ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSIS

Size: px
Start display at page:

Download "ANALYTICAL/CHEMICAL CERTIFICATE OF ANALYSIS"

Transcription

1 Sample Name: Spilanthes acmella extractprodu de: N/A Batch/Lot #: SEX64/003/16-17 Page:1/5 Pesticides Bromophos-methyl Flucythrlnate Methoxychlor Pyrettirums (Clnerin I, Cinerln II,Jasmolln I, Jasmolln II, Pyrethrin I, Pyrethrin II) Acephate Aldrin and dieidrln (sum of) Azinphos-ethyl Azinphos-methyl Bromophos-ethyl Bromopropylate Chlordane (sum of cis-trans-, and oxychlordane) Chlorfenvlnphos Chlorpyrlphos-ethyl Chlorpyriphos-methyl Chlorthal-dimethyl Cyfluthrin (sum of) A-Cyhalothrin MQLTM-0343 (USP<S61>Modifled) bvgc-ms MQLTM-0343 {USP<561>Modified) MQLTM-0343 (LISP<561> Modified) 3ppm Qmg/kg O.OO-O.Olmg/kg 0.00-l,00mg/kg Results: < < < <0.0Smg/kg <O.SOmg/kg

2 Ph#: Sample Name: Spilanthes acmella extract PC#: N/A Page:2/5 Cvpermethfin and Isomers (sum oo DDT (sum of o,p'-d0e,p,p'-dde,o,p'-ddt, p,p'-ddt, o,p'-tde, and p,p-tde Deltamethrin Diarinon Dichlofluanid Dichlorvos Dicofol Dimethoate and omethoate (sum of) Endosulfan (sum of isomers and endosulfan sulphate) Endrin Ethion Etrimphos Fenctiiorophos (sum of fenchlorophos and fenchlorophos-oxon) Fenitrothlon by6c-ms MQLTM^)343 (USP<561> Modified) MQLTM-0343 (USP<551> Modified) 0.5mg/kg OSmg/kg mg/kg <0.S0mg/kg <0.5mg/kg <2.00mg/kg Fenpropathrin ' mg/kg <0.03m6/kg Fensuifothlon (sum of fensuifothlon, fensulfothion-oxon, fensulfothion-oxonsuifon, and fensulfothion-suifon) Fenthion (sum of fenthion, fenthionoxon, fenthion-oxon-suifon,fenthionoxon-sulfoxid, fenthion-sulfon, and fenthion-sulfoxid) ,OSmg/kg Form#038.2 Analytical / Chemical Certificate of Analysis, Revised 06/29/15 DCR201S-0082

3 Plot tf 179 & 180, Cheekatmamldi (V), Bommalramaram (M) Ph U: Sample Name: Spilanthes acmeiia extract PC#: N/A Page:3/5 Fenvalerate Tau-Fluvslinate Fonophos Hept3chlor(sum of heptachlor, os- heptachlorepoxide, andtrans-heptachiorepoxide) j Hexachlorobenzene Hexachlorocyclohexane (sum of isomers a, P-, 6, and E-) Lindan (T-hexachlorocyclohexane) Malathion and malaoxon (sum of) Mecarbam MQLTM-0343 (U5P<561> Modified) MQLTM-0343 (U5P<S61> Modified) O.OO-l.SOmg/kg O.OO-O.QSmg/kg O.OO-O.lmg/kg mg/kg mg/kg O.O-l.OOmg/kg O.GO-O.OSmg/kg Results: <1.50mg/kg <0.1mg/kg <0.30mg/kg <0.60mg/kg Methacriphos Methamidophos Methidathion Mirex Monocrotophos Parathion-ethyl and Paraoxon-ethyl (sum of) Parathlon-methyl and Paraoxon-methyl (sum of) Pendlmethalin Pentachloranisol Permechrin and Isomers (sum of) MQLTM-0343 (LISP<561>Modified) MQLTM-0343 {USP<551> Modified) Q.OO-O.Olmg/kg lOmg/kg mg/kg O.lmg/kg O.OO-O.Olmg/kg mg/kg co.lmgas Phosalone MQLTM-0343{USP<561> Modified) Form# Analytical / Chemical Certificate of Analysis, Revised 06/29/15 DCR201S-0082

4 Stiriti Ayur Therapies PVTLTD Sample Name: Spllanthes acmelia extract Accession ft: Sample Description: Bulk, 10 grams; Page:4/5 Phosmet PIperonyl butoxide Pirimiphos-ethyl Pirimiphos-methyl (sum of pirlmiphosmethyl and N-desethyl-pirimiphos-methyl) Procymidone Profenophos Quintozene (sum of quintozene, pentachloranillne, and methyl pentachlorphenyl sulflde) US Pharmacopeia By GC-MS MQLTM-G343 (USP<561> Modified) By GC-MS USP Limit Levei: mg/kg 0, mg/kg mg/kg mg/kg mg/kg <4.00mg/kg <0.02mg/kg <0.30mg/kg <0.40mg/kg

5 Stirltl Ayur Therapies PVTLTD ACCREDITED Sample Name: Spilanthes acmella extract Sample Description: Bulk, 10 grams; USPharmacopeia Page:5/5 Prepared By: Lisa Ha/Document Control AU /03/16 Reviewed By: Danielle Dobrow/Document Control Supervisor 08/03/16, i5ona2la ISO accredited testing laboratory (Certificate Number ). The requirements of ISO werefollowedfor the test, results and preparation of thiscertificate of analysis. 'sscope of accreditation may be found on A2LA or websites. The aforementioned resultson thisreport are representative of the samplessubmittedand maynot be indicative of the entire manufacture, batch, and/or lot.applicable current CMP's shallalwaysbe used whensampling. GLP's shallalwaysbe practicedby to ensure the most accurate results.

QuEChERS Pesticide Analysis for Fresh Produce*

QuEChERS Pesticide Analysis for Fresh Produce* QuEChERS Pesticide Analysis for Fresh Produce* UCT Products: ECMSSC50CTFS-MP (6 grams MgSO 4, 1.5 g NaCl) ECQUEU1115CT (1.2 grams MgSO 4, 0.4 g PSA, 0.4 g GCB) ECMSC1850CT (1500 mg MgSO 4, 500 mg endcapped

More information

Multi-residue Method for Agricultural Chemicals by GC-MS (Animal and Fishery Products)

Multi-residue Method for Agricultural Chemicals by GC-MS (Animal and Fishery Products) Multi-residue Method for Agricultural Chemicals by GC-MS (Animal and Fishery Products) 1. Analytes For muscle, fat, liver, kidney and fish/shellfish, see Table 5. For milk, egg and honey, see Table 6.

More information

Official Journal of the European Union L 328/9

Official Journal of the European Union L 328/9 6.12.2008 Official Journal of the European Union L 328/9 COMMISSION REGULATION (EC) No 1213/2008 of 5 December 2008 concerning a coordinated multiannual Community control programme for 2009, 2010 and 2011

More information

COMMISSION REGULATION (EU)

COMMISSION REGULATION (EU) L 269/8 Official Journal of the European Union 13.10.2010 COMMISSION REGULATION (EU) No 915/2010 of 12 October 2010 concerning a coordinated multiannual control programme of the Union for 2011, 2012 and

More information

Three-Fold Increase in Productivity for Pesticide Residue Analysis in Baby Food Using Fast Triple Quadrupole GC-MS/MS

Three-Fold Increase in Productivity for Pesticide Residue Analysis in Baby Food Using Fast Triple Quadrupole GC-MS/MS Three-Fold Increase in Productivity for Pesticide Residue Analysis in Baby Food Using Fast Triple Quadrupole GC-MS/MS Cristian Cojocariu,1 Michael T. Hetmanski,2 Paul Silcock,1 and Richard J. Fussell2

More information

[AMI] Multi-residue method, by LC-MSMS, for the quantification of amitraz and its metabolites in fruit, vegetables, cereals and cereal products

[AMI] Multi-residue method, by LC-MSMS, for the quantification of amitraz and its metabolites in fruit, vegetables, cereals and cereal products Multi-residue methods: all the mentioned substances will be searched for. The general reporting limit (RL) (mg/kg) is mentioned on the right side of each pesticide. The limit of quantification may vary

More information

Improved GC/MS Analysis of Tomato Pesticides with Agilent Deactivated Silica Tubing

Improved GC/MS Analysis of Tomato Pesticides with Agilent Deactivated Silica Tubing Improved GC/MS Analysis of Tomato Pesticides with Agilent Deactivated Silica Tubing Agilent Ultimate Plus Deactivated Fused Silica Tubing for Guard Columns Application Note Food Safety Authors Yun Zou

More information

Pesticides Analysis Using the Agilent 5977A Series GC/MSD

Pesticides Analysis Using the Agilent 5977A Series GC/MSD Pesticides Analysis Using the Agilent 5977A Series GC/MSD Application Note Food Testing and Agriculture Authors Jia-jia Wu and Wen-wen Wang Agilent Technologies Co. Ltd (China) Beijing, People s Republic

More information

Routine-grade robustness with the Advanced Electron Ionization source: confirmation of contaminants in food products at trace levels by GC-MS/MS

Routine-grade robustness with the Advanced Electron Ionization source: confirmation of contaminants in food products at trace levels by GC-MS/MS TECHNICAL NOTE 10605 Routine-grade robustness with the Advanced Electron Ionization source: confirmation of contaminants in food products at trace levels by GC-MS/MS Authors Richard Law, 1 Paul Silcock,

More information

Analysis of Pesticides in Baby Foods Using a Triple-Quadrupole GC/MS/MS

Analysis of Pesticides in Baby Foods Using a Triple-Quadrupole GC/MS/MS PO-CONE Analysis of Pesticides in Baby Foods Using a Pittcon 01 -P Laura Chambers, Richard Whitney, Ph.D., Nicole M. Lock, Zhuangzhi Max Wang, Ph.D., Clifford M. Taylor; Shimadzu Scientific Instruments,

More information

GC/Q-TOF MS Surveillance of Pesticides in Food

GC/Q-TOF MS Surveillance of Pesticides in Food GC/Q-TOF MS Surveillance of Pesticides in Food A Combined Workflow for Quantitative and Qualitative Screening of Pesticides using the Agilent MassHunter GC/Q TOF Pesticide Personal Compound Database and

More information

Analysis of Pesticides and Contaminants using HS-SPME-GC/MS and DRS Detection. Blair Surridge, Tyler Dyer, Rene Bilideau, Paloma Bertolin Presoti

Analysis of Pesticides and Contaminants using HS-SPME-GC/MS and DRS Detection. Blair Surridge, Tyler Dyer, Rene Bilideau, Paloma Bertolin Presoti Analysis of Pesticides and Contaminants using HS-SPME-GC/MS and DRS Detection Blair Surridge, Tyler Dyer, Rene Bilideau, Paloma Bertolin Presoti Applied Research at Camosun College Provides funding to

More information

High Throughput Multi-Residue Screening of Drinking Water using the SPE-DEX~ and Pegasus GC-TOF-MS

High Throughput Multi-Residue Screening of Drinking Water using the SPE-DEX~ and Pegasus GC-TOF-MS Application Note No. 098 High Throughput Multi-Residue Screening of Drinking Water using the SPE-DEX~ and Pegasus GC-TOF-MS Steve Scott, Thames Water, Reading, UK Diane Turner. Introduction In cases of

More information

Certificate of pesticide multi-residue analysis by MSMS detection

Certificate of pesticide multi-residue analysis by MSMS detection Multi-residue methods: all the mentioned substances will be searched for. The general reporting limit (RL) (mg/kg) is mentioned on the right side of each pesticide. The limit of quantification may vary

More information

DETERMINATION OF OCs, PCBs AND SYNTHETIC PYRETHROIDS IN ANIMAL FAT

DETERMINATION OF OCs, PCBs AND SYNTHETIC PYRETHROIDS IN ANIMAL FAT DETERMINATION OF OCs, PCBs AND SYNTHETIC PYRETHROIDS IN ANIMAL FAT Peter Hancock 1, Mike Hetmanski 2 and Richard J. Fussell 2 1 Waters Corporation, Atlas Park, Simonsway, Manchester M22 5PP, UK 2 Central

More information

Rugged GC/MS/MS Pesticide Residue Analysis Fulfilling the USDA Pesticide Data Program (PDP) Requirements

Rugged GC/MS/MS Pesticide Residue Analysis Fulfilling the USDA Pesticide Data Program (PDP) Requirements Rugged GC/MS/MS Pesticide Residue Analysis Fulfilling the USDA Pesticide Data Program (PDP) Requirements Application Note Food Safety Author Katerina Mastovska Excellcon International LLC Plymouth Meeting,

More information

Technical Report. Residual Pesticides Analysis of Botanical Ingredients Using Gas Chromatography Triple Quadrupole Mass Spectrometry.

Technical Report. Residual Pesticides Analysis of Botanical Ingredients Using Gas Chromatography Triple Quadrupole Mass Spectrometry. C-E33 Technical Report Residual Pesticides Analysis of Botanical Ingredients Using Gas Chromatography Triple Quadrupole Mass Spectrometry Riki Kitano 1, Tairo Ogura 1, Nicole Lock 1, Robert Clifford 1,

More information

Pure Chromatography. Food Safety Applications. Abstract. Introduction

Pure Chromatography. Food Safety Applications.  Abstract. Introduction Food Safety Applications Mitigating Matrix Effects: Examination of Dilution, QuEChERS, and Calibration Strategies for LC-MS/MS Analysis of Pesticide Residues in Diverse Food Types Abstract By Julie Kowalski,

More information

Original Paper. i 2006 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. 1 Introduction. 1.1 Sorptive extraction

Original Paper. i 2006 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. 1 Introduction. 1.1 Sorptive extraction 66 M. Jµnskµ et al. J. Sep. Sci. 2006, 29,66 80 Marie Jµnskµ 1 Steven J. Lehotay 2 Katerina MaÐtovskµ 2 Jana HajÐlovµ 1 Tal Alon 3 Aviv Amirav 3 1 Department of Food Chemistry and Analysis, Institute of

More information

Evaluation of common organic solvents for gas chromatographic analysis and stability of multiclass pesticide residues

Evaluation of common organic solvents for gas chromatographic analysis and stability of multiclass pesticide residues Journal of Chromatography A, 1040 (2004) 259 272 Evaluation of common organic solvents for gas chromatographic analysis and stability of multiclass pesticide residues Kateřina Maštovská, teven J. Lehotay

More information

Fast GC-MS/MS for High Throughput Pesticides Analysis

Fast GC-MS/MS for High Throughput Pesticides Analysis Application Note: 5227 Fast GC-MS/MS for High Throughput Pesticides Analysis Igor Fochi, Elena Ciceri, Hans-Joachim Huebschmann, Thermo Fisher Scientific, Milan, Italy Ciro D Aniello, Laboratorio D aniello

More information

Analysis of Pesticides in Citrus Oil Using a Shimadzu GCMS-TQ8030. No. GCMS No. SSI-GCMS-1404

Analysis of Pesticides in Citrus Oil Using a Shimadzu GCMS-TQ8030. No. GCMS No. SSI-GCMS-1404 Gas Chromatograph Mass Spectrometer No. GCMS-1404 Analysis of Pesticides in Citrus Oil Using a Shimadzu GCMS-TQ8030 Introduction Contamination of consumer products with pesticides is a growing concern

More information

Safeguarding Food from Pesticides by UHPLC After Extraction with the QuEChERS Method

Safeguarding Food from Pesticides by UHPLC After Extraction with the QuEChERS Method application Note Liquid Chromatography Authors Roberto Troiano Valentina Scanzani PerkinElmer, Italia S.p.A. Monza, Italy Safeguarding Food from s by UHPLC After Extraction with the QuEChERS Method Introduction

More information

Challenging Pesticide Analysis Using an Agilent J&W DB-35ms Ultra Inert GC Column

Challenging Pesticide Analysis Using an Agilent J&W DB-35ms Ultra Inert GC Column Challenging Pesticide Analysis Using an Agilent J&W DB-ms Ultra Inert GC Column Application Note Food Analysis and Environmental Authors Ken Lynam and Doris Smith Agilent Technologies, Inc. 80 Centerville

More information

Matrix-induced effects: a critical point in the gas chromatographic analysis of pesticide residues

Matrix-induced effects: a critical point in the gas chromatographic analysis of pesticide residues Journal of Chromatography A, 800 (1998) 283 295 Matrix-induced effects: a critical point in the gas chromatographic analysis of pesticide residues a a, a a a a b J. Hajslova ˇ *, K. Holadova, V. Kocourek,

More information

Certificate of Analysis

Certificate of Analysis Certificate of Analysis 2139 Certificate Number: 13-92896 Date: 27/11/2013 Client: Stainton Quarry Stainton Quarry Stainton Barnard Castle DL12 8RB Our Reference: 13-92896 Client Reference: Description:

More information

Analytical Test Report 10

Analytical Test Report 10 OLCC #022892C 9 SE Division St. Laboratory ID: 805024-02 Batch ID: AC Date Sampled: 05/07/8 Date Printed: 05//8 Report cannot be used for OLCC/OHA compliance. Date Sampled: 05/07/8 00:00 Date Accepted:

More information

CropLife Australia Insecticide Resistance Management Review Group Mode of Action Classification for Insecticides Valid as at 7 June 2017

CropLife Australia Insecticide Resistance Management Review Group Mode of Action Classification for Insecticides Valid as at 7 June 2017 1* Acetylcholinesterase inhibitors * all members of this class may not be cross resistant 2 GABA-gated chloride channel blockers 1A Carbamates* 1B Organophosphates* 2A Cyclodiene organochlorines 2B Phenylpyrazoles

More information

CropLife Australia Insecticide Resistance Management Review Group Mode of Action Classification for Insecticides Valid as at 22 June 2018

CropLife Australia Insecticide Resistance Management Review Group Mode of Action Classification for Insecticides Valid as at 22 June 2018 1* Acetylcholinesterase inhibitors * all members of this class may not be cross resistant 2 GABA-gated chloride channel blockers 1A Carbamates* 1B Organophosphates* 2A Cyclodiene organochlorines 2B Phenylpyrazoles

More information

Determination of Pesticide Multiresidues in Apple, Pear and Grape using modified QuEChERS and analysis by LC-QTOF MS

Determination of Pesticide Multiresidues in Apple, Pear and Grape using modified QuEChERS and analysis by LC-QTOF MS Determination of Pesticide Multiresidues in Apple, Pear and Grape using modified QuEChERS and analysis by LC-QTOF MS Application Note Authors Renato Zanella, Juliana S. Munaretto, and Manoel L. Martins

More information

Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK

Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK Building 170 Abbot Drive Kent Science Park Sittingbourne Kent ME9 8AZ Contact: Mr C Murr Tel: +44 (0) 01795 411810 E-Mail: chris.murr@qtsanalytical.com

More information

Application of supercritical fluid extraction in multi-residue pesticide analysis of plant matrices

Application of supercritical fluid extraction in multi-residue pesticide analysis of plant matrices Eur Food Res Technol (2003) 216:68 74 DOI 10.1007/s00217-002-0589-8 ORIGINAL PAPER Jan Poustka Kateřina Holadová Jana Hajšová Application of supercritical fluid extraction in multi-residue pesticide analysis

More information

U.S. Department of the Interior U.S. Geological Survey. Water-Resources Investigations Report

U.S. Department of the Interior U.S. Geological Survey. Water-Resources Investigations Report Methods of Analysis by the U.S. Geological Survey National Water Quality Laboratory Determination of Moderate-Use Pesticides and Selected Degradates in Water by C-18 Solid-Phase Extraction and Gas Chromatography/Mass

More information

IMPROVED IDENTIFICATION OF PESTICIDES USING ATMOSPHERIC PRESSURE GAS CHROMATOGRAPHY MASS SPECTROMETRY

IMPROVED IDENTIFICATION OF PESTICIDES USING ATMOSPHERIC PRESSURE GAS CHROMATOGRAPHY MASS SPECTROMETRY IMPROVED IDENTIFICATION OF PESTICIDES USING ATMOSPHERIC PRESSURE GAS CHROMATOGRAPHY MASS SPECTROMETRY Kelly Dorweiler, Senior Scientist Chemical Residue Method Development North American Chemical Residue

More information

Analytical Test Report Birthday Cake OG

Analytical Test Report Birthday Cake OG ORELAP #4096 OLCC #1002112892C Science First. 11119 SE Division St. Portland, OR 97266 (503) 307-0096 Analytical Test Report Birthday Cake OG Gardens of Odin 020-1003851CB2B Laboratory ID: 1710112-03 Batch

More information

Application Note No Introduction. DMI Instrumentation. DMI Method. DMI for Lettuce and Pea Extracts. Lettuce results

Application Note No Introduction. DMI Instrumentation. DMI Method. DMI for Lettuce and Pea Extracts. Lettuce results Application Note No. 082 Multi-Residue Analysis of Pesticides in Samples of Lettuce and Peas Using Large Volume-Difficult Matrix Introduction-Gas Chromatography-Mass Spectrometry (LV-DMI-GC-MS) Richard

More information

Supercritical fluid extraction for the analysis of pesticide residues in miscellaneous samples

Supercritical fluid extraction for the analysis of pesticide residues in miscellaneous samples J. Biochem. Biophys. Methods 43 (000) 313 38 www.elsevier.com/ locate/ jbbm Review Supercritical fluid extraction for the analysis of pesticide residues in miscellaneous samples Noboru Motohashi *, Hideo

More information

Pulsed Splitless Injection and the Extent of Matrix Effects in the Analysis of Pesticides

Pulsed Splitless Injection and the Extent of Matrix Effects in the Analysis of Pesticides Pulsed Splitless Injection and the Extent of Matrix Effects in the Analysis of Pesticides Michal Godula, Jana Hajšlová*, Kateřina Alterová Institute of Chemical Technology, Department of Food Chemistry

More information

Index 1 Residual Pesticides 3 Food Additives 4 Others 2 Veterinary Drugs (Antibiotics and Synthetic Antibacterials) 5 Reference Materials

Index 1 Residual Pesticides 3 Food Additives 4 Others 2 Veterinary Drugs (Antibiotics and Synthetic Antibacterials) 5 Reference Materials C9-E7A Index Residual Pesticides. Analysis of 4 Pesticides With Capillary GC-FTD and GC-ECD () - GC Analysis of 4 Pesticides With Capillary GC-FTD and GC-ECD () - GC Analysis of 4 Pesticides With Capillary

More information

MULTIRESIDUE ANALYSIS OF PRIORITY POLLUTANTS IN SURFACE WATERS USING EXACT MASS GC-TOF MS

MULTIRESIDUE ANALYSIS OF PRIORITY POLLUTANTS IN SURFACE WATERS USING EXACT MASS GC-TOF MS MULTIRESIDUE ANALYSIS OF PRIORITY POLLUTANTS IN SURFACE WATERS USING EXACT MASS GC-TOF MS Peter Hancock and Keith Worrall Waters Corporation, Manchester M22 5PP, UK INTRODUCTION The Dangerous Substances

More information

Multi pesticide residue analysis in tobacco by GCMS/MS using QuEChERS as an extraction method

Multi pesticide residue analysis in tobacco by GCMS/MS using QuEChERS as an extraction method PO-CON463E Multi pesticide residue analysis in tobacco by GCMS/MS using QuEChERS as an extraction method ASMS 04 TP76 Durvesh Sawant (), Dheeraj Handique (), Ankush Bhone (), Prashant Hase (), Sanket Chiplunkar

More information

Bayesian nonparametric model for clustering individual co-exposure to pesticides found in the French diet.

Bayesian nonparametric model for clustering individual co-exposure to pesticides found in the French diet. Bayesian nonparametric model for clustering individual co-exposure to pesticides found in the French diet. Amélie Crépet, Jessica Tressou To cite this version: Amélie Crépet, Jessica Tressou. Bayesian

More information

Multi-residue Analysis for PAHs, PCBs and OCPs on Agilent J&W FactorFour VF-Xms

Multi-residue Analysis for PAHs, PCBs and OCPs on Agilent J&W FactorFour VF-Xms Multi-residue Analysis for PAHs, PCBs and OCPs on Agilent J&W FactorFour VF-Xms Application Note Author Laura Provoost Agilent Technologies, Inc. Introduction In multi-residue analysis different groups

More information

The Pulsed Flame Photometric Detector for analysis of phosphorus pesticides in wastewater and food commodities

The Pulsed Flame Photometric Detector for analysis of phosphorus pesticides in wastewater and food commodities The Pulsed Flame Photometric Detector for analysis of phosphorus pesticides in wastewater and food commodities Application Note Environmental Authors Agilent Technologies, Inc. Introduction Twenty-eight

More information

ARTICLES. Federal Center for Animal Health (VNIIZZh), Yur evets, Vladimir, Russia b

ARTICLES. Federal Center for Animal Health (VNIIZZh), Yur evets, Vladimir, Russia b ISSN 1061-9348, Journal of Analytical Chemistry, 013, Vol. 68, No. 10, pp. 91 93. Pleiades Publishing, Ltd., 013. Original Russian Text V.G. Amelin, D.K. Lavrukhin, A.V. Tret yakov, 013, published in Zhurnal

More information

The Analysis of Organophosphate Pesticides by LC/MS Application

The Analysis of Organophosphate Pesticides by LC/MS Application The Analysis of Organophosphate Pesticides by LC/MS Application LC-MS Authors Paul Zavitsanos Agilent Technologies, Inc. 2850 Centerville Road Wilmington, DE 19808-1610 USA Paul Yang MOE Ontario Canada

More information

Multi-residue GC-MS analysis. Richard Fussell CSL York, UK

Multi-residue GC-MS analysis. Richard Fussell CSL York, UK Multi-residue GC-MS analysis Richard Fussell CSL York, UK e-mail: r.fussell@csl.gov.uk Outline of Presentation Background Gas Chromatography Mass Spectrometry - Options Capabilities and Applications Summary

More information

The Republic of the Union of Myanmar Ministry of Industry

The Republic of the Union of Myanmar Ministry of Industry The Republic of the Union of Myanmar Ministry of Industry Central Leading Board on Prevention of Hazard from Chemical and Related Substances Notification No: 3/2016 The 10 th Waning Day of Nayon 1378 ME

More information

Sensitive and Repeatable Analysis of Pesticides in QuEChERS Extracts with APGC-MS/MS

Sensitive and Repeatable Analysis of Pesticides in QuEChERS Extracts with APGC-MS/MS Sensitive and Repeatable Analysis of Pesticides in QuEChERS Extracts with APGC-MS/MS Dominic Roberts, 1 Sara Stead, 1 and Jennifer A. Burgess 2 1 Waters Corporation, Manchester, UK 2 Waters Corporation,

More information

GOVERNMENT OF TELANGANA ABSTRACT

GOVERNMENT OF TELANGANA ABSTRACT GOVERNMENT OF TELANGANA ABSTRACT Telangana State Pollution Control Board Fee payable to Telangana State Pollution Control Board in respect of analysis for various Analytical parameters and sampling charges

More information

challenge in analysis of multiple pesticide residues

challenge in analysis of multiple pesticide residues INSTITUTE OF CHEMICAL TECHNOLOGY Department of Food Chemistry and Analysis Prague, Czech Republic Jana.Hajslova Hajslova@vscht.czcz GCxGC GC/TOF- MS: challenge in analysis of multiple pesticide residues

More information

Simultaneous analysis of pesticides by GC/MS

Simultaneous analysis of pesticides by GC/MS II.7.1 Simultaneous analysis of pesticides by GC/MS by Shinji Kageyama and Makoto Ueki 7.1 Introduction Agricultual chemicals include not only pesticides for protecting plants, such as insecticides, germicides,

More information

Certificate of analysis 18/007182

Certificate of analysis 18/007182 Page: 1/6 Certificate of analysis 18/007182 BILLA BULGARIA EOOD 55 BULGARIA BOUL. 1404 SOFIA Bulgaria Sample Type: Reference: cauliflower 00BBU18101606; 0241020 Карфиол / Лабораторна проба/контролна проба:

More information

CORESTA Guide N 5 Technical Guide for Pesticide Residues Analysis on Tobacco and Tobacco Products

CORESTA Guide N 5 Technical Guide for Pesticide Residues Analysis on Tobacco and Tobacco Products Cooperation Centre for Scientific Research Relative to Tobacco CORESTA Guide N 5 Technical Guide for Pesticide Residues Analysis on Tobacco and Tobacco Products October 2018 Agrochemicals Analysis Sub-Group

More information

AppNote 4/2004. KEYWORDS Multi-residue method, pesticides, vegetables, fruits, green tea, Stir bar sorptive extraction (SBSE), GC-MS.

AppNote 4/2004. KEYWORDS Multi-residue method, pesticides, vegetables, fruits, green tea, Stir bar sorptive extraction (SBSE), GC-MS. AppNote 4/2004 Multi-Residue Method for Determination of 85 Pesticides in Vegetables, Fruits and Green Tea by Stir Bar Sorptive Extraction and Thermal Desorption GC-MS Nobuo chiai, Kikuo Sasamoto, Hirooki

More information

Evaluating CLP and EPA Methods for Pesticides in Water Using Agilent J&W DB-CLP1/DB-CLP2 GC Columns

Evaluating CLP and EPA Methods for Pesticides in Water Using Agilent J&W DB-CLP1/DB-CLP2 GC Columns Evaluating CLP and EPA Methods for Pesticides in Water Using Agilent J&W DB-CLP/DB-CLP GC Columns Application Note Environmental Authors Doris Smith and Ken Lynam Agilent Technologies, Inc. Abstract The

More information

We are IntechOpen, the first native scientific publisher of Open Access books. International authors and editors. Our authors are among the TOP 1%

We are IntechOpen, the first native scientific publisher of Open Access books. International authors and editors. Our authors are among the TOP 1% We are IntechOpen, the first native scientific publisher of Open Access books 3,350 108,000 1.7 M Open access books available International authors and editors Downloads Our authors are among the 151 Countries

More information

METHOD 4040 SOIL SCREENING FOR TOXAPHENE BY IMMUNOASSAY

METHOD 4040 SOIL SCREENING FOR TOXAPHENE BY IMMUNOASSAY METHOD 4040 SOIL SCREENING FOR TOXAPHENE BY IMMUNOASSAY 1.0 SCOPE AND APPLICATION 1.1 Method 4040 is a procedure for screening soils to determine whether toxaphene (CAS Registry 8001-35-2) is present at

More information

Food Analytical Methods. Versió pre-print

Food Analytical Methods. Versió pre-print Título artículo / Títol article: Comparison of Simple and Rapid Extraction Procedures for the Determination of Pesticide Residues in Fruit Juices by Fast Gas Chromatography Mass Spectrometry Autores /

More information

Zebron MultiResidue GC Columns

Zebron MultiResidue GC Columns Zebron MultiResidue GC Columns A new Generation of Columns for Pesticide Analysis MultiResidue Optimized for pesticide, herbicide and insecticide analysis The use of many pesticides has been limited or

More information

Yokogawa Analytical Systems Inc., Nakacho, Musashino-shi, Tokyo , Japan.

Yokogawa Analytical Systems Inc., Nakacho, Musashino-shi, Tokyo , Japan. Determination of organochlorine pesticides in river water by gas chromatography-negative-ion chemical-ionization mass spectrometry using large volume injection Sadao Nakamura,* Takashi Yamagami and Shigeki

More information

Zebron MultiResidue GC Columns

Zebron MultiResidue GC Columns Zebron MultiResidue GC Columns A New Generation of Columns for Pesticide Analysis MultiResidue Optimized for pesticide, herbicide and insecticide analysis The use of many pesticides has been limited or

More information

Certificate of Analysis

Certificate of Analysis T +44 (0)1462480400, F +44 (0)1462480403, E rpsmh@rpsgroup.com, W rpsgroup.com Report No.: 17-61493-1 Issue No.: 1 Date of Issue 20/06/2017 Certificate of Analysis Customer Details: Malahide Marina, Malahide,,

More information

ROBBATETAL.:JOURNAL OF AOAC INTERNATIONAL VOL. 91, NO. 6,

ROBBATETAL.:JOURNAL OF AOAC INTERNATIONAL VOL. 91, NO. 6, ROBBATETAL.:JOURNAL OF AOAC INTERNATIONAL VOL. 91, NO. 6, 2008 1467 RESIDUES AND TRACE ELEMENTS Quantitative Identification of Pesticides as Target Compounds and Unknowns by Spectral Deconvolution of Gas

More information

Date Issued: April 01, 2013 Expiration Date: June 30, 2013

Date Issued: April 01, 2013 Expiration Date: June 30, 2013 State of Florida Department of Health~Bureau of Public Health Laboratories I his is to certify that ALS ENVIRONMENTAL - SIMI VALLEY 2655 PARK CENTER DRIVE, SUITE A SIMI VALLEY, CA 93065 has complied with

More information

Assessment of uncertainty in pesticide multiresidue analytical methods: main sources and estimation

Assessment of uncertainty in pesticide multiresidue analytical methods: main sources and estimation Analytica Chimica Acta 454 (2002) 297 14 Assessment of uncertainty in pesticide multiresidue analytical methods: main sources and estimation L. Cuadros-Rodríguez a, M.E. Hernández Torres b, E. Almansa

More information

Assessing The Toxicity of Cotton Production

Assessing The Toxicity of Cotton Production Assessing The Toxicity of Cotton Production Zara Niederman Research Associate Lawton Lanier Nalley Assistant Professor of Agricultural Economics Mary Matlock Professor of Agricultural and Ecological Engineering

More information

MISCELLANEOUS CHEMICAL PRODUCTS

MISCELLANEOUS CHEMICAL PRODUCTS CHAPTER 38 MISCELLANEOUS CHEMICAL PRODUCTS Notes 1. This chapter does not cover: (a) separate chemically defined elements or compounds with the exception the following: (1) artificial graphite (heading

More information

Simultaneous determination of 74 kinds of pesticides in Chinese herbal medicine listed in Chinese pharmacopoeia (2015) by GPC-GC-MS/MS

Simultaneous determination of 74 kinds of pesticides in Chinese herbal medicine listed in Chinese pharmacopoeia (2015) by GPC-GC-MS/MS PO-CON1555E Simultaneous determination of 74 kinds of pesticides in Chinese herbal medicine listed in Chinese pharmacopoeia (215) ASMS 215 ThP 34 Huiyan Yang, Jun Fan, Taohong Huang, Shin-ichi Kawano,

More information

Effectiveness of accelerated solvent extraction compared to QuEChERS methods for the multiresidue analysis of pesticides in organic honey by GC-MS/MS

Effectiveness of accelerated solvent extraction compared to QuEChERS methods for the multiresidue analysis of pesticides in organic honey by GC-MS/MS CUSTOMER APPLICATION NOTE 744 Effectiveness of accelerated solvent extraction compared to QuEChERS methods for the multiresidue analysis of pesticides in organic honey by GC-MS/MS Authors Fabrizio Galbiati

More information

CERTIFICATE OF ANALYSIS

CERTIFICATE OF ANALYSIS Product Information: COA: 20180199 Sample ID: D802027-01 Type: Concentrate/Extract Lot Number: 700mg Hemp oil Storage conditions: 4 C Customer: Sunshine Global Sample size: 15 ml 150 South Pine Island

More information

Detection and Mitigation of Organic and Inorganic Pesticide Residues on Sacred Objects at the Rochester Museum & Science Center

Detection and Mitigation of Organic and Inorganic Pesticide Residues on Sacred Objects at the Rochester Museum & Science Center Detection and Mitigation of Organic and Inorganic Pesticide Residues on Sacred Objects at the Rochester Museum & Science Center Prepared For Adele DeRosa, RMSC 657 East Avenue Rochester, New York 14607

More information

Comprehensive Pesticide Analysis in Juice Using a Combination of GC/MS and LC/MS Methods

Comprehensive Pesticide Analysis in Juice Using a Combination of GC/MS and LC/MS Methods Comprehensive Pesticide Analysis in Juice Using a Combination of GC/MS and LC/MS Methods Application Note Food Safety Authors Fadwa Al-Taher, Rima Juskelis, Yang Chen, Jack Cappozzo Institute for Food

More information

Application of gas chromatography atmospheric pressure chemical ionization mass spectrometry for analysis of contaminants in environmental samples

Application of gas chromatography atmospheric pressure chemical ionization mass spectrometry for analysis of contaminants in environmental samples Application of gas chromatography atmospheric pressure chemical ionization mass spectrometry for analysis of contaminants in environmental samples PETR KUKUČKA 1,2 ; ONDŘEJ AUDY 1, DAWEI GENG 2, JORDAN

More information

Extraction of Residual Chlorinated Pesticides from Cotton Matrix As a part from certification method of cotton reference material

Extraction of Residual Chlorinated Pesticides from Cotton Matrix As a part from certification method of cotton reference material Extraction of Residual Chlorinated Pesticides from Cotton Matrix As a part from certification method of cotton reference material Volume 4, Issue 2, Fall2004 Kh. El-Nagar*, Michele Schantz**, Adel B. Shehata*,

More information

Thermo Fisher Scientific GC-MS Solutions for Environmental and Food Analysis

Thermo Fisher Scientific GC-MS Solutions for Environmental and Food Analysis Thermo Fisher Scientific GC-MS Solutions for Environmental and Food Analysis Hans-Joachim Huebschmann, Ph.D. GC/MS Technology Manager, Bremen/Singapore Thermo Scientific GC and GC-MS Product Line Matrix

More information

OREGON Environmental Laboratory Accreditation Program ORELAP Fields of Accreditation ALS Environmental - Simi Valley

OREGON Environmental Laboratory Accreditation Program ORELAP Fields of Accreditation ALS Environmental - Simi Valley MATRIX Reference Code Analyte Code Description ASTM C471M- 14 2014 ASTM D5504-12 2012 3964 Orthorhombic Cyclooctasulfur 4842 1-Propanethiol 6113 2,5-Dimethylthiophene 4544 2-Ethylthiophene 4843 2-Propanethiol

More information

Should you have any questions, please contact our office at (813)

Should you have any questions, please contact our office at (813) October 14, 2013 Comprehensive Engineering Services, Inc. 201 S. Orange Avenue, Suite 1300 Orlando, Florida 32801 Attn: RE: Mr. John F. Petrosillo, P.E. Project Manager Draft Level II Field Screening Report

More information

3. The fee prescribed under Schedule II will be subject to revision.

3. The fee prescribed under Schedule II will be subject to revision. 1 MINISTRY OF ENVIRONMENT, FORESTS & CLIMATE CHANGE (CENTRAL POLLUTION CONTROL BOARD) NOTIFICATION New Delhi, the 24 th October, 2016 Legal/42(3)/87. In exercise of the powers conferred under sub-section

More information

EUROPEAN COMMISSION DIRECTORATE GENERAL FOR HEALTH AND FOOD SAFETY

EUROPEAN COMMISSION DIRECTORATE GENERAL FOR HEALTH AND FOOD SAFETY EUROPEAN COMMISSION DIRECTORATE GENERAL FOR HEALTH AND FOOD SAFETY Safety of the Food Chain Pesticides and Biocides SANTE/11813/017 1 November 017 rev.0 Guidance document on analytical quality control

More information

Organochlorine Pesticides by GCxGC-ECD

Organochlorine Pesticides by GCxGC-ECD Organochlorine Pesticides by GCxGC-ECD LECO Corporation; Saint Joseph, Michigan USA Key Words: GCxGC-ECD, Environmental, Quantification 1. Introduction United States Environmental Protection Agency Method

More information

Chemicals That May Be Absorbed By Skin or Eye Contact

Chemicals That May Be Absorbed By Skin or Eye Contact The following chemicals have been identified by the Occupational Safety and Health Administration (OSHA) 1 and/or the American Conference of Governmental Industrial Hygienists (ACGIH) 2 as chemicals that

More information

KSA Environmental Laboratory Inc.

KSA Environmental Laboratory Inc. February 26, 07 KSA Environmental Laboratory Inc. Hydrologic Associates - Miami Attn: Brad Waller 8925 S.W. 148th Street Suite 212 Miami, FL 33176 RE: Parkland KSA Workorder: Q0012 Dear Brad Waller, Enclosed

More information

SUPELCO. Improved Performance for Cyanopropylphenyldimethylpolysiloxane (SPB-1701, SPB-1301) Capillary Columns

SUPELCO. Improved Performance for Cyanopropylphenyldimethylpolysiloxane (SPB-1701, SPB-1301) Capillary Columns Improved Performance for Cyanopropylphenyldimethylpolysiloxane (SPB-1701, SPB-1301) Capillary Columns L.M. Sidisky, Yizeng Ni, Greg Baney, Rodney George, Katherine K. Stenerson 01-0026 T401044 CFK Discussion

More information

In-Tube Solid-Phase Microextraction and On-Line Coupling with High-Resolution GC

In-Tube Solid-Phase Microextraction and On-Line Coupling with High-Resolution GC In-Tube Solid-Phase Microextraction and On-Line Coupling with High-Resolution GC Hanwen Wang, Wenmin Liu and Yafeng Guan, Dalian Institute of Chemical Physics, Dalian, China. The guest authors validated

More information

ToxFAQs TM. Molecular Models

ToxFAQs TM. Molecular Models Search Index Home Contact Us CONTENTS Search ToxFAQs TM Index of ToxFAQs TM A B C D E F G H I J K L M N O P Q R S T U V W X Y Z Molecular Models NFPA 704 Labels ChemFinder Links Other Resources ToxFAQs

More information

ANNUAL REPORT CITY OF WINNIPEG WATER SUPPLY SYSTEM

ANNUAL REPORT CITY OF WINNIPEG WATER SUPPLY SYSTEM Water and Waste Department Service des eaux et des déchets 2012 ANNUAL REPORT CITY OF WINNIPEG WATER SUPPLY SYSTEM TABLE OF CONTENTS CONTENTS PAGE Section 32(2) a Drinking Water System and Source...1 Section

More information

Drinking-Water Systems Regulation O. Reg. 170/03

Drinking-Water Systems Regulation O. Reg. 170/03 Part III Form 2 Section 11. ANNUAL REPORT. Drinking- System Number: 210002183 Drinking- System Name: Marsville Subdivision Well Supply System Drinking- System Owner: Township of East Garafraxa Drinking-

More information

COMMON IMPLEMENTATION STRATEGY FOR THE WATER FRAMEWORK DIRECTIVE (2000/60/EC)

COMMON IMPLEMENTATION STRATEGY FOR THE WATER FRAMEWORK DIRECTIVE (2000/60/EC) Technical Report - 2014-084 COMMON IMPLEMENTATION STRATEGY FOR THE WATER FRAMEWORK DIRECTIVE (2000/60/EC) Guidance Document No. 33 ON ANALYTICAL METHODS FOR BIOTA MONITORING UNDER THE WATER FRAMEWORK DIRECTIVE

More information

A Complete Monographic Study on Abies pindrow Royle Aerial Parts

A Complete Monographic Study on Abies pindrow Royle Aerial Parts Research Paper A Complete Monographic Study on Abies pindrow Royle Aerial Parts D. KUMAR AND S. KUMAR Centre for Advanced Research in Indian System of Medicine (CARISM), SASTRA University, Thanjavur-613

More information

Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Approach for Determining Pesticide Residues

Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Approach for Determining Pesticide Residues In Press Pesticide Analysis in Methods in Biotechnology, Eds. J.L. Vidal Martinez and A. Garrido Frenich, Humana Press, USA Nov. 2004 6 Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Approach

More information

POTENTIAL VAPOR INTRUSION ENVIRONMENTAL

POTENTIAL VAPOR INTRUSION ENVIRONMENTAL POTENTIAL VAPOR INTRUSION ENVIRONMENTAL INVESTIGATION INVESTIGATION FOR: Michael Lee Bronxville School District 77 Pondfield Road Bronxville, NY 0708 SITE INVESTIGATED: Bronxville Elementary School Parking

More information

95 th Percentiles for Blood and Urine Levels of Chemicals Measured in the Report

95 th Percentiles for Blood and Urine Levels of Chemicals Measured in the Report 95 th Percentiles for and Levels of s Measured in the Report The data summarized here provide 95 th percentile levels for these 148 chemicals by age, sex, and race or ethnicity in NHANES 2001-2002. Scientists

More information

Pesticide Residue Analysis by HRMS

Pesticide Residue Analysis by HRMS Pesticide Residue Analysis by HRMS Definition High Resolution MS (SANCO/12571/2013) Detection using mass spectrometers with high resolving power, typically > 20,000 FWHM FWHM = Full-width at half maximum

More information

ANALYTICAL REPORT. Attn: Dan Spector

ANALYTICAL REPORT. Attn: Dan Spector ANALYTICAL REPORT TestAmerica Laboratories, Inc. Benjamin Road Suite 0 Tampa, FL Tel: ()- TestAmerica Job I: 0-- Client Revision: For: Langan Engineering & Environmental Srvcs 0 NW th Court Suite 00 Miami

More information

High Efficiency, Broad Scope Screening of Pesticides Using Gas Chromatography High Resolution Orbitrap Mass Spectrometry

High Efficiency, Broad Scope Screening of Pesticides Using Gas Chromatography High Resolution Orbitrap Mass Spectrometry High Efficiency, Broad Scope Screening of Pesticides Using Gas Chromatography High Resolution Orbitrap Mass Spectrometry Dominic Roberts,1 Hans Mol,2 Marc Tienstra,2 Cristian Cojocariu,1 and Paul Silcock1

More information

GC and GC-MS Applications for Food Safety Analysis

GC and GC-MS Applications for Food Safety Analysis Application Notebook GC and GC-MS Applications for Food Safety Analysis Pesticides Additional Contaminants Natural Compounds and Food Additives About GC and GC-MS Technology GC and GC-MS Applications

More information

Internet Electronic Journal of Molecular Design

Internet Electronic Journal of Molecular Design CODEN IEJMAT ISSN 1538 6414 Internet Electronic Journal of Molecular Design May 2005, Volume 4, Number 5, Pages 355 366 Editor: Ovidiu Ivanciuc Proceedings of the Internet Electronic Conference of Molecular

More information

Assessment of Pesticide Residues in Some Fruits Using Gas Chromatography Coupled with Micro Electron Capture Detector

Assessment of Pesticide Residues in Some Fruits Using Gas Chromatography Coupled with Micro Electron Capture Detector ISSN-1996-918X Pak. J. Anal. Environ. Chem. Vol. 12, No. 1 & 2 (2011) 76-87 Assessment of Pesticide Residues in Some Fruits Using Gas Chromatography Coupled with Micro Electron Capture Detector Yawar Latif,

More information

Analytical Method for Simultaneous Determination of Pesticides and Pesticide Transformation Products in Water Environment Using GC-MS and LC-MS/MS

Analytical Method for Simultaneous Determination of Pesticides and Pesticide Transformation Products in Water Environment Using GC-MS and LC-MS/MS Analytical Method for Simultaneous Determination of Pesticides and Pesticide Transformation Products in Water Environment Using GC-MS and LC-MS/MS Takashi KONDO*, Miho SAITO*, Takashi KAMEYA*, Koichi FUJIE*,

More information