UNIVERSITI MALAYSIA PERLIS

Transcription

1 Pusat Pengajian/Pusat: Fakulti Teknologi Kejuruteraan (1) Kod kursus/ Course code: PTT 248/4 UNIVERSITI MALAYSIA PERLIS TEACHING PLAN (2) Tajuk kursus/ Course title: Kejuruteraan Reaktor/ Reactor Engineering (3) Nilai unit/ Number of unit: 4 (4) Jenis kursus/ Course type: Teras/Core (5) Prasyarat/ Prerequisite: Tiada/Nil (6) Sinopsis kursus/ Course synopsis: This course concerns with the exploitation of reactions on a commercial scale. It emphasizes fundamental concepts and problem-solving techniques. Topics to be covered include mole balance, conversion and reactor sizing, rate law and stoichiometry, isothermal reactor design, collection and analysis of rate data, multiple reaction, catalysis and catalytic reaction mechanism, and distributions of residence time for reactors. (7) Senarai eksperimen/ List of experiments: 1. Introduction to the laboratory safety. 2. Effect of flow rate on the reaction in a continuous stirred tank reactor (CSTR). 3. Effects of flow rate and reaction temperature on conversion rate in a tubular reactor. 4. Determination of reaction rate constant and reaction order in batch reactor. 5. Effect of temperature on reaction and reaction s activation energy for batch reactor. 6. Effect of residence time on the reaction in catalytic tubular reactor. 7. Effect of pulse change in input concentration to the concentration of solute in stirred tank reactor (CSTR) in series. (8) Pendekatan pembelajaran/ Learning approach: (sbg. contoh kuliah, seminar, amali, lawatan, tutorial, dll. Sila nyatakan sekali bilangan jam) i) Lecture : 42 hours (9) Sumbangan penilaian / Evaluation contribution: (i) Peperiksaan/ Examination: 60% Mid-term Wxaminations = 20% Final Examination = 40% (ii) Kerja kursus / Course work: 40% Assignments = 5% Quizzes = 5% Lab reports = 30% (* Quiz might be given without prior notice) (10) Senarai Buku Tek dan rujukan / List of text books and references

2 i) Fogler, H. S., Elements of Chemical Reaction Engineering. 6th Edition. Prentice Hall Inc. U.S., i) Davis, M. E and Davis, R. J., Fundamentals of Chemical Reaction Engineering. 1st Edition. Mc Graw Hilll, U.S., 2002 ii) Fogler, H. S., Essentials of Chemical Reaction Engineering. 1st Edition. Prentice Hall. U.S., iii) Doraiswamy, L.K and Deniz Uner, Chemical Reaction Engineering: Beyond the Fundamental. CRC Press, iv) Bruce Nauman, E., Chemical Reactor Design, Optimization and Scale up. 2nd Edition. John Wiley & Sons, v) Levenspiel, O., Chemical Reaction Engineering. 3rd Edition. Wiley India Pvt Limited, (11) Panduan Rancangan Mengajar/Teaching Plan Guide Minggu/week 1 (4/9-8/9) Kandungan kursus/ courses content (Panduan/Guidline) Mole Balance Describe the rate of reaction, the general balance equation; apply general mole balance to the three most common types of industrial reactors and the mole balances in terms of conversion. Pensyarah/ Lecturer 2-3 (11/9-22/9) 4-5 (25/9-6/10) 6 (9/10-13/10) 7 (16/10-22/10) 8 (23/10-27/10) Conversion and Reactor Sizing Evaluate equations to size CSTRs and PFRs, define conversion and, compare CSTRs and PFRs and calculate the overall conversions for reactors arranged in series. Laboratory 1: Introduction to the laboratory safety. Rate Law and Stoichiometry Calculate the rate law in terms of concentration and the Arrhenius temperature dependence, the stoichiometric table to write the concentration in terms of conversion and discuss batch and flow reaction system. Laboratory 2: Effect of flow rate on the reaction in a continuous stirred tank reactor (CSTR). Isothermal Reactor Design Analyze the design structure for isothermal reactors and pressure drop in reactors Laboratory 3: Effects of flow rate and reaction temperature on conversion rate in a tubular reactor. Cuti Pertengahan Semester/ Mid-Term Break (16 th - 22 th October 2017) Isothermal Reactor Design Analyze the design structure for isothermal reactors and pressure drop in reactors

3 Laboratory 4: Determination of reaction rate constant and reaction order in batch reactor. 9 (30/10-3/11) (6/11-17/11) (20/11-1/12) (4/12-15/12) Collection and Analysis of Rate Data Analyze the rate law and rate law parameters using graphical and numerical techniques. Describe the method that needs to be taken in using non-linear regression and discuss on reactor selection. Laboratory 5: Effect of temperature on reaction and reaction s activation energy for batch reactor. Multiple Reactions Analyze the different types of multiple reactions (series, series-parallel and Parallel reaction), select a reaction system that maximizes the selectivity and write the algorithm for solving Reaction Engineering problems with multiple reactions. Laboratory 6: Effect of residence time on the reaction in catalytic tubular reactor. Catalysis and Catalytic Reaction Mechanism Evaluate the steps in a heterogeneous reaction (adsorption, surface reaction, and desorption), the ratelimiting step, different types of surface reaction (single site, dual site, and Eley-Rideal) and rate law for Langmuir- Hinshelwood kinetics. Laboratory 7: Effect of pulse change in input concentration to the concentration of solute in stirred tank reactor (CSTR) in series. (1 hours) Distributions Of Residence Times For Reactors Analyze the cumulative F(t), external age E(t), and internal age I(t) residence time distribution (RTD) functions and recognize these function for PFR, CSTR and laminar flow reactions. Apply these functions to calculate the conversion and concentrations exiting a reactor using the segregation model and maximum mixedness model for both single and multiple reactions. 16 Minggu Ulangkaji/ Reversion Week (18 st - 22 th December 2017) Peperiksaan Semester Akhir/ Final Examination (25 th - 14 th January 2017)

4 RANCANGAN MAKMAL & TUTORIAL/ LABORATORY & TUTORIAL PLAN Week/Lab supervision Exp. 1 Exp. 2 Exp. 3 Exp. 4 Plan Lab, Exp. 5 Exp. 6 (Eng. Lab 1, UniCITI) Exp. 7 (Eng. Lab 1, UniCITI) En. Qailani En. Qailani Dr. Siti Nazrah Zailani Dr. Siti Nazrah Zailani 1 NO LAB SESSION 2 All A AND B Group 3 A5, B5 A6, B6 A4, B4 A4, B4 A1, B1 A2, B2 4 A6, B6 A4, B4 A5, B5 A5, B5 A2, B2 A3, B3 5 A4, B4 A5, B5 A6, B6 A6, B6 A3, B3 A1, B1 6 A2, B2 A3, B3 A1, B1 A1, B1 A4, B4 A5, B5 7 MID-TERM BREAK 8 A3, B3 A1, B1 A2, B2 A2, B2 A5, B5 A6, B6 9 A1, B1 A2, B2 A3, B3 A3, B3 A6, B6 A4, B LABORATORY TEST 16 STUDY WEEK 17-19

5 Group A1: 1. DIVIYASHA A/P SIVA SHANMUGAM 2. AMIRA BINTI ABU BAKAR 3. KOAY KEK CHIAN 4. NATTALYNN A/P SU WIT KUMPULAN MAKMAL / LAB GROUP Group B1: 1. KEE HUI MIN 2. MUHAMMAD BADRUL AMIN BIN MUHAMMAD RAFI 3. NURUL HIDAYAH BINTI MAMAT 4. NUR SYAHINDAH BINTI ALIAS Group A2: 1. LAU MING CHYI 2. NORFATIN NABILAH BINTI MUHAMAD 3. BOON KIN YEW 4. ALFIANA BINTI ALFIAN Group A3: 1. TAN CHIA ZHI 2. MUHAMMAD MASRUR BIN MOHD JAMIL 3. NUR ADLINA BINTI MOHD HILMI 4. MARZAITUL AINI BINTI MELI 5. MUHAMMAD FITRI AMRI BIN MANAN Group A4: 1. THUM CARMEN 2. NUR AISYAH BINTI NOORDIN 3. NURUL AMIRAH BINTI RUSLAN 4. NURFATIHATHUL BADRIYAH BINTI SAIFULLEZAN 5. MOHAMMAD ARIF FAHMI BIN CHE HASSAN Group A5: 1. ZULAIKHA HANIM BINTI OSMAN 2. CONNIE CHEAH CHIN GAIK 3. SITI NUR SYAHIRAH BINTI BAKAR 4. MUHAMMAD HAFIZUDDIN BIN HALIM 5. BALQISH BINTI AZMI Group A6: 1. NIK AMALIN 'AISYAH BINTI NEK RASLI 2. MARYAM NAJIHAH BINTI KHAIRUL ANNUAR 3. MOHD NADZRUL BIN PAUZI 4. NUR FATEN KHALILA BINTI MOHAMAD NASIR Group B2: 1. LOH SOON BOON 2. MUHAMMAD AIMAN BIN MOHD SANUSI 3. OOI KHAI YEE 4. SITI NUR AMIRA BINTI ROZANI 5. SHARIFAH NURUL ASHIKIN BINTI SYED BUNI YAMIN Group B3: 1. TAN JIA ROU 2. NURMUHAMMAD HAFIZ BIN NORSHAMSUDIN 3. MUHAMAD ZUHAIRIE BIN AFFRINDI 4. NUR NASUHA BINTI MOHD FADLI 5. NUR SYAIRAH BINTI ABD SHUKOR Group B4: 1. TAN LI TING 2. NOORULAYUNI ATIQAH BINTI YAACOB 3. MOHAMAD AMIR ARSYAD BIN ZAINUN 4. UMI SHAFIQAH AKHTAR BINTI HAJI ABU BAKAR Group B5: 1. YAP BOON CIN 2. NUR IZZAIDAH BINTI MUHAMMAD INDERA 3. NURLISA BT ADZHAR 4. FAREYZAL IKMAL BIN AMRAN 5. AZE EZLEEN BINTI ZAINUDIN Group B6: 1. SHU MENG HONG 2. TUAN AZWA HAZIKAH BINTI TUAN AZIZ 3. OU LI LIAN 4. NURFAZIYATUL AIZA BINTI AMRAN 5. NUR ATHIRAH BINTI MOHD RADZI Each group needs to submit ONE (1) REPORTS for every experiment.