Certificate of Analysis

Transcription

1 Page of 7 Image Safety Cannabinoids Pesticides - Tested Microbials - Tested Mycotoxins - Tested Heavy Metals - Tested Terpenes - Tested Residual-Solvents - Tested Filth - NOT Tested Water Activity - NOT Tested Moisture - NOT Tested Cannabinoids 0.00% Total THC % Total CBD Analyte Weight(%) mg/g D9-THC THCa TOTAL THC CBD 6.89 CBDa TOTAL CBD 6.89 CBN CBDV D8-THC THCV CBG CBGa CBC TOTAL CANNABINOIDS 6.89 D9-THC THCa CBD CBDa CBN CBDV D8-THC THCV CBG CBGa CBC IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of

2 Page 2 of 7 Terpenes Test result % alpha-cedrene alpha-humulene alpha-pinene alpha-terpinene beta-myrcene beta-pinene Borneol Camphene Camphor Caryophyllene oxide Cedrol alpha-bisabolol Isopulegol cis-nerolidol 3-Carene Fenchyl Alcohol Hexahydrothymol Eucalyptol Isoborneol Farnesene Fenchone gamma-terpinene Geraniol Geranyl acetate Guaiol Limonene Linalool Nerol Ocimene alpha-phellandrene Pulegone Sabinene Sabinene hydrate Terpineol Terpinolene trans-caryophyllene trans-nerolidol Valencene Total 0 IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of

3 Page 3 of 7 Pesticides LOQ Action Level Result Units Type Daminozide Acephate Flonicamid Oxamyl Methomyl Thiamethoxam Imidacloprid Dimethoate Acetamiprid Thiacloprid Aldicarb Dichlorvos Propoxur Carbofuran Carbaryl Imazalil Metalaxyl Chlorantraniliprole Phosmet Spiroxamine Naled 0.5 Methiocarb Azoxystrobin Boscalid Paclobutrazol Malathion Myclobutanil Bifenazate Spirotetramat Ethoprophos Fenoxycarb Kresoxim-methyl Tebuconazole Plant growth regulator Pyridine, Aphicide Carbamate,, Nematicide Carbamate,, Metabolite Neonicotinoid Neonicotinoid Organophosphate,, Metabolite Neonicotinoid, Molluscicide, Nematicide Organophosphate,, Metabolite Carbamate,, Nematicide Imidazole Fungicide Phenylamide Fungicide Organophosphate, Morpholine Fungicide Organophosphate, Carbamate, Molluscicide, Bird repellent Fungicide Fungicide Triazole Plant growth regulator; Fungicide Organophosphate, Triazole Fungicide Tetramic acid, Nematicide Carbamate Strobilurin Fungicide, Bactericide Triazole Fungicide IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of

4 Page 4 of 7 Pesticides LOQ Action Level Result Units Type Diazanon Propiconazole Clofentezine Spinosad (Spinosyn A) Prallethrin Trifloxystrobin Piperonyl butoxide Chlorpyrifos Hexythiazox Etoxazole Spiromesifen Pyrethrins (Pyrethrin I) Fenpyroximate Pyridaben Permethrins Abamectin Ba Etofenprox Bifenthrin Fludioxonil Fipronil Cypermethrin Mevinphos 0. Dimethomorph Fenhexamid Coumaphos Spinosad (Spinosyn D) Organophosphate,, Repellent Triazole Fungicide Tetrazine Synthetic pyrethroid Strobilurin Fungicide Cyclic aromatic; Performance enhancer, Synergist Organophosphate Carboxamide Diphenyl oxazoline Tetronic acid Pyrazolium, Pyridazinone, Pyrethroid Pyrethroid, Phenylpyrrole Fungicide Phenylpyrazole Pyrethroid, Veterinary substance Organophosphate, Morpholine Fungicide Hydroxyanilide Fungicide IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of

5 Page 5 of 7 Residual solvent Action Level() /Fail Results() Hexanes (2,3-dimethylbutane),4-Dioxane Pentanes (iso-pentane) Pentanes (neo-pentane) Butanes (iso-butane) 2-Butanol 2-Ethoxyethanol 2-Propanol Acetone Acetonitrile Benzene Butanes (n-butane) Cyclohexane Dichloromethane Hexanes (2,2-dimethylbutane) Xylenes-O (,2-dimethylbenzene) Xylenes-M (,3-dimethylbenzene) Xylenes-P (,4-dimethylbenzene) Ethanol Ethyl acetate Ethylbenzene Ethyl ether Ethylene Oxide Heptane n-hexane Isopropyl acetate Methanol Hexanes (2-methylpentane) Hexanes (3-methylpentane) Pentanes (n-pentane) Propane Tetrahydrofuran Toluene Xylenes IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of

6 Page 6 of 7 Cannabinoid Profile Test Result-Analysis Method :SOP.T.40, SOP.T Reagent LOT ID 039.R R R0 Analytical Batch:DA00333 Dilution Consumables Id A GEN 840C6-840H 849C4-849AK Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T for sample prep and Shimadzu High Sensitivity Method SOP.T.40 for analysis. LOQ for all cannabinoids is mg/l). Mycotoxin Analysis-Analysis Method :SOP.T , SOP.T Analytical Batch:DA00327 Analyte Results Action Level Aflatoxin G2 Aflatoxin G Aflatoxin B2 Aflatoxin B Ochratoxin A+ Aflatoxins B, B2, G, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T for Sample Preparation and SOP.T Procedure for Mycotoxins Quantification Using LCMS. LOQ.0 ppb). Total Aflatoxins (Aflotoxin B, B2, G, G2) must be <20µg/Kg. Ochratoxins must be <20µg/Kg. Micro Analysis-Analysis method :SOP.T Analytical Batch: DA00329 Pathogens Results Aspergillus_terreus_J2 not present in gram. Aspergillus_niger not present in gram. Aspergillus_fumigatus not present in gram. Aspergillus_flavus not present in gram. Salmonella_specific_gene not present in gram. Escherichia_coli_Shigella_spp_ not present in gram. Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoids purification. (Method SOP.T ) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in g of a sample, the sample fails the microbiological-impurity testing. IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of

7 Page 7 of 7 Pesticide Analysis-Analysis Method:SOP.T , SOP.T Analytical Batch :DA00326 Reagent LOT/ID Dilution Consumables ID 039.R05 A GEN Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrations for regulated Pesticides. Currently we analyze for 57 Pesticides. (Method: SOP.T Sample Preparation for Pesticides Analysis via LCMSMS and SOP.T Procedure for Pesticide Quantification Using LCMS). Heavy Metals Analysis-Analysis-Method:SOP.T , SOP.T Analytical Batch: DA0033 Reagent LOT/ID Dilution Consumables ID R0 039.R R03 Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma Mass Spectrometer) which can screen down to below single digit ppb concentrations for regulated heavy metals using Method SOP.T Sample Preparation for Heavy Metals Analysis via ICP-MS and SOP.T Heavy Metals Analysis via ICP-MS. Metal Result Action-Level Arsenic.500 Cadmium Lead Mercury 3 Abbreviation:=Parts Per Million Residual SolventsAnalysis Method:SOP.T Analytical Batch :DA00344 Residual solvents screening is performed using GC-MS which can detect below single digit concentrations. Currently we analyze for 34 Residual solvents. (Method: SOP.T Residual Solvents Analysis via GC-MS). Terpenes screening-analysis-method:sop.t Analytical Batch :DA00345 Terpenoid profile screening is performed using GC-MS with Liquid Injection (Gas Chromatography Mass Spectrometer) which can screen 38 terpenes using Method SOP.T Terpenoid Analysis Via GC-MS/MS. IC=In-control QC parameter, NC=Non-controlled QC parameter, =Not Detected, NA=Not Analyzed, =Parts Per Million, ppb=parts Per Billion. Limit of Detection (LoD) and Limit Of