A0A TEXAS UNIV AT AUSTIN DEPT OF CHEMISTRY F/G 7/5 PHOTOASSISTED WATER-GAS SHIFT REACTION ON PLATINIZED T7TANIAI T--ETCIUI

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1 AA TEXAS UNIV AT AUSTIN DEPT OF CHEMISTRY F/G 7/5 PHOTOASSISTED WATER-GAS SHIFT REACTION ON PLATINIZED T7TANIAI T--ETCIUI APR 82 S FANG. 8 CHEN..J M WHITE N14-75-C-922 UNCLASSIFIED NL

2 OFFICE OF NAVAL RESEARCH Contract N14-75-C-922 Task No. NR TECHNICAL REPORT NO. 22 Photoassisted Water-Gas Shift Reaction on Platinized Titania: The Influence of Preparation Parameters by Shiu-Min Fang, Bor-Her Chen and J. M. White PPrepared for publication in mmm Journal of Physical Chemistry Department of Chemistry University of Texas at Austin Austin, Texas Reproduction in whole or in part is permitted for any purpose of the United States Government. C, This document has been approved for public release and sale; its distribution is unlimited. Li J S I

3 SC.T SECURITY CLASSIFICATION OF THIS PACE (When Date Entered) REPORT DOcuMENTATION PAGE READ INSTRUCTIONS BEFORE COMPLETING FORM I. REPORT NUMBER 12. GOVT ACCESSION NO. 3- RECIPIENT'S CATALOG NUMBER 4. TITLE (and Subtitle) S. TYPE OF REPORT& PERIOD COVERED Photoassisted Water-Gas Shift Reaction on Technical Report 22 Platinized Titania: The Influence of Jan Dec. 31, 198 Preparation P.Arameters 6. PERFORMINo ORG. REPORT NUMBER 7. AUTHOR(s) I. CONTrACT OR GRANT NUMBUR(eJ Shiu-Min Fang, Bor-Her Chen & J. M. White N14-75-C PERFORMING ORGANIZATION NAME AND ADDRESS 1. PROGRAM ELEMENT. PROJECT. TASK AREA 6 WORK UNIT NUMBERS J. M. White Department of Chemistry, University of Tex s Project NR Austin, Texas ,. CONTROLLING OFFICE NAME AND ADDRESS I'. REPORT DATE Department of the Navy. April 12, 1982 Office of Naval Research I. NUMBER Of PAGES Arlington, VA MONITORING AGENCY NAME a AOORSS(i dillffent from Controllinj Offlce) IS. SECURITY CLASS. (o fhis report) SSl. DECLASSIFICATION/DOWNGRAOING SCN9DUL, 16. OISTRI1UTION STATEMENT (of this Report) Approved for public release: Distribution Unlimited 17. DISTRIBUTION STATEMENT (of the abstract entered In Block 2, it different from Report) SUPPLEMENTARY NOTES Preprint, accepted, Journal of Physical Chemistry 1. KEY WORDS (Continue on retrse side it neeary aid Identity by block number) 2. ASSTRACT (Continua on reverse aide It necesary and Id"& 63 bly-ck er) The variation of the rate of the photoassisted water-gas shift reaction over platinized titania with changes in catalyst preparation has been studied. The following parameters were varied: (1)extent of hydrogen reduction; (2) Pt loading; (3)method of depositing Pt; (4)light intensity; and (5)NaOH loading. The reaction rate does not depend on the method of Pt deposition; is first order in light intensity., is not dependent on the chemical state or the Pt loading above 2 wt.%; depends on I DO,F",, 1473 EDITION DO I o Nov fis OSSOLETE S/N *S61 1 6Qrni n up P- an imau rn. sdola ECUIITY CLASSIPICATION OF THIS PAGE (when be iee... ~...

4 Zlock 2. Continued. >reduction of the titania and is strongly dependent on the surface concentration of NaH. From this work, we conclude that when NaOH is present, the rate limiting step in the reaction is the reaction of photoproduced holes with surface GH-I ions. i~

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