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1 MPD Chemicals verview 2015
2 About Us MPD Chemicals is a US-based manufacturer of specialty chemicals with expertise in multiple technical areas including complex organic synthesis, unique monomers, polymer development, organosilicon chemistries and stable isotope labeling. We offer over 4,000 catalog products Custom synthesis 100 years combined operating history 2
3 Locations and Capabilities ver 4000 Catalog Product fferings Numerous Proprietary Custom Products initiated each year Four manufacturing locations on US East Coast Scale: From sub-gram quantities to metric ton production Kilo Lab / R&D Trevose, PA Kilo Lab / R&D Scotia, NY Kilo Lab / R&D King f Prussia, PA Kilo Lab / Pilot Plant Large Scale Production Riegelwood, NC 3
4 Chemical Capabilities verview CARBN-BASED CHEMISTRY SILICN-BASED CHEMISTRY CARBN-BASED CHEMISTRY Specialty Monomers Custom Polymers rganofluorines Custom Synthesis rganosilanes Siloxanes Coupling Agents Custom Synthesis rganic Molecules Isotope Labeling Pharmaceutical Custom Synthesis 4
5 We Serve Multiple End-use Markets Providing custom critical and enabling materials for: Biomedical Devices Wound Care Coatings Adhesives Dental Technologies Chromatography Diagnostic standards Specialty Chemicals Contact and Intraocular Lenses Numerous other high technology industrial applications 5
6 MPD Chemical Services Lab-scale Services Pilot-scale Capabilities Full-scale Custom Manufacturing Chemical Process Development Turn-key Custom Solutions Quick Turn Around Times Quality and Consistency Reliability of Supply Solutions to Address Specific Challenges and Requirements 6
7 Custom Synthesis ur Expertise MPD has a wide range of expertise to support our customers ramping from lab-scale to pilot scale to full-scale production We fill the gap bridging traditional chemical contract research type projects to scales normally associated with large chemical toll manufacturers ur enhanced capabilities enable customers to accelerate their product development cycle. When proprietary materials are required by a customer, sensitivity and understanding of the need for confidentiality and exclusivity (our customers own their IP) 7
8 MPD Catalog Products MPD Chemicals offers a full range of high quality products and services with over 4,000 catalog products and custom solution offerings that address complex requirements. MPD catalog products are manufactured based on proven scientific principles that have been developed internally over the years for customers who require customized material quality and purity. 8
9 Key Strengths Quote and manufacture from sub-gram to metric ton quantities Speed to produce materials Range of chemical handling capabilities Historical database of procedures via catalogue offerings Access to proprietary development partners when other unit operations are needed Where proprietary materials are required by a customer, sensitivity and understanding of the need for confidentiality and exclusivity (our customers own their IP) 9
10 Customer Interaction and Models Interface typically begins with one or more: Customer starting procedure, material specifications, and requested functionality Customers typically need a pathway to scale and economics for their particular application no one size fits all Transparency, simplicity, speed and sensitivity to proprietary information are critical ur customers include large Fortune 500 firms and small venture-backed or private companies Custom Quote in 4 Steps: Step 1: Step 2: Step 3: Step 4: Customer Collaboration for Requirements NDA MPD Specifications Review MPD Provides Quote 10
11 MPD Bridges Contract Research & Toll Manufacturing Contract Research MPD Chemical Provides the Complete Solution Toll Manufacturing Bridging lab-scale to full-scale manufacture Most external firms focus on one end of this spectrum MPD specializes in being able to begin where the customer desires small or large scale We help our customers transition from our lab production to our full-scale manufacture without needing yet another partner 11
12 MPD ffers Full Spectrum of Products and Services from Contract Research to Toll Manufacturing Contract Research MPD Chemical ffers the Full Spectrum of Products & Services Toll Manufacturing MPD Provides Contract Research Services Small scale lab synthesis (grams to kilograms) Labor costs dominate Proof of concept Customers may provide very little information MPD Provides Toll Manufacturing Scale Products Large scale manufacturing (100 s of kilograms) Labor costs diluted Specifications firm No process package required Bridging Lab-scale to Full-scale Manufacture Develop full-scale process Collaborate on specifications 12
13 Reactor Capabilities Development laboratories numerous benchtop work stations/fume hoods for materials development Kilo Laboratories over 20 walk-in hoods with glass reactors up to 50 liter scale ver 10 pilot and larger scale reactors ranging from 30 to 1,000 gallon capacities Larger reactors: Materials of construction glass-lined and Hastelloy Many reactors have vacuum distillation capability Some basic solids handling capabilities are 13
14 Analytical and QC Capabilities ur business units utilize a full suite of analytical equipment for in-process checks and for quality control Shared capabilities between business units Silar and IsoSciences facilities practices fulfill IS 9001:2008 requirements Gas chromatography (multiple) High pressure liquid chromatography (multiple) GPC NMR Mass Spec (UV and Light Scattering detectors) Viscosity measurement multiple instruments UV-Vis FTIR % Water by Karl Fisher method % Solids (moisture or oven solids) DSC Access to others via university relationships 14
15 15
16 Key Strengths Specialty monomer production Purification of critical acrylic monomers, including custom stabilization Custom monomer and polymer production Fluorinated molecules ligomer and pre-polymer development Development of composition for application needs Free radical custom copolymers Step growth customized polymers/oligomers 16
17 Specialty Monomers Acrylates / itaconates / maleates Monofunctional/multi-functional Simple alkyl/arakyl Complex alkyl/functional groups Fluorinated Ethylene oxide-based Acryloyl and methacryloyl chloride management Representative Examples F F H 3 C CH 2 CH 3 CH 2 F H 2 C CH CH 2 H 3 C CH 3 CH 2 17
18 Specialty Monomers Hydrophilic polymer precursors N-vinylpyrrolidone Hydroxyethyl methacrylate Glycidyl ethers High refractive index Carbazole/phenyl/brominated monomers Representative Examples CH 2 N H 2 C H CH 3 18
19 Specialty Polymers Experience producing most free radical polymerization custom copolymers Acrylates, styrene, maleic anhydride Acid, glycidyl ether, fluorinated, ethoxylated functions Silicone-containing copolymers Urethanes Pre-polymers/oligomers Functionalized urethanes Silicon-based specialty polymers TRIS/aminosilane copolymer with organics Acrylated organosilanes 19
20 20
21 Key Compound Families rganosilanes Chlorosilanes Specialty siloxanes, silazanes Coupling agents/adhesion promoters Acrylated and fluorinated organosilanes and siloxanes Representative Examples CH 2 N H 2 N CH 3 H 3 C Si CH CH 3 3 H 3 C Si Si H 3 C H 3 C Si CH 3 H 3 C CH 3 CH 2 H 2 C H 3 C Si Si CH 3 Si CH 3 CH 2 Cl Si Cl H 3 C CH 3 Si CH 3 Si CH 3 NH 2 H 3 C H 3 C CH 3 Si CH 3 H 3 C Si Si CH 3 H 3 C Si H 3 C H 3 C H 3 C H 3 C Si CH 3 CH 3 Si CH 3 CH 3 NH 2 21
22 Monomers / Prepolymers Monomers Acryloxy/vinyl substituted silanes Unique cyclic siloxanes Crosslinkers Telechelic or monofunctional oligomers Carbinol/acrylate/amine terminated polysiloxanes Silicone-ring macromers Hexa/tetrasiloxanes (alkyl substituted) Representative Examples H 3 C CH 3 Si H 3 C CH 3 Si Si CH 3 CH 3 22
23 23
24 About IsoSciences Formed in 2002 to meet the demands of the expanding LC/MS/MS market and the growing needs for isotopically labeled internal standards Specialize in the isotopically labeled custom synthesis of API and metabolites Diverse catalog of compounds used in food, vitamin, steroid, hormone and diagnostic testing 24
25 IsoSciences Facilities Located outside Philadelphia 4800 sq ft lab facility 10 Synthetic hoods 25
26 Analytical Capabilities Purity determination by HPLC, ELSD and GC Structural determination by 1 H, 3 H and 13 C NMR Isotope Incorporation by LC/MS/MS, LC/MS and GC/MS 26
27 Custom Synthesis Stable isotope labeled compounds for use in LC/MS testing Active pharmaceutical intermediate (API Precursors for Positron Emission Tomography (PET) Specialize in complex small molecule custom synthesis Radioactive (Tritium and 14C) synthesis available in New Jersey Facility Customers include pharmaceutical companies, NIST, CDC, NIH and diagnostic laboratories around the world IS 9001:2008 Total Quality Control Complete Traceability 27
28 IsoSciences Custom Quotes: 4 Steps Step 1: Non-confidential overview of capabilities Step 2: NDA customer and IsoSciences exchange Step 3: IsoSciences proposes synthetic route and timeframe Step 4: IsoSciences Provides Quote 28
29 Catalog ver 650 catalog items Focused in clinical diagnostics Vitamins, Steroids and Hormones Distributed through major retailers CertiMassTM Solutions Exact concentration Labeled and unlabeled analytes High purity standards 29
30 Focused Catalog fferings Vitamin D Steroids Food Testing Vitamin D2-[d3] Vitamin D3-[d3] 25-Hydroxyvitamin D3-[d6] 25-Hydroxyvitamin D2-[d3] 3-EPI-25-Hydroxyvitamin D3-[d3] 1,25-Dihydroxyvitamin D3-[d3] 24,25-Dihydroxyvitamin D3 Aldosterone-[d4] Cortisol-[ 13 C 3 ] Estrone-[ 13 C 3 ] Testosterone-[ 13 C 3 ] Androstenedione-[ 13 C 3 ] Progesterone-[ 13 C 3 ] Dihydrotestosterone-[ 13 C 3 ] Thiamine-[ 13 C 4 ] Riboflavin-[ 13 C 4, 15 N 2 ] Folic Acid-[ 13 C 5 ] Vitamin B12-[ 13 C 7 ] Vitamin B5-[ 13 C 3, 15 N] Pyridoxal-[d3] α-tocopherol-[d6] 2 H 2 H 2 H H 30
31 Products Representative Examples 25-Hydroxyvitamin D3-[d6] Cortisol-[ 13 C 3 ] Folic Acid-[ 13 C 5 ] 2 H 2 H 2 H 2 H 2 H 2 H H 13 C H H H H 2 N HN N N N N H N H 13 C 13 C H 13 C 13 C 13 C H H 13 C 13 C Compounds are synthesized and analyzed in house 31
32 LC/MS Application IsoSciences works closely with customers to ensure that the product will be suitable for its intended use. The internal standards that IsoSciences prepare utilize isotopes in non-exchangeable positions, allowing for less trouble shooting during method development. Analytical Chemistry (1988), 60(19) 2131 Note: All 3 are at exactly the same concentration 32
33 Isotope Specialists The focus on 13 C and 15 N labeled compounds allow for co-elution of analyte and internal standard in addition to no loss of label due to acid/base catalyzed exchange. For additional information regarding isotope selection, please visit: 33
34 Detailed Certificate of Analysis Accompanies Each Compound 34
35 MPD Vision Coordination of multiple chemistry expertise with a unified development team Generation of new step change materials from interdisciplinary discussion and development Specialty Acrylics Silanes and Silicones Custom Solutions Custom Polymers Stable Isotopes 35
36 MPD Business Model USING UR INTERDISCIPLINARY ABILITY Focused on technically unique specialty chemical manufacturing Solving problems where technical performance is critical Developing R&D solutions for application problems and partnering with our clients Utilizing in-house chemical expertise 36
37 Contact Carrington Smith, CE office: (215) ext. 202 cell: (610)
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