ISA QATAR : 90 th Seminar
|
|
- Emil Conley
- 5 years ago
- Views:
Transcription
1 ANALYTICAL INSTRUMENTATION & MAINTENANCE SYSTEMS (AIMS) ISA QATAR : 90 th Seminar UTILIZATION OF LASERS IN THE FIELD OF GAS ANALYZERS Presenter: ZAHEER JUDDY
2 Electromagnetic Spectrum
3 Electromagnetic Spectrum x-rays ultraviolet Vis NIR mid -IR FIR microwave radio waves Wavenumbers nuclear electronic vibrational rotational transitions Wavelength in Nanometers
4 Traditional techniques/approach in process Gas Measurements Non-Dispersive & Dispersive Infrared Non-Dispersive & Dispersive Ultraviolet Contact type measurement Next Generations Tunable Diode Laser Absorption Spectroscopy (TDLAS)
5 Infrared (IR) Technology About & Challenges Very Old & First technology Suitable for only measurement of Hetro-atomic molecules Moisture interference with IR Not suitable for interfering background Gases and components Complex Sampling design with removal of moisture MUST. Increased number of consumables and spares
6 NDIR Photometry: AGAIN!! A complexity of optical design with lot of optics components.
7 Components IR analyzer: Degradation of NDIR source. Contamination of filters. Wide band width (CO2/CO) together difficulties Filters NDIR source background interference
8 Ultraviolet (UV) Technology Good for sulfur species H2S, SO2, COS, CS2, etc.. Few Challenges: Shorter lamp life Wide emission line widths & wide Spectral range. Contamination of filters. Moving parts Replacing the filter wheel motors. UV Optics Assembly
9 Filter Location Table (COS / CS 2 Measurement) Filter Position Wavelength Primary Measurement Sv H 2 S NDr COS SO 2 CS 2 Lamp Mn/Ni Cd Mn/Ni Mn/Ni Mn/Ni Cd
10 Traditional Contact type Moisture & Oxygen Measurement Moisture Measurement 1. Aluminum Oxides Response Time in minutes/hours Sensor Probe Chocking Always affected by Glycol, H2S/HCL, mercury and others Difficulties in calibration 2. QCM (Quartz Crystal Microbalance) Faster response & good for low ppm measurement Sensor killing by background corrosive gases Oxygen measurement Zirconium Oxide (ZrO2) Selective for flue gases and clean applications Affected by dust, background mist and hydrocarbon gases
11 Think Out Of The Box???? The only tool when you have in your hand is HAMMER, every thing around looks like NAIL.
12 AMETEK 5100HD PROCESS GAS ANALYZER
13 AMETEK Model 5100HD Overview The AMETEK 5100 series TDLAS gas analyzer is an extractive system & NON Contact type measurement All these species can be measured in variety of background gases There are two versions available. The Model 5100 is single laser, single analyte configuration. Model 5100HD is dual laser, single/multiple analyte single/dual cell configuration. Model 5100HD has dual stream capability. The unit is comprised of fully enclosed optics, electronics, sample handling and built-in verification. The unit is certified for worldwide hazardous area locations. comes with built-in verification and laser line lock as standard.
14 AMETEK Model 5100 Overview Gases Measured Moisture Hydrogen Sulfide Carbon Dioxide Carbon Monoxide Oxygen Methane Ammonia Hydrochloric Acid Acetylene many more coming Industries Served Natural Gas Pipeline Natural Gas Processing Refinery Chemical Petrochemical Hi Purity Gas Many more..
15 Why Tunable Diode Laser Spectroscopy? Non-contact measurement technique No sensor aging calibration concerns No consumables Advantage for applications with high levels of water vapor Lasers last many years before replacement is needed Low cost of ownership No interferences Extremely narrow emission line widths reduce interferences from other species
16 Electromagnetic Spectrum:
17 Wavelength modulation spectroscopy For First harmonic (1f ) detection, the detector signal is demodulated using a reference signal with a frequency equal to that (of the modulation frequency ) used to drive the laser.. For Second harmonic (2f )detection, the detector signal is demodulated using a reference signal twice that used to drive the laser..
18 Vibrational Spectroscopy & Lasers The absorption of infrared radiation results in unique molecular vibrations In the gas-phase samples the individual transitions between discrete vibrational states are observed when measuring with high resolution Lasers have extremely narrow emission lines; hence, they are an excellent tool to probe the unique absorptions of gas phase molecules Normal Vibration Modes for Water O O O H H H H H H
19 Respons e Transmissio n Current (ma) Modulation and Absorption Responses Laser Current Water Absorption Time (seconds) Modulated Laser Signal Detector Response Wavelength (nm) Time (seconds)
20 Analyte, typical absorption line width 0.05 nm Laser scan range, typically nm, Laser spectral line width is ca nm Conventional optical filter bandwidth > 5 nm
21 5100 Block & flow Diagram Sample cell GRIN Lens Mirror Laser Diode Beam Splitter Photodiode Reference Cell GRIN Lens Temperature Control Current Control Photodiode ELectronics Unit
22 Relative Absorbance Comparison of Water and Natural Gas Water vapor spectrum offset for clarity um, 5394 cm-1 Water Vapor Natural Gas Wavelength (nm)
23 Key feature of 5100 : Line-Lock By adjusting the TEC temperature, the analyzer will tune the laser to emit a specific frequency that would be absorbed by Line Locking under Laser Temperature the analytes. of C. Reference and Sample Spectra check the peak ( line ) in the spectrum. The peak ( line ) is locked if its index is at a certain position in the spectrum, varying by a line-lock window F Signal C 26.8 C 25.5 C C C 2F Signal Spectral Index Spectral Index
24 Advantages of LASER: Precise measurement
25 Advantages of LASER: Precise measurement
26 DFB Tunable Laser Diode The Heart of it All Very Accurate!! Can be tuned to measure to the accuracy level.
27 Laser/Fiber Panel 5100
28 Reference Cell TDLAS
29 Verifying the Reference cell function:
30 Sample cell
31 Select Wisely: Don t Load all your application on LASERS, you need to be careful on the following. Always provide complete stream composition. Moisture and H2S in nitrogen is different than moisture and H2S in methane. Proper sampling system
32 COMMON ISSUES WITH SAMPLING SYSTEM 1. Sample Line Issues Longer distance??? As near as tapping point possible (less than 10 meters) 2. Probe Installation Issues 3. Big SHELTER/HVAC Issues Maintenance issues 4. Location of Tapping Points difficult to install and maintenance 5. SS 316 Electro Polished Tubes 6. Range issues for Analyzers 7. High H2S Exposure
33 Points considerations in Process Analyzers 33
34 Probe Installation Issues No heating/ Jacketing Proper Probe Heating with Jacketing
35 Probe selection for high pressure process line Analyzers
36 Probe Installation Location Difficult location for Probe installation
37 Heated Sample line selection & Installation Shortest length between tapping point and analyzer less than 10 meters Proper bending & Installation of sample line by AIMS
38 Poor Installation sample line
39 Sample installation Best Practices
40 Correct type of Heated Sample line selection Teflon: Inert but temperature limitations (dewpoint temperature), permeation Stainless Steel: welded, seamless but cleanliness and adsorption problems with some applications ElectroPolished: improved surface finish for improved absorption resistance ElectroPolished/Coated: for a product that is inert as Teflon but strong as steel Weatherproof Jacket Electric Traced Steam Traced Insulation Process Lines Steam Supply & Condensate Return Buffered High Temp Bundle CEMS Designs
41 Case Study 1 : ZADCO Analyzer application : ZADCO off-shore plant Service : Glycol Dehydration Unit Issue : Glycol & Liquide Carryover Played with all the traditional techniques and was failing. Aims studied the case and proposed AMETEK 5100-HD for the application. It has now been 5 years they are running smoothly.
42 Data Sheet
43 Case Study 2 : GASCO Analyzer application : Acid Gas Flare Measurement O2 in ppm : Range ppm. H2S in the stream is 20% Analyzer is in ESD loop
44 Data Sheet For Case 2
45 Case Study 3: QP Service : Recycle Gas compressor suction Application : Moisture measurement. Process stream contains 15 ppm Chlorine (HCL). Existing : Al2O3
46 Data Sheet For Case 3
47 Case Study 4 : PDO OMAN Analyzer application : Acid Gas Flare Measurement O2 : 0-2% H2S in the stream Analyzer is in ESD loop
48 Installation in PDO, OMAN
New advances in folded pathlength technology for Process Tunable Diode Laser Absorption Spectrometers (TDLAS)
New advances in folded pathlength technology for Process Tunable Diode Laser Absorption Spectrometers (TDLAS) Jean-Nicolas Adami, PhD Head of Strategic Product Group Gas Analytics Mettler-Toledo GmbH,
More informationGaseous CEMS technology
GAS CEMS EXTRACTIVE IN-SITU COLD DRY HOT WET DRY DILUTION PROBE/ POINT IN-STACK CROSS STACK OUT OF STACK Gaseous CEMS technology Probe (at stack) Heated filter Heated sample line Condenser Pump Analyzers
More informationWhite Paper. Overview: NDIR Definition:
Title: NDIR Technology Overview, Compliance, and Comparison to Other Generally Available Gas Measurement Technologies TSN Number: 06 File:\\MII- SRV1\Metron\Bridge_Analyzers\Customer_Service_Documentation\White_Papers\06
More informationVALIDATION STUDY OF FTIR-BASED EMISSIONS MEASUREMENTS AT A MUNICIPAL WASTE COMBUSTOR
AP-157 VALIDATION STUDY OF FTIR-BASED EMISSIONS MEASUREMENTS AT A MUNICIPAL WASTE COMBUSTOR Grant M. Plummer, Ph.D. Peter Zemek, Ph.D. Special Projects Manager Applications Manager Enthalpy Analytical,
More informationIntroduction to Electromagnetic Radiation and Radiative Transfer
Introduction to Electromagnetic Radiation and Radiative Transfer Temperature Dice Results Visible light, infrared (IR), ultraviolet (UV), X-rays, γ-rays, microwaves, and radio are all forms of electromagnetic
More informationREAL TIME MEASUREMENTS OF ACETYLENE IN ETHYLENE MANUFACTURING PROCESS. FIELD TRIALS OF THE TDLAS BASED ANALYZER
REAL TIME MEASUREMENTS OF ACETYLENE IN ETHYLENE MANUFACTURING PROCESS. FIELD TRIALS OF THE TDLAS BASED ANALYZER Airat Amerov, Mike Fuller John Orendorff, John Howse AMETEK Process Instruments, LyondellBasell
More informationCantilever enhanced tunable diode laser photoacoustic spectroscopy in gas purity measurement case study: acetylene in ethylene
Cantilever enhanced tunable diode laser photoacoustic spectroscopy in gas purity measurement case study: acetylene in ethylene Juho Uotila, Jussi Raittila, Ismo Kauppinen ¹Gasera Ltd., Tykistökatu 4, 20520
More informationVALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur
VALLIAMMAI ENGINEERING COLLEGE SRM Nagar, Kattankulathur 603 203 DEPARTMENT OF ELECTRONICS AND INSTRUMENTATION ENGINEERING QUESTION BANK V SEMESTER EI6501 Analytical Instruments Regulation 2013 Academic
More informationProcess Analyzer and Sampling Systems
Process Analyzer and Sampling Systems Course Price 3050 Course Description Analytical instruments used for online chemical analysis of process streams or plant environments are generally called Process
More informationPROCESS GAS ANALYZERS FOR THE MEASUREMENT OF AMMONIA AND ACETYLENE CONCENTRATION
PROCESS GAS ANALYZERS FOR THE MEASUREMENT OF AMMONIA AND ACETYLENE CONCENTRATION Airat Amerov Mike Fuller AMETEK Process Instruments, AMETEK Process Instruments, 15 Freeport Road, Pittsburgh, PA 15 Freeport
More informationRS DYNAMICS ECOPROBE 5. Portable IR/PID Gas Analyzer PID. PID and IR Analyzers
RS DYNAMICS ECOPROBE 5 Portable IR/PID Gas Analyzer PID + IR PID and IR Analyzers General ECOPROBE 5 has two autonomous analyzers in one case. The combination of analyzers provides a set of data designed
More information2001 Spectrometers. Instrument Machinery. Movies from this presentation can be access at
2001 Spectrometers Instrument Machinery Movies from this presentation can be access at http://www.shsu.edu/~chm_tgc/sounds/sound.html Chp20: 1 Optical Instruments Instrument Components Components of various
More informationAtmospheric Analysis Gases. Sampling and analysis of gaseous compounds
Atmospheric Analysis Gases Sampling and analysis of gaseous compounds Introduction - External environment (ambient air) ; global warming, acid rain, introduction of pollutants, etc - Internal environment
More informationFourier transform infrared spectroscopy (FTIR) is a method used to obtain an infrared
Fourier Transform Infrared Spectroscopy: Low Density Polyethylene, High Density Polyethylene, Polypropylene and Polystyrene Eman Mousa Alhajji North Carolina State University Department of Materials Science
More informationOverview Brochure Comprehensive range of instrumentation for the measurement of moisture and oxygen
Overview Brochure 2016 Comprehensive range of instrumentation for the measurement of moisture and oxygen Overview Brochure Relative Humidity Probes and Transmitters Repeatable RH and temperature measurement
More informationReprinted from February Hydrocarbon
February2012 When speed matters Loek van Eijck, Yokogawa, The Netherlands, questions whether rapid analysis of gases and liquids can be better achieved through use of a gas chromatograph or near infrared
More informationSERVOTOUGH SpectraScan
SERVOTOUGH SpectraScan Continuous, real-time analysis of light hydrocarbons Jan Hordijk - Servomex Hydrocarbon stream analysis 5 major technologies used in HydroCarbon land for gas: IR (Infra Red) Laser
More informationReal-time ppb CO 2 Impurity Detection by an Advanced FTIR- UVF System
Real-time ppb CO 2 Impurity Detection by an Advanced FTIR- UVF System Presented at the BevTech Conference, Albuquerque, NM 2018 by Charles M. Phillips Ph.D., Max Analytical Technologies Mark Taylor, Vice
More informationDesign and Development of a Smartphone Based Visible Spectrophotometer for Analytical Applications
Design and Development of a Smartphone Based Visible Spectrophotometer for Analytical Applications Bedanta Kr. Deka, D. Thakuria, H. Bora and S. Banerjee # Department of Physicis, B. Borooah College, Ulubari,
More information3 - Atomic Absorption Spectroscopy
3 - Atomic Absorption Spectroscopy Introduction Atomic-absorption (AA) spectroscopy uses the absorption of light to measure the concentration of gas-phase atoms. Since samples are usually liquids or solids,
More informationMeasurement Technique and its Application to Trace Components of Atmospheric Gas
F e a t u r e A r t i c l e Feature Article Measurement Technique and its Application to Trace Components of Atmospheric Gas Junji Kato From early on, HORIBA has been developing and adopting various measurement
More informationUV3000. Accurate, precise, and portable ambient gas point analyzer
UV3000 Accurate, precise, and portable ambient gas point analyzer The Cerex UV3000 is a multifunction analyzer designed to detect part per billion (ppb) to percent level concentrations of multiple gases
More informationComparison of HCD5000 DewPoint Duo to Condumax II
EXECUTIVE SUMMARY This document compares the technology and products of ZEGAZ Instruments (US) to that of Michell Instruments (UK) in the field of hydrocarbon and water dewpoint measurement. INTRODUCTION
More informationAlternative Monitoring Technologies: A Brief Overview
Alternative Monitoring Technologies: A Brief Overview a technical solution to meet every need Cemtek Environmental Inc. 3041 S. Orange Ave. Santa Ana, CA 92707 800-400-0200 www.cemteks.com 1 What s New?
More informationFar UV Absorbance Detector
Far UV Absorbance Detector Theory Most organic and inorganic species absorb strongly in the far UV. Notable exceptions are the inert gases, helium and nitrogen which absorb very weakly in this region.
More informationUV Hound Series. Dependable High Quality Air Monitoring. Accurate Readings Within Seconds. Portable UVDOAS Multi-gas Analyzers. Multi-Gas Capability
UV Hound Series Portable UVDOAS Multi-gas Analyzers Multi-Gas Capability Dependable High Quality Air Monitoring Individual VOCs PPB Sensitivity Non-Contact Optical Measurement Automated Reporting Configurable
More informationInnovations In Optics. Zaheer Juddy - AIMS
Innovations In Optics Zaheer Juddy - AIMS POWER OF OPTICS POWER OF OPTICS Conventional Measurement Techniques is Leaning towards OPTICS POWER OF OPTICS have given us a wide range of Entries to meet Modern
More informationBecause light behaves like a wave, we can describe it in one of two ways by its wavelength or by its frequency.
Light We can use different terms to describe light: Color Wavelength Frequency Light is composed of electromagnetic waves that travel through some medium. The properties of the medium determine how light
More informationDEPARTMENT OF ELECTRONICS AND INSTRUMENTATION ENGINEERING SRM NAGAR, KATTANKULATHUR-603203 EI 2302 ANALYTICAL INSTRUMENTS QUESTION BANK UNIT I COLORIMETRY AND SPECTROPHOTOMETRY Part A 1. State Lambert
More informationTaking fingerprints of stars, galaxies, and interstellar gas clouds
- - Taking fingerprints of stars, galaxies, and interstellar gas clouds Absorption and emission from atoms, ions, and molecules Periodic Table of Elements The universe is mostly hydrogen H and helium He
More informationTaking Fingerprints of Stars, Galaxies, and Other Stuff. The Bohr Atom. The Bohr Atom Model of Hydrogen atom. Bohr Atom. Bohr Atom
Periodic Table of Elements Taking Fingerprints of Stars, Galaxies, and Other Stuff Absorption and Emission from Atoms, Ions, and Molecules Universe is mostly (97%) Hydrogen and Helium (H and He) The ONLY
More informationSULFUR RECOVERY ANALYZERS; UV Diode-Array Fiber- Optics Technology
SULFUR RECOVERY ANALYZERS; UV Diode-Array Fiber- Optics Technology Yoav Barshad Applied Analytics, Inc. 29 Domino Drive Concord, Massachusetts, 01742 KEYWORDS Sulfur recovery, H2S, SO2, tail gas, UV, Spectroscopy,
More information2101 Atomic Spectroscopy
2101 Atomic Spectroscopy Atomic identification Atomic spectroscopy refers to the absorption and emission of ultraviolet to visible light by atoms and monoatomic ions. It is best used to analyze metals.
More informationThe Nature of Light. We have a dual model
Light and Atoms Properties of Light We can come to understand the composition of distant bodies by analyzing the light they emit This analysis can tell us about the composition as well as the temperature
More informationIR Spectrography - Absorption. Raman Spectrography - Scattering. n 0 n M - Raman n 0 - Rayleigh
RAMAN SPECTROSCOPY Scattering Mid-IR and NIR require absorption of radiation from a ground level to an excited state, requires matching of radiation from source with difference in energy states. Raman
More informationTaking fingerprints of stars, galaxies, and interstellar gas clouds. Absorption and emission from atoms, ions, and molecules
Taking fingerprints of stars, galaxies, and interstellar gas clouds Absorption and emission from atoms, ions, and molecules 1 Periodic Table of Elements The universe is mostly hydrogen H and helium He
More informationHL-800K Infrared Laser Thermometer. -50 C to +800 C (13:1 ratio) User Manual
HL-800K Infrared Laser Thermometer -50 C to +800 C (13:1 ratio) User Manual TABLE OF CONTENTS INTRODUCTION... 3 FEATURES... 3 WIDE APPLICATION RANGE... 3 SAFETY... 3 DISTANCE & SPOT SIZE... 4 SPECIFICATIONS...
More informationLAB007 Industrial Analytical Chemistry & Process Analyzer System
LAB007 Industrial Analytical Chemistry & Process Analyzer System H.H. Sheikh Sultan Tower (0) Floor Corniche Street Abu Dhabi U.A.E www.ictd.ae ictd@ictd.ae Course Introduction: Analytical instruments
More informationQuestions, Myths and Misconceptions about Using Photoionization Detectors
Questions, Myths and Misconceptions about Using Photoionization Detectors Solvent, fuel and other VOC vapours are pervasively common in many workplace environments. Increased awareness of the toxicity
More informationLASERS AGAIN? Phys 1020, Day 17: Questions? LASERS: Next Up: Cameras and optics Eyes to web: Final Project Info
LASERS AGAIN? Phys 1020, Day 17: Questions? LASERS: 14.3 Next Up: Cameras and optics Eyes to web: Final Project Info 1 Group Exercise Your pennies will simulate a two state atom; tails = ground state,
More informationChemistry 524--Final Exam--Keiderling Dec. 12, pm SES
Chemistry 524--Final Exam--Keiderling Dec. 12, 2002 --4-8 pm -- 238 SES Please answer all questions in the answer book provided. Calculators, rulers, pens and pencils are permitted plus one 8.5 x 11 sheet
More informationESS15 Lecture 7. The Greenhouse effect.
ESS15 Lecture 7 The Greenhouse effect. Housekeeping. First midterm is in one week. Open book, open notes. Covers material through end of Friday s lecture Including today s lecture (greenhouse effect) And
More informationValidation Study of FTIR-Based Emissions Measurements at a Municipal Waste Combustor
13th North American Waste to Energy Conference May 23-25, 2005, Orlando, Florida USA NAWTEC13-3158 Validation Study of FTIR-Based Emissions Measurements at a Municipal Waste Combustor G. J. Aldina Jeffrey
More informationIndustrial In-line and Multi Component Monitor Using Absorption Spectroscopy and Its Application
FFeature Article Article Industrial In-line and Multi Component Monitor Using Absorption Spectroscopy and Its Application Yoko NAKAI HORIBA s CS-Series chemical concentration monitors that use ultraviolet
More informationLecture 0. NC State University
Chemistry 736 Lecture 0 Overview NC State University Overview of Spectroscopy Electronic states and energies Transitions between states Absorption and emission Electronic spectroscopy Instrumentation Concepts
More informationABB temperature measurement Radiation thermometry. Measurement made easy. Process temperature measurement practice--non-contacting
Whitepaper_ WP_T_Non-Contacting_Temperature_Measurement ABB temperature measurement Radiation thermometry Measurement made easy Process temperature measurement practice--non-contacting By Gary Freeman,
More informationFTIR Spectrometer. Basic Theory of Infrared Spectrometer. FTIR Spectrometer. FTIR Accessories
FTIR Spectrometer Basic Theory of Infrared Spectrometer FTIR Spectrometer FTIR Accessories What is Infrared? Infrared radiation lies between the visible and microwave portions of the electromagnetic spectrum.
More informationChemistry Instrumental Analysis Lecture 3. Chem 4631
Chemistry 4631 Instrumental Analysis Lecture 3 Quantum Transitions The energy of a photon can also be transferred to an elementary particle by adsorption if the energy of the photon exactly matches the
More informationSpectroscopic Applications of Quantum Cascade Lasers
Spectroscopic Applications of Quantum Cascade Lasers F.K. Tittel, A. Kosterev, and R.F. Curl Rice University Houston, USA OUTLINE fkt@rice.edu http://www.ruf.rice.edu/~lasersci/ PQE 2000 Snowbird, UT Motivation
More informationFLAME PHOTOMETRY AIM INTRODUCTION
FLAME PHOTOMETRY AIM INTRODUCTION Atomic spectroscopy is based on the absorption, emission or fluorescence process of light by atoms or elementary ions. Information for atomic scale is obtained in two
More informationAtomization. In Flame Emission
FLAME SPECTROSCOPY The concentration of an element in a solution is determined by measuring the absorption, emission or fluorescence of electromagnetic by its monatomic particles in gaseous state in the
More information25 Instruments for Optical Spectrometry
25 Instruments for Optical Spectrometry 25A INSTRUMENT COMPONENTS (1) source of radiant energy (2) wavelength selector (3) sample container (4) detector (5) signal processor and readout (a) (b) (c) Fig.
More informationS is referred to as sour. The sulfide loading lends an unpleasant odor and makes the water corrosive. Additionally, the presence of H 2
Application Summary Analytes: S (hydrogen sulfide), (ammonia) Detection Technology: OMA-300 Process Analyzer Process Stream: stripped sour water Introduction In the context of petrochemical refining and
More informationAnalytical Technologies in Biotechnology Prof. Dr. Ashwani K Sharma Department of Biotechnology Indian Institute of Technology, Roorkee
Analytical Technologies in Biotechnology Prof. Dr. Ashwani K Sharma Department of Biotechnology Indian Institute of Technology, Roorkee Module - 6 Spectroscopic Techniques Lecture - 2 UV-Visible Spectroscopy
More informationhigh energy state for the electron in the atom low energy state for the electron in the atom
Atomic Spectra Objectives The objectives of this experiment are to: 1) Build and calibrate a simple spectroscope capable of measuring wavelengths of visible light. 2) Measure several wavelengths of light
More informationInstructor: Welcome to. Phys 774: Principles of Spectroscopy. Fall How can we produce EM waves? Spectrum of Electromagnetic Radiation and Light
Welcome to Phys 774: Principles of Spectroscopy Fall 2007 Instructor: Andrei Sirenko Associate Professor at the Dept. of Physics, NJIT http://web.njit.edu/~sirenko 476 Tiernan Office hours: After the classes
More informationExperiment 24: Spectroscopy
Experiment 24: Spectroscopy Figure 24.1: Spectroscopy EQUIPMENT High Voltage Power Supply Incandescent Light Source (3) Gas Discharge Tubes: 1. Helium 2. Hydrogen 3. Unknown Element Spectrometer Felt (1)
More informationIntroduction to FT-IR Spectroscopy
Introduction to FT-IR Spectroscopy An FT-IR Spectrometer is an instrument which acquires broadband NIR to FIR spectra. Unlike a dispersive instrument, i.e. grating monochromator or spectrograph, an FT-IR
More informationSpectroscopy: Introduction. Required reading Chapter 18 (pages ) Chapter 20 (pages )
Spectroscopy: Introduction Required reading Chapter 18 (pages 378-397) Chapter 20 (pages 424-449) Spectrophotometry is any procedure that uses light to measure chemical concentrations Properties of Light
More informationAdvanced Spectroscopy Laboratory
Advanced Spectroscopy Laboratory - Raman Spectroscopy - Emission Spectroscopy - Absorption Spectroscopy - Raman Microscopy - Hyperspectral Imaging Spectroscopy FERGIELAB TM Raman Spectroscopy Absorption
More informationSynthesis and Infrared Spectrum of Nitric Oxide 1
Synthesis and Infrared Spectrum of Nitric Oxide 1 Purpose: Infrared spectroscopy is used to determine the force constant of the bond in nitric oxide. Prelab: Reading: Section 6.1 and 6.2 in Brown, LeMay,
More informationTraining Coarse ECOPROBE 5 CHEMISTRY RS DYNAMICS
Training Coarse ECOPROBE 5 CHEMISTRY Contents Ecoprobe analytical principles Photoionization Infrared spectroscopy Oxygen measurement Pollutants Types and responses Head space New application of Ecoprobe
More informationInfrared Spectroscopy
Infrared Spectroscopy Introduction Spectroscopy is an analytical technique which helps determine structure. It destroys little or no sample. The amount of light absorbed by the sample is measured as wavelength
More informationExperiment #9. Atomic Emission Spectroscopy
Introduction Experiment #9. Atomic Emission Spectroscopy Spectroscopy is the study of the interaction of light with matter. This interaction can be in the form of the absorption or the emission of electromagnetic
More informationChapter 12 Mass Spectrometry and Infrared Spectroscopy
Organic Chemistry, 6 th Edition L. G. Wade, Jr. Chapter 12 Mass Spectrometry and Infrared Spectroscopy Jo Blackburn Richland College, Dallas, TX Dallas County Community College District 2006, Prentice
More informationSkoog Chapter 6 Introduction to Spectrometric Methods
Skoog Chapter 6 Introduction to Spectrometric Methods General Properties of Electromagnetic Radiation (EM) Wave Properties of EM Quantum Mechanical Properties of EM Quantitative Aspects of Spectrochemical
More informationLASERS. Dr D. Arun Kumar Assistant Professor Department of Physical Sciences Bannari Amman Institute of Technology Sathyamangalam
LASERS Dr D. Arun Kumar Assistant Professor Department of Physical Sciences Bannari Amman Institute of Technology Sathyamangalam General Objective To understand the principle, characteristics and types
More informationFTIR measurement of NH 3, HCN, SO 2, H 2 S and COS in pulverized lignite oxy-fuel flames Daniel Fleig, Stefan Hjärtstam and Daniel Kühnemuth
FTIR measurement of NH 3, HCN, SO 2, H 2 S and COS in pulverized lignite oxy-fuel flames Daniel Fleig, Stefan Hjärtstam and Daniel Kühnemuth Abstract Nitrogen and sulphur compounds are investigated in
More information1) Introduction 2) Photo electric effect 3) Dual nature of matter 4) Bohr s atom model 5) LASERS
1) Introduction 2) Photo electric effect 3) Dual nature of matter 4) Bohr s atom model 5) LASERS 1. Introduction Types of electron emission, Dunnington s method, different types of spectra, Fraunhoffer
More informationSub-category: Physics and Principles of Measurement Topic: Monitoring anesthetic gases and vapours Date: January 15-17, 2016 Language: English
Course n : Course 3 Title: RESPIRATORY PHYSIOLOGY, PHYSICS AND PATHOLOGY IN RELATION TO ANAESTHESIA AND INTENSIVE CARE Sub-category: Physics and Principles of Measurement Topic: Monitoring anesthetic gases
More informationElectromagnetic Radiation and Scientific Instruments. PTYS April 1, 2008
Electromagnetic Radiation and Scientific Instruments PTYS 206-2 April 1, 2008 Announcements Deep Impact 6 PM Wednesday Night Pizza, no beer Watch at home if you can t watch here. It will be discussed in
More informationReliability issues of photonic components for space applications
Reliability issues of photonic components for space applications Demetrio López February 21 st 2017 esccon 2016 1 Agenda 1. Short introduction to ALTER TECHNOLOGY 2. Photonic parts for Space Applications.
More informationUNIT 4 Part 2 Measurements of Environmental Air Pollution Parameters j
UNIT 4 Part 2 Measurements of Environmental Air Pollution Parameters j 1 Environmental Air Pollution The addition of any harmful material (having harmful effects on our lives) to our atmosphere is called
More informationSpectrophotometry. Dr. Shareef SHAIK ASST. PROFESSOR Pharmacology
Spectrophotometry Dr. Shareef SHAIK ASST. PROFESSOR Pharmacology Content Introduction Beer-Lambert law Instrument Applications Introduction 3 Body fluids such as blood, csf and urine contain organic and
More informationKinds of Energy. Defining Energy is Hard! EXPLAIN: 1. Energy and Radiation. Conservation of Energy. Sco; Denning CSU ESMEI ATS 1
Defining Energy is Hard! EXPLAIN: 1. Energy and Radiation Energy is the capacity to perform work (but physicists have a special definition for work, too!) Part of the trouble is that scientists have appropriated
More informationPhys 100 Astronomy (Dr. Ilias Fernini) Review Questions for Chapter 5
Phys 100 Astronomy (Dr. Ilias Fernini) Review Questions for Chapter 5 MULTIPLE CHOICE 1. What is the wavelength of the longest wavelength light visible to the human eye? a. 400 nm b. 4000 nm c. 7000 nm
More informationChapter 4 Spectroscopy
Chapter 4 Spectroscopy The beautiful visible spectrum of the star Procyon is shown here from red to blue, interrupted by hundreds of dark lines caused by the absorption of light in the hot star s cooler
More informationInstrumental Analysis: Spectrophotometric Methods
Instrumental Analysis: Spectrophotometric Methods 2007 By the end of this part of the course, you should be able to: Understand interaction between light and matter (absorbance, excitation, emission, luminescence,fluorescence,
More informationPreview from Notesale.co.uk Page 1 of 38
F UNDAMENTALS OF PHOTONICS Module 1.1 Nature and Properties of Light Linda J. Vandergriff Director of Photonics System Engineering Science Applications International Corporation McLean, Virginia Light
More informationR O Y G B V. Spin States. Outer Shell Electrons. Molecular Rotations. Inner Shell Electrons. Molecular Vibrations. Nuclear Transitions
Spin States Molecular Rotations Molecular Vibrations Outer Shell Electrons Inner Shell Electrons Nuclear Transitions NMR EPR Microwave Absorption Spectroscopy Infrared Absorption Spectroscopy UV-vis Absorption,
More informationCH0302 Process Instrumentation. Lecture 9 Composition Analysis
CH0302 Process Instrumentation Lecture 9 Composition Analysis Department of Chemical Engineering School of Bioengineering SRM University Kattankulathur 603203 4/3/15 Chemical Engineering 1 Industrial significance
More informationEmission spectrum of H
Atomic Spectroscopy Atomic spectroscopy measures the spectra of elements in their atomic/ionized states. Atomic spectrometry, exploits quantized electronic transitions characteristic of each individual
More informationChapter 2. Heating Earth's Surface & Atmosphere
Chapter 2 Heating Earth's Surface & Atmosphere Topics Earth-Sun Relationships Energy, Heat and Temperature Mechanisms of Heat Transfer What happens to Incoming Solar Radiation? Radiation Emitted by the
More informationChem Homework Set Answers
Chem 310 th 4 Homework Set Answers 1. Cyclohexanone has a strong infrared absorption peak at a wavelength of 5.86 µm. (a) Convert the wavelength to wavenumber.!6!1 8* = 1/8 = (1/5.86 µm)(1 µm/10 m)(1 m/100
More informationPutting Near-Infrared Spectroscopy (NIR) in the spotlight. 13. May 2006
Putting Near-Infrared Spectroscopy (NIR) in the spotlight 13. May 2006 0 Outline What is NIR good for? A bit of history and basic theory Applications in Pharmaceutical industry Development Quantitative
More informationSPECTROSCOPY Basic concepts part 1
SPECTROSCOPY Basic concepts part 1 Spectroscopy is the science of spectra, i.e. it involves a measurement of a property that is a function of the frequency of the light Umeå 2006-04-10 Bo Karlberg Light
More informationApplication of IR Raman Spectroscopy
Application of IR Raman Spectroscopy 3 IR regions Structure and Functional Group Absorption IR Reflection IR Photoacoustic IR IR Emission Micro 10-1 Mid-IR Mid-IR absorption Samples Placed in cell (salt)
More informationInfra Red Spectroscopy
CH 2252 Instrumental Methods of Analysis Unit I Infra Red Spectroscopy M. Subramanian Assistant Professor Department of Chemical Engineering Sri Sivasubramaniya Nadar College of Engineering Kalavakkam
More informationPAPER No. 12: ORGANIC SPECTROSCOPY MODULE No. 4: Basic principles and Instrumentation for IR spectroscopy
Subject Chemistry Paper No and Title Module No and Title Module Tag Paper 12: Organic Spectroscopy Module 4: Basic principles and Instrumentation for IR spectroscopy CHE_P12_M4_e-Text TABLE OF CONTENTS
More informationThe Claviature of Gas Analysis
The Claviature of Gas Analysis Mass spectrometric gas analysis for quality assurance of gases and gas mixtures High purity and special gases are becoming increasingly important in the development of modern
More informationElectromagnetic Waves
4/15/12 Chapter 26: Properties of Light Field Induction Ok, so a changing magnetic field causes a current (Faraday s law) Why do we have currents in the first place? electric fields of the charges Changing
More informationIncreasing energy. ( 10 4 cm -1 ) ( 10 2 cm -1 )
The branch of science which deals with the interaction of electromagnetic radiation with matter is called spectroscopy The energy absorbed or emitted in each transition corresponds to a definite frequency
More informationrequency generation spectroscopy Rahul N
requency generation spectroscopy Rahul N 2-11-2013 Sum frequency generation spectroscopy Sum frequency generation spectroscopy (SFG) is a technique used to analyze surfaces and interfaces. SFG was first
More informationPrentice Hall EARTH SCIENCE
Prentice Hall EARTH SCIENCE Tarbuck Lutgens Chapter 24 Studying the Sun 24.1 The Study of Light Electromagnetic Radiation Electromagnetic radiation includes gamma rays, X-rays, ultraviolet light, visible
More informationAssessing Unknown Odors and Chemicals
Treat yourself to better rental service. Thank You for Attending Today s Webinar: Assessing Unknown Odors and Chemicals Your Host Matt DeLacluyse Operations Mgr RAECO Rents mattd@raecorents.com Featured
More informationEMISSION SPECTROSCOPY
IFM The Department of Physics, Chemistry and Biology LAB 57 EMISSION SPECTROSCOPY NAME PERSONAL NUMBER DATE APPROVED I. OBJECTIVES - Understand the principle of atomic emission spectra. - Know how to acquire
More informationFLS980 Series Reference Guide
FLS980 Series Reference Guide Integrating Sphere for Measurements of Fluorescence Quantum Yields and Spectral Reflectance Revision 1 Copyrights Copyright 2016 Edinburgh Instruments Ltd. All rights reserved.
More informationLight Matter Interactions: Theory and Applications (LMITA) What is Light?
What is Light? Light is a Form of Electromagnetic Radiation Light and Matter Fundamentals Light is a manifestation of electromagnetic force. Matter is composed of charged particles, or atoms, which consist
More informationPHYS 160 Astronomy Test #2 Fall 2017 Version A
PHYS 160 Astronomy Test #2 Fall 2017 Version A I. True/False (1 point each) Circle the T if the statement is true, or F if the statement is false on your answer sheet. 1. A blackbody emits all of its radiation
More informationAtomic Emission Spectra
Atomic Emission Spectra Objectives The objectives of this laboratory are as follows: To build and calibrate a simple meter-stick spectroscope that is capable of measuring wavelengths of visible light.
More information