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C, C/min to 00 C Inj.: 0 C Det.: ECD, 0 C Carrier gas: Helium, 0 C Injection: µl, splitless (0. min) Liner: mm ID double taper Sample: Custom mix in MTBE, each component at 0.µg/mL Excellent Peak Shapes and Resolution 0. Etridiazole. Chlorneb. Propachlor. Trifuluralin. a-bhc. Hexachlorobenzene. b-bhc. g-bhc. d-bhc 0. Chlorothalonil. Heptachlor. Aldrin. Dacthal. Heptachlor epoxide. g-chlordane. Endosulfan I. a-chlordane., -DDE/Dieldrin. Endrin 0. Endosulfan II. Chlorobenzilate., -DDD. Endrin aldehyde. Endosulfan sulfate., -DDT. Methoxychlor. cis/trans-permethrin G00 Pesticides - US EPA Method 0 Chlorinated Pesticides (Fast GC) Column: Equity-, m x 0.0mm ID, 0.0µm Cat. No.: 0-U Oven: 00 C, 0 C/min to 00 C, C/min to 0 C ( min) Inj.: C Det.: ECD, 0 C Carrier Gas: Hydrogen, 0cm/sec, constant Injection: µl, splitless (0. min) Liner: mm ID single taper Sample: 0ppb of a component chlorinated pesticide standard (Cat. No. -U).,,,-Tetrachloro-m-xylene (surr.). a-bhc. b-bhc. g-bhc. d-bhc. Heptachlor. Aldrin. Heptachlor epoxide. g-chlordane 0. Endosulfan I. a-chlordane., -DDE. Dieldrin. Endrin. Endosulfan II., -DDD. Endrin aldehyde. Endosulfan sulfate., -DDT 0. Endrin ketone. Methoxychlor. Decachlorobiphenyl (surr.) 0, G00

33 Pesticides - US EPA Method 0 Chlorinated Pesticides (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Column: SPB-0, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 00 C ( min), C/min to 0 C, C/min to 00 C (0 min) Inj.: C Det.: ECD, 0 C Carrier gas: Helium, 00 C Injection:.0µL, splitless (0. min) Liner: mm ID double taper Sample: 0ppb of a component chlorinated pesticide standard (Cat. No. -U).,,,-Tetrachloro-m-xylene (surr.). a-bhc. b-bhc. g-bhc. d-bhc. Heptachlor. Aldrin. Heptachlor epoxide. g-chlordane 0. Endosulfan I. a-chlordane., -DDE. Dieldrin. Endrin. Endosulfan II., -DDD. Endrin aldehyde. Endosulfan sulfate., -DDT 0. Endrin ketone. Methoxychlor. Decachlorobiphenyl (surr.) Equity- Excellent Peak Shape and Resolution G00 Equity-0 program ends at 0 C 0, G00 SPB G00

34 Pesticides - US EPA Method Organophosphorus Pesticides (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to 00 C Inj.: 0 C Det.: NPD, 0 C Carrier gas: Helium, 0 C Injection:.0uL, splitless (0. min) Liner: mm ID double taper Sample: 0ng on-column of a custom organophosphorus pesticides mix,. Dichlorvos. Mevinphos. Trichlorfon. TEPP. Thionazin. Demeton O. Ethoprop. Naled. Dicrotophos 0. Monocrotophos. Sulfotepp. Carbophenothion 0, Excellent Peak Shapes and Resolutions, 0. Phorate. Demeton S. Dimethoate. Terbufos. Fonophos. Diazinon. Disulfoton 0. Dichlorofenthion. Phosphamidon. Chlorpyrifos methyl. Methyl parathion. Ronnel 0. Fenitrothion. Malathion. Aspon. Chlorpyrifos. Fenthion 0. Trichloronate. Chlorfenvinphos. Crotoxyphos. Storophos. Tokuthion. Merphos. Fensulfothion. Ethion. Bolstar. Famphur 0. Carbophenothion. Phosmet. EPN. Azinphos-methyl. Leptophos. Azinphos-ethyl. Coumaphos, G000 Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 0 C ( min), C/min to 0 C ( min) Inj.: 0 C Det.: NPD, 00 C Carrier gas: Helium, 0 C Injection: µl, splitless (0. min) Liner: mm double taper Sample: Custom mix diluted to 0ppm (hexane/acetone :),,,0,. Dichlorvos. Mevinphos. Trichlorfon. Demeton O. Thionazin. Ethoprop. TEPP. Naled. Phorate 0. Sulfotepp. Demeton S. Terbufos,,, 0,,0, 0. Diazinon. Fonophos. Dicrotophos. Disulfoton. Dichlorofenthion. Monocrotophos. Chlorpyrifos methyl 0. Dimethoate. Phosphamidon isomer. Ronnel. Merphos. Aspon. Chloropyrifos. Methyl parathion. Trichloronate. Phosphamidon isomer. Malathion 0. Fenitrothion. Fenthion. Ethyl Parathion. Chlorfenvinphos. Tokuthion. Crotoxyphos. Stirophos. Ethion. Bolstar. Carbophenothion 0. Fensulfothion. Famphur. Leptophos. EPN. Phosmet. Azinphos-methyl. Azinphos-ethyl. Coumaphos G0000

35 Pesticides - US EPA Method Organophosphorus Pesticides (GC/MS) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), C/min to 0 C ( min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier gas: Helium, 0 C Injection:.0µL, splitless (0. min) Liner: mm ID double taper Sample: 0ng on-column of a custom organophosphorus pesticides mix. Dichlorvos. Mevinphos. Trichlorfon. TEPP. Thionazin. Demeton O. Ethoprop. Naled. Dicrotophos 0. Monocrotophos. Sulfotepp. Carbophenothion. Phorate. Demeton S. Dimethoate. Terbufos. Fonophos. Diazinon. Disulfoton 0. Dichlorofenthion. Phosphamidon. Chlorpyrifos methyl. Methyl parathion. Ronnel. Fenitrothion. Malathion. Aspon. Chlorpyrifos. Fenthion 0. Trichloronate. Chlorfenvinphos. Crotoxyphos. Stirophos. Tokuthion. Merphos. Fensulfothion. Ethion. Bolstar. Famphur 0. Carbophenothion. Phosmet. EPN. Azinphos-methyl. Leptophos. Azinphos-ethyl. Coumaphos Excellent Peak Shapes and Resolution, 0,0,, 0, 0 Excellent Peak Shapes and Resolution G000

36 Phenols - US EPA Method 0 Phenols (GC) Column: Equity-, 0m x 0.mm ID, 0.µm. Phenol Cat. No.: 0-U. -Chlorophenol Oven: 0 C, C/min to 00 C. -Methylphenol Inj.: C. -Methylphenol Det.: FID, 0 C. -Methylphenol Carrier gas: Helium, 0 C. -Nitrophenol Injection:.0µL, 00: split.,-dimethylphenol Liner: Split, cup design.,-dichlorophenol Sample: Phenols Mix, 0µg/mL each component (Cat. No. ),.,-Dichlorophenol 0. -Chloro--methylphenol.,,-Trichlorophenol.,,-Trichlorophenol.,,-Trichlorophenol.,,-Trichlorophenol.,,-Trichlorophenol.,-Dinitrophenol. -Nitrophenol.,,,-Tetrachlorophenol.,,,-Tetrachlorophenol 0.,,,-Tetrachlorophenol. -Methyl-,-dinitrophenol.,,-Trichlorophenol. Pentachlorophenol. Dinoseb 0 0, Excellent Peak Shape G00 Phenols - US EPA Method 0 Methylated Phenols (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C (. min), C/min to 00 C Inj.: 0 C Det.: ECD, 0 C Carrier gas: Helium, 0 C Injection:.0µL, splitless (0. sec) Liner: mm ID double taper, splitless (0. sec) Sample: µg/ml Phenols Mix (00µL of a 0µg/mL mix/00µl Diazomethane).,-Dichlorophenol. -Chloro--methylphenol.,-Dichlorophenol.,,-Trichlorophenol. -Nitrophenol.,,-Trichlorophenol. -Nitrophenol.,,-Trichlorophenol.,,-Trichlorophenol, 0.,,-Trichlorophenol.,,-Trichlorophenol.,,,-Tetrachlorophenol.,,,-Tetrachlorophenol.,,,-Tetrachlorophenol.,-Dinitrophenol. Pentachlorophenol. -Methyl-,-dinitrophenol. Dinoseb Excellent Peak Shape 0, G000

37 Semivolatiles - Phthalate Esters (GC) Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Column: Equity-0, 0m x 0.mm ID, 0.µm Cat. No.: -U Oven: 0 C ( min), 0 C/min to C ( min) Inj.: 0 C Det.: FID, C Carrier gas: Helium,.mL/min, constant Injection:.0µL, splitless (0. min) Liner: mm ID single taper Sample: 0ng on-column of a custom phthalate ester mix. Dimethyl phthalate. Diethyl phthalate. Benzyl benzoate. Diisobutyl phthalate. Dibutyl phthalate. Bis(-Methoxyethyl)phthalate. Bis(-Methyl--pentyl)phthalate isomer. Bis(-Ethoxyethyl)phthalate. Diamyl phthalate 0. Di-n-hexyl phthalate. Butyl benzyl phthalate. Hexyl--ethylhexyl phthalate. Bis(-Butoxyethyl)phthalate. Dicyclohexyl phthalate. Bis(-Ethylhexyl)phthalate. Di-n-octyl phthalate. Di-n-nonyl phthalate Equity- Excellent Peak Shapes and Resolution 0 Excellent Peak Shape Low FID Bleed C 0 0 G000 Excellent Peak Shapes and Resolution Equity-0 program ends at 0 C 0 Low FID Bleed 0 C 0 0 G0000

38 Semivolatiles - US EPA Method 0 Semivolatile Compounds (GC/MS), Primary Analyte List Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to 00 C, 0 C/min to 00 C, 0 C/min to C (. min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier gas: Helium, pressure programmed, 0psi (0.0 min), ramp to 0psi (0.0 min), ramp to.psi ( min), ramp to psi (hold for remainder of run) Injection:.0µL, splitless (0. min) Liner: mm ID single taper Sample: 0ng on-column of a component semivolatile standard, internal standards, and surrogates. Pyridine. N-Nitrosodimethylamine. -Fluorophenol (Surr.). Phenol-d (Surr.). Phenol. Aniline. Bis(-Chloroethyl)ether. -Chlorophenol-d (Surr.). -Chlorophenol 0.,-Dichlorobenzene.,-Dichlorobenzene-d (Int. Std.).,-Dichlorobenzene. Benzyl alcohol.,-dichlorobenzene-d (Surr.).,-Dichlorobenzene. -Methylphenol. Bis(-Chloroisopropyl)ether. -Methylphenol. N-Nitroso-di-n-propylamine 0. Hexachloroethane. Nitrobenzene-d (Surr.). Nitrobenzene. Isophorone. -Nitrophenol.,-Dimethylphenol. Benzoic acid. Bis(-Chloroethoxy)methane.,-Dichlorophenol.,,-Trichlorobenzene 0. Naphthalene-d (Int. Std.). Naphthalene. -Chloroaniline. Hexachlorobutadiene. -Chloro--methylphenol. -Methylnaphthalene. Hexachlorocyclopentadiene.,,-Trichlorophenol.,,-Trichlorophenol. -Fluorobiphenyl (Surr.) 0. -Chloronaphthalene. -Nitroaniline. Dimethyl phthalate. Acenaphthylene.,-Dinitrotoluene. -Nitroaniline. Acenaphthene-d0 (Int. Std.). Acenaphthene.,-Dinitrophenol. -Nitrophenol 0. Dibenzofuran.,-Dinitrotoluene. Diethyl phthalate. Fluorene. -Chlorophenyl phenyl ether. -Nitroaniline. -Methyl-,-dinitrophenol. N-Nitrosodiphenylamine. Azobenzene.,,-Tribromophenol (Surr.) 0. -Bromophenyl phenyl ether. Hexachlorobenzene. Pentachlorophenol. Phenanthrene-d0 (Int. Std.). Phenanthrene. Anthracene. Carbazole. Di-n-butyl phthalate. Fluoranthene. Benzidine 0. Pyrene. Aramite#. Terphenyl-d (Surr.). Aramite#.,'-Dimethylbenzidine. Butylbenzyl phthalate.,'-dichlorobenzidine. Bis(-Ethylhexyl) phthalate. Benzo(a)anthracene. Chrysene-d (Int. Std.) 0. Chrysene. Di-n-octyl phthalate. Benzo(b)fluoranthene. Benzo(k)fluoranthene. Benzo(a)pyrene. Perylene-d (Int. Std.). Indeno(,,-cd)pyrene. Dibenz(a,h)anthracene. Benzo(g,h,i)perylene, Excellent Peak Shapes and Resolution 0 0, 0 0, Great Phenol Response 0 0 Great Pentachlorophenol Response 0 0 Excellent Peak Shapes and Resolution 0 Low MS Bleed 0 G00

39 Semivolatiles - US EPA Method 0 Semivolatile Compounds (GC/MS), Supplemental Appendix IX List Column: Equity-, 0m x 0.mm ID, 0.µm Cat. No.: 0-U Oven: 0 C ( min), 0 C/min to 00 C, 0 C/min to 00 C, 0 C/min to C (. min) Inj.: 0 C MSD Interface: C Scan Range: -0m/z Carrier gas: Helium, pressure programmed, 0psi (0.0 min), ramp to 0psi (0.0 min), ramp to.psi ( min), ramp to psi (hold for remainder of run) Injection:.0µL, splitless (0. min) Liner: mm ID single taper Sample: 0ng on-column of a component semivolatile standard, internal standards, and surrogates.,-dioxane. Pyridine. -Picoline. N-Nitroso-methylethylamine. Methyl methanesulfonate. -Fluorophenol (surr). N-Nitrosodiethylamine. Ethyl methanesulfonate. Phenol-d (surr) 0. Aniline. Pentachloroethane. -Chlorophenol-d (surr).,-dichlorobenzene-d (internal std.). Benzyl alcohol.,-dichlorobenzene-d (surr). -Methylphenol. N-Nitrosopyrrolidine. Acetophenone. N-Nitrosomorpholine 0. o-toluidine. Nitrobenzene-d (surr). N-Nitrosopiperidine. o,o,o-triethylphosphorothioate. a,a-dimethylphenethylamine. Naphthalene-d (internal std.).,-dichlorophenol. Hexachloropropene-. Phenylenediamine. N-Nitrosodibutylamine 0. Safrole. -Methylnaphthalene.,,,-Tetrachlorobenzene. Isosafrole. -Fluorobiphenyl (surr). Isosafrole-.,-Naphthoquinone.,-Dinitrobenzene.,-Dinitrobenzene 0 0. Acenaphthene-d0 0. Pentachlorobenzene. -Naphthylamine.,,,-Tetrachlorophenol. -Naphthylamine.,,,-Tetrachlorophenol. -Nitro-o-toluidine. Thionazin. Diphenylamine.,,-Tribromophenol (surr). Sulfotep 0.,,-Trinitrobenzene. Diallate-. Phorate. Phenacetin. Diallate-. Dimethoate. -Aminobiphenyl. Pronamide Excellent Peak Shapes and Resolution 0,. Pentachloronitrobenzene. Phenanthrene-d0 (internal std.) 0. Disulfoton. Dinoseb. Methyl parathion. -Nitroquinoline--oxide. Parathion. Methapyrilene. Isodrin. p-terphenyl-d (surr). -Dimethylaminoazobenzene. Chlorobenzilate 0. Famphur. Kepone. -Acetylaminofluorene. Chrysene-d (internal std.).,-dimethylbenz(a)anthracene. Perylene-d (internal std.). -Methylcholanthrene. Dibenzo(a,j)acridine 0,, Low MS Bleed G00

40 Solvents - Industrial Solvents (GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Column: WAX 0, 0m x 0.mm ID,.0µm Cat. No.: Column: Equity-0, 0m x 0.mm ID,.0µm Cat. No.: -U Oven: C ( min), C/min to 0 C ( min) Inj.: 0 C Det.: FID, 0 C Carrier gas: Helium, C Injection: 0.µL, split 00: Liner: Split, cup design Sample: 0.µL of a component neat solvent mixture Equity- 0, Excellent Peak Shapes and Response,,,0, 0,. Methanol. Methyl formate. Ethanol. Acetone. -Propanol. Ethyl formate.,-dichloroethylene. Methylene chloride. Methyl acetate 0. -Propanol. trans-,-dichloroethylene.,-dichloroethane. -Butanone. sec-butanol. Hexane. Ethyl acetate. Chloroform. Tetrahydrofuran. Isobutanol 0. -Methoxyethanol,0.,-Dichloroethane.,,-Trichloroethane. Isopropyl acetate. n-butanol. Benzene. Carbon tetrachloride. -Nitropropane. Trichloroethylene.,-Dioxane 0. -Ethoxyethanol (cellosolve). n-propyl acetate. -Methyl--pentanone. Isoamyl alcohol. Dimethylformamide. Toluene. Isobutyl acetate. -Hexanone. Mesityl oxide. Tetrachloroethene 0. n-butyl acetate, 0. Diacetone alcohol. Chlorobenzene. -Methyl--hexanone. Ethyl benzene. m-xylene. p-xylene. Isoamyl acetate. Cyclohexanol. Styrene 0. o-xylene.,,,-tetrachloroethane. -Ethoxyethyl acetate. Butyl cellosolve. n-amyl acetate. -Methylcyclohexanol.,-Dichlorobenzene. -Methylphenol. -Methylphenol. -Methylphenol, G00 WAX 0,,, 0,,,,,, 0,0,, G00,, Equity-0,,,,, 0 0 0, 0 0,

41 Solvents - Pharmaceutical Solvents, Class (GC) Oven: C ( min), C/min to 00 C Inj.: C Det.: FID, 0 C Carrier gas: Helium, 0cm/sec, constant Injection: µl, split : Liner: mm ID single taper Sample: Class I: ppm in DMSO (Cat. No. ) Class I Concentration Retention Time Identification (µg/ml) Equity- WAX 0 OVI-G.,-Dichloroethylene ,,-Trichloroethane ,-Dichloroethane Carbon tetrachloride Benzene Class Solvents on Equity- Column: 0m x 0.mm ID,.0µm w/m intermediate polarity guard Cat. No.: -U, Class Solvents on WAX 0 Column: 0m x 0.mm ID,.0µm Cat. No.: 0-U G00, Class Solvents on OVI-G G00 Column: 0m x 0.mm ID x.0µm w/m intermediate polarity guard Cat. No.: G00

42 Solvents - Pharmaceutical Solvents, Class (GC) Oven: C ( min), C/min to 00 C Inj.: C Det.: FID, 0 C Carrier gas: Helium, 0cm/sec, constant Class II Concentration Retention Time Identification (µg/ml) Equity- WAX 0 OVI-G. Methanol Acetonitrile Methylene chloride Nitromethane 0.. NI. Hexane cis-,-dichloroethylene Chloroform Methoxyethanol 0....,-Dimethoxyethane Cyclohexane Ethylene glycol Formamide Trichloroethylene ,-Dioxane NI = not integrated Class Solvents on Equity- Column: 0m x 0.mm ID,.0µm w/m intermediate polarity guard Cat. No.: -U Injection: µl, split : Liner: mm ID single taper Sample: Class II: (Cat. No. ) + n-methylpyrrolidone, 0-000ppm in DMSO Class II Concentration Retention Time Identification (µg/ml) Equity- WAX 0 OVI-G. -Ethoxyethanol Methylcyclohexane Pyridine Toluene Dimethylformamide Methyl butyl ketone Chlorobenzene Dimethylacetamide *. m-xylene...0. p-xylene...0. o-xylene.... n-methylpyrrolidone Tetralin Sulfolane *coelutes w/solvent, 0 0, Class Solvents on WAX 0 G00 Column: 0m x 0.mm ID,.0µm Cat. No.: 0-U 0, 0, G00 Class Solvents on OVI-G Column: 0m x 0.mm ID,.0µm w/m intermediate polarity guard Cat. No.: 0, 0, G00

43 Solvents - Pharmaceutical Solvents, Class (GC) Oven: C ( min), C/min to 00 C Inj.: C Det.: FID, 0 C Carrier gas: Helium, 0cm/sec, constant Class III Concentration Retention Time Identification (µg/ml) Equity- WAX 0 OVI-G. Ethanol Acetone Propanol Pentane Ethyl ether Ethyl formate Methyl acetate Propanol Methyl-t-butyl ether Acetic acid 000 NI.0.. -Butanone sec-butanol Ethyl acetate Tetrahydrofuran NI = not integrated Class Solvents on Equity- Column: 0m x 0.mm ID,.0µm w/m intermediate polarity guard Cat. No.: -U Injection: µl, split : Liner: mm ID single taper Sample: Class III: custom mix, approx. 000ppm in MeOH Class III Concentration Retention Time Identification (µg/ml) Equity- WAX 0 OVI-G. Iso-Butanol n-butanol Isopropyl acetate Heptane Propyl acetate Isoamyl alcohol Methyl--pentanone n-amyl alcohol Isobutyl acetate Butyl acetate Dimethyl sulfoxide Anisole Cumene , 0,, Class Solvents on WAX 0 Column: 0m x 0.mm ID,.0µm Cat. No.: 0-U G00,, Class Solvents on OVI-G Column: 0m x 0.mm ID,.0µm w/m intermediate polarity guard Cat. No.:, 0 0 G G00

44 Solvents - Residual Solvents (GC) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: -U Oven: 0 C ( min), C/min to 00 C Inj.: C Det.: FID, 0 C Carrier gas: Helium, 0 C Injection:.0µL, split 0: Liner: Split, cup design Sample: ng on-column of a component solvent standard in DMSO. Methanol. Ethanol. Acetonitrile. Acetone. -Propanol. Ethyl ether.,-dichloroethylene. Freon. Methylene chloride 0. Methyl-t-butyl ether. -Butanone. Hexane. Ethyl acetate. Chloroform. Tetrahydrofuran.,,-Trichloroethane.,-Dichloroethane. Carbon tetrachloride. Benzene 0. Trichloroethylene.,-Dioxane. -Methyl--pentanone. Toluene. Dimethylformamide Excellent Peak Shapes and Response, 0, 0 G

45 Volatiles - Indoor Air (GC/MS) Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 0-U Oven: C ( min), C/min to 00 C, 0 C/min to 0 C (0 min) Inj.: 0 C MSD Interface: 0 C Scan Range: -0 m/z Carrier gas: Helium, C Injection:.0µL, 0: split Liner: Split, cup design Sample: 0ng on-column of the Japanese Indoor Air Standards Mix (Cat. No. -U) 0. Ethanol. Acetone. -Propanol. Methylene chloride. -Propanol. -Butanone. Hexane. Ethyl acetate. Chloroform 0.,-Dichloroethane.,-Dimethylpentane.,,-Trichloroethane. Benzene. -Butanol. Carbon tetrachloride.,-dichloropropane. Bromodichloromethane. Isooctane. Trichloroethene 0. Heptane. -Methyl--pentanone. Toluene. Chlorodibromomethane. n-butyl acetate,,,, 0, G000 Column: Equity-, 0m x 0.mm ID,.0µm Cat. No.: 00-U Oven: C, ( min), C/min to 00 C, C/min to 0 C (0 min) Inj.: 0 C MSD Interface: 00 C Scan Range: -0 m/z Carrier gas: Helium, cm/sec, constant Injection:.0µL, 0: split Liner: Dual tapered Sample: 00ng on-column of the Japanese Indoor Air Standards Mix (Cat. No. -U). Ethanol. Acetone. -Propanol. Methylene chloride. -Propanol. -Butanone. Hexane. Ethyl acetate. Chloroform 0.,-Dichloroethane.,-Dimethyl pentane.,,-trichloroethane. -Butanol. Benzene. Carbon tetrachloride.,-dichloropropane. Bromodichloroethane. Iso-octane. Trichloroethene 0. Heptane. -Methyl--pentanone. Toluene. Chlorodibromomethane. n-butyl acetate. Octane. Tetrachloroethylene. Ethyl benzene. m/p-xylenes (partially resolved). Octane. Tetrachloroethylene. Ethylbenzene. m/p-xylene. Styrene 0. o-xylene. Nonane. a-pinene. -Ethylbenzene. -Ethylbenzene.,,-Trimethylbenzene. -Ethyltoluene. b-pinene.,,-trimethylbenzene. Styrene 0. o-xylene. Nonane. a-pinene. -Ethylbenzene. -Ethylbenzene.,,-Trimethylbenzene. -Ethyl toluene. b-pinene.,,-trimethylbenzene. Decane 0.,-Dichlorobenzene.,,-Trimethylbenzene. Limonene. Decane 0.,-Dichlorobenzene.,,-Trimethylbenzene. Limonene. Nonanal. Undecane.,,,-Tetramethylbenzene. Decanal. Dodecane. Tridecane. Tetradecane 0. Pentadecane. Hexadecane,, 0, Nonanal. Undecane.,,,-Tetramethylbenzene. Decanal. Dodecane. Tridecane. Tetradecane 0. Pentadecane. Hexadecane Excellent Peak Shapes and Resolution G00

46 GC Accessories Agilent Technologies Instruments Supeltex Capillary Column Ferrules (Short) Use with original Agilent/HP nut or Supelco 0-U replacement nut (P/N -U). We offer the short style ferrules for Agilent/ HP GC's. This design will fit the standard Agilent/ HP capillary nut. They are offered in M-A (% polyamide/% graphite), M- (00% graphite), and CapSeal (graphite/aluminum) versions. Ferrule Type Temp. Limit Qty. Cat. No mm column ID x 0.mm ferrule ID M-A 00 C 0 0-U 0 0-U M- 0 C 0 -U 0 -U CapSeal Bullet 0 C mm column ID x 0.mm ferrule ID M-A 00 C 0 0-U 0 0-U M- 0 C 0 0-U 0 -U CapSeal Bullet 0 C mm column ID x 0.mm ferrule ID M-A 00 C 0 0-U 0 0-U M- 0 C 0 0-U 0 -U CapSeal Bullet 0 C 0 0 Column Nuts for Agilent/HP Use with short Supeltex ferrules (see above). -U These column nuts are replacements for damaged or misplaced original Agilent/HP nuts. They are to be used with the shorter design ferrules for Agilent/HP GC's. Description Cat. No. Column Nuts (pk. of ) -U Accessory Case for Agilent/HP GC Capillary Products We offer a clear plastic storage case with a foam insert. The foam easily stores your capillary accessories. The foam has been cut out to hold your Pk/ inlet liners, Pk/0 septa, Pk/0 ferrules, Pk/ Therm-O-Rings, Column nuts, and Pk/0 Inlet Seals. Description Cat. No. GC Accessory Case for Agilent Technologies 0-U Supeltex Capillary Column Ferrules (General Purpose) 0 Use with Supelco Ferrule Nut Adapter (P/N 0-U or 0). These are the original Supeltex ferrules. Use these ferrules if you have replaced the original Agilent/HP nut with Supelco's Ferrule Nut Adapter. They are offered in M- (ceramic-filled Teflon), M-A (% polyamide/ % graphite), M-B (% polyamide/% graphite), M- (00% graphite), and CapSeal (graphite/aluminum) versions. Ferrule Type Temp. Limit Qty. Cat. No mm column ID x 0.mm ferrule ID M-A 00 C M-A -hole 00 C M-A Indented Blank 00 C 0 M-B 0 C 0 0-U M- 0 C U CapSeal Bullet 0 C 0-U 0.mm column ID x 0.mm ferrule ID M-A 00 C 0 M-A -hole 00 C M-A Indented Blank 00 C 0 M-B 0 C 0 M- 0 C 0 0 CapSeal Bullet 0 C 0.mm column ID x 0.mm ferrule ID M- 0 C 0 M-A 00 C 0 0 M-A Indented Blank 00 C 0 M-B 0 C 0 M- 0 C CapSeal Bullet 0 C 0.mm column ID x.0mm ferrule ID M-A Indented Blank 00 C 0 M- 0 C mm column id x.mm ferrule id M-A 00 C 0 M-A Indented Blank 00 C 0 M- 0 C 0 0 Drill to fit your column. Supelco Ferrule Nut Adapters 0-U Use with general purpose Supeltex ferrules (see above). P0000 Install fused silica capillary columns without restrictions on ferrule choice. These adapters enable you to use general purpose Supeltex and other /" compression capillary ferrules in your Agilent/HP 0, 0, 0, 0, 0, or 0 system. Description Cat. No. Adapters (pk. of ) 0-U Adapters, Knurled (pk. of ) 0 P000

47 Supeltex Capillary Ferrules (Long) Use with original Agilent/HP MSD Source Nut, SSNE Style Nut (P/N 0-U), or Supelco MSD Source Nut(P/N ). We offer a preconditioned ferrule for Agilent/ HP GC/MS applications in M-A material (% polyamide/% graphite). -U Description Qty. Cat. No mm column ID 0 -U x 0.mm ferrule ID 0 0-U 0.mm column ID 0 -U x 0.mm ferrule ID 0 0-U 0.mm column ID 0 -U x 0.mm ferrule ID 0 0-U Column Nut for Agilent/HP MSD Use with long Supeltex ferrules. These column nuts are replacements for damaged or misplaced original Agilent/HP MSD nuts. They are to be used with the longer design ferrules for Agilent/HP GC's. Description Qty. Cat. No. SSNE style columns nut 0-U MSD Source Nut for GC/MS Interface Use with long or generalpurpose Supeltex ferrules. These column nuts can be used to replace damaged or misplaced original Agilent/HP source nuts. The nuts are made of brass to prevent damage to MSD source P000 threads. An enlarged knurled end allows easy finger tightening for a leak tight seal. Description Cat. No. MSD Source Nut Thermogreen LB- Septa P000 P000 Inlet Seals -U The inlet seal on an Agilent/HP GC must be regularly changed to prevent sample adsorption due to accumulation of sample residue and/or septum fragments. We manufacture replacment seals of high quality stainless steel for analyses of non-reactive compounds, and stainless steel seals plated with pure gold for applications requiring more inertness. No brighteners are used in the plating process. Stainless steel washers are included with each type of seal. Description Cat. No. Stainless Steel Inlet Seals (pk. of ) -U Stainless Steel Inlet Seals (pk. of 0) -U Stainless Steel Inlet Seals, 00 Seals w/0 washers -U Gold Plated Inlet Seals (pk. of ) -U Gold Plated Inlet Seals (pk. of 0) -U Therm-O-Ring Seals for Capillary Inlet Liners 00-U Exclusive from Supelco. New high temperature O-ring seals can be used with inlet temperatures up to C without sticking or fragmenting. Fit both.mm OD (split) and.mm OD (splitless) Agilent/HP capillary liners, and any /" OD capillary liner that uses an O-ring seal. Superior replacement for Viton O-rings. Description Cat. No. Therm-O-Ring Seals (pk. of 0) 00-U Therm-O-Ring Seals (pk. of ) 00-U Deactivated Glass Inlet Liners Our liners feature: High temperature silanization, to ensure inertness Consistent dimensions, tolerances and quality In-house manufacturing that meets or exceeds instrument manufacturer s specifications All Models, 0, 0, 0, 0. (pk/). P000 P000 Lowest bleed of any septum we have tested. Extremely low bleed over a wide range of inlet temperatures 00 C to 0 C Already conditioned, ready to use Easier needle penetration and high puncture tolerance ideal for autosamplers Rubber formulation exclusive to Supelco 0 (Pk. of 0). P0000 Description Cat. No. Split Injection. x.mm, mm ID, wool packed 00. x.mm, cup design 000. x.mm, cup design, wool packed 00 Splitless. x.mm, tapered 00. x.mm, tapered, wool packed 00. x.mm, mm ID 00. x.mm, dual tapered 00 Direct/Wire-Bore. x.mm,.mm ID 00. x.mm, 0.mm ID, SPME 0 Description Diameter Cat. No. 0A, 0 mm (/ ) 0 00 Series, 0.mm (/ ) 0 0/0, 0, OCI Ports mm (/ ) 0

48 GC Accessories PerkinElmer Instruments Supeltex Capillary Column Ferrules -U Use with original PerkinElmer / or SSNE Style Nuts (p/n 0-U). P000 Supeltex Capillary Column Ferrules (General Purpose) Use with / compression nuts. P000 0 Ferrule Type Temp. Limit Qty. Cat. No. Ferrule Type Temp. Limit Qty. Cat. No mm column ID x 0.mm ferrule ID M-A 00 C 0 -U 0 0-U M- 0 C 0 0-U 0 0-U CapSeal Bullet 0 C 0.mm column ID x 0.mm ferrule ID M-A 00 C 0 -U 0 0-U M- 0 C 0 0-U 0 0-U CapSeal Bullet 0 C -U 0.mm column ID x 0.mm ferrule ID M-A 00 C 0 -U 0 0-U M- 0 C 0 0-U 0 0-U CapSeal Bullet 0 C mm column ID x.0mm ferrule ID CapSeal Bullet 0 C -U SSNE Style Column Nut Description Qty. Cat. No. SSNE Style Column Nut 0-U Therm-O-Ring Seals Exclusive from Supelco. New high temperature O-ring seals can be used with inlet temperatures up to C without sticking or fragmenting. They fit / capillary liners. Description Qty. Cat. No. Therm-O-Ring Seals 00-U Thermogreen LB- Septa Lowest bleed of any septum we have tested. Extremely low bleed over a wide range of inlet temperatures 00 C to 0 C Already conditioned, ready to use Easier needle penetration and high puncture tolerance ideal for autosamplers Rubber formulation exclusive to Supelco Sigma series, 00 & 0, 000 Auto Sampler Description Qty. Cat. No..0mm mm column ID x 0.mm ferrule ID M-A 00 C M- 0 C U 0.mm column ID x 0.mm ferrule ID M-A 00 C 0 M- 0 C mm column ID x 0.mm ferrule ID M-A 00 C 0 0 M- 0 C Swagelok / Compression Nut These nuts permit use of general purpose Supeltex and other / compression capillary ferrules. Description Qty. Cat. No. Swagelok / brass nut 0 0 Inlet Liners (Pk/). Our liners feature: High temperature silanization, to ensure inertness In-house manufacturing that meets or exceeds instrument manufacturer s specifications Description Cat. No. Auto System 000 Split/Splitless Capillary Injector Split Injection mm x 0.,mm ID 00 mm x 0., mm ID 00 Splitless mm x 0., mm ID 0 mm x 0., 0.mm ID, SPME 0 PPS (Programmed Split/Splitless) Split Injection mm x mm, mm ID 0 Splitless mm x mm, mm ID 0 Direct/On-Column/Other mm x mm, On-Column 0 Accessory Cases for PerkinElmer GC Capillary Products We offer a clear plastic storage case with a foam insert. The foam easily stores your capillary accessories. The foam has been cut out to hold your Pk/ inlet liners, Pk/0 septa, Pk/0 ferrules, Pk/ Therm-O-Rings, and Column nuts. Description Cat. No. GC Accessory Case for PerkinElmer 0-U

49 GC Accessories Varian Instruments Supeltex Capillary Column Ferrules Use with Varian Nut (p/n 0-U). -U Ferrule Type Temp. Limit Qty. Cat. No mm column ID x 0.mm ferrule ID M-A 00 C 0 -U 0 0-U M- 0 C 0 0-U 0 0-U CapSeal Bullet 0 C 0.mm column ID x 0.mm ferrule ID M-A 00 C 0 -U 0 0-U M- 0 C 0 0-U 0 0-U CapSeal Bullet 0 C -U 0.mm column ID x 0.mm ferrule ID M-A 00 C 0 -U 0 0-U M- 0 C 0 0-U 0 0-U CapSeal Bullet 0 C mm column ID x.0mm ferrule ID CapSeal Bullet 0 C -U Column Nuts Description Cat. No. Column Nut for Varian GC (pk. of ) 0-U Thermogreen LB- Septa Lowest bleed of any septum we have tested. Extremely low bleed over a wide range of inlet temperatures 00 C to 0 C Already conditioned, ready to use Description Diameter Cat. No. Injectors mm 0-U Packed column injectors.mm 0 SPI mm 0 Capillary Injectors mm 0.mm Saturn GC/MS.mm P000 Deactivated Glass Inlet Liners (Pk/). Our liners feature: High temperature silanization, to ensure inertness Consistent dimensions, tolerances and quality In-house manufacturing that meets or exceeds instrument manufacturer s specifications Description Cat. No. Model CP Injector Split Injection. x.mm, mm ID, wool packed 00. x.mm, cup design 000. x.mm, cup design, wool packed 00. x.mm, cup design, 0% OV- on Chromosorb packed 00 Splitless. x.mm, tapered 00. x.mm, tapered, wool packed 00. x.mm, mm ID 00. x.mm, dual taper 00 Direct/On-Column. x.mm,.mm ID 00 SPME. x.mm, 0.mm ID 0 Model 0/0 Injector Split Injection x.mm, with frit 000 x.mm, Packed with 0% OV- on Chromosorb packed 00 x., unpacked 0 x.mm, with baffle 000 x.mm, wool packed 00 x.mm, w/cup unpacked 00 Splitless x.mm, straight 000 x.mm, SPME, 0.mm ID 0 Direct/On-Column x.mm, fused silica 0 x 0., universal flash, 0.mm ID columns 0 Model 0- SPI Direct/On-Column x.mm, direct injection, 0 x mm,.mm ID, frit 0 x.mm, wool packed 0 Model 0 Injector Split Injection x mm,.mm ID, unpacked 0 x mm,.mm ID, frit 0 x mm,.mm ID, packed 0 x mm, mm ID, split/splitless, wool packed 0 Splitless x mm, mm ID, unpacked 0 x mm, 0.mm ID, unpacked 0 x mm, 0.mm ID, temp ramp mode 0 Accessory Case for Varian GC Capillary Products We offer a clear plastic storage case with a foam insert. The foam easily stores your capillary accessories. The foam has been cut out to hold your Pk/ inlet liners, Pk/0 septa, Pk/0 ferrules, and Column nuts. Description Cat. No. GC Accessory Case for Varian 0-U

50 We are committed to the success of our Customers, Employees, and Shareholders through leadership in Life Science, High Technology, and Service The Service You Deserve 0 Easy Ordering Supelco offers many ways to easily place your order or inquire about an existing order. You can call, fax, or visit our web site hours a day, days a week. In the USA and Canada, please contact us at: Phone : 00-- / Fax: -- Web: sigma-aldrich.com/supelco Other countries, contact your local Sigma-Aldrich representative. For more information, visit sigma-aldrich.com Ready to order products? Searching for Material Safety Data Sheets or other product information? Need a new catalog? Many of your questions can be answered at our award winning web site. Go to sigma-aldrich.com/supelco to search for products, check up-to-the-minute availability, place orders, check order status, or directly trace the order shipment with a tracking number that is hot linked to the carrier s web site. You can check status and trace an order in two clicks! On-Time Delivery Still waiting for capillary GC columns that you ordered last week or last month? Not getting responsive customer service? Get the service you deserve today with products that meet your performance demands and are delivered when you need them. Same day shipping is our mission. Supelco s aim is to ship all stock products ordered by PM Eastern Time on the same day. Superior Support When you want additional information about a product, or help with a problem, our knowledgeable Technical Service chemists and our extensive library of free technical literature are just a telephone call, fax message, or away. We are always ready to respond to your questions, suggestions, criticisms, and changing needs. In the USA and Canada: please contact us at the following telephone numbers Monday - Friday during the hours of AM - PM Eastern Time Phone: / --0 Fax: / -- techservice@sial.com Other countries, contact your local Sigma-Aldrich representative. For more information, visit sigma-aldrich.com from the Company You Trust

51 Equity Capillary GC Columns Ordering Information Equity- Capillary GC Columns Phase: bonded; poly(dimethylsiloxane) Temp. Limits: 0. and 0.mm ID: -0 C to /0 C 0.mm ID: -0 C to 00/0 C (<=.µm d f ) -0 C to 0/0 C (>.µm d f ) Length (m) d f (µm) Cat. No. 0.0mm ID 0. 0-U 0. 0-U 0. 0-U 0.mm ID U 0. 0-U U U.0 0-U U U U 0.mm ID U 0. 0-U U U U U U U U U 0.mm ID U U 0. 0-U U.0 0-U U. 0-U 0. 0-U 0. 0-U.0 0-U U U.0 0-U U U Equity- Capillary GC Columns Phase: bonded; poly(% diphenyl/% dimethylsiloxane) Temp. Limits: 0. and 0.mm ID: -0 C to /0 C 0.mm ID: -0 C to 00/0 C(<=.µm d f ) -0 C to 0/0 C (>.µm d f ) Length (m) d f (µm) Cat. No. 0.0mm ID U 0.0mm ID U U U 0. 0-U 0.mm ID 0. 0-U U U U.0 0-U U U 0.mm ID 0. 0-U U U U U 0.0 -U 0.0 -U 0.mm ID 0. -U U U 0.0 -U. -U 0. -U 0.0 -U 0.0 -U.0 -U 0.0 -U 0.0 -U Equity-0 Capillary GC Columns Phase: bonded: poly(% cyanopropylphenyl/% dimethylsiloxane) Temp. Limits: 0. and 0.mm ID: subambient to 0 C 0.mm ID: subambient to 0 C Trademarks Agilent - Agilent Technologies Aroclor - Monsanto Co. CapSeal Bullet, Equity, SPB, Supelco, WAX, Supeltex, Therm-O-Ring, Thermogreen - Sigma Aldrich Co. Chromsorb - Manville Corp. OV - Ohio Valley Specialty Chemical Co. PerkinElmer - PerkinElmer Corp. Swagelok - Crawford Fitting Co. Viton - E.I. dupont de Nemours Length (m) d f (µm) Cat. No. 0.0mm ID 0.0 -U 0.mm ID 0. -U U U.0 -U 0.0 -U 0.0 -U 0.mm ID 0. -U U U.0 -U 0.0 -U 0.0 -U 0.mm ID 0. -U U.0 -U 0.0 -U. -U 0. -U

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