Development of roasting parameters for the ConRoast process with low-sulphur feedstock
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- Phyllis Burns
- 5 years ago
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1 31_El:ml Jul 2/6/09 1:19 M g 65 Sy Dvlm f g m f h CR wh lw-ulhu fdk by E. El* d J. Wh h CR f h du f lum gu ml vlv h u f fludzd bd f h mvl f ulhu fm by g mlg DC- fu. wk w d u 2007 Hz Rh Gld, Cld vd h d y f mml b dgd by h. h du h l bhd h wk, h gl f l m b ud mlg fu fd, h ul f vu g m m f l m (ully dul ulhu d h f f lm), d h m f h ul m f mml dg. Idu I 2007, h w ggd by Mk vg h g m vlvd h mvl f ulhu fm lw-ulhu lum gu ml (GM) f h CR.1,2 h vlv DC--fu mlg f ddd GM, d vd lv dl m mlg. O d dvg f h CR v dl m mlg hqu h bly mv ulhu uu dd g um f h mlg fu. Cuu g llw f h mvl f h ulhu SO 2 f l vy ulhu d. h h bvu vml dvg v dl m mlg. I f, du h u f h DC mlg, h my qum f h g h CR mly m f h fd ml f mvl f ulhu. h w mv muh ulhu bl, d hv ulhu h fu fd f l h 0.5% (whh l h h ulhu f h fd ml h Mk h mld xvly v h fw y h DC- fu). Wh h f Hz Rh, h dvld l g gmm vg h l g m f ulhu mvl fm yl lw-ulhu GM. h my m vgd w: g mu, h u f xyg-hd fludzg, d x. Sdly, h f f lm h GM w vgd. Fd ml h fd ml h f vg f h g m f h CR w Suh Af GM wh ml ulhd ulhu f 7.2%. bl I hw h hml ly f h ud h gmm. Whl xd h yl uh h wuld b dud mmlly fl k wh lvly hgh mu (xmly 16% mu), l fd uh fl k lvly mll l u. hf, h ml w dd, llw um fdg h l. W w md h dg h bbl mu lvl f h mml fl-k fd. h d ll ulhu f ugu g. Addl ful wuld hf b qud m h mu qud f dd g. A h l l f h CR dd k l Suh Af, l w h h ulml ful. F f fdg h l h l u, h l w bldd wh h ml f h d mu dg hl qum f ulml ful f h ul d. Cl vd fm 3% 7%. h Suh Af l h w ud d 60% fxd b, 17% h, 23% vll, d 0.4% ulhu. * *h USA I. Hz Rh I. h Suh Af Iu f Mg d Mllugy, SA ISSN X/ h w f ublhd h SAIMM lum Cf, lum fm, 6 9 Ob h Jul f h Suh Af Iu f Mg d Mllugy VOLUME 108 REFEREED AER JULY
2 31_El:ml Jul 2/6/09 1:19 M g 66 Dvlm f g m f h CR bl I GM- hml ly Elm C, m % S F F Mg Sl S2- (by dff) 6.94 N 2.85 Cu 1.89 C 1.42 Al 1.20 CO C l 0.34 C 0.24 N 0.09 M 0.09 C 0.08 Z 0.03 b m d m S 45 m A 11.5 m m Hg 0.28 m <10 m l l u d du h u mlyd f h l g w Hz 200-mm dm fludzd bd. h l u 200 mm dm by 4 m hgh, d ud f 310 l l. h vl hud d lhll l fu, d h l hg lm lld h z. g d d ld lvg h flud bd yl f h u f lg d l. h mg ld d g hugh bg-hu f fl mvl f ul. h bg-hu fu l l d ml fl. Sld du lld, hd h yl d bg-hu, whh md gul b. h g, xl hg w ld h fludzd bd by gzg h ll h. Wh h vl hd xmly 600 C, h fd f h ul w d. h xd f h fd ml wh h fludzg w xhm, d h u f h xl h w mly m f d gy l fm h l-l qum. h g mu f h bd w lld by djug h xl h w m h gy bl. h fd ml w xmly f u d w xd h h mjy f h l dud wuld b d d d fm h fludzd bd. hf, bd ml w md h hml k, llwg h flud bd lly bubblg bd fludz gm. h g bd ml w lum wh ml z f 356 µm. Axmly 70 kg f g bd w ddd h 1.5 m g bd dh. h m bd ml w ud f 1 hugh 14 bf bg ld by lv ml wh ml z f 500 µm f 15 d 16. (h lv lg-lg bd mdum, h l muh w mg ml.) A xyg-hd w ud h fludzg mdum. h fludzg g d h bd v wd-bx (lum hmb) qud wh bubbl- uy dbu h fludzg g v h -l f h. h fludzg g h (ludg u d fd-gu ug flw) md ufl vly (SSV) f 0.75 m/ h bd. h SSV w luld bd h md h bd z, djud f g mu d u. h vlum bu fm w h w jd h fd w ludd h vly lul. Fd bld w d fm d l ml vdd by Mk. h mu f l bldd wh h w bd hl gy- d m-bl lul h dd h xd l qum m ugu g d. A w fd w ud m h d l bld l um. h l um vdd h v u y umlly f h fd h vl. h fd bld w jd h bd 165 mm bv h dbu. h xhu xyg w lld by djug h fd f h /l mxu. W w jd h bd wh mzg zzl mul h ~16% mu xd h fl-k fd mml. R du w lld uuly hd h yl d bg-hu. h w mvd dlly d h vd d wghd ly. A ml f h yl d bg-hu du dug h dy- d f h w ulld f m-quv l ulhu ly ug LECO ly. h m ml w l quvly lyd f ulhu fm. h xhu g fm h bg-hu w dd hugh Vu d kdbd ubb mv SO 2 fm h g bf bg xhud h mh. A 50% NOH lu w ddd h ubb w m H g h 9. A df f w ud vyg h xhu g fm h ym d l h u h flud-bd vl. Gu du fm h w mld mmdly dwm f h bg-hu. h g d hugh hll mv mu, d w uuly lyd f xyg, ulhu dxd, b dxd, d b mxd. Addlly, h fludzg w uuly lyd f xyg. Rg bl II hw h mx f g dud, dg h g d, d b g ul f h. h l d f ml mx f h g mu (850, 900, d 950 C) d fu fludzg xyg lvl (21, 25, d 30% xyg by vlum). wd h d f h gmm, hgh mu d d xyg h fludzg w vgd fuh m du h ulhu h ld du. Addlly, h ff f d xyg h xhu, d h u f lv bd mdum w vgd. 66 JANUARY 2009 VOLUME 108 REFEREED AER h Jul f h Suh Af Iu f Mg d Mllugy
3 31_El:ml Jul 2/12/09 2:03 M g 67 Dvlm f g m f h CR bl II Summy f d d ul D 21 Aug 22 Aug 22 Aug 23 Aug 23 Aug 23 Aug 24 Aug 24 Aug S m 19:00 11:00 17:00 11:00 14:00 18:00 15:00 19:30 Ed m 22:00 15:00 21:00 13:00 17:00 21:00 18:00 21:30 Du, m g m Bd mu, C O 2 l, (%) O 2 xhu, (%) mum Shll mu, C Bd mu, C Fbd m., C Cyl m., C Bg-hu m., C Fludzg flw, f3/m W flw, kg/h Smuld mu, (%) Fd, kg/h Cyl u, kg/h S l, (%) , (%) S Bg-hu u, kg/h Sl, (%) , (%) S2-(by dff), (%) Off-g m O2, (%) CO 2, (%) CO, (%) SO 2, (%) D 24 Aug 27 Aug 27 Aug 28 Aug 28 Aug 29 Aug 30 Aug 30 Aug S m 12:00 11:00 14:00 9:30 15:00 13:00 10:30 12:30 Ed m 14:00 13:00 16:30 11:00 17:00 15:00 11:45 14:20 Du, m g m Bd mu, C O 2 l, (%) O 2 xhu, (%) mum Shll mu, C Bd mu, C Fbd m., C Cyl m., C Bg-hu m., C Fludzg flw, f3/m W flw, kg/h Smuld mu, (%) Fd, kg/h Cyl u, kg/h Sl, (%) , (%) S Bg-hu u, kg/h Sl, (%) , (%) S2-(by dff), (%) Off-g m O 2, (%) CO 2, (%) CO, (%) SO 2, (%) N: h fludzg flw hw -m u (f3/m fm) h u m wdly ud wh h. h dd d f 70ºF d 1 m. h Jul f h Suh Af Iu f Mg d Mllugy VOLUME 108 REFEREED AER JULY
4 31_El:ml Jul 2/6/09 1:19 M g 68 Dvlm f g m f h CR 1 hugh 3 vd h g f mu fm C, ug mb h fludzg g. Exhu g xyg w hld bw 2.0 d 2.5% xyg by vlum ( dy b). Ud h d, vully dff w h l ulhu f h l fu f g mu; hwv, l du ulhd ulhu f h l w dmd g mu d fm C, d ll d ulhd ulhu wh mu d fuh 950 C. 4 hugh 6 vd h m g f g mu, ug hd 25% xyg by vlum f fludz. Ag, xhu g xyg w gd bw 2.0 d 2.5% xyg. Wh h hd fludzg, lgh d l l ulhu w fu f g mu. Sulhd ulhu f h l g dd wh h g mu w d fm C, wh fuh d 950 C. 7 hugh 9 w m vg h g ul wh 30% xyg h fludzg g. Ufuly, 7 d 8 w lgud by l du h fd ym, d vy ll b gld fm h ul. Hwv, C mhly, d lly duld h ul f 6, dg h g h fludzg xyg h muh l ff h l d ulhd ulhu f h l h d g mu. 10 hugh 12 lkd fuh fludzg g xyg 35% by vlum. h m l duld h ul (f l d ulhd ulhu h l fu f mu) h w lw fludzg xyg lvl. 13 w dd lk h ff f d xyg h xhu g (d x ). h w u 950 C ug mb f fludz, wh g xhu xyg f % by vlum (dy b). h ul w gfly dff fm h f 3, d % xyg h xhu. 14 d 15 lkd fuh h mu C. 14 hwd h gf du l ulhu f h l bl by g vy hgh g mu, d h lm l lm f ulhd ulhu bl. 15 w dul f 14, ug lv h bd mdum d f h gul lum h hd b ud f ll vu. h ul ly duld h f 14, bu hwd ulhd ulhu lvl h g f vu (900 d 950 C). Flly, 16 w dud vg h ff f -g l fm vu 950 C dm f fuh g f h l uld fuh du h l d/ ulhd ulhu. l ulhu w dud, bu ulhd ulhu md uhgd, dg h w bl dm ulh mg h l. Rdul ulhu ul h m u f h g w dm h ffv f fludzd bd g f mvg ulhu fm h fd. bl III hw h ul f dul ulhu h ld du fm h vu. I w dmd h du ulhd ulhu lvl f h l u wh h mu d fm C, d h fuh du f ulhd ulhu mu byd 950 C d u. Hwv, gf ulh ulhu m h l ll mu gg fm C. Oly wh h g mu d C, d gf du (dm) f h ulh k l. h g d h bl ulh fmd h l dug g. h lgh uxd, gv h lum f h fd. Clum ulh mlly qu vy hgh mu (1 000 C d g) f dm ud xdzg d. lm Ah f h gmm w vg h f f lm dug g. 13 du w ld k h fllwg lm: I, Rh, Ru, Z, b, M, Sb, S, Au, A,, B, d V. 13 d hgh mu (950 C) wh 21% xyg ( m) fludzg. bl IV hw h lm y f 13. A mllugl bl f h lm dd h ll f h lm m wh h ld du fm g (d hf bm f h mlg fu fd) wh h x f lum, f whh vy ll w ud f h ld du. A ubly bl h wuld mlly b xd vllz ud g d. Hwv, h h l h h y bb u. h m lkly du h lkl f h fd. Iml f mml dg h ul f h l-g gmm dd h fllwg b lu: Fludzd-bd g vbl u f h mvl f ulhd ulhu fm ulhu-bg GM d by h CR. Lw (xmly 0.1%) dul ulhd ulhu lvl bl by g mu 900 C d bv whu ug xyg-hd. Oxyg hm hw l dvg m f ul. Alkl-h lm h GM my fm bl ulh, whh dfful dm g mu blw C. Rg mu h g wuld l dg f f, d wuld hv ml f ful um g lw-ulhu. Addlly, h l f bd gglm d h l blm mu f C d bv wuld b f. Ivg f h l f h mlg h lvl f ulh h l dd by h wd. Of h lm h w kd, lum w ud f h ld du f h l u, 68 JANUARY 2009 VOLUME 108 REFEREED AER h Jul f h Suh Af Iu f Mg d Mllugy
5 31_El:ml Jul 2/6/09 1:19 M g 69 Dvlm f g m f h CR bl III Cl ulfu ul mu ( C) Il O2 (%) S du (%) SO4 2- S S Sulhu du (%) du dbu (by dff) l, (%) f S (%) SO , , , b , , d 1 000, , Sml f hgh xhu O 2 ( %) b Sml f g xhu O 2 ( %) 4.5% x O 2 d Olv bd Olv bd, 3 yl bl IV lm ly f fd d du fm 13 Elm U Fd Cyl du Bg-hu du I z/ Rh z/ Ru z/ Z % b % M % Sb % S m Au m A m m B m V m d my hf qu d h dg f mml xhu lg qum, f xml h g-lg f ulhu d l. Alhugh d b bbd h l u, huld b b md h h lm w vgd ly ul f ul, d h lm lk ylly d u h g h f ym m lvl. Clu h g wk lly dmd h bl d h l ulhu f GM fm 7.2% lw 0.3% h yl du, wh 0.4% wghd vg f h yl d bg-hu du. Akwldgm h f h hl ff f Hz Rh gfully kwldgd, lg wh h x h f flud bd l-l qum. Rdy J f Mk vdd muh d bkgud fm, kwldg f h CR, d ugm ublh h. Flly, Bm lum Sml (h kw Idd lum), wh ud h wk flly, l kwldgd d hkd. Rf 1. JONES, R.. DC mlg f dd-d ulhd, Sulhd Smlg. Sh R.L. d Sh H.Y. (d.), MS, Sl, Fbuy 2002, JONES, R.., BARCZA, N.A., KAIURA, G., O CONNELL, G., d HANNAFORD,. m f ml ulhd by g d fu du, US 6,699,302 (Mh 2004). h Jul f h Suh Af Iu f Mg d Mllugy VOLUME 108 REFEREED AER JANUARY
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