Analytical Test Report Birthday Cake OG

Transcription

1 ORELAP #4096 OLCC # C Science First SE Division St. Portland, OR (503) Analytical Test Report Birthday Cake OG Gardens of Odin CB2B Laboratory ID: Batch ID: 0578 Metrc Tag: 1A DF Date Sampled: 10/28/17 Date Printed: 11/7/17 Analytical Method: De Backer, Journal of Chromatography b SOP 19 & 20 Potency Analysis Cannabinoids (% weight) Moisture Adjusted Notes THCA Total THC delta 9-THC CBGA CBDA CBD CBN CBG CBC % Total CBD % Moisture Analysis Method/SOP: SOP 7 Moisture: 15.3 % Water Activity Analysis Method/SOP: SOP 8 Results above 0.65 fail state testing requirements and will be highlighted Red. Water Activity: PASS Chris Nielsen, Lab Director 11/7/2017 Page 1 of 4 Sample tested in compliance with OAR (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

2 ORELAP #4096 OLCC # C Science First SE Division St. Portland, OR (503) Analytical Test Report Birthday Cake OG Gardens of Odin CB2B Laboratory ID: Terpene Analysis Analysis Method/SOP: Terp Analyte Result ug/g alpha-bisabolol Camphene delta-3-carene beta-caryophyllene Caryophyllene Oxide p-cymene Eucalyptol Geraniol Guaiol alpha-humulene Isopulegol Limonene 2915 Linalool 1017 beta-myrcene 2051 Ocimene alpha-pinene beta-pinene gamma-terpinene alpha-terpinene Terpinolene cis-nerolidol Total Terpenes 7993 Chris Nielsen, Lab Director 11/7/2017 Page 2 of 4 Sample tested in compliance with OAR (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

3 ORELAP #4096 OLCC # C Science First SE Division St. Portland, OR (503) Analytical Test Report Birthday Cake OG Gardens of Odin CB2B Laboratory ID: Batch: B17J155 - Potency Blank(B17J155-BLK1) Quality Control Potency Analyte Result LOQ Units %Recovery Limits Extracted Analyzed THCA % delta 9-THC % CBGA % CBDA % CBD % CBN % CBG % CBC % LCS(B17J155-BS1) Analyte % Recovery LOQ Units %Recovery Limits Extracted Analyzed THCA % /31/17 16:28 11/01/17 06:34 delta 9-THC % /31/17 16:28 11/01/17 06:34 CBDA % /31/17 16:28 11/01/17 06:34 CBD % /31/17 16:28 11/01/17 06:34 Batch: B17J146 - Grav Blank(B17J146-BLK1) Moisture Content Analyte Result LOQ Units %Recovery Limits Extracted Analyzed Percent Moisture % 10/30/17 17:40 10/30/17 17:40 Batch: B17J147 - WA Blank(B17J147-BLK1) Analyte Result LOQ Units %Recovery Limits Extracted Analyzed Water Activity AW 10/31/17 09:14 10/31/17 09:14 Notes Notes Notes Notes Chris Nielsen, Lab Director 11/7/2017 Page 3 of 4 Sample tested in compliance with OAR (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

4 ORELAP #4096 OLCC # C Science First SE Division St. Portland, OR (503) Analytical Test Report Birthday Cake OG Gardens of Odin CB2B Laboratory ID: Notes and Definitions B Analyte detected in method blank, but not associated samples. B2 Analyte detected in sample and associate methold blank. C Interference due to co-elution. D Initial result exceeded calibration range, reported data are based on analysis of a dilution. H Non-homogenous samle matrix affecting RPD and/or QC. I Manual Integration was performed. L Duplicate sample relative precent difference (RPD) exceeds QC limits. M Anomalous results due to matrix interference P Peaks manually split. Q1 QC out of limits but still ok Q2 Quality Control outside QC limits. Data considered estimate. Q3 CCV was above the acceptance criteria. Non-detect samples are considered acceptable. Q4 CCV was below the acceptance criteria, however the sample still exceeds the regulatory limit. R Marginal Exceedence. U Reported result is an estimate. The analyte was detected above the calibration range. X Problems with initial analysis, reported data are from reinjection of prepared sample. <LOQ - Results below the Limit of Quantitation - Compound not detected Chris Nielsen, Lab Director 11/7/2017 Page 4 of 4 Sample tested in compliance with OAR (TNI standards). Lab accredited for CBDA, THCA, CBD, THC, and sampling. These results relate only to the sample included on this report. The report may not be reproduced except in full, without the written permission of Rose City Labs.

5 Customer: Rose City Labs SE Division St. Portland Oregon United States Product identity: Client/Metrc ID: Sample Date: Laboratory ID: Grower: Relinquished by: Temp: Weight Received: Odin Composite C 1A E /28/ Subcontract Daniel Huson 13.4 C g Sample Results Pesticides Method AOAC & EN (mod) Units mg/kg Batch Analyze 11/7/17 12:00:00 Analyte Result Limits LOQ Status Notes Analyte Result Limits LOQ Status Notes Abamectin pass Acephate pass Acequinocyl pass Acetamiprid pass Aldicarb pass Azoxystrobin pass Cyfluthrin (incl. Beta-Cyfl pass Bifenazate pass Bifenthrin pass Boscalid pass Carbaryl pass Carbofuran pass Chlorantraniliprole pass Chlorfenapyr pass Chlorpyrifos pass Clofentezine pass Cypermethrin pass Daminozide pass Diazinon pass Dichlorvos pass Dimethoate pass Ethoprophos pass Etofenprox pass Etoxazole pass Fenoxycarb pass Fenpyroximate pass Fipronil pass Flonicamid pass Fludioxonil pass Hexythiazox pass Imazalil pass Imidacloprid pass Kresoxim-methyl pass Malathion pass Metalaxyl pass Methiocarb pass Methomyl pass Parathion-Methyl pass MGK pass Myclobutanil pass Naled pass Oxamyl pass Paclobutrazole pass Permethrin pass Phosmet pass Piperonyl butoxide pass Page 1 of 8

6 Pesticides Method AOAC & EN (mod) Units mg/kg Batch Analyze 11/7/17 12:00:00 Analyte Result Limits LOQ Status Notes Analyte Result Limits LOQ Status Notes Prallethrin pass Propiconazole pass Propoxur pass Pyrethrins pass Pyridaben pass Spinosad pass Spiromesifen pass Spirotetramat pass Spiroxamine pass Tebuconazole pass Thiacloprid pass Thiamethoxam pass Trifloxystrobin pass Page 2 of 8

7 Abbreviations Limits: Action Levels per OAR , OAR , OAR Limit(s) of Quantitation (LOQ): The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be reported with a specified degree of confidence. Units of Measure g = Gram mg/kg = Milligram per kilogram % wt = µg/g divided by 10,000 Approved Signatory Derrick Tanner General Manager Page 3 of 8

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12 Code Q Q1 Q2 Q3 Q4 Q5 Q6 R R1 R2 LOQ1 LOQ2 B B1 B2 Explanation of QC Flag Comments: Explanation Matrix interferences affecting spike or surrogate recoveries. Quality control result biased high. Only non-detect samples reported. Quality control outside QC limits. Data considered estimate. Sample concentration greater than four times the amount spiked. Non-homogenous sample matrix, affecting RPD result and/or % recoveries. Spike results above calibration curve. Quality control outside QC limits. Data acceptable based on remaining QC. Relative percent difference (RPD) outside control limit. RPD non-calculable, as sample or duplicate results are less than five times the LOQ. Sample replicates RPD non-calculable, as only one replicate is within the analytical range. Quantitation level raised due to low sample volume and/or dilution. Quantitaion level raised due to matrix interference. Analyte detected in method blank, but not in associated samples. The sample concentration is greater than 5 times the blank concentration. The sample concentration is less than 5 times the blank concentration. Page 8 of 8